#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/72/2227298.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227298_Fobs loop_ _publ_author_name 'Nenwa, Justin' 'Belombe, Michel M.' 'Ngoune, Jean' 'Fokwa, Boniface P. T.' _publ_section_title ; 4-(Dimethylamino)pyridinium trans-diaquabis[oxalato(2{-})-\k^2^O^1^,O^2^]chromate(III) ; _journal_coeditor_code BX2312 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1410 _journal_volume 66 _journal_year 2010 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 120.626 _cell_angle_gamma 90.000 _cell_length_a 11.5240 _cell_length_b 20.3720 _cell_length_c 7.3550 _exptl_crystal_F_000 795.87 _reflns_d_resolution_high 0.7486 _[local]_cod_data_source_file bx2312Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' boni93C2 in C2 C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 440.66 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 61585.87 46933.15 1532.61 o 4 0 0 27051.54 29266.14 771.46 o 6 0 0 146.59 201.98 10.89 o 8 0 0 14273.22 14628.72 383.41 o 10 0 0 5403.20 5318.31 146.37 o 12 0 0 30.23 41.21 11.53 o 1 1 0 2424.41 2106.65 167.03 o 3 1 0 117.83 85.73 3.80 o 5 1 0 1067.84 1215.73 23.14 o 7 1 0 16.90 23.93 4.32 o 9 1 0 205.23 217.04 9.87 o 11 1 0 144.36 189.02 16.90 o 13 1 0 31.42 55.69 9.58 o 0 2 0 258.38 1.67 1.03 o 2 2 0 58.26 53.10 2.48 o 4 2 0 129.78 128.14 5.00 o 6 2 0 403.30 383.09 10.07 o 8 2 0 36.43 48.80 5.72 o 10 2 0 4.60 7.77 4.88 o 12 2 0 39.21 60.24 9.81 o 1 3 0 671.19 546.10 11.79 o 3 3 0 4918.08 5007.55 64.04 o 5 3 0 2719.57 2432.58 39.41 o 7 3 0 1184.58 1130.84 19.45 o 9 3 0 2377.35 2237.03 43.10 o 11 3 0 1372.17 1366.97 43.96 o 13 3 0 43.19 47.12 9.87 o 0 4 0 154.53 181.35 7.63 o 2 4 0 1754.52 1721.12 26.73 o 4 4 0 9062.87 9665.50 133.10 o 6 4 0 5554.98 5828.32 114.83 o 8 4 0 1813.84 1838.55 43.51 o 10 4 0 868.99 894.81 24.32 o 12 4 0 436.20 471.40 24.70 o 1 5 0 1980.69 2100.02 33.74 o 3 5 0 1379.82 1546.96 21.79 o 5 5 0 909.02 1030.43 17.05 o 7 5 0 10.30 15.50 3.77 o 9 5 0 74.29 73.16 7.54 o 11 5 0 2.31 3.45 3.40 o 13 5 0 1.48 8.92 5.95 o 0 6 0 20434.93 20547.99 579.18 o 2 6 0 3536.10 3507.34 57.34 o 4 6 0 93.67 86.71 4.76 o 6 6 0 1421.52 1303.36 52.72 o 8 6 0 1343.74 1314.06 28.60 o 10 6 0 231.29 232.74 13.80 o 12 6 0 101.17 113.33 13.67 o 1 7 0 8860.89 8578.23 119.58 o 3 7 0 8743.70 9172.54 152.58 o 5 7 0 3823.74 3986.38 54.13 o 7 7 0 93.84 90.84 6.35 o 9 7 0 54.13 58.38 7.85 o 11 7 0 734.62 790.68 27.11 o 0 8 0 1704.14 2180.53 33.36 o 2 8 0 838.43 829.25 18.17 o 4 8 0 3093.54 3358.34 44.52 o 6 8 0 41.20 38.92 4.50 o 8 8 0 249.58 232.33 12.32 o 10 8 0 0.35 5.84 3.96 o 12 8 0 191.29 214.91 29.45 o 1 9 0 2.94 3.88 2.02 o 3 9 0 2487.96 2735.71 44.63 o 5 9 0 401.07 365.99 10.15 o 7 9 0 260.21 259.29 11.58 o 9 9 0 4.27 11.56 4.19 o 11 9 0 616.71 645.34 28.25 o 0 10 0 10895.02 11703.29 290.78 o 2 10 0 5392.50 5484.18 85.79 o 4 10 0 1503.69 1527.54 41.80 o 6 10 0 1628.64 1626.33 30.76 o 8 10 0 2327.61 2353.31 65.33 o 10 10 0 1394.49 1375.22 52.93 o 12 10 0 278.09 257.00 32.13 o 1 11 0 5344.09 5254.70 60.46 o 3 11 0 241.25 287.89 8.70 o 5 11 0 7.34 15.43 3.37 o 7 11 0 2542.67 2578.34 58.40 o 9 11 0 1854.95 1804.27 45.74 o 11 11 0 86.13 90.43 12.75 o 0 12 0 1132.31 1184.59 29.41 o 2 12 0 100.01 106.76 6.17 o 4 12 0 0.26 1.98 2.28 o 6 12 0 283.96 278.13 10.73 o 8 12 0 361.73 323.71 19.80 o 10 12 0 53.61 56.44 10.81 o 1 13 0 4937.42 4926.09 63.34 o 3 13 0 294.93 254.46 8.93 o 5 13 0 74.50 88.58 6.37 o 7 13 0 1183.49 1196.86 35.34 o 9 13 0 1709.21 1621.40 45.05 o 11 13 0 434.10 433.91 25.14 o 0 14 0 4729.66 5079.80 99.91 o 2 14 0 2711.86 2834.15 61.56 o 4 14 0 214.65 209.17 8.61 o 6 14 0 11.30 10.84 4.51 o 8 14 0 551.48 544.59 25.85 o 10 14 0 953.99 967.72 36.68 o 1 15 0 77.24 102.52 6.86 o 3 15 0 554.04 514.16 17.48 o 5 15 0 594.58 580.97 18.07 o 7 15 0 84.34 74.85 11.99 o 9 15 0 1.55 13.00 6.36 o 11 15 0 11.13 19.44 6.90 o 0 16 0 9278.88 9838.70 183.42 o 2 16 0 3472.75 3606.13 53.92 o 4 16 0 102.71 114.16 9.44 o 6 16 0 101.82 115.35 11.39 o 8 16 0 740.12 685.66 29.71 o 10 16 0 648.90 673.27 31.55 o 1 17 0 6038.15 6144.61 71.21 o 3 17 0 3.61 7.03 3.55 o 5 17 0 158.61 152.81 11.06 o 7 17 0 916.14 896.15 33.49 o 9 17 0 1269.81 1236.81 42.09 o 0 18 0 32.98 50.06 8.10 o 2 18 0 190.28 219.17 10.97 o 4 18 0 422.83 416.13 16.40 o 6 18 0 144.06 129.73 15.12 o 8 18 0 37.81 46.12 9.49 o 1 19 0 168.27 152.51 9.58 o 3 19 0 207.95 205.08 12.81 o 5 19 0 624.95 600.02 23.05 o 7 19 0 47.16 49.90 10.05 o 9 19 0 1.41 9.90 5.74 o 0 20 0 36.30 34.97 8.52 o 2 20 0 939.34 925.38 24.47 o 4 20 0 2829.82 2795.76 65.59 o 6 20 0 1420.69 1344.66 45.62 o 8 20 0 508.71 515.12 27.41 o 1 21 0 11.97 27.86 6.40 o 3 21 0 438.45 436.60 17.56 o 5 21 0 541.71 482.56 21.15 o 7 21 0 91.08 90.89 13.19 o 0 22 0 20.62 25.62 10.16 o 2 22 0 11.22 15.88 5.29 o 4 22 0 0.52 10.17 4.30 o 6 22 0 19.47 33.12 7.94 o 1 23 0 1593.30 1521.93 44.31 o 3 23 0 611.38 681.44 25.32 o 5 23 0 242.16 303.43 25.98 o 7 23 0 157.17 169.26 20.20 o 0 24 0 762.98 801.87 50.26 o 2 24 0 581.78 621.05 28.17 o 4 24 0 216.91 216.73 18.62 o 6 24 0 37.11 40.59 9.93 o 1 25 0 53.64 58.75 10.00 o 3 25 0 88.66 94.40 15.15 o 5 25 0 124.81 137.75 25.44 o 0 26 0 471.52 397.37 33.14 o 2 26 0 253.71 249.44 20.82 o 1 27 0 1277.86 1329.94 45.70 o -13 1 1 199.87 224.51 19.10 o -11 1 1 286.39 331.81 15.66 o -9 1 1 908.42 903.29 23.67 o -7 1 1 310.31 270.41 8.50 o -5 1 1 177.20 232.99 6.28 o -3 1 1 4934.39 4546.07 74.80 o -1 1 1 21255.02 22249.94 595.57 o 1 1 1 6671.15 6959.42 96.56 o 3 1 1 73.13 147.64 5.01 o 5 1 1 8.43 5.21 2.79 o 7 1 1 1586.21 1583.74 23.73 o 9 1 1 667.72 737.01 23.44 o 11 1 1 21.54 35.47 7.72 o -12 2 1 1080.52 1089.32 32.11 o -10 2 1 2352.97 2325.34 37.79 o -8 2 1 1449.77 1394.53 28.51 o -6 2 1 1722.26 1581.24 27.46 o -4 2 1 9043.35 9432.51 114.45 o -2 2 1 28876.69 28424.34 507.14 o 0 2 1 15751.81 15935.80 329.27 o 2 2 1 1988.36 1985.29 23.81 o 4 2 1 2811.19 2772.33 29.74 o 6 2 1 3455.06 3447.85 65.06 o 8 2 1 2661.45 2726.69 60.09 o 10 2 1 939.56 952.97 33.83 o 12 2 1 139.91 157.35 17.05 o -13 3 1 92.43 102.17 12.88 o -11 3 1 131.49 130.13 11.07 o -9 3 1 0.40 1.91 3.44 o -7 3 1 29.57 42.34 4.16 o -5 3 1 1959.52 1883.06 31.77 o -3 3 1 3159.01 3256.43 35.40 o -1 3 1 84.90 108.76 2.41 o 1 3 1 663.66 737.40 9.89 o 3 3 1 825.26 776.64 16.22 o 5 3 1 1308.10 1326.31 19.54 o 7 3 1 144.75 165.69 8.43 o 9 3 1 4.08 2.86 4.67 o 11 3 1 31.14 39.57 7.99 o -12 4 1 410.43 391.82 19.16 o -10 4 1 336.69 313.56 12.85 o -8 4 1 485.52 477.95 14.03 o -6 4 1 3344.13 3592.81 63.77 o -4 4 1 7676.29 7943.41 85.07 o -2 4 1 4701.88 4742.15 77.80 o 0 4 1 63.41 52.93 3.04 o 2 4 1 244.89 207.78 5.36 o 4 4 1 3336.71 3219.85 41.39 o 6 4 1 2626.12 2686.29 35.38 o 8 4 1 848.17 856.45 20.33 o 10 4 1 192.31 200.46 14.88 o 12 4 1 61.44 66.37 11.28 o -13 5 1 264.69 280.01 25.59 o -11 5 1 403.87 396.01 18.64 o -9 5 1 1067.42 1047.65 38.84 o -7 5 1 2097.52 1980.95 47.73 o -5 5 1 2184.78 1767.91 24.46 o -3 5 1 4120.69 3975.94 72.26 o -1 5 1 1801.84 2003.97 16.50 o 1 5 1 466.74 461.32 8.84 o 3 5 1 120.89 221.26 6.34 o 5 5 1 2523.94 2345.37 31.60 o 7 5 1 4598.19 4678.33 78.79 o 9 5 1 1031.71 1029.95 27.00 o 11 5 1 14.69 18.79 5.49 o -12 6 1 860.87 889.64 33.56 o -10 6 1 172.87 166.37 10.52 o -8 6 1 80.52 76.54 7.10 o -6 6 1 3047.56 3391.22 43.50 o -4 6 1 12769.64 14109.01 146.76 o -2 6 1 6890.49 6982.86 121.34 o 0 6 1 658.03 597.05 12.06 o 2 6 1 2434.49 2554.31 39.70 o 4 6 1 4876.03 5382.54 86.03 o 6 6 1 1972.17 2030.68 44.01 o 8 6 1 284.03 299.13 12.50 o 10 6 1 174.35 192.12 14.81 o 12 6 1 323.21 337.35 27.49 o -13 7 1 320.86 353.44 22.46 o -11 7 1 50.47 63.57 10.51 o -9 7 1 93.88 79.70 7.53 o -7 7 1 12.71 23.95 3.15 o -5 7 1 2739.49 3113.94 53.25 o -3 7 1 5086.45 5668.15 120.43 o -1 7 1 170.83 145.41 4.66 o 1 7 1 38.48 58.50 3.08 o 3 7 1 1479.55 1510.09 35.94 o 5 7 1 2144.98 2271.34 49.70 o 7 7 1 171.62 182.76 10.02 o 9 7 1 34.02 38.75 6.46 o 11 7 1 1.77 1.23 5.93 o -12 8 1 2180.56 2350.27 55.98 o -10 8 1 20.30 15.59 5.04 o -8 8 1 2433.77 2423.67 57.38 o -6 8 1 1593.33 1652.29 37.52 o -4 8 1 32964.49 36302.70 829.34 o -2 8 1 9545.24 9631.63 187.48 o 0 8 1 4607.76 5982.18 83.36 o 2 8 1 1289.38 1259.44 23.34 o 4 8 1 14856.15 15790.57 290.03 o 6 8 1 2128.41 2005.57 47.64 o 8 8 1 337.99 335.82 14.89 o 10 8 1 20.43 23.52 7.64 o -13 9 1 1108.96 1111.97 40.23 o -11 9 1 904.99 890.24 28.72 o -9 9 1 3.96 9.34 3.15 o -7 9 1 33.27 28.92 4.89 o -5 9 1 6421.37 6710.52 127.56 o -3 9 1 14380.20 15713.07 241.39 o -1 9 1 4775.70 4686.28 58.12 o 1 9 1 189.43 139.14 5.18 o 3 9 1 3037.09 3128.19 69.99 o 5 9 1 5327.15 5434.27 120.59 o 7 9 1 935.46 874.99 22.66 o 9 9 1 41.01 44.04 8.05 o 11 9 1 135.98 158.04 19.26 o -12 10 1 46.08 42.16 8.56 o -10 10 1 177.05 145.68 13.08 o -8 10 1 13.02 12.79 4.30 o -6 10 1 40.88 39.40 4.18 o -4 10 1 142.51 111.49 5.50 o -2 10 1 148.16 138.71 5.75 o 0 10 1 1562.63 1697.99 23.32 o 2 10 1 269.71 284.67 7.97 o 4 10 1 68.54 81.21 5.49 o 6 10 1 224.54 246.00 10.67 o 8 10 1 19.21 13.68 5.65 o 10 10 1 225.08 231.27 18.95 o -11 11 1 143.91 169.16 14.49 o -9 11 1 1198.82 1288.84 38.42 o -7 11 1 1816.96 1910.75 37.62 o -5 11 1 138.50 102.78 5.69 o -3 11 1 315.80 224.32 7.47 o -1 11 1 2280.28 2007.39 31.66 o 1 11 1 433.50 327.53 8.56 o 3 11 1 121.98 174.81 7.12 o 5 11 1 290.24 284.15 9.66 o 7 11 1 2366.11 2403.14 72.61 o 9 11 1 907.11 939.89 29.89 o 11 11 1 19.69 35.12 10.18 o -12 12 1 107.74 99.18 16.30 o -10 12 1 2152.72 2063.12 43.81 o -8 12 1 4027.13 4032.85 84.82 o -6 12 1 946.30 882.25 21.38 o -4 12 1 154.34 106.91 5.76 o -2 12 1 4022.67 4063.95 49.91 o 0 12 1 6702.36 7224.23 105.35 o 2 12 1 282.44 230.42 7.90 o 4 12 1 26.88 45.01 4.60 o 6 12 1 1933.14 1905.90 33.34 o 8 12 1 4280.97 4272.21 140.70 o 10 12 1 969.04 886.19 34.75 o -11 13 1 198.81 231.48 19.86 o -9 13 1 111.49 118.63 12.16 o -7 13 1 514.46 521.19 17.66 o -5 13 1 2010.54 1921.01 59.99 o -3 13 1 1430.34 1372.21 25.99 o -1 13 1 156.39 144.19 6.88 o 1 13 1 231.90 223.37 8.43 o 3 13 1 1164.75 1093.50 21.69 o 5 13 1 1010.28 938.70 22.86 o 7 13 1 269.74 274.04 16.23 o 9 13 1 130.18 141.84 15.92 o -12 14 1 424.69 429.74 30.58 o -10 14 1 112.47 110.88 14.57 o -8 14 1 8.63 12.85 4.13 o -6 14 1 1113.90 1132.21 25.24 o -4 14 1 4983.00 5263.73 90.56 o -2 14 1 2323.35 2304.20 43.47 o 0 14 1 141.59 143.42 7.08 o 2 14 1 1387.56 1319.91 38.93 o 4 14 1 3134.18 3115.36 83.51 o 6 14 1 841.67 851.10 26.16 o 8 14 1 57.81 64.33 11.33 o 10 14 1 76.37 84.76 12.92 o -11 15 1 582.18 545.00 34.72 o -9 15 1 803.89 779.29 31.47 o -7 15 1 11.81 11.81 3.99 o -5 15 1 602.14 562.32 15.73 o -3 15 1 1015.29 1112.09 19.33 o -1 15 1 9678.23 10031.28 229.42 o 1 15 1 4215.06 4456.25 50.13 o 3 15 1 25.59 25.37 4.83 o 5 15 1 158.52 155.89 10.67 o 7 15 1 352.96 353.19 21.80 o 9 15 1 626.07 696.43 31.26 o -10 16 1 234.31 226.40 19.96 o -8 16 1 348.87 336.35 18.26 o -6 16 1 156.61 180.77 11.35 o -4 16 1 339.86 360.34 13.90 o -2 16 1 2920.81 3010.98 41.82 o 0 16 1 4771.83 4788.77 69.42 o 2 16 1 1168.87 1140.03 28.12 o 4 16 1 178.24 198.32 10.42 o 6 16 1 374.91 360.95 21.08 o 8 16 1 302.86 292.92 21.96 o -11 17 1 18.94 42.66 8.88 o -9 17 1 0.09 7.52 5.77 o -7 17 1 103.38 109.71 11.73 o -5 17 1 28.07 31.80 5.77 o -3 17 1 17.41 25.32 5.11 o -1 17 1 194.34 215.49 9.25 o 1 17 1 0.61 2.97 3.79 o 3 17 1 96.97 96.85 8.18 o 5 17 1 59.86 62.93 9.03 o 7 17 1 222.33 222.26 19.19 o 9 17 1 1.60 8.99 5.73 o -10 18 1 383.29 436.32 25.55 o -8 18 1 411.93 416.98 23.76 o -6 18 1 960.46 888.12 27.87 o -4 18 1 2224.04 2229.54 33.08 o -2 18 1 1771.37 1660.82 27.48 o 0 18 1 274.83 221.30 11.07 o 2 18 1 139.25 148.55 9.99 o 4 18 1 809.02 819.05 26.18 o 6 18 1 1580.71 1478.84 43.51 o 8 18 1 879.25 859.07 35.51 o -9 19 1 3.25 15.26 6.42 o -7 19 1 354.99 347.74 18.99 o -5 19 1 5207.63 4970.46 65.14 o -3 19 1 3076.96 2886.55 55.21 o -1 19 1 523.42 477.62 17.35 o 1 19 1 679.95 649.30 18.24 o 3 19 1 1806.35 1686.65 42.11 o 5 19 1 3601.62 3388.91 64.68 o 7 19 1 506.37 502.22 26.48 o -8 20 1 51.71 60.36 10.96 o -6 20 1 11.54 14.74 5.47 o -4 20 1 7.56 10.57 4.56 o -2 20 1 1.18 4.73 3.98 o 0 20 1 14.34 20.21 5.26 o 2 20 1 11.72 17.70 4.13 o 4 20 1 4.22 4.94 4.30 o 6 20 1 38.32 46.11 10.16 o 8 20 1 28.79 38.41 8.50 o -9 21 1 1.01 10.67 6.24 o -7 21 1 44.34 55.38 10.27 o -5 21 1 853.77 782.89 31.19 o -3 21 1 913.17 918.24 28.45 o -1 21 1 28.44 47.47 8.12 o 1 21 1 5.29 5.84 3.82 o 3 21 1 329.34 321.01 15.47 o 5 21 1 667.87 624.94 28.75 o 7 21 1 180.73 200.43 19.74 o -8 22 1 191.02 193.46 21.84 o -6 22 1 318.86 322.98 21.71 o -4 22 1 698.67 686.59 29.22 o -2 22 1 1808.27 1879.37 41.58 o 0 22 1 1682.66 1719.94 45.19 o 2 22 1 439.23 457.83 20.43 o 4 22 1 297.32 320.28 21.06 o 6 22 1 663.00 682.33 31.39 o -7 23 1 2.44 11.71 6.77 o -5 23 1 124.86 140.39 15.91 o -3 23 1 345.87 361.72 18.68 o -1 23 1 312.62 316.58 20.41 o 1 23 1 307.88 313.59 19.90 o 3 23 1 242.91 288.85 19.92 o 5 23 1 64.42 81.54 11.80 o -6 24 1 12.33 17.47 7.53 o -4 24 1 284.56 344.28 22.19 o -2 24 1 432.44 446.96 24.07 o 0 24 1 139.52 130.65 14.88 o 2 24 1 43.94 60.31 9.58 o 4 24 1 85.36 123.48 21.48 o -5 25 1 816.87 819.27 34.59 o -3 25 1 1375.95 1405.85 52.34 o -1 25 1 189.78 196.94 18.15 o 1 25 1 51.66 61.30 9.99 o 3 25 1 577.83 609.97 44.29 o -4 26 1 104.51 91.19 16.11 o -2 26 1 243.22 234.86 20.17 o 0 26 1 206.99 194.38 19.01 o 2 26 1 31.75 27.10 9.37 o -1 27 1 2.93 17.01 12.09 o -14 0 2 144.27 168.99 24.83 o -12 0 2 9.58 14.08 6.75 o -10 0 2 5942.64 5999.23 126.39 o -8 0 2 19892.62 19437.39 381.27 o -6 0 2 245.38 180.32 8.05 o -4 0 2 12563.11 14683.44 137.62 o -2 0 2 48193.75 49863.69 1368.80 o 0 0 2 194182.69 163818.28 4767.67 o 2 0 2 20902.06 20508.02 254.80 o 4 0 2 1286.87 1359.90 24.29 o 6 0 2 278.34 271.23 18.40 o 8 0 2 3541.04 3577.36 119.30 o 10 0 2 1017.98 930.93 54.57 o -13 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3809.86 76.08 o 7 3 2 615.59 625.74 20.55 o 9 3 2 486.61 491.75 21.42 o 11 3 2 411.14 396.83 28.60 o -14 4 2 390.27 420.16 24.27 o -12 4 2 353.19 358.17 16.12 o -10 4 2 304.66 278.78 13.56 o -8 4 2 2913.07 2828.94 34.23 o -6 4 2 16543.23 17930.07 161.73 o -4 4 2 16916.68 17862.68 258.70 o -2 4 2 244.27 257.29 5.79 o 0 4 2 3628.39 4037.34 38.43 o 2 4 2 2879.22 2614.01 40.56 o 4 4 2 9919.54 10038.37 137.83 o 6 4 2 3233.52 3167.26 103.17 o 8 4 2 269.17 285.93 14.80 o 10 4 2 177.63 224.79 15.91 o -13 5 2 8.20 13.51 5.48 o -11 5 2 16.82 16.70 4.47 o -9 5 2 133.91 141.07 9.64 o -7 5 2 18.28 32.43 4.63 o -5 5 2 1670.75 1833.15 20.06 o -3 5 2 80.96 72.54 4.28 o -1 5 2 2180.60 2352.36 37.74 o 1 5 2 19.24 18.03 1.96 o 3 5 2 863.76 928.37 16.58 o 5 5 2 171.97 179.51 9.46 o 7 5 2 25.12 26.34 5.19 o 9 5 2 18.53 14.37 4.59 o 11 5 2 1.00 11.08 7.31 o -14 6 2 566.77 587.34 29.34 o -12 6 2 76.30 76.73 10.34 o -10 6 2 27.39 29.63 4.93 o -8 6 2 1739.50 1628.78 31.93 o -6 6 2 4412.25 4486.31 94.60 o -4 6 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