#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:46:27 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181193 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/72/2227255.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227255_Fobs loop_ _publ_author_name 'Gzella, Andrzej K.' 'Chrzanowska, Maria' 'Dreas, Agnieszka' 'Meissner, Zofia' _publ_section_title ; (4S)-({-})-4-Benzyl-2,2-dimethyl-3-o-toluoyl-1,3-oxazolidine ; _journal_coeditor_code BT5373 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2850 _journal_volume 66 _journal_year 2010 _space_group_IT_number 18 _symmetry_space_group_name_Hall 'P 2 2ab' _symmetry_space_group_name_H-M 'P 21 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.9951 _cell_length_b 17.2768 _cell_length_c 9.1899 _exptl_crystal_F_000 664.00 _reflns_d_resolution_high 0.7964 _cod_data_source_file bt5373Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'chrz0408 in P2(1)2(1)2; Gzella et al.' _shelx_refln_list_code 4 _shelx_f_calc_maximum 62.01 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 5.97 3.89 0.11 o 6 0 0 1149.62 1107.32 15.90 o 8 0 0 272.48 267.28 2.94 o 10 0 0 1648.23 1568.80 13.99 o 12 0 0 197.47 190.17 1.09 o 1 1 0 890.64 781.62 6.21 o 3 1 0 388.20 373.20 3.21 o 4 1 0 54.60 43.09 0.57 o 5 1 0 210.29 231.37 1.72 o 6 1 0 106.57 110.55 1.08 o 7 1 0 90.19 93.11 0.83 o 8 1 0 13.06 16.18 0.35 o 9 1 0 1.94 4.05 0.38 o 10 1 0 200.92 207.85 0.92 o 11 1 0 0.36 0.50 0.20 o 12 1 0 112.63 110.67 1.26 o 13 1 0 11.47 9.98 0.17 o 1 2 0 350.41 327.42 2.25 o 3 2 0 1099.67 1091.92 5.93 o 4 2 0 386.79 402.34 1.18 o 5 2 0 148.31 150.81 0.68 o 6 2 0 333.44 351.27 1.38 o 7 2 0 84.13 92.13 0.80 o 8 2 0 89.87 73.21 1.14 o 9 2 0 14.48 13.83 0.40 o 10 2 0 67.51 59.55 0.51 o 11 2 0 12.66 12.07 0.28 o 12 2 0 614.55 630.24 6.56 o 13 2 0 71.42 69.30 0.55 o 1 3 0 150.01 148.03 0.74 o 2 3 0 198.84 194.69 0.70 o 3 3 0 5.88 5.83 0.15 o 4 3 0 927.88 849.02 4.35 o 5 3 0 164.08 186.17 1.01 o 6 3 0 91.96 104.55 0.99 o 7 3 0 89.96 74.71 1.16 o 8 3 0 1.47 1.94 0.16 o 9 3 0 1.06 0.83 0.12 o 10 3 0 442.90 441.88 4.85 o 11 3 0 51.87 54.79 0.46 o 12 3 0 12.06 10.02 0.34 o 13 3 0 0.16 0.81 0.18 o 1 4 0 137.84 129.68 0.41 o 2 4 0 1798.59 1594.03 7.83 o 3 4 0 341.54 357.42 2.92 o 4 4 0 275.14 279.11 0.87 o 5 4 0 117.36 84.52 0.93 o 6 4 0 3.69 4.92 0.25 o 7 4 0 67.01 62.78 0.83 o 8 4 0 13.12 11.58 0.38 o 9 4 0 173.79 163.87 0.76 o 10 4 0 124.73 124.74 0.79 o 11 4 0 196.57 196.94 2.97 o 12 4 0 44.69 47.81 0.57 o 13 4 0 111.37 109.79 0.64 o 2 5 0 1156.36 1090.94 9.61 o 4 5 0 1506.74 1572.23 8.21 o 5 5 0 1274.16 1352.03 11.80 o 6 5 0 7.20 6.74 0.22 o 7 5 0 3.68 2.25 0.18 o 8 5 0 11.18 13.43 0.26 o 9 5 0 146.19 146.73 1.40 o 10 5 0 43.99 43.27 0.43 o 11 5 0 208.40 217.40 1.24 o 12 5 0 116.38 119.57 0.81 o 0 6 0 1209.02 1160.31 10.51 o 1 6 0 2166.06 2064.12 14.15 o 2 6 0 593.11 583.48 4.35 o 3 6 0 1945.53 1841.60 11.44 o 4 6 0 981.75 1025.39 3.12 o 5 6 0 890.40 908.98 2.68 o 6 6 0 8.72 12.99 0.35 o 7 6 0 12.72 11.68 0.53 o 8 6 0 74.71 78.64 0.41 o 9 6 0 351.91 343.73 2.37 o 10 6 0 147.87 141.18 1.56 o 11 6 0 244.03 266.96 1.31 o 12 6 0 99.82 100.99 0.71 o 1 7 0 28.29 17.21 0.29 o 2 7 0 842.21 840.02 4.10 o 3 7 0 1905.33 1952.66 15.92 o 4 7 0 110.34 110.34 0.79 o 5 7 0 289.65 299.68 1.36 o 6 7 0 13.25 16.95 0.31 o 7 7 0 8.24 9.18 0.32 o 8 7 0 37.93 38.65 0.65 o 9 7 0 24.79 22.95 0.34 o 10 7 0 14.20 15.67 0.41 o 11 7 0 7.52 9.40 0.49 o 12 7 0 20.28 20.83 0.33 o 0 8 0 432.81 444.82 1.97 o 1 8 0 30.92 25.25 0.31 o 2 8 0 2.49 1.15 0.17 o 3 8 0 579.33 625.57 2.31 o 4 8 0 15.21 12.00 0.37 o 5 8 0 24.94 27.55 0.58 o 6 8 0 140.22 144.54 1.66 o 7 8 0 15.52 16.50 0.24 o 8 8 0 27.32 27.99 0.27 o 9 8 0 49.29 45.62 0.69 o 10 8 0 65.79 64.81 0.50 o 11 8 0 0.11 0.46 0.15 o 1 9 0 533.27 485.41 3.97 o 2 9 0 305.22 311.32 1.89 o 3 9 0 454.53 439.72 1.52 o 4 9 0 500.75 506.04 2.34 o 5 9 0 491.77 521.75 3.51 o 6 9 0 16.93 17.64 0.42 o 7 9 0 12.45 14.16 0.75 o 8 9 0 13.48 12.01 0.21 o 9 9 0 11.86 9.45 0.24 o 10 9 0 2.41 6.35 0.21 o 11 9 0 77.88 81.72 0.45 o 0 10 0 2839.17 2870.77 49.97 o 1 10 0 295.22 316.69 2.96 o 2 10 0 232.12 221.10 1.66 o 3 10 0 11.19 13.11 0.39 o 4 10 0 266.77 243.86 1.99 o 5 10 0 17.12 17.12 0.24 o 6 10 0 215.63 212.30 3.01 o 7 10 0 0.42 0.44 0.35 o 8 10 0 218.60 213.90 4.03 o 9 10 0 18.72 10.44 1.74 o 10 10 0 16.94 17.32 0.43 o 11 10 0 88.17 90.71 0.69 o 1 11 0 116.71 123.38 0.94 o 2 11 0 0.28 0.65 0.21 o 3 11 0 50.30 51.50 1.32 o 4 11 0 1124.15 1113.04 4.33 o 5 11 0 741.41 716.50 3.78 o 6 11 0 96.42 86.50 1.24 o 7 11 0 13.12 11.35 0.41 o 8 11 0 204.44 181.02 1.98 o 9 11 0 44.41 38.56 0.92 o 10 11 0 0.08 0.19 0.23 o 11 11 0 5.47 6.06 0.23 o 0 12 0 331.69 303.49 1.93 o 1 12 0 33.68 40.09 0.58 o 2 12 0 66.14 65.51 1.01 o 3 12 0 29.44 32.44 0.43 o 4 12 0 184.75 186.18 0.91 o 5 12 0 31.73 32.98 0.59 o 6 12 0 9.51 13.03 0.41 o 7 12 0 340.64 293.51 1.64 o 8 12 0 305.70 300.81 4.30 o 9 12 0 0.00 0.28 0.18 o 10 12 0 3.55 2.46 0.24 o 11 12 0 0.05 1.02 0.14 o 1 13 0 38.22 37.90 0.32 o 2 13 0 193.97 191.56 0.91 o 3 13 0 37.05 30.13 0.33 o 4 13 0 1080.17 1005.38 4.85 o 5 13 0 96.79 83.41 0.86 o 6 13 0 581.38 551.64 2.19 o 7 13 0 36.87 37.93 0.62 o 8 13 0 20.16 23.85 0.41 o 9 13 0 3.58 3.59 0.19 o 10 13 0 5.68 6.04 0.24 o 11 13 0 55.96 56.74 0.38 o 0 14 0 19.37 19.34 0.83 o 1 14 0 299.99 283.75 0.96 o 2 14 0 152.59 143.68 0.97 o 3 14 0 15.65 17.53 0.27 o 4 14 0 12.60 10.42 0.35 o 5 14 0 199.65 181.04 1.23 o 6 14 0 48.80 55.35 0.71 o 7 14 0 71.53 66.44 0.75 o 8 14 0 8.05 11.11 0.26 o 9 14 0 17.10 12.46 2.18 o 10 14 0 0.73 0.77 0.15 o 1 15 0 21.60 21.11 0.26 o 2 15 0 79.00 69.65 0.53 o 3 15 0 39.08 34.23 0.37 o 4 15 0 182.86 163.03 1.08 o 5 15 0 211.48 201.49 1.23 o 6 15 0 4.98 7.24 0.33 o 7 15 0 100.55 101.87 0.61 o 8 15 0 16.60 16.43 0.24 o 9 15 0 2.09 2.09 0.13 o 0 16 0 500.27 479.35 9.11 o 1 16 0 4.91 4.75 0.18 o 2 16 0 44.11 48.58 0.72 o 3 16 0 18.03 20.75 0.42 o 4 16 0 5.27 4.26 0.24 o 5 16 0 1.06 2.50 0.34 o 6 16 0 30.09 36.34 0.74 o 7 16 0 1.84 1.55 0.16 o 8 16 0 53.03 44.65 0.34 o 9 16 0 37.11 30.28 0.75 o 1 17 0 0.00 0.17 0.12 o 2 17 0 70.79 73.46 1.25 o 3 17 0 0.23 0.20 0.16 o 4 17 0 70.35 69.75 0.74 o 5 17 0 197.02 211.80 0.77 o 6 17 0 3.04 2.84 0.12 o 7 17 0 5.39 6.75 0.20 o 8 17 0 8.44 8.47 0.45 o 0 18 0 258.97 261.96 2.41 o 1 18 0 24.24 22.53 0.29 o 2 18 0 0.51 0.60 0.14 o 3 18 0 134.26 141.31 0.90 o 4 18 0 333.81 346.55 3.43 o 5 18 0 102.53 101.69 0.61 o 6 18 0 40.35 33.56 0.31 o 7 18 0 4.58 3.12 0.51 o 1 19 0 1.07 1.35 0.16 o 2 19 0 23.89 23.14 0.27 o 3 19 0 1.43 0.90 0.13 o 4 19 0 7.82 10.14 0.27 o 5 19 0 41.66 45.85 0.33 o 6 19 0 0.02 0.04 0.09 o 0 20 0 126.88 134.43 0.81 o 1 20 0 0.44 0.82 0.11 o 2 20 0 1.14 1.93 0.14 o 3 20 0 31.13 31.40 0.45 o 4 20 0 9.07 8.09 0.15 o 5 20 0 25.14 22.85 0.27 o 1 21 0 107.38 122.80 0.64 o 2 21 0 20.51 18.80 0.27 o 3 21 0 1.12 2.12 0.09 o 2 0 1 40.65 57.73 0.33 o 3 0 1 22.64 21.80 0.36 o 4 0 1 70.27 66.44 0.68 o 5 0 1 79.55 68.54 0.82 o 6 0 1 32.93 34.11 0.85 o 7 0 1 266.61 304.45 2.54 o 8 0 1 57.72 65.67 0.48 o 9 0 1 110.18 113.97 0.96 o 10 0 1 222.98 226.83 2.58 o 11 0 1 676.26 684.05 7.71 o 12 0 1 115.12 119.98 0.90 o 13 0 1 13.61 13.18 0.27 o -13 1 1 35.08 35.65 0.41 o -12 1 1 12.47 12.76 0.25 o -11 1 1 144.25 148.63 0.76 o -10 1 1 118.22 116.19 0.69 o -9 1 1 3.21 3.97 0.19 o -8 1 1 16.47 16.01 0.33 o -7 1 1 6.79 7.92 0.34 o -6 1 1 297.00 317.23 3.03 o -5 1 1 25.41 23.54 0.34 o -4 1 1 16.42 17.29 0.24 o -3 1 1 1418.94 1352.81 16.28 o -1 1 1 1048.72 915.05 9.29 o 0 1 1 931.37 797.60 4.94 o 1 1 1 1051.65 918.82 14.63 o 3 1 1 1426.44 1411.36 15.32 o 4 1 1 16.64 16.80 0.21 o 5 1 1 25.96 23.73 0.39 o 6 1 1 291.29 312.36 1.56 o 7 1 1 6.75 8.27 0.83 o 8 1 1 16.63 15.93 0.28 o 9 1 1 3.18 4.22 0.33 o 10 1 1 118.63 116.33 0.99 o 11 1 1 143.06 149.76 0.76 o 12 1 1 12.94 13.37 0.26 o 13 1 1 35.06 35.02 0.37 o -13 2 1 72.23 74.37 0.56 o -12 2 1 28.24 29.71 0.44 o -11 2 1 108.32 112.48 0.65 o -10 2 1 192.96 196.47 4.44 o -9 2 1 521.61 513.49 8.14 o -8 2 1 628.87 621.25 6.16 o -7 2 1 161.64 181.55 0.97 o -6 2 1 932.49 954.45 3.44 o -5 2 1 1329.33 1365.47 12.47 o -4 2 1 700.50 690.00 6.99 o 3 2 1 3845.80 3251.24 24.55 o 4 2 1 697.09 674.84 2.91 o 5 2 1 1332.95 1353.80 10.32 o 6 2 1 929.39 957.10 5.38 o 7 2 1 163.91 181.85 1.23 o 8 2 1 627.12 624.69 6.33 o 9 2 1 521.75 520.60 2.11 o 10 2 1 191.31 196.88 3.73 o 11 2 1 107.81 110.22 0.65 o 12 2 1 27.93 29.38 0.33 o -13 3 1 9.20 8.36 0.23 o -12 3 1 1.44 1.84 0.25 o -11 3 1 46.96 49.72 0.44 o -10 3 1 331.22 330.91 1.11 o -9 3 1 480.62 477.13 2.57 o -8 3 1 349.31 356.28 5.22 o -7 3 1 143.34 135.81 1.80 o -6 3 1 488.12 514.44 3.49 o -5 3 1 642.92 722.99 5.91 o -4 3 1 1134.17 1146.13 5.48 o -3 3 1 322.79 315.81 2.53 o -2 3 1 740.79 733.99 4.15 o 2 3 1 733.83 715.05 3.53 o 3 3 1 324.90 312.81 0.80 o 4 3 1 1130.99 1124.01 5.29 o 5 3 1 642.38 711.67 3.58 o 6 3 1 492.76 519.21 4.75 o 7 3 1 143.11 137.13 1.16 o 8 3 1 347.70 353.46 2.22 o 9 3 1 481.14 472.15 3.96 o 10 3 1 331.04 336.65 0.90 o 11 3 1 47.67 50.05 0.45 o 12 3 1 1.60 1.67 0.25 o -13 4 1 85.57 85.89 0.56 o -12 4 1 238.83 244.98 1.18 o -11 4 1 27.06 27.90 0.63 o -10 4 1 129.72 138.72 0.71 o -9 4 1 18.49 17.54 0.48 o -8 4 1 32.47 38.12 0.40 o -7 4 1 154.95 156.96 1.20 o -6 4 1 896.48 945.06 4.41 o -5 4 1 657.09 670.11 3.57 o -4 4 1 1144.80 1189.00 9.69 o -3 4 1 301.23 283.36 0.76 o -2 4 1 1490.51 1351.33 6.29 o -1 4 1 22.79 25.31 0.25 o 0 4 1 185.76 183.72 0.62 o 1 4 1 22.16 24.43 0.29 o 2 4 1 1487.30 1364.96 12.17 o 3 4 1 299.75 279.37 1.90 o 4 4 1 1141.81 1172.95 9.45 o 5 4 1 663.54 681.88 3.26 o 6 4 1 895.86 935.63 8.04 o 7 4 1 154.88 160.20 1.25 o 8 4 1 31.90 37.27 0.51 o 9 4 1 18.49 17.37 0.34 o 10 4 1 130.20 139.37 0.60 o 11 4 1 27.73 28.56 0.34 o 12 4 1 238.80 244.61 1.18 o -13 5 1 30.81 31.26 0.33 o -12 5 1 265.37 265.57 1.19 o -11 5 1 82.08 82.29 0.78 o -10 5 1 50.61 53.43 0.47 o -9 5 1 52.11 45.81 0.78 o -8 5 1 160.49 142.08 1.51 o -7 5 1 63.26 67.58 1.05 o -6 5 1 7.04 5.02 0.48 o -5 5 1 1289.12 1353.95 5.43 o -4 5 1 389.74 424.18 3.09 o -3 5 1 451.20 445.16 1.88 o -2 5 1 1720.62 1612.03 12.78 o -1 5 1 1945.04 1825.58 6.83 o 0 5 1 29.50 22.28 0.24 o 1 5 1 1950.96 1821.23 8.38 o 2 5 1 1717.35 1643.25 7.18 o 3 5 1 447.68 440.81 2.11 o 4 5 1 391.80 426.22 3.92 o 5 5 1 1292.15 1348.34 4.97 o 6 5 1 6.63 4.63 0.23 o 7 5 1 62.66 70.27 0.84 o 8 5 1 162.31 143.23 1.06 o 9 5 1 52.66 46.76 0.65 o 10 5 1 50.86 53.52 0.37 o 11 5 1 81.94 81.69 0.53 o 12 5 1 266.10 267.49 1.18 o -13 6 1 103.26 97.44 0.49 o -12 6 1 72.02 76.93 0.62 o -11 6 1 137.57 129.81 0.93 o -10 6 1 97.07 93.87 0.64 o -9 6 1 9.27 10.71 0.32 o -8 6 1 71.95 72.65 1.03 o -7 6 1 285.60 290.38 5.67 o -6 6 1 57.41 55.54 0.58 o -5 6 1 750.92 777.27 7.79 o -4 6 1 240.58 219.29 2.56 o -3 6 1 504.18 518.78 2.95 o -2 6 1 1512.10 1522.40 11.44 o -1 6 1 3132.48 2891.21 22.30 o 0 6 1 962.83 893.72 6.41 o 1 6 1 3118.22 2846.10 37.62 o 2 6 1 1509.36 1497.30 6.27 o 3 6 1 503.00 516.18 3.74 o 4 6 1 237.62 214.16 1.59 o 5 6 1 745.21 790.58 4.52 o 6 6 1 57.43 58.17 0.59 o 7 6 1 283.67 288.04 5.16 o 8 6 1 71.05 68.65 0.44 o 9 6 1 9.49 10.93 0.20 o 10 6 1 96.33 94.51 0.62 o 11 6 1 138.31 129.91 0.65 o 12 6 1 72.01 80.02 0.63 o -12 7 1 35.68 35.02 0.40 o -11 7 1 60.59 59.62 0.61 o -10 7 1 99.69 99.99 0.61 o -9 7 1 104.38 95.78 0.63 o -8 7 1 245.62 249.63 3.25 o -7 7 1 18.02 21.81 0.39 o -6 7 1 36.45 36.18 0.48 o -5 7 1 446.15 483.78 2.89 o -4 7 1 196.71 203.07 2.63 o -3 7 1 264.35 282.78 1.70 o -2 7 1 130.45 144.87 1.43 o -1 7 1 743.54 762.73 3.19 o 0 7 1 2313.40 2197.51 10.94 o 1 7 1 743.81 770.53 6.09 o 2 7 1 130.01 143.79 0.76 o 3 7 1 266.66 282.05 1.84 o 4 7 1 195.62 202.23 1.56 o 5 7 1 447.08 490.86 1.60 o 6 7 1 35.76 36.67 0.49 o 7 7 1 17.84 20.98 0.23 o 8 7 1 246.38 252.11 0.93 o 9 7 1 102.95 94.40 1.11 o 10 7 1 100.44 100.81 0.63 o 11 7 1 60.57 59.98 0.44 o -12 8 1 2.34 2.87 0.16 o -11 8 1 20.64 21.00 0.37 o -10 8 1 132.24 134.37 0.69 o -9 8 1 78.98 86.04 0.78 o -8 8 1 43.32 39.91 0.41 o -7 8 1 328.80 328.44 6.15 o -6 8 1 415.91 383.83 10.40 o -5 8 1 95.18 104.55 1.07 o -4 8 1 637.58 649.34 3.98 o -3 8 1 1671.95 1718.34 16.58 o -2 8 1 824.40 845.55 9.96 o -1 8 1 470.40 482.21 4.37 o 0 8 1 14.42 16.73 0.34 o 1 8 1 466.28 476.83 3.82 o 2 8 1 818.79 847.18 4.50 o 3 8 1 1670.92 1712.42 13.43 o 4 8 1 641.75 644.58 12.32 o 5 8 1 96.27 107.11 0.95 o 6 8 1 415.50 387.11 3.62 o 7 8 1 327.12 327.54 3.20 o 8 8 1 43.73 40.21 0.43 o 9 8 1 79.56 87.01 0.81 o 10 8 1 131.65 135.84 1.12 o 11 8 1 20.69 20.82 0.40 o -11 9 1 69.50 72.01 0.41 o -10 9 1 18.98 19.99 0.28 o -9 9 1 99.25 99.74 1.05 o -8 9 1 370.73 357.62 1.53 o -7 9 1 150.57 137.38 1.81 o -6 9 1 54.54 53.46 2.02 o -5 9 1 5.44 5.00 0.23 o -4 9 1 39.60 36.24 0.50 o -3 9 1 335.09 340.33 2.86 o -2 9 1 423.50 417.39 2.97 o -1 9 1 343.60 350.15 1.40 o 0 9 1 275.67 283.69 1.13 o 1 9 1 342.37 348.06 2.78 o 2 9 1 421.98 416.97 2.72 o 3 9 1 333.97 342.20 1.60 o 4 9 1 39.79 37.72 0.59 o 5 9 1 5.18 4.42 0.49 o 6 9 1 55.92 53.98 0.92 o 7 9 1 150.49 136.97 0.85 o 8 9 1 372.18 356.09 1.13 o 9 9 1 98.07 97.44 1.10 o 10 9 1 18.94 20.39 0.62 o 11 9 1 69.45 73.70 0.66 o -11 10 1 5.20 5.38 0.24 o -10 10 1 124.68 122.56 0.94 o -9 10 1 44.61 42.49 0.95 o -8 10 1 22.86 26.00 1.15 o -7 10 1 114.45 117.92 1.17 o -5 10 1 16.61 17.22 0.53 o -4 10 1 57.86 60.92 1.12 o -3 10 1 350.67 374.79 2.14 o -2 10 1 96.78 98.04 0.71 o -1 10 1 77.11 78.27 0.63 o 0 10 1 26.33 35.31 0.71 o 1 10 1 76.68 79.42 0.78 o 2 10 1 98.88 101.06 0.79 o 3 10 1 352.43 372.96 4.31 o 4 10 1 58.38 60.28 0.76 o 5 10 1 16.47 16.69 0.53 o 6 10 1 89.08 86.88 0.69 o 7 10 1 113.42 115.97 0.68 o 8 10 1 23.03 25.17 0.94 o 9 10 1 44.39 42.38 0.66 o 10 10 1 124.40 124.98 0.97 o 11 10 1 5.17 5.82 0.25 o -11 11 1 0.99 1.60 0.17 o -10 11 1 3.36 3.19 0.26 o -9 11 1 292.70 298.91 1.55 o -8 11 1 132.34 130.82 1.10 o -7 11 1 7.10 7.89 0.39 o -6 11 1 199.31 211.46 3.82 o -4 11 1 133.67 141.60 1.83 o -3 11 1 271.86 276.50 3.78 o -2 11 1 74.40 81.96 1.07 o -1 11 1 317.90 314.46 3.51 o 0 11 1 136.01 156.97 1.64 o 1 11 1 319.33 316.62 1.43 o 2 11 1 75.73 85.41 1.58 o 3 11 1 273.53 275.22 2.02 o 4 11 1 133.35 133.90 1.50 o 5 11 1 397.98 391.24 3.89 o 6 11 1 198.20 209.10 1.10 o 7 11 1 6.78 7.32 0.26 o 8 11 1 133.18 130.51 1.06 o 9 11 1 291.84 297.17 1.57 o 10 11 1 3.50 3.75 0.28 o 11 11 1 0.92 1.51 0.17 o -11 12 1 23.77 23.55 0.29 o -10 12 1 40.05 42.45 0.52 o -9 12 1 25.81 24.49 0.48 o -8 12 1 30.45 28.20 0.57 o -6 12 1 88.10 83.07 0.88 o -5 12 1 98.78 101.93 0.90 o -4 12 1 260.23 253.41 2.05 o -3 12 1 92.08 92.70 2.11 o -2 12 1 162.46 165.93 1.59 o -1 12 1 105.30 98.89 1.72 o 0 12 1 8.86 10.79 0.33 o 1 12 1 104.71 97.28 1.03 o 2 12 1 164.25 166.23 2.20 o 3 12 1 92.57 88.51 1.52 o 4 12 1 259.25 241.57 1.39 o 5 12 1 98.97 99.22 0.96 o 6 12 1 87.57 81.50 0.87 o 7 12 1 244.86 221.49 1.24 o 8 12 1 29.99 27.34 0.45 o 9 12 1 25.47 25.03 0.34 o 10 12 1 40.53 42.35 0.53 o 11 12 1 23.53 23.50 0.31 o -10 13 1 16.84 18.61 0.34 o -8 13 1 1.66 1.37 0.42 o -6 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