#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:45:49 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181192 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/71/2227154.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227154_Fobs loop_ _publ_author_name 'Viljoen, J. Augustinus' 'Visser, Hendrik G.' 'Roodt, Andreas' _publ_section_title ; Tetrakis(1,3-diphenylpropane-1,3-dionato)hafnium(IV) ; _journal_coeditor_code BG2349 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1053 _journal_page_last m1054 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.618 _cell_angle_gamma 90.000 _cell_length_a 24.8456 _cell_length_b 10.2236 _cell_length_c 19.3155 _exptl_crystal_F_000 2160.00 _reflns_d_resolution_high 0.7570 _cod_data_source_file bg2349Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 10RTV3_0ma in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 530.73 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 560.88 0.00 1.49 o 2 0 0 281669.75 -21.49 10.75 o 3 0 0 135.22 -11.75 5.88 o 4 0 0 99844.52 132199.11 3674.95 o 5 0 0 2050.64 2078.19 75.77 o 6 0 0 18409.76 16156.40 364.11 o 7 0 0 1632.24 1437.38 134.80 o 8 0 0 53488.32 59562.91 1219.97 o 9 0 0 1527.13 1355.48 79.61 o 10 0 0 1341.11 739.17 57.03 o 11 0 0 2342.22 2122.74 124.43 o 12 0 0 44683.27 46492.55 824.52 o 13 0 0 5112.15 4746.23 151.64 o 14 0 0 28512.47 28060.61 545.48 o 15 0 0 4403.82 4371.98 289.09 o 16 0 0 29275.28 28950.48 596.80 o 17 0 0 5454.04 5384.32 184.64 o 18 0 0 14870.56 14495.66 352.00 o 19 0 0 3250.47 2968.02 146.68 o 20 0 0 14820.90 14034.47 404.79 o 21 0 0 7026.84 7015.44 291.67 o 22 0 0 25465.44 24790.13 678.95 o 23 0 0 2682.24 2984.85 314.52 o 24 0 0 7766.09 8606.13 532.64 o 25 0 0 3784.26 3392.95 356.60 o 26 0 0 6206.84 5937.68 470.58 o 27 0 0 6649.89 6993.89 518.84 o 28 0 0 4936.47 5832.05 490.53 o 29 0 0 9577.03 8875.45 602.19 o 30 0 0 8444.13 8289.95 460.50 o 31 0 0 4398.63 4350.09 356.21 o 32 0 0 2275.45 2537.81 391.07 o 1 1 0 1854.35 -5.17 2.58 o 2 1 0 1176.40 -6.83 3.41 o 3 1 0 753.46 592.88 50.10 o 4 1 0 1939.02 1771.42 32.48 o 5 1 0 3374.80 3406.77 54.09 o 6 1 0 326.26 333.62 20.04 o 7 1 0 425.19 452.28 25.23 o 8 1 0 525.33 611.76 39.80 o 9 1 0 2164.19 2279.17 62.45 o 10 1 0 83.49 89.10 25.54 o 11 1 0 4152.63 4498.11 105.72 o 12 1 0 5741.50 6013.86 130.16 o 13 1 0 313.18 270.49 37.97 o 14 1 0 0.23 46.70 37.04 o 15 1 0 13.33 -12.48 32.58 o 16 1 0 405.91 461.61 54.97 o 17 1 0 0.75 -13.80 40.39 o 18 1 0 362.35 417.71 50.11 o 19 1 0 253.22 190.01 43.64 o 20 1 0 833.20 764.10 83.79 o 21 1 0 7.08 101.14 52.28 o 22 1 0 513.76 574.47 79.33 o 23 1 0 1.51 -23.91 69.89 o 24 1 0 207.26 251.62 112.14 o 25 1 0 50.90 -6.25 75.86 o 26 1 0 52.95 -13.96 83.28 o 27 1 0 67.83 11.86 108.73 o 28 1 0 152.80 119.90 105.83 o 29 1 0 154.51 168.63 148.83 o 30 1 0 34.34 45.63 108.64 o 31 1 0 181.05 269.85 126.27 o 32 1 0 11.06 125.22 139.15 o 0 2 0 167922.89 279070.59 5599.67 o 1 2 0 61033.98 76526.62 901.82 o 2 2 0 140763.89 220923.48 2793.70 o 3 2 0 2316.46 1713.24 45.21 o 4 2 0 25928.38 26036.21 291.55 o 5 2 0 407.10 358.57 22.42 o 6 2 0 72863.30 84786.78 829.05 o 7 2 0 5637.94 4979.23 85.29 o 8 2 0 48018.19 52099.39 596.54 o 9 2 0 7902.08 7187.71 121.53 o 10 2 0 27284.84 26978.83 341.41 o 11 2 0 56050.57 63902.22 798.01 o 12 2 0 16857.40 15070.07 295.05 o 13 2 0 13535.62 13665.02 209.80 o 14 2 0 36876.46 36422.57 491.72 o 15 2 0 10822.80 10799.61 197.18 o 16 2 0 29463.18 30104.98 430.06 o 17 2 0 2214.87 2251.36 107.92 o 18 2 0 18351.89 17379.28 291.32 o 19 2 0 2758.84 2895.50 219.10 o 20 2 0 18875.77 18584.95 493.35 o 21 2 0 12408.16 12112.85 352.02 o 22 2 0 11606.37 10666.97 380.27 o 23 2 0 1903.45 1933.08 187.88 o 24 2 0 12197.58 11897.88 392.30 o 25 2 0 3310.73 3685.38 389.74 o 26 2 0 7608.27 7381.20 318.54 o 27 2 0 3053.24 2813.55 265.17 o 28 2 0 7775.98 7802.26 341.95 o 29 2 0 5016.30 5785.44 305.70 o 30 2 0 5221.64 5848.64 399.94 o 31 2 0 2757.17 2631.56 236.78 o 1 3 0 12687.60 13669.21 197.27 o 2 3 0 8647.25 8198.90 142.97 o 3 3 0 387.54 416.64 27.60 o 4 3 0 2013.40 2193.57 59.12 o 5 3 0 343.64 266.35 43.11 o 6 3 0 136.91 178.49 23.95 o 7 3 0 223.66 273.09 38.56 o 8 3 0 1302.22 1361.04 49.99 o 9 3 0 4132.41 4706.12 116.26 o 10 3 0 645.48 717.29 47.79 o 11 3 0 1102.62 1175.89 58.54 o 12 3 0 3453.90 3538.58 99.38 o 13 3 0 786.01 824.26 57.14 o 14 3 0 290.64 535.71 109.26 o 15 3 0 300.94 326.60 45.89 o 16 3 0 299.80 289.98 46.07 o 17 3 0 147.27 90.68 42.49 o 18 3 0 708.77 814.70 100.55 o 19 3 0 936.64 1107.86 190.00 o 20 3 0 138.05 93.23 63.08 o 21 3 0 278.78 327.64 82.99 o 22 3 0 508.39 499.96 125.04 o 23 3 0 3434.80 2701.01 240.40 o 24 3 0 2.01 134.81 111.04 o 25 3 0 1829.93 1722.75 215.88 o 26 3 0 4.52 -48.93 125.00 o 27 3 0 34.80 -12.72 93.12 o 28 3 0 621.36 811.08 154.70 o 29 3 0 189.22 349.47 130.31 o 30 3 0 587.80 902.84 166.13 o 31 3 0 324.76 390.85 167.67 o 0 4 0 59549.37 64758.93 1124.37 o 1 4 0 11348.96 11894.37 208.42 o 2 4 0 92097.91 110079.62 1226.87 o 3 4 0 107.61 77.07 23.18 o 4 4 0 73818.99 82734.95 999.53 o 5 4 0 148.42 136.26 25.45 o 6 4 0 71663.77 81432.35 926.59 o 7 4 0 2253.22 2248.71 118.85 o 8 4 0 54940.38 59229.18 770.32 o 9 4 0 2214.15 2103.51 75.66 o 10 4 0 44703.01 47145.08 638.20 o 11 4 0 7522.80 7272.06 152.92 o 12 4 0 31806.39 32427.72 457.50 o 13 4 0 7805.13 7949.67 176.02 o 14 4 0 26919.44 28180.71 417.97 o 15 4 0 5248.97 5360.32 170.79 o 16 4 0 13974.27 14391.86 288.63 o 17 4 0 81.07 115.64 46.89 o 18 4 0 15726.95 14818.23 347.32 o 19 4 0 3144.41 3014.94 204.34 o 20 4 0 10043.31 9323.11 302.18 o 21 4 0 1896.20 2074.66 242.39 o 22 4 0 13603.56 12288.53 486.41 o 23 4 0 7352.55 7801.08 391.66 o 24 4 0 8340.12 8476.90 415.72 o 25 4 0 4033.93 4438.24 315.58 o 26 4 0 10688.93 10316.79 768.23 o 27 4 0 4437.57 4374.64 333.12 o 28 4 0 5127.80 4831.71 284.56 o 29 4 0 2256.17 1798.89 207.30 o 30 4 0 3563.17 3546.92 269.52 o 1 5 0 8441.45 8684.23 169.95 o 2 5 0 2808.79 3201.95 88.38 o 3 5 0 4046.48 4717.66 104.61 o 4 5 0 1282.36 1390.89 56.91 o 5 5 0 156.65 95.08 28.51 o 6 5 0 72.68 138.07 33.83 o 7 5 0 2142.65 2051.34 112.22 o 8 5 0 77.03 148.93 35.46 o 9 5 0 45.18 74.97 30.81 o 10 5 0 290.97 429.11 64.28 o 11 5 0 68.31 54.71 38.21 o 12 5 0 596.27 691.95 63.64 o 13 5 0 33.45 81.08 39.38 o 14 5 0 902.81 911.82 82.35 o 15 5 0 153.91 184.26 52.64 o 16 5 0 257.74 242.75 62.46 o 17 5 0 5868.32 6089.90 206.02 o 18 5 0 8.27 -31.51 52.17 o 19 5 0 928.49 900.44 99.06 o 20 5 0 88.18 177.09 83.77 o 21 5 0 2126.26 1946.33 173.41 o 22 5 0 9.93 -12.55 90.08 o 23 5 0 3826.29 3817.73 305.48 o 24 5 0 364.03 491.83 209.67 o 25 5 0 330.07 463.34 153.38 o 26 5 0 269.23 212.86 210.68 o 27 5 0 18.97 178.25 135.37 o 28 5 0 233.36 311.53 155.38 o 29 5 0 921.29 1288.96 465.28 o 0 6 0 60630.51 63337.89 1349.62 o 1 6 0 360.33 279.58 54.12 o 2 6 0 62423.39 66601.84 1153.84 o 3 6 0 2814.01 2905.25 114.74 o 4 6 0 69914.26 77645.13 1069.67 o 5 6 0 345.56 398.58 50.58 o 6 6 0 27045.87 25873.49 420.41 o 7 6 0 3278.01 3172.20 111.77 o 8 6 0 30554.81 30828.29 489.58 o 9 6 0 3300.64 2997.44 111.91 o 10 6 0 28363.23 28084.40 461.80 o 11 6 0 3718.29 3504.41 143.08 o 12 6 0 13206.86 13103.87 509.55 o 13 6 0 3527.08 3351.10 180.15 o 14 6 0 7417.21 7154.90 219.78 o 15 6 0 128.50 31.09 51.08 o 16 6 0 13409.79 13022.23 404.20 o 17 6 0 5521.72 5454.14 205.54 o 18 6 0 9745.87 9503.12 279.22 o 19 6 0 4118.91 4075.44 231.89 o 20 6 0 17033.44 17496.02 510.55 o 21 6 0 5747.62 5537.31 285.66 o 22 6 0 6173.21 5903.00 291.70 o 23 6 0 3547.81 3763.23 287.20 o 24 6 0 6887.36 6571.75 386.85 o 25 6 0 6051.12 6517.40 395.32 o 26 6 0 6314.57 6047.19 393.39 o 27 6 0 1578.72 1528.62 240.09 o 28 6 0 5061.66 5243.56 389.54 o 1 7 0 1151.66 1160.12 108.01 o 2 7 0 5.06 56.95 57.61 o 3 7 0 3574.00 3424.13 172.08 o 4 7 0 1317.18 1377.55 117.99 o 5 7 0 3287.56 3161.36 213.58 o 6 7 0 37.37 107.02 47.58 o 7 7 0 1214.39 1166.76 91.19 o 8 7 0 41.67 99.11 48.59 o 9 7 0 4448.29 4977.62 176.57 o 10 7 0 102.04 104.83 51.86 o 11 7 0 1783.13 1853.63 137.57 o 12 7 0 1039.09 981.40 95.48 o 13 7 0 3255.59 3236.09 177.17 o 14 7 0 1565.18 1678.41 121.43 o 15 7 0 3900.71 3867.37 175.62 o 16 7 0 2177.00 2122.83 139.31 o 17 7 0 9260.49 8567.87 325.42 o 18 7 0 113.00 18.51 77.24 o 19 7 0 949.72 1023.91 142.79 o 20 7 0 375.44 430.90 113.46 o 21 7 0 2317.28 2365.32 206.69 o 22 7 0 320.72 365.05 121.49 o 23 7 0 121.43 113.65 102.37 o 24 7 0 26.06 -100.93 92.91 o 25 7 0 240.87 356.75 154.45 o 26 7 0 13.09 228.50 161.61 o 27 7 0 15.08 325.79 201.28 o 0 8 0 22518.04 22052.60 828.64 o 1 8 0 61.20 110.78 68.92 o 2 8 0 19173.73 18170.14 509.36 o 3 8 0 213.25 248.40 133.89 o 4 8 0 20737.72 19904.79 461.82 o 5 8 0 1552.81 1353.26 102.46 o 6 8 0 12222.14 11900.55 297.90 o 7 8 0 166.01 213.39 59.66 o 8 8 0 16109.89 16223.83 371.40 o 9 8 0 1443.81 1509.95 129.37 o 10 8 0 20367.66 19468.07 475.17 o 11 8 0 2452.68 2297.02 244.38 o 12 8 0 17576.27 18098.90 415.08 o 13 8 0 4498.72 4016.71 222.14 o 14 8 0 12582.60 12320.99 332.47 o 15 8 0 3409.48 3056.77 206.06 o 16 8 0 6804.09 6514.44 401.42 o 17 8 0 7526.50 7188.64 311.41 o 18 8 0 9390.58 9157.84 486.72 o 19 8 0 7156.61 7095.71 324.37 o 20 8 0 5432.54 4919.26 517.50 o 21 8 0 1238.90 1599.73 185.23 o 22 8 0 5720.12 5425.28 305.64 o 23 8 0 590.17 649.12 147.87 o 24 8 0 5084.37 5808.46 408.09 o 25 8 0 492.28 405.38 144.36 o 1 9 0 341.19 288.60 88.81 o 2 9 0 101.76 53.54 76.53 o 3 9 0 274.76 254.49 76.26 o 4 9 0 584.54 545.15 123.11 o 5 9 0 4574.26 4596.40 298.51 o 6 9 0 144.04 256.59 69.48 o 7 9 0 2598.00 2746.65 221.99 o 8 9 0 1062.14 1094.56 109.91 o 9 9 0 4906.71 4627.37 216.37 o 10 9 0 6.86 -39.80 58.16 o 11 9 0 3673.92 3969.63 185.55 o 12 9 0 578.08 585.35 116.34 o 13 9 0 1865.88 2048.91 181.00 o 14 9 0 1650.96 1414.78 160.07 o 15 9 0 322.46 140.73 96.01 o 16 9 0 295.34 143.93 102.48 o 17 9 0 1819.63 1609.46 179.04 o 18 9 0 199.83 312.25 140.19 o 19 9 0 526.73 612.40 137.21 o 20 9 0 431.17 476.91 135.46 o 21 9 0 1676.17 1622.80 195.57 o 22 9 0 237.25 307.02 135.08 o 23 9 0 1861.12 1989.14 326.23 o 0 10 0 18773.41 17293.26 753.36 o 1 10 0 137.45 64.24 95.91 o 2 10 0 24117.37 23541.55 561.66 o 3 10 0 12.30 -0.71 70.89 o 4 10 0 10187.26 10359.94 405.44 o 5 10 0 882.02 990.99 122.72 o 6 10 0 20307.38 19405.21 572.28 o 7 10 0 760.50 730.45 111.36 o 8 10 0 13239.98 13264.93 357.90 o 9 10 0 386.24 492.87 112.87 o 10 10 0 8549.43 8218.94 730.77 o 11 10 0 404.26 584.13 125.69 o 12 10 0 7855.60 7562.14 330.09 o 13 10 0 123.09 138.28 96.25 o 14 10 0 3922.70 4058.76 257.20 o 15 10 0 259.11 280.72 147.38 o 16 10 0 2793.49 3231.90 244.85 o 17 10 0 947.35 1106.54 172.26 o 18 10 0 5260.87 4942.91 300.38 o 19 10 0 2155.48 2379.45 389.24 o 20 10 0 6486.35 6415.72 346.85 o 21 10 0 1619.14 2071.81 273.55 o 1 11 0 3025.54 3283.34 197.26 o 2 11 0 14.16 109.31 95.22 o 3 11 0 4456.03 4745.29 420.01 o 4 11 0 824.04 892.12 162.70 o 5 11 0 1073.38 1110.06 181.21 o 6 11 0 395.94 369.70 189.96 o 7 11 0 2770.76 2656.75 236.83 o 8 11 0 23.96 283.75 120.40 o 9 11 0 937.33 988.63 177.69 o 10 11 0 115.79 298.08 114.03 o 11 11 0 3106.04 2833.73 431.20 o 12 11 0 469.49 441.93 128.87 o 13 11 0 2748.52 2307.13 260.20 o 14 11 0 52.23 114.44 113.79 o 15 11 0 1681.10 1625.10 199.19 o 16 11 0 346.45 143.39 118.82 o 17 11 0 150.66 171.09 119.94 o 18 11 0 286.35 429.68 170.05 o 0 12 0 7537.67 7528.28 573.62 o 1 12 0 23.32 134.88 163.93 o 2 12 0 7004.35 7245.22 581.63 o 3 12 0 1.58 -68.48 143.18 o 4 12 0 7103.48 8400.68 631.88 o 5 12 0 1345.37 1242.83 311.75 o 6 12 0 6950.51 6821.35 594.07 o 7 12 0 1724.37 2176.90 395.04 o 8 12 0 7246.15 6682.78 608.86 o 9 12 0 875.82 614.82 263.79 o 10 12 0 3576.01 3393.92 483.36 o 11 12 0 877.43 677.13 276.25 o 12 12 0 2217.21 2648.04 463.88 o 13 12 0 545.77 781.81 232.59 o 14 12 0 869.68 567.02 309.47 o 1 13 0 978.54 853.59 270.05 o 2 13 0 29.23 125.27 137.53 o 3 13 0 1640.09 1883.41 384.58 o 4 13 0 203.03 128.68 201.32 o 5 13 0 2867.50 2323.07 410.08 o 6 13 0 246.94 83.02 203.41 o 7 13 0 1844.01 1014.66 324.36 o 8 13 0 46.18 -116.21 178.46 o -32 1 1 4248.01 4413.52 673.34 o -31 1 1 6548.62 5941.01 338.14 o -30 1 1 3768.06 3512.73 252.57 o -29 1 1 6343.13 6217.59 326.31 o -28 1 1 7244.18 7427.52 400.85 o -27 1 1 13650.08 13230.16 642.11 o -26 1 1 8975.54 8355.50 326.66 o -25 1 1 6463.09 6544.96 285.52 o -24 1 1 6356.60 6358.70 368.50 o -23 1 1 5030.31 5243.57 238.78 o -22 1 1 1921.63 2004.53 114.66 o -21 1 1 6755.01 6290.22 156.59 o -20 1 1 3646.14 3392.39 112.28 o -19 1 1 14015.93 13854.71 243.53 o -18 1 1 4727.92 4846.15 200.86 o -17 1 1 29703.47 28809.41 442.52 o -16 1 1 5123.87 5204.49 131.86 o -15 1 1 29746.98 29879.16 624.17 o -14 1 1 5502.62 5593.99 129.48 o -13 1 1 68785.00 79503.95 1041.64 o -12 1 1 6326.51 6199.66 129.68 o -11 1 1 87792.46 104231.22 1331.87 o -10 1 1 5129.14 5292.69 137.93 o -9 1 1 19661.64 18826.42 256.16 o -8 1 1 2180.60 2072.34 54.95 o -7 1 1 35993.28 37967.61 438.65 o -6 1 1 3361.57 2985.89 65.54 o -5 1 1 111854.20 159337.52 1707.26 o -4 1 1 15833.30 16608.74 200.90 o -2 1 1 104.58 -9.96 4.98 o -1 1 1 107186.42 -3.36 3.73 o 0 1 1 141.03 -4.87 2.44 o 1 1 1 131415.00 -9.39 4.70 o 2 1 1 383.57 -46.00 23.00 o 3 1 1 89713.01 121379.52 2605.21 o 4 1 1 19438.44 22299.61 231.84 o 5 1 1 68765.67 80765.91 778.97 o 6 1 1 404.36 316.02 21.86 o 7 1 1 23958.04 23067.16 281.03 o 8 1 1 5321.07 4981.05 133.33 o 9 1 1 14932.73 12936.90 225.48 o 10 1 1 16186.91 15403.63 246.56 o 11 1 1 33457.99 33011.86 551.73 o 12 1 1 32802.76 36345.13 516.47 o 13 1 1 41483.02 42293.96 596.23 o 14 1 1 2881.59 2733.24 93.79 o 15 1 1 23904.61 23936.25 379.59 o 16 1 1 6018.63 5749.71 146.05 o 17 1 1 28255.61 29428.73 422.40 o 18 1 1 3906.96 3740.16 126.62 o 19 1 1 10046.72 9636.44 242.32 o 20 1 1 4275.07 4161.14 192.71 o 21 1 1 10010.53 9032.96 243.95 o 22 1 1 11174.51 10877.20 278.86 o 23 1 1 15309.41 14599.69 434.52 o 24 1 1 7162.14 6987.74 290.83 o 25 1 1 9549.33 9338.99 349.25 o 26 1 1 5742.07 5962.09 289.07 o 27 1 1 12912.37 13260.26 466.26 o 28 1 1 4372.88 4728.14 276.19 o 29 1 1 8853.10 8552.31 363.75 o 30 1 1 4579.32 4427.85 507.89 o 31 1 1 4669.14 4473.53 327.98 o -32 2 1 12.78 195.06 146.73 o -31 2 1 455.88 557.01 149.75 o -30 2 1 158.10 216.19 122.44 o -29 2 1 879.35 747.96 144.87 o -28 2 1 93.59 89.32 95.73 o -27 2 1 616.13 523.90 124.71 o -26 2 1 77.67 67.63 88.65 o -25 2 1 111.58 77.87 85.56 o -24 2 1 400.74 368.58 99.30 o -23 2 1 988.95 707.34 143.47 o -22 2 1 224.70 197.75 104.16 o -21 2 1 1795.93 1708.16 132.04 o -20 2 1 544.19 718.20 94.04 o -19 2 1 4029.19 3485.96 147.23 o -18 2 1 4.16 -6.25 37.23 o -17 2 1 1134.95 1251.68 77.14 o -16 2 1 1606.96 1576.50 80.49 o -15 2 1 2322.40 2432.21 93.83 o -14 2 1 419.53 471.88 45.48 o -13 2 1 8089.29 7990.34 155.61 o -12 2 1 19.83 70.23 27.41 o -11 2 1 1.75 49.66 27.68 o -10 2 1 1725.12 1851.21 73.78 o -9 2 1 221.47 270.83 27.07 o -8 2 1 3564.41 3993.00 78.83 o -7 2 1 5394.98 5227.44 86.08 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