#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:46:27 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181193 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/72/2227268.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227268_Fobs loop_ _publ_author_name 'Liu, Jia-Lu' 'Liu, Jian-Feng' 'Zhao, Guo-Liang' _publ_section_title ; Bis[\m-2-(4-hydroxyphenyl)acetato]-\k^3^O,O':O;\k^3^O:O,O'-bis{aqua(4,4'-bipyridine-\kN)bis[2-(4-hydroxyphenyl)acetato-\k^2^O,O']ytterbium(III)} monohydrate ; _journal_coeditor_code BT5388 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1489 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 83.269 _cell_angle_beta 72.377 _cell_angle_gamma 71.441 _cell_length_a 11.6885 _cell_length_b 16.1322 _cell_length_c 18.4560 _exptl_crystal_F_000 1616.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file bt5388Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' J in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 400.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 11493.39 11908.15 266.54 o 2 0 0 86928.90 83233.15 1682.59 o 3 0 0 1394.54 1537.88 39.23 o 4 0 0 12865.33 13717.08 194.14 o 5 0 0 18912.65 18566.27 259.19 o 6 0 0 147.25 106.91 22.10 o 7 0 0 16371.75 16214.24 278.27 o 8 0 0 11760.22 12408.32 339.09 o 9 0 0 1249.02 1196.05 115.52 o 10 0 0 1640.89 1774.87 177.54 o 11 0 0 113.09 102.42 86.57 o 12 0 0 1416.71 1164.57 401.98 o -12 1 0 33.74 46.70 89.93 o -11 1 0 556.45 440.45 114.08 o -10 1 0 1.37 0.00 99.09 o -9 1 0 6533.20 6543.28 592.04 o -8 1 0 7617.03 6954.79 629.52 o -7 1 0 9492.95 9456.57 558.07 o -6 1 0 13039.47 12947.11 206.04 o -5 1 0 5991.25 5897.57 111.74 o -4 1 0 9337.17 9728.06 151.29 o -3 1 0 5232.32 5433.71 85.92 o -2 1 0 76733.63 75198.15 1253.56 o -1 1 0 62443.82 61973.99 1259.33 o 0 1 0 2203.42 0.00 4.37 o 2 1 0 3640.62 3806.11 70.71 o 3 1 0 265.20 331.16 25.04 o 4 1 0 37423.93 38016.42 467.93 o 5 1 0 3601.52 3714.33 77.13 o 6 1 0 37401.52 37497.61 483.28 o 7 1 0 2009.10 2027.61 66.59 o 8 1 0 5891.52 5418.28 234.58 o 9 1 0 2077.82 2107.10 145.16 o 10 1 0 530.71 605.35 99.10 o 11 1 0 2748.96 2224.08 174.52 o 12 1 0 155.83 103.84 100.96 o -12 2 0 53.59 82.57 96.41 o -11 2 0 654.94 610.93 128.96 o -10 2 0 8543.47 9154.17 382.40 o -9 2 0 181.41 181.23 95.89 o -8 2 0 10666.29 10468.82 377.17 o 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1693.02 1898.77 59.27 o 2 3 0 24.98 22.51 13.13 o 3 3 0 74464.50 73616.79 1253.16 o 4 3 0 12960.91 13381.00 199.10 o 5 3 0 5138.57 5146.37 91.85 o 6 3 0 4836.56 4633.34 96.58 o 7 3 0 17.00 17.40 16.56 o 8 3 0 217.21 252.19 30.78 o 9 3 0 839.13 860.79 68.48 o 10 3 0 7096.15 6978.81 194.34 o 11 3 0 7809.20 8271.48 295.76 o 12 3 0 273.56 254.51 91.43 o 13 3 0 2230.10 2159.21 232.45 o -11 4 0 5275.23 4749.73 315.76 o -10 4 0 2718.13 2655.97 231.49 o -9 4 0 524.78 399.19 107.44 o -8 4 0 0.43 0.00 69.34 o -7 4 0 18.65 0.00 47.72 o -6 4 0 7762.63 7819.75 166.51 o -5 4 0 17769.06 18611.70 284.91 o -4 4 0 7154.81 7142.97 131.61 o -3 4 0 43183.89 42403.00 568.54 o -2 4 0 1963.99 1966.44 70.82 o -1 4 0 1923.97 1988.12 112.31 o 0 4 0 3416.33 3489.28 82.39 o 1 4 0 21411.23 21550.96 526.38 o 2 4 0 119720.82 110549.45 2250.35 o 3 4 0 261.15 222.40 35.38 o 4 4 0 63186.88 65594.77 960.72 o 5 4 0 9303.20 9710.74 159.92 o 6 4 0 15.80 9.00 14.92 o 7 4 0 3677.44 3712.23 92.47 o 8 4 0 437.75 393.12 43.40 o 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2582.60 79.13 o 2 7 0 838.69 924.06 62.24 o 3 7 0 11657.59 13101.84 287.17 o 4 7 0 386.01 293.93 41.44 o 5 7 0 12613.04 11674.17 221.31 o 6 7 0 2972.64 3138.00 122.88 o 7 7 0 12959.54 12796.99 293.55 o 8 7 0 5829.49 6105.01 159.78 o 9 7 0 581.31 468.55 51.68 o 10 7 0 37.01 22.90 34.20 o 11 7 0 35.55 0.00 36.18 o 12 7 0 4337.42 4451.66 341.70 o 13 7 0 2107.33 1838.69 284.70 o -9 8 0 4193.16 3843.97 337.25 o -8 8 0 3191.74 3216.60 151.50 o -7 8 0 2280.96 2193.79 129.17 o -6 8 0 4986.29 5164.86 347.45 o -5 8 0 22.81 12.48 30.76 o -4 8 0 7217.00 7601.99 188.16 o -3 8 0 3475.27 3370.60 101.01 o -2 8 0 19318.57 19856.14 322.39 o -1 8 0 18463.61 17779.87 290.42 o 0 8 0 2750.78 3086.88 80.05 o 1 8 0 713.09 588.93 82.24 o 2 8 0 868.38 907.37 45.95 o 3 8 0 8948.92 8149.67 212.31 o 4 8 0 26373.97 27283.24 534.38 o 5 8 0 5365.63 5592.16 176.47 o 6 8 0 34249.70 34686.57 661.80 o 7 8 0 229.50 221.53 46.99 o 8 8 0 147.86 174.73 48.15 o 9 8 0 78.07 29.48 34.07 o 10 8 0 782.01 803.72 77.26 o 11 8 0 6576.09 6811.60 247.49 o 12 8 0 178.47 45.14 91.44 o 13 8 0 3730.36 4300.44 310.78 o -9 9 0 122.29 85.09 106.31 o -8 9 0 2587.96 2520.10 196.97 o -7 9 0 991.82 1052.68 113.51 o -6 9 0 357.02 250.10 62.70 o -5 9 0 1224.12 1392.23 111.74 o -4 9 0 36.17 23.54 39.80 o -3 9 0 20100.48 19510.12 419.51 o -2 9 0 4455.28 4476.52 130.22 o -1 9 0 11278.67 11148.17 206.99 o 0 9 0 2647.88 2466.40 76.72 o 1 9 0 81.63 63.22 22.75 o 2 9 0 37952.44 38111.66 831.50 o 3 9 0 3718.06 3560.11 235.90 o 4 9 0 24730.61 24467.42 498.55 o 5 9 0 33741.40 34357.48 662.84 o 6 9 0 1025.76 1017.91 80.78 o 7 9 0 4298.48 4762.97 162.65 o 8 9 0 495.37 516.09 68.05 o 9 9 0 3527.85 3816.80 136.01 o 10 9 0 8304.93 8510.14 252.07 o 11 9 0 1073.44 1229.08 95.81 o 12 9 0 6390.53 6678.82 291.36 o 13 9 0 412.57 439.08 135.17 o -8 10 0 212.55 191.92 129.01 o -7 10 0 525.60 429.26 82.34 o -6 10 0 3530.45 3437.73 176.10 o -5 10 0 1122.51 942.08 101.83 o -4 10 0 21815.66 21255.87 603.99 o -3 10 0 22.62 58.24 37.15 o -2 10 0 6532.69 6773.50 158.92 o -1 10 0 125.95 99.78 29.83 o 0 10 0 102.64 46.07 25.57 o 1 10 0 6870.25 7123.73 207.48 o 2 10 0 128.46 178.40 28.32 o 3 10 0 39300.93 37703.14 601.14 o 4 10 0 10415.20 10939.05 281.13 o 5 10 0 8362.77 8158.16 412.93 o 6 10 0 1656.13 1549.70 102.90 o 7 10 0 1109.38 1185.61 94.78 o 8 10 0 1105.51 1254.18 96.58 o 9 10 0 2918.13 2991.91 142.45 o 10 10 0 11651.82 11956.85 323.06 o 11 10 0 9294.38 9208.83 342.64 o 12 10 0 55.69 27.92 49.60 o -8 11 0 284.44 286.89 79.41 o -7 11 0 174.52 166.75 70.67 o -6 11 0 3719.54 4032.80 193.21 o -5 11 0 6211.96 6051.10 224.27 o -4 11 0 3155.95 2983.32 135.63 o -3 11 0 9211.99 8975.15 334.58 o -2 11 0 9.15 0.00 29.85 o -1 11 0 2995.26 3021.39 201.07 o 0 11 0 1323.15 1424.00 71.28 o 1 11 0 5509.04 5495.19 124.46 o 2 11 0 37776.85 37149.20 610.18 o 3 11 0 25.41 31.31 27.69 o 4 11 0 9133.14 8780.12 284.45 o 5 11 0 1139.22 1205.56 101.06 o 6 11 0 315.23 380.96 96.60 o 7 11 0 8229.02 8345.80 248.54 o 8 11 0 838.52 905.11 91.75 o 9 11 0 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61.70 o 1 15 0 68.81 7.52 46.59 o 2 15 0 20.78 0.00 39.37 o 3 15 0 11427.47 10620.40 263.97 o 4 15 0 14159.68 13910.04 387.38 o 5 15 0 320.10 296.92 72.59 o 6 15 0 10763.69 11062.40 467.69 o 7 15 0 1176.23 1150.28 119.88 o 8 15 0 98.89 134.17 63.08 o 9 15 0 1248.89 1264.75 210.53 o 10 15 0 155.14 140.31 72.37 o -3 16 0 6544.57 7018.94 335.42 o -2 16 0 1780.63 1474.82 139.98 o -1 16 0 561.87 508.27 77.40 o 0 16 0 137.46 71.18 73.02 o 1 16 0 204.69 176.20 62.45 o 2 16 0 10796.95 10788.46 279.89 o 3 16 0 4408.90 4239.20 167.96 o 4 16 0 5304.46 5524.43 407.79 o 5 16 0 5504.08 5519.46 442.36 o 6 16 0 4.14 47.59 60.07 o 7 16 0 11.37 21.20 60.89 o 8 16 0 351.44 340.05 87.11 o 9 16 0 3227.16 3473.37 202.63 o 10 16 0 4776.87 4482.06 327.09 o -2 17 0 1216.09 1236.62 321.25 o -1 17 0 90.66 116.41 72.99 o 0 17 0 523.97 320.33 94.39 o 1 17 0 3644.02 3787.00 199.69 o 2 17 0 40.68 0.00 49.12 o 3 17 0 13658.71 13238.83 430.76 o 4 17 0 2471.23 2425.23 175.93 o 5 17 0 437.79 425.58 87.11 o 6 17 0 85.95 143.31 68.87 o 7 17 0 5.59 29.64 64.93 o 8 17 0 7072.29 6842.83 390.68 o 9 17 0 1913.79 2081.12 170.07 o 0 18 0 1536.43 1514.06 145.20 o 1 18 0 2020.81 2256.68 168.55 o 2 18 0 8397.14 8432.62 288.86 o 3 18 0 36.37 110.99 59.28 o 4 18 0 2556.75 2429.45 232.25 o 5 18 0 3.66 0.00 62.45 o 6 18 0 764.70 884.67 121.05 o 7 18 0 5451.32 5244.48 419.77 o 4 19 0 27.17 83.79 75.55 o -7 -18 1 705.52 645.20 108.35 o -6 -18 1 327.59 179.28 78.85 o -5 -18 1 317.92 242.03 104.77 o -4 -18 1 233.84 196.44 81.36 o -3 -18 1 9590.83 8680.78 432.04 o -2 -18 1 738.18 610.83 96.44 o -1 -18 1 3631.98 3327.75 197.71 o 0 -18 1 2165.91 2245.22 172.38 o -8 -17 1 65.98 38.39 68.05 o -7 -17 1 87.28 85.54 68.56 o -6 -17 1 133.73 81.86 70.04 o -5 -17 1 1719.90 1488.49 145.38 o -4 -17 1 9946.45 9646.08 330.20 o -3 -17 1 799.39 878.88 117.28 o -2 -17 1 12548.21 12735.56 361.52 o -1 -17 1 383.74 243.27 74.16 o 0 -17 1 177.29 134.11 70.80 o 1 -17 1 487.15 358.78 77.00 o 2 -17 1 214.25 97.52 76.35 o -9 -16 1 1062.19 889.58 118.66 o -8 -16 1 298.47 320.38 83.53 o -7 -16 1 100.41 58.19 61.47 o -6 -16 1 6498.89 5958.86 334.79 o -5 -16 1 2500.03 2673.28 178.06 o -4 -16 1 6089.86 6404.67 252.37 o -3 -16 1 10407.23 9872.61 260.78 o -2 -16 1 46.13 43.84 46.02 o -1 -16 1 700.60 803.47 136.46 o 0 -16 1 88.50 81.42 63.27 o 1 -16 1 1703.88 1822.40 128.55 o 2 -16 1 6666.42 6869.20 293.98 o 3 -16 1 193.91 79.18 99.05 o -10 -15 1 982.82 1282.18 140.53 o -9 -15 1 242.40 174.31 72.99 o -8 -15 1 241.70 243.22 80.04 o -7 -15 1 5999.35 5446.68 308.71 o -6 -15 1 20.09 35.31 56.36 o -5 -15 1 14932.44 14886.60 406.91 o -4 -15 1 6696.76 6161.68 237.37 o -3 -15 1 7234.30 6655.44 199.98 o -2 -15 1 526.94 525.56 70.37 o -1 -15 1 11.50 0.00 54.29 o 0 -15 1 5347.84 5427.70 385.14 o 1 -15 1 3231.73 3577.35 161.32 o 2 -15 1 5237.40 5195.03 423.41 o 3 -15 1 10015.79 10396.98 322.71 o 4 -15 1 140.95 27.42 82.59 o -11 -14 1 2786.15 3106.11 221.91 o -10 -14 1 0.99 0.00 58.80 o -9 -14 1 938.99 1039.77 115.49 o -8 -14 1 2888.54 3214.18 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