#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/72/2227259.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227259_Fobs loop_ _publ_author_name 'Yuan, Xian-You' 'Zhang, Min' 'Ng, Seik Weng' _publ_section_title ; (5-n-Heptyl-2-hydroxymethyl-1,3-dioxan-2-yl)methanol ; _journal_coeditor_code BT5378 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2918 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.938 _cell_angle_gamma 90.000 _cell_length_a 5.8030 _cell_length_b 54.0168 _cell_length_c 9.1018 _exptl_crystal_F_000 1088.00 _reflns_d_resolution_high 0.7808 _[local]_cod_data_source_file bt5378Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 361.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2924.87 3473.73 161.62 o 4 0 0 59.53 80.89 23.90 o 6 0 0 1029.60 977.37 94.75 o 1 1 0 900.29 808.05 37.83 o 2 1 0 7887.83 7338.60 196.91 o 3 1 0 78.54 78.77 13.02 o 4 1 0 469.64 432.32 23.51 o 5 1 0 4.35 -24.36 27.40 o 6 1 0 65.26 132.28 42.37 o 7 1 0 0.29 88.60 58.33 o 1 2 0 747.33 660.58 21.02 o 2 2 0 697.76 791.02 36.69 o 3 2 0 107.86 115.53 16.25 o 4 2 0 0.86 6.77 15.07 o 5 2 0 0.00 -26.46 26.46 o 6 2 0 646.70 623.43 55.01 o 7 2 0 454.48 538.99 75.72 o 1 3 0 5079.34 5180.16 171.11 o 2 3 0 2699.85 2518.63 72.29 o 3 3 0 118.63 97.90 15.67 o 4 3 0 0.51 4.31 15.47 o 5 3 0 13.23 6.14 28.40 o 6 3 0 17.49 48.40 39.18 o 7 3 0 61.57 142.98 62.14 o 2 4 0 2142.55 2116.42 62.21 o 3 4 0 97.77 118.83 21.28 o 4 4 0 10.03 19.67 16.08 o 5 4 0 24.33 15.31 28.27 o 6 4 0 5.57 36.36 40.92 o 7 4 0 37.04 84.60 53.52 o 1 5 0 1592.12 1559.90 65.30 o 2 5 0 12.81 6.53 9.37 o 3 5 0 43.17 15.36 14.10 o 4 5 0 48.97 69.97 21.34 o 5 5 0 7.47 7.69 27.92 o 6 5 0 38.65 12.79 40.39 o 7 5 0 513.80 783.13 76.01 o 0 6 0 32.55 41.82 7.80 o 1 6 0 101.75 105.15 10.62 o 3 6 0 7.34 2.93 12.66 o 4 6 0 40.91 62.82 29.00 o 5 6 0 264.80 274.37 33.02 o 6 6 0 32.90 51.18 40.51 o 7 6 0 453.55 801.08 83.75 o 1 7 0 10787.74 10609.90 279.07 o 2 7 0 2.21 -1.45 9.34 o 3 7 0 19.23 17.87 12.84 o 4 7 0 82.16 117.32 40.99 o 5 7 0 144.97 136.06 28.44 o 6 7 0 209.72 190.84 47.23 o 7 7 0 2870.98 2813.48 141.73 o 1 8 0 835.45 760.43 25.14 o 2 8 0 1960.57 1981.23 58.86 o 3 8 0 321.05 290.90 19.73 o 4 8 0 1431.80 1262.98 58.96 o 5 8 0 4.89 38.76 30.22 o 6 8 0 0.27 -1.57 39.36 o 7 8 0 138.24 281.38 72.68 o 1 9 0 986.78 923.23 29.42 o 2 9 0 448.33 490.36 21.27 o 3 9 0 207.48 208.23 23.48 o 4 9 0 211.29 224.30 24.73 o 5 9 0 96.73 122.80 28.38 o 6 9 0 0.20 -5.26 38.30 o 7 9 0 100.33 87.54 92.76 o 1 10 0 2975.05 2894.83 71.38 o 2 10 0 1907.82 1872.46 56.65 o 4 10 0 828.80 815.58 36.63 o 5 10 0 231.18 325.27 77.57 o 6 10 0 0.80 -7.05 39.52 o 7 10 0 3.36 39.42 52.63 o 1 11 0 246.01 236.04 10.49 o 2 11 0 726.03 721.73 27.56 o 3 11 0 48.23 31.83 13.84 o 4 11 0 379.11 390.74 41.73 o 5 11 0 413.51 475.18 93.42 o 6 11 0 65.54 91.85 43.65 o 7 11 0 7.16 20.90 52.13 o 0 12 0 117.49 91.43 15.43 o 1 12 0 479.43 445.35 15.40 o 2 12 0 1345.11 1399.55 64.37 o 3 12 0 75.22 50.28 14.60 o 4 12 0 251.98 193.41 113.17 o 5 12 0 512.41 627.35 55.33 o 6 12 0 16.77 28.81 38.90 o 7 12 0 6.70 42.43 52.68 o 1 13 0 30.40 32.93 10.04 o 2 13 0 2088.96 2246.94 66.98 o 3 13 0 219.24 212.79 20.70 o 4 13 0 4.33 3.50 22.63 o 5 13 0 417.78 567.72 72.68 o 6 13 0 604.60 721.49 70.14 o 7 13 0 18.12 16.59 53.28 o 1 14 0 1237.22 1198.39 32.92 o 2 14 0 1613.49 1725.09 53.77 o 3 14 0 539.19 462.47 24.26 o 4 14 0 5.35 17.80 24.09 o 5 14 0 299.13 305.49 66.37 o 6 14 0 3.03 18.67 40.18 o 7 14 0 0.01 36.34 73.68 o 1 15 0 1817.76 1709.15 44.83 o 2 15 0 66.47 44.74 11.91 o 3 15 0 463.12 423.97 26.05 o 4 15 0 332.75 352.36 39.55 o 5 15 0 571.78 502.29 64.88 o 6 15 0 301.84 417.30 58.84 o 7 15 0 3.04 13.27 77.66 o 0 16 0 9909.55 9251.67 410.70 o 1 16 0 1567.16 1488.26 39.81 o 2 16 0 1054.52 1043.59 42.61 o 3 16 0 942.52 889.59 35.38 o 4 16 0 1373.84 1207.41 62.52 o 5 16 0 6.30 37.78 32.93 o 6 16 0 3.48 -22.35 40.99 o 7 16 0 63.73 48.62 78.65 o 1 17 0 1726.36 1633.90 43.27 o 2 17 0 2657.76 2542.03 66.11 o 3 17 0 398.90 366.08 22.50 o 4 17 0 86.31 58.74 26.96 o 5 17 0 384.83 210.91 197.47 o 6 17 0 84.39 150.65 62.56 o 7 17 0 0.94 -0.66 74.51 o 0 18 0 9251.44 8067.88 360.75 o 1 18 0 35.57 32.44 7.01 o 2 18 0 1186.58 1134.25 38.89 o 3 18 0 77.99 109.25 18.19 o 4 18 0 362.73 316.43 39.53 o 5 18 0 214.92 139.93 59.07 o 6 18 0 0.82 54.00 43.82 o 7 18 0 1.95 -30.86 79.65 o 1 19 0 13.11 25.78 16.64 o 2 19 0 113.99 115.57 33.19 o 3 19 0 2243.97 2198.06 69.92 o 4 19 0 116.29 104.70 30.38 o 5 19 0 138.63 118.84 38.24 o 6 19 0 131.21 106.49 46.57 o 7 19 0 7.00 67.20 84.79 o 1 20 0 1543.06 1493.76 47.32 o 2 20 0 13648.87 13995.32 329.11 o 3 20 0 46.45 57.70 13.37 o 4 20 0 5.82 -19.16 26.72 o 5 20 0 301.22 348.60 48.69 o 6 20 0 38.46 30.34 45.55 o 7 20 0 12.67 -20.24 74.84 o 1 21 0 92.22 148.39 57.58 o 2 21 0 8255.98 8251.00 197.96 o 3 21 0 1390.82 1269.74 39.91 o 4 21 0 112.31 74.59 28.91 o 5 21 0 6.81 -7.77 32.70 o 6 21 0 237.59 307.32 79.65 o 7 21 0 13.11 -29.04 75.50 o 0 22 0 24.99 24.69 14.52 o 1 22 0 1183.80 1134.20 39.06 o 2 22 0 67.98 74.82 11.55 o 3 22 0 16.77 39.29 13.65 o 4 22 0 49.20 88.32 30.09 o 5 22 0 542.38 515.86 60.15 o 6 22 0 3.29 24.39 60.90 o 7 22 0 0.40 6.31 76.66 o 1 23 0 321.58 377.58 19.52 o 2 23 0 3.78 -0.48 9.21 o 3 23 0 775.07 683.89 26.65 o 4 23 0 555.40 556.19 32.67 o 5 23 0 61.61 38.17 36.37 o 6 23 0 84.95 95.41 66.21 o 7 23 0 88.32 117.98 83.80 o 0 24 0 260.19 247.91 30.70 o 1 24 0 34.61 28.45 9.31 o 2 24 0 222.42 268.06 22.56 o 3 24 0 417.16 455.54 21.46 o 4 24 0 48.01 102.03 47.28 o 5 24 0 0.47 23.86 24.89 o 6 24 0 16.21 21.07 59.41 o 1 25 0 16.52 27.54 20.41 o 2 25 0 2106.71 2216.97 60.31 o 3 25 0 225.06 238.04 19.08 o 4 25 0 1269.91 1163.42 49.78 o 5 25 0 1238.36 1058.27 66.44 o 6 25 0 108.03 118.31 70.03 o 1 26 0 983.91 898.82 29.37 o 2 26 0 646.47 602.86 24.26 o 3 26 0 761.80 735.68 28.80 o 4 26 0 608.99 654.13 36.19 o 5 26 0 569.89 680.16 70.86 o 6 26 0 1.33 -60.40 60.40 o 1 27 0 33.67 89.43 30.15 o 2 27 0 53.69 84.95 29.84 o 3 27 0 1033.81 1044.08 43.06 o 4 27 0 1374.18 1293.56 54.15 o 5 27 0 611.73 575.35 60.90 o 6 27 0 44.34 47.22 47.90 o 1 28 0 518.58 499.05 20.65 o 2 28 0 2077.88 1841.49 52.00 o 3 28 0 2177.44 2080.40 72.41 o 4 28 0 147.42 148.31 35.06 o 5 28 0 358.71 300.16 49.94 o 6 28 0 4.15 -6.30 51.11 o 1 29 0 11.82 22.89 10.57 o 2 29 0 99.82 104.71 14.06 o 3 29 0 62.99 128.75 19.23 o 4 29 0 135.17 131.53 46.63 o 5 29 0 69.90 87.36 41.43 o 6 29 0 20.45 18.93 61.48 o 0 30 0 37.57 20.78 28.46 o 1 30 0 224.07 219.96 17.07 o 2 30 0 298.39 294.17 22.50 o 3 30 0 504.93 566.89 30.88 o 4 30 0 0.01 -17.42 29.67 o 5 30 0 69.81 45.70 42.38 o 6 30 0 0.03 41.60 52.03 o 1 31 0 138.20 145.63 24.31 o 2 31 0 26.13 20.98 17.81 o 3 31 0 1608.29 1818.78 178.30 o 4 31 0 11.11 8.36 30.85 o 5 31 0 113.64 93.05 43.82 o 6 31 0 136.50 138.86 57.65 o 0 32 0 0.22 -6.58 13.76 o 1 32 0 510.38 466.67 21.07 o 2 32 0 0.55 8.73 15.77 o 3 32 0 11693.92 11132.79 385.17 o 4 32 0 27.37 51.43 34.13 o 5 32 0 8.14 6.76 39.26 o 6 32 0 18.96 -41.70 52.15 o 1 33 0 0.39 52.68 15.86 o 2 33 0 223.89 202.60 22.11 o 4 33 0 162.04 165.35 76.66 o 5 33 0 198.02 92.31 45.05 o 6 33 0 48.44 53.85 53.55 o 0 34 0 18.84 11.06 15.62 o 1 34 0 337.45 330.98 19.14 o 2 34 0 189.87 201.28 22.57 o 3 34 0 1175.92 1216.08 64.88 o 4 34 0 672.48 683.23 51.15 o 5 34 0 36.11 97.26 47.13 o 6 34 0 11.07 -16.05 53.28 o 1 35 0 28.20 53.60 13.08 o 2 35 0 25.30 25.99 16.97 o 3 35 0 1179.60 1214.94 64.94 o 4 35 0 514.24 444.56 51.77 o 5 35 0 295.22 278.63 53.36 o 6 35 0 15.74 31.52 53.56 o 0 36 0 59.11 42.20 17.47 o 1 36 0 462.56 408.21 21.08 o 2 36 0 159.64 165.16 21.90 o 3 36 0 76.62 139.73 74.34 o 4 36 0 185.80 180.83 43.89 o 5 36 0 219.31 166.75 50.86 o 6 36 0 108.82 121.57 59.05 o 1 37 0 50.17 63.05 14.87 o 2 37 0 242.82 250.67 25.75 o 3 37 0 1621.69 1551.93 77.47 o 4 37 0 186.19 147.80 39.66 o 5 37 0 30.00 75.19 45.72 o 6 37 0 8.73 -12.52 54.60 o 0 38 0 47.50 24.93 19.91 o 1 38 0 111.59 112.70 16.55 o 2 38 0 6.00 -3.58 17.53 o 3 38 0 150.78 166.67 35.52 o 4 38 0 207.70 240.65 44.14 o 5 38 0 156.84 226.28 50.56 o 6 38 0 79.41 125.18 59.78 o 1 39 0 63.58 92.48 25.29 o 2 39 0 7.95 21.16 18.76 o 3 39 0 6.60 25.15 29.98 o 4 39 0 1304.75 1089.31 67.82 o 5 39 0 98.37 94.02 44.72 o 6 39 0 118.50 131.16 61.26 o 0 40 0 240.70 259.86 43.48 o 1 40 0 500.18 487.17 23.82 o 2 40 0 12.94 30.26 19.87 o 3 40 0 24.31 46.67 37.50 o 4 40 0 131.36 141.63 39.56 o 5 40 0 115.00 101.87 47.44 o 6 40 0 116.67 69.00 58.33 o 1 41 0 381.17 406.59 30.17 o 2 41 0 210.94 240.13 36.68 o 3 41 0 93.80 76.62 48.54 o 4 41 0 100.58 106.64 40.21 o 5 41 0 136.01 149.38 49.67 o 0 42 0 263.41 213.05 86.95 o 1 42 0 312.33 377.45 27.07 o 2 42 0 831.20 720.63 36.57 o 3 42 0 121.34 113.90 36.23 o 4 42 0 28.74 20.15 37.74 o 5 42 0 20.47 26.06 44.63 o 1 43 0 473.55 437.30 25.52 o 2 43 0 359.34 377.00 30.38 o 3 43 0 19.87 24.54 32.22 o 4 43 0 87.53 101.11 40.40 o 5 43 0 125.02 106.99 48.89 o 0 44 0 115.53 136.47 46.13 o 1 44 0 242.68 254.43 24.11 o 2 44 0 1.45 37.21 22.31 o 3 44 0 163.98 154.65 37.31 o 4 44 0 2.04 -20.71 38.50 o 5 44 0 14.02 107.64 88.61 o 1 45 0 0.00 33.50 18.00 o 2 45 0 268.97 302.88 31.77 o 3 45 0 134.30 85.37 36.02 o 4 45 0 3.41 -38.33 38.92 o 5 45 0 171.23 154.26 53.10 o 0 46 0 0.30 13.02 23.64 o 1 46 0 417.11 430.89 34.42 o 2 46 0 4.70 79.98 41.40 o 3 46 0 195.89 162.43 40.70 o 4 46 0 17.55 4.00 40.71 o 5 46 0 1.28 29.04 50.11 o 1 47 0 55.45 99.31 20.69 o 2 47 0 675.39 608.54 49.70 o 3 47 0 37.45 68.43 35.46 o 4 47 0 3.60 -8.42 42.35 o 5 47 0 3.23 80.01 51.77 o 0 48 0 264.56 275.61 35.61 o 1 48 0 9.77 27.09 19.38 o 2 48 0 78.20 101.53 46.38 o 3 48 0 212.18 169.10 40.60 o 4 48 0 61.81 94.57 46.51 o 5 48 0 21.15 44.84 53.08 o 1 49 0 0.50 15.55 19.15 o 2 49 0 476.35 412.69 69.53 o 3 49 0 58.69 65.24 44.97 o 4 49 0 111.39 35.33 43.97 o 5 49 0 432.52 462.33 69.72 o 0 50 0 0.01 10.66 28.34 o 1 50 0 3.66 14.57 22.11 o 2 50 0 407.32 371.04 69.53 o 3 50 0 80.19 53.33 36.43 o 4 50 0 0.61 8.23 72.51 o 5 50 0 32.75 64.91 58.95 o 1 51 0 165.51 232.15 34.07 o 2 51 0 11.91 35.69 31.45 o 3 51 0 21.41 19.56 37.91 o 4 51 0 181.13 138.89 46.14 o 0 52 0 53.04 51.62 31.14 o 1 52 0 1895.96 1827.32 69.82 o 2 52 0 128.73 106.13 36.44 o 3 52 0 1.07 -29.06 37.25 o 4 52 0 0.08 -23.69 43.90 o 1 53 0 720.89 805.85 43.26 o 2 53 0 90.10 58.53 34.75 o 3 53 0 1.12 35.46 41.15 o 4 53 0 104.83 72.64 48.15 o 0 54 0 761.30 721.49 50.69 o 1 54 0 5.47 135.26 29.87 o 2 54 0 25.35 19.94 43.81 o 3 54 0 52.18 -4.39 39.31 o 4 54 0 0.60 -10.46 44.47 o 1 55 0 24.00 73.19 29.99 o 2 55 0 1.88 33.96 36.26 o 3 55 0 6.25 -23.89 39.31 o 4 55 0 21.94 70.22 48.47 o 0 56 0 13.50 29.70 58.41 o 1 56 0 10.07 48.99 30.38 o 2 56 0 1.45 -17.53 55.67 o 3 56 0 5.37 -6.22 40.39 o 4 56 0 0.37 -22.33 48.28 o 1 57 0 619.05 693.86 54.19 o 2 57 0 221.44 212.54 47.09 o 3 57 0 40.41 16.91 39.41 o 4 57 0 4.13 3.10 49.65 o 0 58 0 44.03 46.13 57.91 o 1 58 0 422.44 542.66 46.88 o 2 58 0 24.51 42.32 41.01 o 3 58 0 42.48 -19.54 42.47 o 4 58 0 0.78 -38.70 51.50 o 1 59 0 272.01 411.82 44.85 o 2 59 0 129.40 130.34 46.38 o 3 59 0 1.49 32.87 44.80 o 0 60 0 0.74 12.94 59.57 o 1 60 0 423.07 527.02 87.28 o 2 60 0 0.28 -3.45 41.23 o 3 60 0 21.37 -35.63 49.95 o 1 61 0 57.22 141.54 66.54 o 2 61 0 7.37 34.84 61.15 o 3 61 0 19.42 32.89 47.66 o 0 62 0 1047.82 1090.87 101.22 o 1 62 0 253.73 369.71 78.82 o 2 62 0 15.53 42.02 45.00 o 3 62 0 26.03 76.09 53.20 o 1 63 0 45.76 100.89 67.20 o 2 63 0 17.48 -18.64 48.12 o 3 63 0 150.37 139.33 79.98 o 0 64 0 826.11 1045.74 101.39 o 1 64 0 2.09 1.00 66.21 o 2 64 0 20.33 -13.11 67.54 o 1 65 0 22.86 22.24 65.05 o 2 65 0 0.20 -32.36 71.68 o 0 66 0 416.16 661.59 101.22 o 1 66 0 0.56 -30.53 69.86 o 2 66 0 7.67 -34.68 71.19 o 1 67 0 0.02 -14.10 69.69 o 0 68 0 48.56 22.90 74.84 o 1 68 0 43.89 155.15 80.48 o -7 0 1 174.92 218.71 80.65 o -5 0 1 53.20 78.65 41.98 o -3 0 1 229.91 200.72 21.25 o 1 0 1 7407.60 7454.41 332.70 o 3 0 1 587.78 549.58 45.47 o 5 0 1 21.07 6.10 29.74 o 7 0 1 2.93 116.65 82.97 o -7 1 1 12.83 57.26 62.48 o -6 1 1 557.35 572.56 51.57 o -5 1 1 113.54 104.36 31.85 o -4 1 1 7.26 0.14 15.30 o -3 1 1 62.73 43.96 13.23 o -2 1 1 407.77 362.53 14.11 o -1 1 1 18638.16 20231.07 464.70 o 0 1 1 291.73 279.94 18.75 o 1 1 1 16796.39 16415.25 508.18 o 2 1 1 253.69 267.84 20.47 o 3 1 1 230.15 264.66 27.10 o 4 1 1 0.54 12.95 22.02 o 5 1 1 0.01 12.77 24.97 o 6 1 1 2.60 101.67 69.78 o 7 1 1 433.73 592.47 77.78 o -7 2 1 10.97 27.57 49.55 o -6 2 1 1181.13 1107.90 71.28 o -5 2 1 91.51 97.38 32.36 o -4 2 1 282.13 306.30 22.24 o -3 2 1 400.31 341.15 16.90 o -2 2 1 264.60 275.73 15.42 o -1 2 1 2844.53 3038.11 102.22 o 0 2 1 2618.19 2007.35 103.05 o 1 2 1 1704.14 1731.07 60.55 o 2 2 1 584.91 546.90 27.87 o 3 2 1 1101.24 1163.73 50.68 o 4 2 1 0.08 18.52 18.87 o 5 2 1 2.76 15.63 25.56 o 6 2 1 1449.13 1512.63 91.76 o 7 2 1 19.16 0.06 52.14 o -7 3 1 11.37 -5.34 49.31 o -6 3 1 6.09 30.88 36.48 o -5 3 1 374.88 377.88 44.11 o -4 3 1 530.49 513.64 28.64 o -3 3 1 83.18 83.05 12.12 o -2 3 1 1175.79 1082.93 32.60 o -1 3 1 165.42 243.20 25.80 o 0 3 1 161.91 145.07 9.40 o 1 3 1 2596.39 2376.94 79.90 o 2 3 1 49.34 18.84 14.31 o 3 3 1 97.60 145.53 22.81 o 4 3 1 2.89 -3.88 19.36 o 5 3 1 8.44 28.48 27.08 o 6 3 1 1397.93 1527.64 90.56 o 7 3 1 57.48 148.59 59.10 o -7 4 1 4.29 25.30 48.28 o -6 4 1 207.39 227.06 45.64 o -5 4 1 231.30 254.66 38.70 o -4 4 1 63.80 51.90 15.52 o -3 4 1 10.78 8.27 10.26 o -2 4 1 228.56 264.52 14.20 o -1 4 1 4535.74 4737.18 132.26 o 0 4 1 156.73 160.44 15.85 o 1 4 1 3879.77 3550.91 115.75 o 2 4 1 107.34 108.99 34.35 o 3 4 1 106.76 113.86 21.18 o 4 4 1 188.22 214.59 25.81 o 5 4 1 220.39 304.85 42.83 o 6 4 1 621.61 768.28 68.23 o 7 4 1 6.10 29.33 79.15 o -7 5 1 17.73 92.66 101.22 o -6 5 1 75.48 102.55 38.48 o -5 5 1 281.18 279.32 39.98 o -4 5 1 203.52 179.62 28.22 o -3 5 1 128.18 132.65 13.30 o -2 5 1 3467.96 3498.25 84.95 o -1 5 1 27054.25 27901.12 791.25 o 0 5 1 36.69 33.50 4.54 o 1 5 1 2564.93 2535.26 84.89 o 2 5 1 2650.78 2769.52 95.85 o 3 5 1 40.74 68.36 16.39 o 4 5 1 3.39 8.37 19.51 o 5 5 1 177.03 193.76 48.37 o 6 5 1 3.83 108.71 44.06 o 7 5 1 173.77 219.72 155.90 o -7 6 1 653.52 774.76 81.37 o -6 6 1 255.78 273.54 47.06 o -5 6 1 179.80 225.16 37.26 o -4 6 1 200.92 207.34 25.76 o -3 6 1 16.75 11.47 10.54 o -2 6 1 1107.42 1118.33 56.73 o -1 6 1 6447.55 6435.91 229.40 o 0 6 1 775.09 827.32 24.81 o 1 6 1 660.94 594.28 26.85 o 2 6 1 1516.13 1398.69 75.00 o 3 6 1 1184.04 1134.66 42.45 o 4 6 1 399.05 448.16 31.42 o 5 6 1 31.57 51.40 33.20 o 6 6 1 1032.32 1266.16 201.61 o 7 6 1 1099.57 1046.92 84.23 o -7 7 1 457.77 546.17 72.48 o -6 7 1 0.84 27.34 35.38 o -5 7 1 99.54 101.19 52.35 o -4 7 1 300.51 334.37 29.88 o -3 7 1 482.02 449.75 19.33 o -2 7 1 855.50 873.88 72.43 o -1 7 1 5543.28 5720.96 204.60 o 0 7 1 2319.39 2220.41 55.37 o 1 7 1 1987.97 1985.12 57.82 o 2 7 1 2201.13 2427.09 72.46 o 3 7 1 446.48 456.29 25.07 o 4 7 1 3.36 18.48 19.55 o 5 7 1 190.07 236.87 53.02 o 6 7 1 596.98 760.16 105.70 o 7 7 1 61.08 205.70 61.48 o -7 8 1 358.22 397.25 90.10 o -6 8 1 29.19 82.08 38.35 o -5 8 1 369.57 437.52 46.78 o -4 8 1 643.15 559.60 31.16 o -3 8 1 54.74 39.33 12.23 o -2 8 1 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