#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/71/2227161.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227161_Fobs loop_ _publ_author_name 'Yih, Kuang-Hway' 'Wang, Hsiao-Fen' 'Lee, Gene-Hsiang' _publ_section_title ; Bis(carbonyl-\kC)(N,N-dimethylthiocarbamoyl-\k^2^C,S)(pyridine-2-thiolato-\k^2^N,S)(triphenylphosphine-\kP)molybdenum(II) ; _journal_coeditor_code BG2366 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1189 _journal_page_last m1190 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.563 _cell_angle_gamma 90.000 _cell_length_a 20.0947 _cell_length_b 15.8720 _cell_length_c 17.8596 _exptl_crystal_F_000 2496.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file bg2366Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ic14165 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 609.20 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 41.44 2.75 6.25 o 2 0 0 22247.26 24336.16 562.66 o 3 0 0 12938.32 12162.15 511.64 o 4 0 0 27143.12 29635.11 607.71 o 5 0 0 176038.06 195157.84 3489.69 o 6 0 0 40485.36 42580.52 880.37 o 7 0 0 2236.53 2414.90 209.33 o 8 0 0 190823.47 197571.17 3481.35 o 9 0 0 10769.35 11326.52 405.54 o 10 0 0 16234.32 15974.89 517.49 o 11 0 0 8108.51 8724.53 549.96 o 12 0 0 6420.48 7150.65 960.67 o 13 0 0 30457.78 29674.18 843.87 o 14 0 0 12381.62 12123.77 547.56 o 15 0 0 12105.20 12373.22 681.72 o 16 0 0 19970.96 18145.86 685.02 o 17 0 0 3408.29 3383.26 354.91 o 18 0 0 53.76 647.03 404.64 o 19 0 0 109.34 486.34 242.04 o 20 0 0 2335.04 2271.11 308.35 o 21 0 0 3403.76 3948.33 461.18 o 22 0 0 5.23 -13.02 242.50 o 23 0 0 2355.95 2202.22 421.74 o 24 0 0 2305.39 2829.88 481.63 o 1 1 0 556.72 232.54 23.28 o 2 1 0 240.71 278.75 25.77 o 3 1 0 2673.07 2673.40 85.57 o 4 1 0 4684.34 4995.87 133.19 o 5 1 0 34147.58 36522.41 532.86 o 6 1 0 2642.17 2514.33 134.95 o 7 1 0 242.97 342.72 77.77 o 8 1 0 231.01 231.66 75.47 o 9 1 0 1539.27 1792.92 138.86 o 10 1 0 5090.13 5334.32 228.87 o 11 1 0 61.45 144.95 83.13 o 12 1 0 184.84 245.56 96.03 o 13 1 0 1414.08 1505.18 158.67 o 14 1 0 2123.45 2517.62 204.59 o 15 1 0 366.38 604.47 133.36 o 16 1 0 1349.30 1384.53 174.87 o 17 1 0 1851.35 1974.86 283.12 o 18 1 0 35.44 212.23 115.61 o 19 1 0 513.37 834.02 147.53 o 20 1 0 189.91 238.56 150.86 o 21 1 0 0.23 51.54 146.27 o 22 1 0 138.79 275.83 170.22 o 23 1 0 7.39 112.15 206.04 o 24 1 0 296.28 86.43 227.28 o 0 2 0 371128.31 390822.75 5616.94 o 1 2 0 1297.31 1030.71 55.74 o 2 2 0 34467.55 37293.04 450.85 o 3 2 0 3634.96 3146.98 127.20 o 4 2 0 1775.34 1577.59 86.16 o 5 2 0 6302.31 6237.67 163.71 o 6 2 0 15832.67 15556.16 300.71 o 7 2 0 1502.87 1266.72 107.49 o 8 2 0 54064.28 53264.68 790.58 o 9 2 0 1517.39 1409.33 160.82 o 10 2 0 2047.70 2314.07 162.59 o 11 2 0 356.02 593.88 107.74 o 12 2 0 20570.27 19474.01 444.27 o 13 2 0 21260.41 18823.08 450.05 o 14 2 0 4976.90 5127.13 275.60 o 15 2 0 13589.54 12426.17 414.55 o 16 2 0 7878.95 8316.82 365.51 o 17 2 0 531.19 532.33 132.99 o 18 2 0 338.21 498.59 138.80 o 19 2 0 2163.04 2455.38 298.84 o 20 2 0 2912.43 3440.85 303.24 o 21 2 0 5041.76 5452.19 390.35 o 22 2 0 182.42 329.98 160.78 o 23 2 0 3811.56 3410.60 364.14 o 24 2 0 896.86 1417.89 254.22 o 1 3 0 1006.03 922.77 64.39 o 2 3 0 2104.17 2052.05 201.45 o 3 3 0 8827.87 8897.30 173.80 o 4 3 0 49.52 26.36 46.97 o 5 3 0 267.73 388.86 74.63 o 6 3 0 1353.54 1541.03 128.54 o 7 3 0 1217.11 1492.49 120.18 o 8 3 0 2005.59 2490.35 148.03 o 9 3 0 7087.56 6754.44 229.99 o 10 3 0 1120.06 1250.93 132.46 o 11 3 0 4981.53 4999.80 393.93 o 12 3 0 1789.79 1632.12 157.15 o 13 3 0 309.02 288.90 105.17 o 14 3 0 3844.45 4445.74 258.07 o 15 3 0 17.24 69.17 103.53 o 16 3 0 3532.10 3292.41 249.60 o 17 3 0 868.73 1093.85 154.82 o 18 3 0 683.64 856.91 164.87 o 19 3 0 0.61 54.90 148.17 o 20 3 0 1029.17 1137.05 198.16 o 21 3 0 753.29 876.53 181.67 o 22 3 0 657.33 613.11 181.15 o 23 3 0 127.11 410.62 223.37 o 24 3 0 250.59 357.60 231.30 o 0 4 0 85736.24 88065.38 1561.92 o 1 4 0 989.80 1344.12 57.42 o 2 4 0 109.28 79.87 52.66 o 3 4 0 2325.64 3156.12 138.89 o 4 4 0 14.47 61.12 54.80 o 5 4 0 289.92 340.02 62.79 o 6 4 0 8853.72 7874.02 392.45 o 7 4 0 6860.97 6808.00 428.93 o 8 4 0 40315.25 37151.84 602.62 o 9 4 0 6984.57 6291.48 222.48 o 10 4 0 35.53 46.77 71.49 o 11 4 0 108.96 130.60 87.02 o 12 4 0 15260.14 13511.19 398.14 o 13 4 0 6026.30 6526.97 289.74 o 14 4 0 1711.35 2229.10 183.94 o 15 4 0 13695.20 13556.86 422.34 o 16 4 0 13404.05 13125.19 637.66 o 17 4 0 264.47 338.22 145.33 o 18 4 0 59.89 79.15 130.47 o 19 4 0 1399.20 1324.45 351.78 o 20 4 0 1667.79 2117.47 251.55 o 21 4 0 6827.86 6661.43 498.51 o 22 4 0 132.58 127.22 186.76 o 23 4 0 6066.52 7476.85 546.56 o 24 4 0 603.96 1098.28 225.61 o 1 5 0 286.64 239.41 52.26 o 2 5 0 899.90 834.95 90.12 o 3 5 0 2155.95 2763.31 143.89 o 4 5 0 2643.92 2710.15 145.77 o 5 5 0 265.78 172.78 46.44 o 6 5 0 5557.57 5577.40 174.25 o 7 5 0 7045.12 6510.43 222.96 o 8 5 0 456.26 342.64 92.94 o 9 5 0 1256.74 1147.18 114.91 o 10 5 0 396.02 504.18 97.71 o 11 5 0 1776.95 1947.48 161.63 o 12 5 0 3864.10 4115.60 296.81 o 13 5 0 91.13 265.32 173.51 o 14 5 0 841.44 1073.55 138.90 o 15 5 0 1579.57 1625.62 196.38 o 16 5 0 315.20 238.26 161.73 o 17 5 0 493.65 211.83 133.28 o 18 5 0 20.72 338.34 146.18 o 19 5 0 363.23 723.20 207.44 o 20 5 0 149.79 433.76 195.86 o 21 5 0 362.28 969.40 220.82 o 22 5 0 2466.63 2954.95 342.67 o 23 5 0 82.35 276.41 247.99 o 24 5 0 5.73 90.25 203.16 o 0 6 0 37656.66 35833.23 1089.63 o 1 6 0 6724.56 6542.49 169.94 o 2 6 0 11.65 14.86 57.73 o 3 6 0 682.37 590.53 96.24 o 4 6 0 3883.09 4014.59 176.94 o 5 6 0 1294.68 1732.87 131.17 o 6 6 0 8752.10 8228.02 185.78 o 7 6 0 7286.25 7172.32 211.44 o 8 6 0 38116.74 36486.14 545.98 o 9 6 0 9029.63 8521.88 297.69 o 10 6 0 4242.58 4670.44 204.18 o 11 6 0 1063.30 873.60 117.35 o 12 6 0 117.60 230.00 88.12 o 13 6 0 5502.88 6009.31 262.43 o 14 6 0 492.95 431.92 128.86 o 15 6 0 9987.51 9182.53 406.93 o 16 6 0 5376.05 5457.44 522.41 o 17 6 0 6536.03 6628.88 472.45 o 18 6 0 602.94 592.82 235.61 o 19 6 0 574.00 658.24 188.66 o 20 6 0 543.10 774.15 328.71 o 21 6 0 7132.31 5969.71 481.91 o 22 6 0 20.64 175.32 286.29 o 23 6 0 4905.78 5419.91 480.00 o 1 7 0 1664.86 1810.08 106.94 o 2 7 0 27417.40 28206.15 530.66 o 3 7 0 261.58 660.15 93.61 o 4 7 0 7513.63 8305.29 254.53 o 5 7 0 3100.43 3001.21 176.73 o 6 7 0 3610.55 3412.89 246.85 o 7 7 0 32285.60 31095.06 468.73 o 8 7 0 2606.19 2495.50 221.62 o 9 7 0 8362.93 8548.87 255.30 o 10 7 0 2265.39 2224.01 152.94 o 11 7 0 303.49 462.11 92.28 o 12 7 0 482.94 908.37 130.04 o 13 7 0 93.34 337.80 104.59 o 14 7 0 4.90 140.04 145.73 o 15 7 0 2253.30 2270.64 271.40 o 16 7 0 340.13 261.99 166.39 o 17 7 0 3981.80 3335.94 343.93 o 18 7 0 1683.43 1416.48 246.36 o 19 7 0 22.46 129.37 151.52 o 20 7 0 70.37 516.39 202.07 o 21 7 0 95.91 219.79 257.31 o 22 7 0 1416.49 1666.98 284.58 o 23 7 0 226.37 558.17 217.29 o 0 8 0 58089.30 57442.94 1173.18 o 1 8 0 8097.27 7638.74 206.46 o 2 8 0 1485.37 1395.76 131.45 o 3 8 0 399.01 258.14 89.36 o 4 8 0 4583.08 4910.43 229.24 o 5 8 0 1388.66 1616.22 144.73 o 6 8 0 10010.07 10277.38 315.26 o 7 8 0 8851.06 8988.61 358.12 o 8 8 0 25388.79 23700.81 598.01 o 9 8 0 3533.11 3185.84 212.13 o 10 8 0 5865.80 5431.27 493.81 o 11 8 0 5360.30 4655.98 343.45 o 12 8 0 17.50 30.68 136.04 o 13 8 0 5953.22 5689.20 407.59 o 14 8 0 3893.15 3968.80 377.81 o 15 8 0 8245.40 8314.40 515.87 o 16 8 0 1154.63 1337.27 230.31 o 17 8 0 4394.03 4845.54 680.80 o 18 8 0 124.94 466.26 173.99 o 19 8 0 4.26 448.02 180.40 o 20 8 0 7.48 182.53 230.59 o 21 8 0 7373.55 7980.14 566.36 o 22 8 0 198.86 120.60 204.33 o 1 9 0 1326.90 1461.08 109.87 o 2 9 0 16614.62 16404.24 328.23 o 3 9 0 895.66 1127.89 142.12 o 4 9 0 2663.67 3213.42 201.68 o 5 9 0 5455.70 5701.16 401.34 o 6 9 0 8270.38 8604.62 438.62 o 7 9 0 10938.86 10777.55 721.36 o 8 9 0 692.68 983.68 114.11 o 9 9 0 2634.51 2693.29 210.69 o 10 9 0 3557.35 3440.73 297.32 o 11 9 0 18.58 138.14 138.56 o 12 9 0 135.73 164.63 139.83 o 13 9 0 1682.16 1646.90 231.75 o 14 9 0 273.12 335.76 164.86 o 15 9 0 5680.01 4948.41 474.32 o 16 9 0 31.15 608.98 187.63 o 17 9 0 550.84 583.71 186.58 o 18 9 0 3926.75 3862.73 387.27 o 19 9 0 147.25 215.64 195.38 o 20 9 0 20.36 -63.02 171.64 o 21 9 0 219.98 387.03 218.91 o 22 9 0 2597.31 2459.76 348.41 o 0 10 0 54771.80 55728.08 1191.14 o 1 10 0 4430.97 4189.15 206.98 o 2 10 0 9861.86 10773.82 265.51 o 3 10 0 67.15 -68.78 73.07 o 4 10 0 2597.78 2626.13 192.07 o 5 10 0 1874.55 2157.95 179.07 o 6 10 0 12725.82 12746.36 380.30 o 7 10 0 7924.88 7764.81 313.64 o 8 10 0 27042.96 26053.17 841.07 o 9 10 0 10374.08 9909.94 481.85 o 10 10 0 14904.98 14210.84 627.57 o 11 10 0 745.92 750.82 179.50 o 12 10 0 2.01 -100.66 176.90 o 13 10 0 2835.53 3257.30 324.00 o 14 10 0 664.27 386.21 176.78 o 15 10 0 10721.22 9776.91 675.58 o 16 10 0 1280.86 1281.99 238.92 o 17 10 0 4468.99 4673.79 557.28 o 18 10 0 551.91 620.94 210.24 o 19 10 0 0.06 41.68 196.12 o 20 10 0 75.12 161.59 213.52 o 21 10 0 4192.91 4868.79 464.27 o 1 11 0 16390.94 16210.43 361.56 o 2 11 0 7490.15 7351.90 387.46 o 3 11 0 31.85 15.82 92.80 o 4 11 0 770.07 1019.70 219.12 o 5 11 0 1290.78 1507.38 161.53 o 6 11 0 12555.81 11624.81 384.88 o 7 11 0 8963.32 8554.06 444.15 o 8 11 0 576.38 801.02 173.75 o 9 11 0 1927.37 2294.56 258.33 o 10 11 0 4431.04 4398.77 355.93 o 11 11 0 2267.97 2070.95 256.34 o 12 11 0 549.13 714.23 222.22 o 13 11 0 5546.08 5419.18 420.10 o 14 11 0 1923.01 1844.71 268.08 o 15 11 0 3755.34 3227.27 340.34 o 16 11 0 1855.47 1701.27 263.08 o 17 11 0 1093.51 952.67 301.82 o 18 11 0 2700.44 2368.70 319.65 o 19 11 0 358.99 329.55 206.31 o 20 11 0 39.00 740.01 269.33 o 21 11 0 5.55 -183.07 202.27 o 0 12 0 4791.73 5420.48 297.17 o 1 12 0 2600.92 3174.18 284.37 o 2 12 0 9329.09 9149.24 354.88 o 3 12 0 13.05 123.61 120.38 o 4 12 0 4546.80 4753.18 458.81 o 5 12 0 47.79 94.92 92.01 o 6 12 0 10591.75 10809.59 505.26 o 7 12 0 4315.68 4001.14 330.35 o 8 12 0 10563.68 9884.07 496.51 o 9 12 0 6111.88 6048.03 414.72 o 10 12 0 2649.04 2720.67 323.72 o 11 12 0 1842.42 2155.17 325.01 o 12 12 0 681.59 523.72 173.30 o 13 12 0 303.92 171.11 157.28 o 14 12 0 5903.03 5226.00 426.95 o 15 12 0 1799.20 2508.26 310.37 o 16 12 0 1939.83 2512.89 325.22 o 17 12 0 1157.80 1397.77 263.51 o 18 12 0 1033.89 1296.47 314.75 o 19 12 0 133.97 879.54 226.40 o 20 12 0 42.02 575.35 239.13 o 1 13 0 10476.92 9537.55 430.49 o 2 13 0 8002.58 7798.16 548.44 o 3 13 0 372.50 287.11 125.24 o 4 13 0 1.01 4.90 87.32 o 5 13 0 37.24 155.59 121.11 o 6 13 0 5185.15 5152.40 367.04 o 7 13 0 9379.59 8179.68 457.19 o 8 13 0 26.11 287.80 145.23 o 9 13 0 1504.85 1298.33 245.69 o 10 13 0 1415.31 1668.39 256.60 o 11 13 0 64.82 287.73 212.17 o 12 13 0 249.46 254.00 158.54 o 13 13 0 3390.24 3034.59 386.92 o 14 13 0 2936.66 3029.55 331.81 o 15 13 0 2261.51 2250.45 302.53 o 16 13 0 900.22 529.05 189.73 o 17 13 0 89.55 340.90 191.18 o 18 13 0 944.68 1094.48 241.12 o 19 13 0 19.44 22.07 188.17 o 0 14 0 1426.40 1191.08 264.33 o 1 14 0 43.55 274.69 129.92 o 2 14 0 82.24 298.97 129.91 o 3 14 0 195.06 230.04 118.02 o 4 14 0 37.40 155.46 140.06 o 5 14 0 105.65 254.13 132.06 o 6 14 0 11192.26 10700.17 562.21 o 7 14 0 218.57 198.60 142.84 o 8 14 0 2342.39 2483.81 275.68 o 9 14 0 5478.48 5791.12 418.99 o 10 14 0 37.56 281.42 195.78 o 11 14 0 654.67 926.57 210.54 o 12 14 0 2129.85 2157.61 314.42 o 13 14 0 234.18 248.19 282.83 o 14 14 0 3157.46 2565.40 312.09 o 15 14 0 12.95 -13.44 159.02 o 16 14 0 466.06 513.82 190.14 o 17 14 0 2019.90 1962.34 298.48 o 18 14 0 119.52 147.66 202.13 o 1 15 0 1701.07 1826.00 227.44 o 2 15 0 1431.64 1270.86 188.24 o 3 15 0 3179.45 2949.32 342.88 o 4 15 0 14.47 102.32 148.30 o 5 15 0 1287.18 1282.42 254.82 o 6 15 0 537.17 190.01 161.34 o 7 15 0 3012.86 2854.55 289.57 o 8 15 0 2451.30 2197.67 261.39 o 9 15 0 1633.16 1731.53 498.66 o 10 15 0 429.56 1335.06 313.41 o 11 15 0 374.95 780.87 192.30 o 12 15 0 5.13 262.61 171.32 o 13 15 0 151.13 261.38 182.10 o 14 15 0 2087.84 1616.50 262.44 o 15 15 0 2827.44 2693.82 337.60 o 16 15 0 1542.57 1823.60 283.34 o 17 15 0 666.17 601.47 228.91 o 0 16 0 5347.80 5196.47 540.05 o 1 16 0 269.19 272.21 139.34 o 2 16 0 4396.78 4211.86 414.90 o 3 16 0 2.54 -69.42 148.27 o 4 16 0 39.83 120.80 164.91 o 5 16 0 39.63 200.81 204.76 o 6 16 0 2525.48 2699.60 519.78 o 7 16 0 167.48 153.18 167.83 o 8 16 0 2339.93 2360.72 339.81 o 9 16 0 2029.88 1766.83 303.19 o 10 16 0 1375.18 1819.32 240.68 o 11 16 0 482.91 640.60 185.79 o 12 16 0 68.13 -67.54 281.88 o 13 16 0 684.11 633.42 229.17 o 14 16 0 3520.47 3526.05 365.09 o 15 16 0 365.78 592.37 208.80 o 1 17 0 3219.52 3306.03 365.69 o 2 17 0 944.30 881.35 223.40 o 3 17 0 1552.76 1534.56 273.78 o 4 17 0 1174.90 1335.29 330.15 o 5 17 0 233.86 393.13 192.94 o 6 17 0 678.84 736.06 213.26 o 7 17 0 2307.41 1890.88 304.12 o 8 17 0 1655.79 1537.73 294.78 o 9 17 0 331.90 543.45 273.78 o 10 17 0 238.44 354.38 213.72 o 11 17 0 874.26 1028.44 298.13 o 12 17 0 267.26 688.92 259.87 o 13 17 0 171.25 199.83 205.05 o 14 17 0 1706.43 1740.27 431.67 o 0 18 0 1334.63 1068.14 413.52 o 1 18 0 2262.46 2298.89 421.93 o 2 18 0 2271.20 2561.92 344.05 o 3 18 0 614.34 589.36 215.87 o 4 18 0 66.48 245.78 189.80 o 5 18 0 245.00 813.52 219.63 o 6 18 0 662.52 920.69 334.52 o 7 18 0 77.22 54.11 191.37 o 8 18 0 509.88 433.91 223.07 o 9 18 0 2409.56 1878.74 529.98 o 10 18 0 1537.05 1591.86 460.34 o 11 18 0 1039.37 1458.24 302.70 o 12 18 0 1.46 325.54 223.76 o 1 19 0 2414.88 2728.46 455.21 o 2 19 0 159.04 -72.83 254.05 o 3 19 0 1412.68 1292.45 265.55 o 4 19 0 51.25 283.42 285.07 o 5 19 0 206.49 147.27 194.21 o 6 19 0 1488.37 1435.26 270.85 o 7 19 0 407.53 749.41 236.80 o 8 19 0 262.27 218.77 224.03 o 9 19 0 596.24 685.06 240.08 o 0 20 0 185.78 -87.38 357.92 o 1 20 0 890.26 1868.74 576.36 o 2 20 0 1086.32 1334.94 371.99 o 3 20 0 622.84 1044.06 439.45 o 4 20 0 9.08 621.36 395.30 o 5 20 0 177.03 718.90 213.91 o -25 1 1 871.21 1069.14 244.68 o -24 1 1 86.57 127.88 194.20 o -23 1 1 68.86 312.38 201.14 o -22 1 1 587.29 526.28 165.68 o -21 1 1 2461.56 2352.00 405.51 o -20 1 1 1123.58 1474.20 187.17 o -19 1 1 11628.64 11619.09 470.68 o -18 1 1 25228.95 23184.09 814.23 o -17 1 1 9749.40 9944.40 413.06 o -16 1 1 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