#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/72/2227210.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227210_Fobs loop_ _publ_author_name 'Sadeghi, Omid' 'Amini, Mostafa M.' 'Ng, Seik Weng' _publ_section_title ; Poly[(\m~3~-4-carboxypyridine-3-carboxylato-\k^3^N:O^3^:O^4^)(triphenylphosphine-\kP)silver(I)] ; _journal_coeditor_code BT5322 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1162 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 115.206 _cell_angle_gamma 90.000 _cell_length_a 14.2472 _cell_length_b 10.2431 _cell_length_c 16.3146 _exptl_crystal_F_000 1080.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file bt5322Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 341.09 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 34462.06 25056.41 2870.81 o 2 0 0 921.51 998.30 18.11 o 3 0 0 466.23 437.76 11.24 o 4 0 0 9642.33 8889.18 133.80 o 5 0 0 11433.50 11164.97 221.64 o 6 0 0 1118.13 1060.80 25.25 o 7 0 0 4624.25 4366.50 75.38 o 8 0 0 13507.17 13130.34 201.83 o 9 0 0 1551.17 1555.80 37.53 o 10 0 0 224.69 294.70 21.97 o 11 0 0 14.82 8.41 15.80 o 12 0 0 7826.92 7874.77 136.59 o 13 0 0 15562.16 15645.78 249.75 o 14 0 0 1343.80 1437.94 44.79 o 15 0 0 2072.41 2041.03 55.50 o 16 0 0 1231.22 1229.99 61.56 o 1 1 0 11371.32 11192.14 413.99 o 2 1 0 12215.80 12045.94 175.45 o 3 1 0 6643.28 6598.11 75.22 o 4 1 0 2.28 13.69 3.55 o 5 1 0 9008.37 9280.11 99.93 o 6 1 0 17202.78 16731.11 185.95 o 7 1 0 20210.68 20088.64 210.72 o 8 1 0 168.86 142.82 7.74 o 9 1 0 3910.95 3838.51 50.71 o 10 1 0 2704.80 2802.42 41.27 o 11 1 0 14031.95 14098.58 157.53 o 12 1 0 2239.63 2190.59 37.18 o 13 1 0 108.30 109.17 9.68 o 14 1 0 7674.59 7717.94 98.36 o 15 1 0 2039.27 2078.22 46.25 o 16 1 0 92.43 93.89 12.64 o 0 2 0 58615.82 48627.76 1400.19 o 1 2 0 8346.94 8575.88 89.16 o 2 2 0 26451.22 24782.01 865.67 o 3 2 0 12854.63 13898.43 559.77 o 4 2 0 15399.95 14573.65 567.76 o 5 2 0 5231.59 4969.27 82.27 o 6 2 0 2028.76 2029.01 28.35 o 7 2 0 614.15 536.58 14.12 o 8 2 0 6666.70 6320.98 74.76 o 9 2 0 5638.54 5597.16 68.88 o 10 2 0 133.71 153.89 9.43 o 11 2 0 1715.49 1728.57 30.93 o 12 2 0 2237.77 2287.01 38.42 o 13 2 0 2796.91 2746.36 44.70 o 14 2 0 2265.80 2211.79 46.67 o 15 2 0 504.28 483.68 21.46 o 16 2 0 620.85 672.78 26.61 o 1 3 0 326.37 425.18 6.96 o 2 3 0 8144.59 8145.18 85.79 o 3 3 0 11769.12 11652.29 122.71 o 4 3 0 36.95 34.86 4.36 o 5 3 0 16941.80 17565.65 225.60 o 6 3 0 3013.31 2971.39 44.36 o 7 3 0 4430.19 4529.07 80.99 o 8 3 0 682.94 443.86 53.99 o 9 3 0 47.74 42.44 5.42 o 10 3 0 7121.96 6847.10 233.52 o 11 3 0 2196.96 2247.43 46.28 o 12 3 0 217.00 197.77 11.88 o 13 3 0 34.88 36.72 6.96 o 14 3 0 98.93 90.00 11.47 o 15 3 0 804.21 843.79 28.34 o 16 3 0 1213.06 1268.82 45.89 o 0 4 0 17.16 4.17 2.34 o 1 4 0 14036.20 14552.44 150.70 o 2 4 0 1326.44 1346.84 22.92 o 3 4 0 4639.25 4700.01 52.77 o 4 4 0 10075.89 10351.07 110.54 o 5 4 0 223.65 288.47 10.18 o 6 4 0 325.55 283.50 10.16 o 7 4 0 34.76 40.38 5.47 o 8 4 0 469.10 463.76 23.93 o 9 4 0 5321.21 5278.90 76.54 o 10 4 0 1100.54 1029.51 74.18 o 11 4 0 2594.94 2588.52 61.13 o 12 4 0 4096.93 4102.98 67.70 o 13 4 0 1304.12 1285.41 32.90 o 14 4 0 386.75 401.14 24.80 o 15 4 0 74.33 64.69 14.25 o 1 5 0 649.56 589.37 10.01 o 2 5 0 6945.47 7487.73 96.61 o 3 5 0 1445.90 1514.07 30.26 o 4 5 0 2530.56 2649.39 33.42 o 5 5 0 2818.50 2792.65 36.02 o 6 5 0 720.60 682.77 19.13 o 7 5 0 6.05 4.99 2.49 o 8 5 0 831.79 846.95 21.58 o 9 5 0 726.70 643.39 36.25 o 10 5 0 1826.24 1818.27 37.85 o 11 5 0 299.59 301.67 20.24 o 12 5 0 27.86 13.82 9.53 o 13 5 0 34.13 12.16 9.89 o 14 5 0 3.86 9.31 10.40 o 15 5 0 367.98 335.66 26.78 o 0 6 0 649.82 833.05 19.39 o 1 6 0 190.25 217.41 6.52 o 2 6 0 1971.43 2230.11 35.95 o 3 6 0 110.20 110.82 7.79 o 4 6 0 4522.11 4501.76 65.01 o 5 6 0 884.33 894.42 21.45 o 6 6 0 839.03 807.72 79.91 o 7 6 0 698.01 729.45 26.10 o 8 6 0 936.15 1051.58 33.33 o 9 6 0 1308.62 1283.00 36.99 o 10 6 0 437.84 434.79 17.91 o 11 6 0 45.84 39.41 11.12 o 12 6 0 3.86 -10.97 7.31 o 13 6 0 280.60 257.32 22.80 o 14 6 0 18.83 -2.90 9.72 o 1 7 0 611.23 655.96 23.81 o 2 7 0 3378.12 3319.22 50.44 o 3 7 0 2626.56 2610.42 42.73 o 4 7 0 638.48 611.98 17.54 o 5 7 0 5721.98 5766.44 82.59 o 6 7 0 3524.89 3516.02 56.79 o 7 7 0 160.29 162.38 14.90 o 8 7 0 911.94 654.36 136.09 o 9 7 0 1.75 9.45 6.33 o 10 7 0 1375.27 1351.18 42.53 o 11 7 0 693.75 718.75 31.70 o 12 7 0 52.19 66.54 24.74 o 13 7 0 4.50 -3.84 9.25 o 14 7 0 12.77 17.93 12.05 o 0 8 0 1518.72 1500.34 55.38 o 1 8 0 512.07 585.95 23.00 o 2 8 0 838.07 857.29 20.69 o 3 8 0 28.62 32.87 5.91 o 4 8 0 7812.61 7801.60 106.90 o 5 8 0 284.03 277.00 13.28 o 6 8 0 33.29 46.38 7.60 o 7 8 0 250.86 187.78 28.66 o 8 8 0 405.38 389.11 21.56 o 9 8 0 4879.25 4681.54 95.22 o 10 8 0 1879.00 1844.56 52.55 o 11 8 0 188.63 212.54 20.60 o 12 8 0 1040.87 998.63 50.52 o 13 8 0 289.36 302.47 26.14 o 1 9 0 1664.05 1518.41 49.78 o 2 9 0 2163.55 2094.40 51.12 o 3 9 0 2928.85 2884.98 66.06 o 4 9 0 776.60 735.35 27.94 o 5 9 0 2087.09 2063.71 40.41 o 6 9 0 1823.87 1856.55 38.49 o 7 9 0 4373.84 4141.13 95.87 o 8 9 0 32.82 25.44 9.75 o 9 9 0 1879.69 1817.23 51.76 o 10 9 0 1261.53 1190.67 41.99 o 11 9 0 915.54 953.54 38.47 o 12 9 0 230.57 199.35 34.76 o 0 10 0 8648.69 8664.00 216.02 o 1 10 0 776.90 876.40 32.00 o 2 10 0 145.21 173.88 16.47 o 3 10 0 1307.19 1294.46 39.86 o 4 10 0 1340.58 1351.40 41.06 o 5 10 0 3818.67 3886.05 82.66 o 6 10 0 1335.01 1341.82 64.68 o 7 10 0 2218.40 2157.54 84.99 o 8 10 0 4841.15 4842.91 110.74 o 9 10 0 1114.63 1120.52 40.45 o 10 10 0 143.61 154.03 18.66 o 11 10 0 2.56 8.57 25.51 o 1 11 0 4467.75 4519.81 93.95 o 2 11 0 1793.65 1816.62 51.03 o 3 11 0 185.83 167.62 18.96 o 4 11 0 308.61 298.85 21.81 o 5 11 0 3.15 11.36 9.02 o 6 11 0 4803.06 4630.61 143.44 o 7 11 0 2146.38 2173.04 88.60 o 8 11 0 3.24 -17.71 11.81 o 9 11 0 744.42 721.42 51.09 o 0 12 0 5508.68 5499.09 158.23 o 1 12 0 2333.10 2347.73 62.42 o 2 12 0 22.49 12.39 10.04 o 3 12 0 2975.18 2951.09 72.62 o 4 12 0 2045.57 2138.06 59.35 o 5 12 0 2967.47 3054.35 109.99 o 6 12 0 228.16 172.98 29.39 o 7 12 0 511.63 481.46 42.60 o 1 13 0 284.27 272.08 46.69 o 2 13 0 4345.16 4492.33 99.45 o 3 13 0 2237.86 2093.44 88.13 o -17 1 1 151.61 134.21 14.61 o -16 1 1 97.66 74.52 11.62 o -15 1 1 67.04 77.80 9.63 o -14 1 1 46.70 49.04 9.05 o -13 1 1 655.96 642.70 19.05 o -12 1 1 938.09 944.29 22.28 o -11 1 1 442.27 432.41 21.54 o -10 1 1 58.99 73.00 6.85 o -9 1 1 55.04 58.00 8.63 o -8 1 1 2557.83 2643.57 36.90 o -7 1 1 2161.89 2292.74 31.99 o -6 1 1 1882.03 1854.37 28.79 o -5 1 1 1402.22 1430.09 20.59 o -4 1 1 1216.50 1244.38 17.71 o -3 1 1 12972.21 12935.83 155.57 o -2 1 1 28.27 21.53 2.12 o -1 1 1 2478.14 2584.93 27.65 o 0 1 1 3358.58 3281.34 39.76 o 1 1 1 19.41 23.06 1.86 o 2 1 1 15204.40 15100.13 156.97 o 3 1 1 110.14 111.25 4.38 o 4 1 1 1977.41 2143.59 27.29 o 5 1 1 2684.64 2709.48 34.29 o 6 1 1 3894.29 4037.44 49.08 o 7 1 1 117.13 120.34 7.03 o 8 1 1 855.40 804.05 17.02 o 9 1 1 4.22 4.62 3.79 o 10 1 1 256.91 251.70 10.84 o 11 1 1 1786.33 1834.17 32.20 o 12 1 1 158.97 154.13 10.50 o 13 1 1 1013.80 1070.38 25.38 o 14 1 1 1111.45 1124.36 31.79 o 15 1 1 47.21 64.44 10.76 o 16 1 1 9.31 -1.99 14.11 o -16 2 1 9.40 0.59 10.55 o -15 2 1 694.89 717.12 25.83 o -14 2 1 530.85 514.22 21.87 o -13 2 1 1205.17 1190.16 30.47 o -12 2 1 3385.86 3433.48 50.53 o -11 2 1 2733.85 2848.72 44.11 o -10 2 1 75.33 76.18 6.95 o -9 2 1 143.81 155.14 10.37 o -8 2 1 1044.47 1013.16 19.33 o -7 2 1 1915.68 1811.26 26.99 o -6 2 1 4532.82 4234.07 155.68 o -5 2 1 8.24 16.94 8.94 o -4 2 1 3041.37 3295.46 38.70 o -3 2 1 2556.60 2724.53 31.68 o -2 2 1 92.26 137.53 4.19 o -1 2 1 10462.81 10696.34 110.15 o 0 2 1 16245.32 15505.10 507.67 o 1 2 1 6160.15 6187.32 97.74 o 2 2 1 24135.78 23583.38 249.37 o 3 2 1 10787.49 11074.23 135.11 o 4 2 1 7879.25 8098.63 101.96 o 5 2 1 1617.10 1763.04 28.88 o 6 2 1 1566.18 1392.03 21.88 o 7 2 1 1265.50 1072.46 19.29 o 8 2 1 8.65 20.12 4.89 o 9 2 1 2760.66 2695.47 39.23 o 10 2 1 405.24 423.84 13.77 o 11 2 1 391.05 385.55 14.88 o 12 2 1 675.63 712.86 19.57 o 13 2 1 114.15 124.60 12.30 o 14 2 1 2227.06 2244.68 47.57 o 15 2 1 959.62 943.01 30.37 o 16 2 1 45.74 27.20 12.20 o -16 3 1 1408.82 1454.12 49.49 o -15 3 1 1013.75 1034.66 30.95 o -14 3 1 19.28 26.32 6.80 o -13 3 1 2942.14 2989.08 47.11 o -12 3 1 4639.99 4607.81 78.45 o -11 3 1 171.24 183.37 15.21 o -10 3 1 60.68 68.96 9.21 o -9 3 1 3018.40 3124.54 52.49 o -8 3 1 14623.93 14584.49 184.48 o -7 3 1 5318.06 5123.93 61.28 o -6 3 1 732.01 976.45 16.99 o -5 3 1 554.35 398.44 9.29 o -4 3 1 11094.88 11082.28 116.86 o -3 3 1 3733.18 3664.92 41.51 o -2 3 1 1350.66 1425.56 22.52 o -1 3 1 5446.35 5578.66 59.67 o 0 3 1 29797.20 28251.37 294.77 o 1 3 1 13671.33 13591.86 199.25 o 2 3 1 9207.40 9852.62 122.24 o 3 3 1 13045.66 13440.10 139.92 o 4 3 1 9605.26 9760.62 104.46 o 5 3 1 14172.13 14410.46 152.14 o 6 3 1 3336.41 3416.80 50.87 o 7 3 1 311.98 261.94 12.62 o 8 3 1 5384.88 5342.87 65.35 o 9 3 1 6079.53 6144.99 76.11 o 10 3 1 235.80 263.22 15.28 o 11 3 1 21.68 24.23 6.30 o 12 3 1 1486.06 1451.84 38.32 o 13 3 1 4845.94 5046.17 81.41 o 14 3 1 1658.07 1675.12 40.18 o 15 3 1 482.40 499.16 22.71 o -16 4 1 1965.20 2016.28 90.65 o -15 4 1 2844.77 2877.33 72.88 o -14 4 1 1147.39 1106.25 40.08 o -13 4 1 1227.55 1223.06 27.02 o -12 4 1 1012.83 974.72 27.58 o -11 4 1 6731.13 6597.85 97.13 o -10 4 1 6223.06 6182.10 83.82 o -9 4 1 3540.81 3473.48 47.32 o -8 4 1 44.52 54.76 5.45 o -7 4 1 4892.89 4775.68 58.02 o -6 4 1 8687.47 8519.56 94.43 o -5 4 1 10273.74 10425.60 112.12 o -4 4 1 241.97 241.84 11.49 o -3 4 1 18501.07 18919.45 228.78 o -2 4 1 25616.76 25643.95 306.79 o -1 4 1 16399.35 17278.33 178.38 o 0 4 1 137.34 131.10 4.34 o 1 4 1 15608.52 16437.80 169.12 o 2 4 1 12800.44 12772.52 154.10 o 3 4 1 13497.44 13348.79 181.62 o 4 4 1 10927.09 11505.98 122.60 o 5 4 1 856.62 757.84 14.36 o 6 4 1 2548.86 2416.77 33.29 o 7 4 1 1423.96 1317.00 22.46 o 8 4 1 944.82 951.81 19.22 o 9 4 1 565.34 536.23 42.04 o 10 4 1 8712.76 8717.01 120.71 o 11 4 1 7092.10 6968.32 100.73 o 12 4 1 544.82 523.18 22.01 o 13 4 1 173.98 179.46 14.62 o 14 4 1 1143.51 1184.31 42.63 o 15 4 1 1534.46 1675.58 53.65 o -15 5 1 17.34 9.87 10.83 o -14 5 1 1164.59 1210.74 43.15 o -13 5 1 1478.47 1469.22 46.44 o -12 5 1 2098.14 2204.57 45.43 o -11 5 1 1403.90 1458.98 34.11 o -10 5 1 625.96 604.99 20.39 o -9 5 1 7216.26 7252.16 119.38 o -8 5 1 10779.94 10994.84 122.56 o -7 5 1 269.36 262.62 8.99 o -6 5 1 184.23 223.01 7.92 o -5 5 1 441.14 327.76 11.67 o -4 5 1 13943.22 13718.78 171.20 o -3 5 1 10446.88 10163.70 128.66 o -2 5 1 4628.71 5136.65 69.15 o -1 5 1 8088.84 8471.11 90.43 o 0 5 1 3026.90 2881.15 34.41 o 1 5 1 9881.22 9715.02 103.12 o 2 5 1 5508.01 5775.73 64.21 o 3 5 1 2721.80 2769.35 39.31 o 4 5 1 24710.72 24191.02 250.83 o 5 5 1 16291.12 16574.60 175.15 o 6 5 1 319.12 377.22 10.59 o 7 5 1 474.16 477.09 12.73 o 8 5 1 2416.16 2433.86 36.10 o 9 5 1 8760.72 8939.17 104.02 o 10 5 1 3380.45 3407.76 73.88 o 11 5 1 1391.85 1357.97 42.57 o 12 5 1 3391.13 3444.41 177.71 o 13 5 1 1604.80 1726.95 52.15 o 14 5 1 598.94 603.26 31.69 o 15 5 1 418.51 493.05 30.45 o -15 6 1 1545.28 1573.39 94.62 o -14 6 1 1108.80 1114.57 74.84 o -13 6 1 503.98 496.83 27.47 o -12 6 1 11.85 9.28 8.77 o -11 6 1 3659.21 3318.80 230.11 o -10 6 1 12526.91 12282.04 164.79 o -9 6 1 4933.08 4896.98 75.95 o -8 6 1 2665.72 2719.87 48.02 o -7 6 1 5389.67 5548.63 80.96 o -6 6 1 4130.07 4405.87 186.66 o -5 6 1 7672.92 7580.99 120.87 o -4 6 1 76.45 72.25 6.84 o -3 6 1 11333.21 11136.98 141.57 o -2 6 1 10853.56 10798.51 136.76 o -1 6 1 3991.66 4169.79 48.21 o 0 6 1 152.07 156.50 6.39 o 1 6 1 1382.40 1359.72 23.70 o 2 6 1 4669.59 4603.86 57.41 o 3 6 1 15198.56 15429.22 162.11 o 4 6 1 2251.01 2344.34 35.37 o 5 6 1 6375.92 6441.70 89.13 o 6 6 1 1662.10 1706.29 33.01 o 7 6 1 765.64 719.16 20.35 o 8 6 1 1434.67 1464.89 31.87 o 9 6 1 191.51 163.26 16.15 o 10 6 1 8570.84 8250.94 175.99 o 11 6 1 5403.30 5422.98 107.69 o 12 6 1 1092.37 1056.12 40.39 o 13 6 1 66.43 54.12 13.32 o 14 6 1 324.28 297.34 25.25 o -14 7 1 258.74 196.42 30.27 o -13 7 1 1642.24 1570.45 50.70 o -12 7 1 2754.96 2723.77 122.58 o -11 7 1 1023.23 1029.60 37.81 o -10 7 1 862.33 785.35 24.50 o -9 7 1 2719.80 2614.27 49.18 o -8 7 1 6298.89 6059.06 89.76 o -7 7 1 2418.64 2385.07 43.93 o -6 7 1 671.30 685.58 19.85 o -5 7 1 2373.97 2227.49 48.55 o -4 7 1 3021.71 2942.92 76.76 o -3 7 1 6224.22 6402.28 87.96 o -2 7 1 561.91 541.88 15.94 o -1 7 1 4463.98 4494.81 70.83 o 0 7 1 11495.04 11536.36 123.34 o 1 7 1 10192.16 10427.17 112.38 o 2 7 1 835.65 902.46 20.46 o 3 7 1 3215.26 3399.84 52.47 o 4 7 1 6291.53 6273.36 107.49 o 5 7 1 6538.10 6446.76 111.81 o 6 7 1 1483.24 1463.46 30.90 o 7 7 1 2311.02 2337.53 43.22 o 8 7 1 4055.88 4137.20 84.04 o 9 7 1 1998.25 1997.11 52.60 o 10 7 1 1864.05 1747.22 50.04 o 11 7 1 84.66 83.99 14.05 o 12 7 1 2416.94 2428.50 65.92 o 13 7 1 2526.03 2405.97 77.34 o -13 8 1 415.52 431.94 27.57 o -12 8 1 2059.41 2182.65 74.59 o -11 8 1 2204.09 2155.99 58.78 o -10 8 1 1243.69 1234.34 41.09 o -9 8 1 743.55 790.78 38.68 o -8 8 1 83.14 77.90 9.55 o -7 8 1 1408.14 1413.29 39.77 o -6 8 1 7973.74 7928.08 110.79 o -5 8 1 3788.45 4055.00 63.63 o -4 8 1 550.25 535.08 17.29 o -3 8 1 1942.30 2040.26 36.95 o -2 8 1 3468.15 3605.46 55.32 o -1 8 1 8773.26 8707.07 206.12 o 0 8 1 679.25 697.04 25.02 o 1 8 1 4174.66 4090.87 79.07 o 2 8 1 4341.56 4335.93 64.13 o 3 8 1 2758.04 2766.72 46.16 o 4 8 1 94.54 90.05 8.74 o 5 8 1 323.84 327.77 19.72 o 6 8 1 2530.60 2576.16 46.51 o 7 8 1 4521.74 4600.78 101.14 o 8 8 1 321.26 352.15 21.64 o 9 8 1 1573.05 1574.43 68.60 o 10 8 1 2153.39 2136.21 58.18 o 11 8 1 2643.29 2605.20 67.70 o 12 8 1 1821.48 1767.74 55.20 o -12 9 1 1549.81 1491.26 49.99 o -11 9 1 666.55 622.87 30.67 o -10 9 1 6.29 -5.15 7.92 o -9 9 1 451.21 449.75 24.51 o -8 9 1 2288.60 2271.79 45.92 o -7 9 1 6963.66 6800.58 100.48 o -6 9 1 287.22 342.96 15.80 o -5 9 1 3503.54 3646.82 60.08 o -4 9 1 1631.04 1646.74 44.37 o -3 9 1 994.92 1008.12 32.99 o -2 9 1 265.57 236.46 35.17 o -1 9 1 3479.73 3412.97 134.18 o 0 9 1 6714.31 6865.32 123.18 o 1 9 1 1592.85 1643.65 43.53 o 2 9 1 193.04 167.53 15.12 o 3 9 1 983.86 1035.69 86.89 o 4 9 1 9.71 10.48 7.62 o 5 9 1 1258.15 1260.14 36.68 o 6 9 1 3766.55 3507.52 153.65 o 7 9 1 1008.63 1023.34 35.22 o 8 9 1 5541.03 5381.12 193.07 o 9 9 1 872.49 899.57 35.33 o 10 9 1 38.03 51.64 13.11 o 11 9 1 2.67 -5.07 9.51 o -11 10 1 287.90 295.71 24.73 o -10 10 1 278.75 287.58 23.93 o -9 10 1 161.41 201.63 27.03 o -8 10 1 181.19 188.99 18.43 o -7 10 1 220.16 263.27 31.10 o -6 10 1 2163.06 2151.64 56.06 o -5 10 1 360.02 357.56 21.53 o -4 10 1 356.23 361.28 24.30 o -3 10 1 301.23 252.83 18.58 o -2 10 1 736.87 798.93 52.38 o -1 10 1 2176.80 2198.57 80.34 o 0 10 1 382.33 381.93 21.40 o 1 10 1 333.18 328.59 19.85 o 2 10 1 1830.65 1839.05 49.21 o 3 10 1 1821.96 1728.23 47.14 o 4 10 1 22.14 36.72 19.55 o 5 10 1 0.41 8.11 7.82 o 6 10 1 1376.08 1362.65 64.03 o 7 10 1 2181.62 2014.84 82.47 o 8 10 1 9.81 5.99 9.59 o 9 10 1 1061.46 968.75 37.84 o 10 10 1 136.54 122.10 17.15 o -9 11 1 395.68 351.21 40.14 o -8 11 1 1.87 6.71 15.05 o -7 11 1 329.56 323.35 36.89 o -6 11 1 27.20 28.80 10.37 o -5 11 1 0.37 -3.02 9.56 o -4 11 1 107.50 117.15 15.57 o -3 11 1 9.44 15.56 9.23 o -2 11 1 39.51 39.06 10.95 o -1 11 1 202.57 186.17 18.06 o 0 11 1 120.34 113.43 15.32 o 1 11 1 75.11 89.28 13.57 o 2 11 1 338.79 355.05 21.76 o 3 11 1 59.89 57.54 12.23 o 4 11 1 542.55 544.18 26.82 o 5 11 1 32.69 31.62 16.78 o 6 11 1 203.83 256.76 33.32 o 7 11 1 202.24 189.73 29.88 o 8 11 1 2.78 -4.90 13.38 o 9 11 1 0.33 0.19 15.27 o -7 12 1 233.56 249.08 34.21 o -6 12 1 1429.86 1373.54 69.16 o -5 12 1 52.93 57.98 13.50 o -4 12 1 156.99 149.11 17.86 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