#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/72/2227277.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227277_Fobs loop_ _publ_author_name 'Black, Harrison M.' 'Baughman, Russell G.' _publ_section_title ; 1-(4-Bromo-3-chlorophenyl)-3-methoxy-3-methylurea (chlorbromuron) ; _journal_coeditor_code BV2148 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2221 _journal_volume 66 _journal_year 2010 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.3872 _cell_length_b 9.5037 _cell_length_c 21.5117 _exptl_crystal_F_000 1168.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file bv2148Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CHLBROMN in Pbca [Best Latts]' _shelx_refln_list_code 4 _shelx_f_calc_maximum 337.84 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 388.17 550.58 25.70 o 4 0 0 78584.65 73138.95 577.63 o 6 0 0 15823.09 16662.09 288.14 o 8 0 0 8300.86 9096.04 190.74 o 10 0 0 878.41 783.25 58.17 o 12 0 0 1982.61 2323.39 96.05 o 2 1 0 16.06 35.26 11.36 o 4 1 0 9214.78 10996.17 1172.85 o 6 1 0 4823.64 6039.33 469.41 o 8 1 0 99.61 97.25 36.57 o 10 1 0 35.74 52.17 72.04 o 12 1 0 352.84 364.96 61.21 o 0 2 0 10169.73 10807.97 166.39 o 2 2 0 25747.59 22870.63 257.70 o 4 2 0 315.61 290.85 26.38 o 6 2 0 779.96 787.31 39.91 o 8 2 0 11.15 -18.94 50.73 o 10 2 0 225.83 307.08 55.46 o 12 2 0 0.38 83.20 85.90 o 2 3 0 2335.46 2334.21 85.22 o 4 3 0 87.99 62.23 27.73 o 6 3 0 1069.64 1019.99 44.64 o 8 3 0 428.24 353.07 51.41 o 10 3 0 3.56 -14.20 54.79 o 12 3 0 12.30 -16.23 89.96 o 0 4 0 17168.54 17163.97 261.08 o 2 4 0 27029.29 23325.84 287.46 o 4 4 0 7478.37 6298.51 171.13 o 6 4 0 13305.36 11698.09 192.77 o 8 4 0 1350.98 1210.05 54.79 o 10 4 0 2484.58 2707.57 87.93 o 12 4 0 184.50 310.46 96.05 o 2 5 0 1011.26 1045.02 48.02 o 4 5 0 454.16 374.72 37.20 o 6 5 0 228.32 163.01 43.29 o 8 5 0 57.68 49.38 47.35 o 10 5 0 90.54 163.01 76.43 o 0 6 0 7973.17 8602.95 183.30 o 2 6 0 1532.87 1385.91 60.87 o 4 6 0 46.53 77.11 41.26 o 6 6 0 2434.50 2002.78 98.75 o 8 6 0 509.18 487.67 48.02 o 10 6 0 110.47 152.86 79.81 o 2 7 0 1369.62 1399.44 62.23 o 4 7 0 148.85 183.98 46.67 o 6 7 0 0.29 10.82 45.32 o 8 7 0 59.80 -35.17 70.34 o 10 7 0 281.25 353.07 85.90 o 0 8 0 2088.88 2552.00 102.13 o 2 8 0 2275.73 2359.23 96.72 o 4 8 0 1948.06 2293.62 83.20 o 6 8 0 428.78 487.67 71.02 o 8 8 0 175.01 156.25 79.14 o 2 9 0 88.20 131.22 67.64 o 4 9 0 1241.90 1035.55 77.11 o 6 9 0 65.78 -25.70 78.46 o 8 9 0 37.68 34.50 86.58 o 0 10 0 543.31 569.52 79.81 o 2 10 0 789.77 859.69 79.14 o 4 10 0 500.63 456.56 83.20 o 6 10 0 8.48 103.49 86.58 o 2 11 0 19.76 -87.25 87.25 o 1 1 1 23787.29 21719.12 1398.18 o 2 1 1 3250.52 3785.28 353.90 o 3 1 1 8643.11 8833.33 811.29 o 4 1 1 99.68 153.88 20.50 o 5 1 1 10174.62 11563.52 600.02 o 6 1 1 619.80 747.88 24.21 o 7 1 1 774.07 690.85 30.05 o 8 1 1 661.71 712.67 27.27 o 9 1 1 2247.15 2568.83 74.32 o 10 1 1 31.83 28.63 27.46 o 11 1 1 254.08 264.25 39.22 o 12 1 1 89.42 123.47 42.52 o 13 1 1 276.90 308.27 47.43 o 0 2 1 4623.49 5087.89 157.94 o 1 2 1 8532.49 9333.63 702.43 o 2 2 1 14222.49 12406.89 140.85 o 3 2 1 313.23 273.95 15.78 o 4 2 1 3458.39 3197.00 102.75 o 5 2 1 64.81 72.25 35.85 o 6 2 1 4071.68 3818.07 114.28 o 7 2 1 2007.17 2100.27 153.88 o 8 2 1 2084.08 2085.64 117.35 o 9 2 1 5.16 42.40 38.02 o 10 2 1 829.95 841.12 41.13 o 11 2 1 156.61 140.24 56.43 o 12 2 1 222.21 323.58 61.68 o 13 2 1 175.00 127.19 67.91 o 1 3 1 26240.49 26325.19 1372.36 o 2 3 1 477.88 494.63 29.08 o 3 3 1 9814.04 7951.00 132.46 o 4 3 1 4078.42 3748.71 108.56 o 5 3 1 8063.51 7464.35 129.37 o 6 3 1 288.21 255.36 36.86 o 7 3 1 3855.63 3740.69 99.48 o 8 3 1 138.32 159.91 34.91 o 9 3 1 1025.97 1039.23 40.89 o 10 3 1 127.90 104.79 38.98 o 11 3 1 937.92 940.27 62.18 o 12 3 1 144.47 154.18 64.08 o 13 3 1 207.43 154.42 69.82 o 0 4 1 2348.51 2436.87 75.08 o 1 4 1 2489.26 2752.64 109.64 o 2 4 1 594.14 671.58 25.23 o 3 4 1 1264.72 1098.97 36.34 o 4 4 1 582.57 528.78 34.16 o 5 4 1 1841.22 1677.83 57.83 o 6 4 1 78.09 34.83 32.13 o 7 4 1 178.48 205.66 40.92 o 8 4 1 302.67 380.42 67.98 o 9 4 1 82.60 168.33 43.29 o 10 4 1 13.84 9.47 53.09 o 11 4 1 0.19 -30.45 60.72 o 12 4 1 43.22 132.30 67.20 o 1 5 1 2431.91 2483.95 111.00 o 2 5 1 318.92 341.41 24.15 o 3 5 1 235.79 163.15 24.87 o 4 5 1 165.85 131.29 25.58 o 5 5 1 579.20 508.06 30.10 o 6 5 1 239.97 221.22 30.61 o 7 5 1 224.69 228.65 32.52 o 8 5 1 9.29 -33.72 33.72 o 9 5 1 126.26 82.24 56.14 o 10 5 1 14.16 51.54 53.80 o 11 5 1 7.09 -56.59 60.74 o 12 5 1 46.00 50.41 69.58 o 0 6 1 7793.73 8316.77 128.41 o 1 6 1 1401.29 1404.54 62.38 o 2 6 1 25.55 6.43 27.74 o 3 6 1 208.56 218.14 50.73 o 4 6 1 1759.12 1586.57 46.86 o 5 6 1 1869.57 1727.99 44.70 o 6 6 1 702.79 646.66 33.72 o 7 6 1 185.82 231.10 32.76 o 8 6 1 870.28 832.27 34.91 o 9 6 1 179.88 202.12 50.70 o 10 6 1 16.28 28.41 78.80 o 11 6 1 6.67 24.79 96.72 o 1 7 1 3382.85 3786.57 80.15 o 2 7 1 49.94 7.78 53.77 o 3 7 1 6662.20 6768.83 95.64 o 4 7 1 4.07 13.87 32.52 o 5 7 1 81.07 82.52 33.00 o 6 7 1 404.28 306.34 32.76 o 7 7 1 1044.20 1141.45 57.15 o 8 7 1 91.49 170.79 49.74 o 9 7 1 375.17 375.41 61.89 o 10 7 1 2.62 62.51 59.78 o 0 8 1 437.59 427.76 35.63 o 1 8 1 907.17 953.93 34.46 o 2 8 1 207.60 183.03 34.67 o 3 8 1 2126.30 2023.51 133.92 o 4 8 1 225.06 239.32 33.96 o 5 8 1 132.19 166.16 32.76 o 6 8 1 129.66 166.31 47.83 o 7 8 1 141.12 114.65 52.13 o 8 8 1 177.66 95.15 56.20 o 9 8 1 111.79 198.01 86.92 o 1 9 1 162.30 125.02 23.91 o 2 9 1 89.62 56.90 47.59 o 3 9 1 5.07 20.12 100.78 o 4 9 1 0.71 -1.66 77.11 o 5 9 1 6.92 18.41 53.08 o 6 9 1 33.27 113.97 57.15 o 7 9 1 38.80 75.69 73.73 o 8 9 1 72.39 11.62 61.46 o 0 10 1 65.73 95.37 54.52 o 2 10 1 339.60 405.02 55.48 o 3 10 1 0.21 -70.28 99.77 o 4 10 1 2.89 23.34 56.44 o 5 10 1 26.99 46.05 58.82 o 6 10 1 12.64 19.95 61.70 o 1 11 1 58.10 77.98 44.04 o 2 11 1 2.54 70.96 70.68 o 3 11 1 197.18 255.00 63.61 o 0 0 2 9144.88 7210.27 85.90 o 1 0 2 8246.02 9266.73 657.45 o 2 0 2 3103.61 3703.21 139.34 o 3 0 2 10.13 29.08 26.38 o 4 0 2 24944.88 27939.47 372.69 o 5 0 2 5242.03 6523.07 215.09 o 6 0 2 2800.05 3379.22 121.07 o 7 0 2 25.29 66.29 45.32 o 8 0 2 507.10 514.73 52.76 o 9 0 2 1550.82 1803.24 77.11 o 10 0 2 512.46 592.51 55.46 o 11 0 2 404.02 345.63 77.78 o 12 0 2 448.61 560.72 86.58 o 13 0 2 42.78 4.73 93.34 o 1 1 2 17451.16 17467.54 1603.34 o 2 1 2 40702.72 38060.03 6605.25 o 3 1 2 27561.92 27667.74 3698.14 o 4 1 2 41.18 41.71 40.24 o 5 1 2 8236.46 9298.17 555.65 o 6 1 2 291.29 319.50 29.87 o 7 1 2 11298.09 12370.07 535.02 o 8 1 2 824.26 891.16 91.99 o 9 1 2 1395.29 1435.04 44.56 o 10 1 2 0.33 6.18 38.48 o 11 1 2 947.67 1025.72 58.11 o 12 1 2 31.67 53.39 60.26 o 13 1 2 151.62 205.46 88.94 o 0 2 2 3352.31 3343.38 125.13 o 1 2 2 11118.27 11574.68 1258.42 o 2 2 2 24281.13 20399.80 253.64 o 3 2 2 3938.46 3400.87 144.75 o 4 2 2 457.87 492.41 27.73 o 5 2 2 4572.84 4324.81 165.71 o 6 2 2 709.01 685.18 41.26 o 7 2 2 1471.60 1609.12 73.73 o 8 2 2 991.22 1043.66 56.14 o 9 2 2 17.32 -39.23 54.79 o 10 2 2 327.61 285.43 56.14 o 11 2 2 47.28 99.43 79.14 o 12 2 2 6.10 100.11 86.58 o 13 2 2 22.75 -18.94 94.69 o 1 3 2 15715.85 15604.45 1492.45 o 2 3 2 189.83 197.50 23.00 o 3 3 2 3757.39 2907.11 140.01 o 4 3 2 1256.47 1212.08 45.32 o 5 3 2 2840.61 2309.86 85.90 o 6 3 2 143.49 82.52 39.23 o 7 3 2 1683.32 1467.76 58.85 o 8 3 2 8.93 13.53 49.38 o 9 3 2 229.87 224.56 54.79 o 10 3 2 46.38 81.17 55.46 o 11 3 2 655.18 593.19 86.58 o 12 3 2 10.33 186.01 88.61 o 13 3 2 24.21 -13.53 98.08 o 0 4 2 677.59 802.19 43.29 o 1 4 2 790.21 788.73 26.38 o 2 4 2 1068.39 1031.49 43.29 o 3 4 2 2236.87 2034.57 80.49 o 4 4 2 70.80 79.81 32.47 o 5 4 2 141.99 150.16 35.85 o 6 4 2 538.60 474.82 41.94 o 7 4 2 1007.31 856.98 48.70 o 8 4 2 191.53 290.85 49.38 o 9 4 2 163.96 199.53 51.41 o 10 4 2 274.40 297.61 77.11 o 11 4 2 143.58 62.23 87.25 o 12 4 2 189.51 103.49 96.72 o 1 5 2 16275.66 17058.65 1259.77 o 2 5 2 1705.67 1738.31 66.96 o 3 5 2 8856.51 8207.94 175.86 o 4 5 2 397.23 411.24 38.55 o 5 5 2 6366.27 5283.25 143.39 o 6 5 2 33.67 31.79 42.61 o 7 5 2 1532.43 1458.96 62.90 o 8 5 2 67.45 170.45 47.35 o 9 5 2 1855.88 1888.47 79.14 o 10 5 2 47.63 77.78 76.43 o 11 5 2 401.84 382.83 89.28 o 12 5 2 37.10 92.66 99.43 o 0 6 2 2898.73 3373.81 145.42 o 1 6 2 23.13 54.03 28.59 o 2 6 2 875.82 955.73 42.61 o 3 6 2 2.60 95.37 39.91 o 4 6 2 893.93 844.81 45.99 o 5 6 2 1550.30 1216.14 54.11 o 6 6 2 483.67 470.76 46.67 o 7 6 2 235.84 229.29 46.67 o 8 6 2 49.85 -31.79 46.67 o 9 6 2 170.84 100.78 72.37 o 10 6 2 115.10 61.55 80.49 o 11 6 2 0.63 22.32 89.28 o 1 7 2 3.53 6.04 32.70 o 2 7 2 170.96 228.62 45.32 o 3 7 2 80.21 83.20 47.35 o 4 7 2 21.48 -46.67 46.67 o 5 7 2 191.78 153.54 46.67 o 6 7 2 832.58 761.61 48.70 o 7 7 2 8.11 -59.52 64.93 o 8 7 2 41.89 18.26 71.02 o 9 7 2 8.87 38.55 77.11 o 10 7 2 53.89 10.82 85.90 o 0 8 2 16.60 -49.38 49.38 o 1 8 2 96.86 107.85 35.09 o 2 8 2 746.22 739.97 50.73 o 3 8 2 34.96 46.67 48.02 o 4 8 2 6.32 52.08 47.35 o 5 8 2 11.88 35.85 44.64 o 6 8 2 14.15 -52.08 68.31 o 7 8 2 57.22 145.42 72.37 o 8 8 2 286.72 355.78 80.49 o 9 8 2 14.05 146.10 83.87 o 1 9 2 1398.15 1655.76 54.24 o 2 9 2 0.85 108.90 66.29 o 3 9 2 224.56 263.11 69.67 o 4 9 2 178.31 66.29 71.70 o 5 9 2 1133.02 1353.45 82.52 o 6 9 2 57.69 58.85 78.46 o 7 9 2 317.68 394.33 85.22 o 8 9 2 13.74 42.61 87.25 o 0 10 2 135.49 255.00 78.46 o 1 10 2 227.93 176.83 56.43 o 2 10 2 149.19 248.23 76.43 o 3 10 2 54.24 87.25 78.46 o 4 10 2 35.76 114.99 79.81 o 5 10 2 13.00 34.50 83.20 o 6 10 2 5.47 20.97 87.25 o 1 11 2 5.11 -63.37 63.37 o 2 11 2 8.57 -22.32 87.93 o 1 1 3 601.60 711.55 92.06 o 2 1 3 770.54 886.31 179.24 o 3 1 3 23856.44 24506.15 3571.66 o 4 1 3 4.63 4.45 47.35 o 5 1 3 399.96 473.41 26.52 o 6 1 3 297.55 360.92 30.37 o 7 1 3 1168.14 1221.81 56.48 o 8 1 3 23.37 16.17 81.84 o 9 1 3 301.92 387.54 39.69 o 10 1 3 189.77 181.46 39.44 o 11 1 3 0.82 67.64 77.11 o 12 1 3 19.37 -24.01 119.38 o 13 1 3 0.26 -32.16 66.48 o 0 2 3 25512.65 26179.51 277.32 o 1 2 3 2486.54 2673.86 253.31 o 2 2 3 114137.75 79250.78 492.41 o 3 2 3 2632.86 2278.74 86.58 o 4 2 3 14998.77 12854.04 234.71 o 6 2 3 15318.55 14372.52 238.09 o 7 2 3 182.34 198.86 46.67 o 8 2 3 3856.82 3879.07 142.72 o 9 2 3 193.88 228.62 55.46 o 10 2 3 2423.10 2648.73 97.40 o 11 2 3 171.49 244.18 79.81 o 12 2 3 582.37 699.38 89.96 o 13 2 3 10.88 154.89 94.69 o 1 3 3 2057.81 2311.41 249.25 o 2 3 3 132.60 129.87 23.67 o 3 3 3 996.40 815.04 45.32 o 4 3 3 2409.08 2376.14 89.28 o 5 3 3 1957.23 1952.73 75.76 o 6 3 3 12.00 77.11 39.23 o 7 3 3 1547.66 1494.81 64.93 o 8 3 3 353.09 384.86 51.41 o 9 3 3 93.92 117.69 54.11 o 10 3 3 56.31 41.26 55.46 o 11 3 3 1.14 -4.06 83.20 o 12 3 3 51.05 -90.64 90.64 o 0 4 3 13493.90 15151.72 254.32 o 1 4 3 76.32 113.48 20.98 o 2 4 3 929.94 1049.75 47.35 o 3 4 3 213.30 243.50 31.11 o 4 4 3 5703.19 4968.73 157.60 o 5 4 3 110.40 157.60 36.52 o 6 4 3 69.63 92.66 40.58 o 7 4 3 164.55 225.24 45.99 o 8 4 3 1557.36 1519.16 60.20 o 9 4 3 0.54 -51.41 51.41 o 10 4 3 36.77 39.91 76.43 o 11 4 3 25.25 -3.38 87.25 o 12 4 3 125.46 119.04 96.05 o 1 5 3 270.09 261.00 26.25 o 2 5 3 114.77 99.43 35.17 o 3 5 3 297.87 243.50 36.52 o 4 5 3 582.85 554.64 39.23 o 5 5 3 93.14 108.22 40.58 o 6 5 3 42.52 87.93 43.29 o 7 5 3 403.62 316.55 47.35 o 8 5 3 142.55 114.99 48.70 o 9 5 3 5.68 41.26 68.99 o 10 5 3 0.94 -64.93 77.11 o 11 5 3 1.62 -43.29 87.25 o 12 5 3 54.23 171.80 98.08 o 0 6 3 11944.26 12459.03 206.30 o 1 6 3 1297.40 1579.00 137.98 o 2 6 3 1805.76 1787.01 74.40 o 3 6 3 464.12 434.24 43.29 o 4 6 3 9926.37 8736.20 155.57 o 5 6 3 168.45 216.44 44.64 o 6 6 3 1453.56 1400.80 52.76 o 7 6 3 584.65 538.40 48.02 o 8 6 3 1142.52 1166.09 49.38 o 9 6 3 86.56 154.89 73.05 o 10 6 3 314.20 334.13 83.20 o 11 6 3 157.95 78.46 89.96 o 1 7 3 77.51 37.15 33.39 o 2 7 3 156.19 128.51 45.99 o 3 7 3 868.32 978.73 49.38 o 4 7 3 30.82 56.14 45.99 o 5 7 3 133.20 129.19 46.67 o 6 7 3 5.98 -17.59 45.32 o 7 7 3 268.03 217.12 66.96 o 8 7 3 249.86 162.33 72.37 o 9 7 3 74.53 85.22 77.78 o 10 7 3 20.19 40.58 85.22 o 0 8 3 212.36 154.89 51.41 o 1 8 3 333.00 372.13 36.31 o 2 8 3 1788.16 1862.09 90.64 o 3 8 3 204.00 168.42 48.02 o 4 8 3 766.30 797.46 50.73 o 5 8 3 34.21 10.15 65.61 o 6 8 3 815.47 758.23 73.73 o 7 8 3 88.93 79.14 74.40 o 8 8 3 42.59 -33.82 79.14 o 9 8 3 6.47 -85.90 85.90 o 1 9 3 6.73 48.19 49.23 o 2 9 3 44.03 52.08 67.64 o 3 9 3 48.59 -69.67 69.67 o 4 9 3 132.78 121.07 72.37 o 5 9 3 13.78 -77.11 77.11 o 6 9 3 33.34 -23.00 79.14 o 7 9 3 70.27 158.95 82.52 o 8 9 3 0.39 -51.41 87.93 o 0 10 3 131.62 285.43 79.81 o 1 10 3 605.40 657.45 96.72 o 2 10 3 615.44 872.54 81.84 o 3 10 3 64.99 106.19 78.46 o 4 10 3 4.86 27.73 80.49 o 5 10 3 13.54 -45.99 83.87 o 6 10 3 183.85 261.76 89.28 o 1 11 3 53.92 -57.45 63.85 o 2 11 3 78.73 224.56 87.93 o 0 0 4 314.55 295.58 19.62 o 1 0 4 14114.18 15848.62 1636.85 o 2 0 4 13782.56 16252.20 263.79 o 3 0 4 5687.03 6951.22 214.41 o 4 0 4 27594.22 30128.26 388.92 o 5 0 4 149.18 163.69 37.88 o 6 0 4 5072.09 5099.95 195.48 o 7 0 4 220.67 200.89 48.02 o 8 0 4 3644.27 3843.22 150.83 o 9 0 4 1080.41 1265.52 59.52 o 10 0 4 2868.29 2949.04 102.81 o 11 0 4 115.88 154.22 77.11 o 12 0 4 656.91 802.87 89.28 o 13 0 4 96.92 119.04 94.02 o 1 1 4 2996.50 3270.80 351.27 o 2 1 4 7282.50 8188.80 1451.86 o 3 1 4 17139.02 18514.10 2799.90 o 4 1 4 632.87 660.38 65.95 o 5 1 4 3509.32 3867.82 128.22 o 6 1 4 21.90 1.31 30.12 o 7 1 4 2655.37 2992.12 186.01 o 8 1 4 772.88 865.79 39.44 o 9 1 4 1183.05 1146.58 104.16 o 10 1 4 598.52 616.82 40.65 o 11 1 4 213.34 273.46 55.95 o 12 1 4 21.24 18.22 60.97 o 13 1 4 194.05 116.09 67.43 o 0 2 4 224.08 227.27 22.32 o 1 2 4 10748.46 12084.21 1269.24 o 2 2 4 1830.39 1830.30 71.02 o 3 2 4 484.51 473.47 26.38 o 4 2 4 5318.65 5403.65 173.15 o 5 2 4 448.33 425.45 34.50 o 6 2 4 324.44 346.99 40.58 o 7 2 4 2.62 8.12 45.32 o 8 2 4 75.99 33.14 52.76 o 9 2 4 3.70 -16.23 55.46 o 10 2 4 267.37 298.96 56.14 o 11 2 4 33.04 187.36 79.81 o 12 2 4 120.98 -51.41 88.61 o 1 3 4 7257.31 7955.58 739.29 o 2 3 4 898.92 971.97 46.67 o 3 3 4 5339.66 4307.90 154.22 o 4 3 4 3039.13 2620.32 95.37 o 5 3 4 80.56 19.62 34.50 o 6 3 4 598.04 589.13 41.94 o 7 3 4 1106.49 1088.98 57.49 o 8 3 4 502.05 574.93 52.08 o 9 3 4 5.72 -41.94 54.11 o 10 3 4 497.50 481.59 55.46 o 11 3 4 473.94 551.25 85.90 o 12 3 4 53.31 45.99 90.64 o 0 4 4 847.86 736.58 43.29 o 1 4 4 4611.06 5475.67 412.93 o 2 4 4 19505.89 18104.82 259.06 o 3 4 4 7790.90 7212.98 177.21 o 4 4 4 9915.71 8140.98 179.92 o 5 4 4 426.19 423.42 38.55 o 6 4 4 4076.45 3659.92 129.87 o 7 4 4 1135.84 1103.19 50.05 o 8 4 4 1940.87 1863.44 68.99 o 9 4 4 287.07 295.58 52.08 o 10 4 4 740.33 848.19 81.17 o 11 4 4 236.73 194.12 89.28 o 12 4 4 25.32 -21.64 95.37 o 1 5 4 9212.41 10151.58 681.12 o 2 5 4 1496.46 1594.24 66.29 o 3 5 4 4471.14 4000.82 144.75 o 4 5 4 3.07 1.35 37.88 o 5 5 4 2191.55 1860.74 72.37 o 6 5 4 219.67 162.33 43.97 o 7 5 4 404.16 384.86 48.02 o 8 5 4 2009.42 1586.12 58.85 o 9 5 4 883.34 917.18 73.73 o 10 5 4 372.67 319.93 79.14 o 11 5 4 91.90 59.52 88.61 o 0 6 4 608.50 639.18 44.64 o 1 6 4 1262.20 1471.33 97.06 o 2 6 4 956.41 959.12 43.97 o 3 6 4 111.60 183.98 41.26 o 4 6 4 2538.61 2311.89 110.93 o 5 6 4 48.43 87.25 43.97 o 6 6 4 1383.98 1223.58 50.73 o 7 6 4 1.76 23.00 45.99 o 8 6 4 5.24 25.03 66.29 o 9 6 4 22.98 -63.58 74.40 o 10 6 4 221.42 281.38 82.52 o 11 6 4 8.58 -86.58 90.64 o 1 7 4 11.75 -49.38 50.05 o 2 7 4 345.52 395.01 46.67 o 3 7 4 259.97 234.03 48.02 o 4 7 4 282.20 288.14 47.35 o 5 7 4 211.00 188.71 47.35 o 6 7 4 24.23 104.16 45.32 o 7 7 4 24.32 43.29 65.61 o 8 7 4 97.04 29.76 71.70 o 9 7 4 6.72 -2.03 78.46 o 10 7 4 12.50 112.28 85.90 o 0 8 4 1751.08 2037.27 98.75 o 1 8 4 7.65 -26.27 35.35 o 2 8 4 214.98 290.85 49.38 o 3 8 4 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