#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/73/2227310.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227310_Fobs loop_ _publ_author_name 'Shen, Shi-De' 'Feng, Xiao-Dong' 'Yang, Wei-Hua' 'Yao, Chang-Sheng' _publ_section_title ; 5'-Amino-2-oxo-2',3'-dihydrospiro[indoline-3,7'-thieno[3,2-b]pyran]-6'-carbonitrile 1',1'-dioxide ; _journal_coeditor_code CI5148 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2448 _journal_volume 66 _journal_year 2010 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.611 _cell_angle_gamma 90.000 _cell_length_a 30.6690 _cell_length_b 8.1760 _cell_length_c 12.2290 _exptl_crystal_F_000 1360.00 _reflns_d_resolution_high 0.7095 _[local]_cod_data_source_file ci5148Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' _m100624c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 270.44 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4652.11 707.23 1348.10 o 6 0 0 25803.31 26369.67 1006.08 o 8 0 0 3319.92 3780.82 133.17 o 10 0 0 17359.74 18367.63 152.98 o 12 0 0 13.77 45.51 7.27 o 14 0 0 1288.98 1441.97 41.51 o 16 0 0 4242.06 4079.09 41.71 o 18 0 0 7624.50 8542.12 147.28 o 20 0 0 3380.15 3157.78 53.26 o 22 0 0 6948.41 6697.64 204.42 o 24 0 0 31475.44 34106.70 268.39 o 26 0 0 495.65 465.94 26.01 o 28 0 0 432.61 478.79 34.29 o 30 0 0 2605.02 2717.17 67.40 o 32 0 0 256.93 240.80 13.84 o 34 0 0 530.11 579.19 32.77 o 36 0 0 35.88 30.55 15.08 o 38 0 0 68.45 63.24 59.14 o 3 1 0 513.34 528.98 6.45 o 5 1 0 5058.91 5666.80 35.82 o 7 1 0 24734.90 21853.52 1513.93 o 9 1 0 2211.00 2464.79 32.40 o 11 1 0 13322.07 15870.79 190.89 o 13 1 0 614.42 673.15 13.77 o 15 1 0 3550.88 3886.81 72.41 o 17 1 0 2195.44 1979.80 76.74 o 19 1 0 763.86 774.59 32.90 o 21 1 0 832.04 867.10 25.76 o 23 1 0 5054.90 5057.54 68.23 o 25 1 0 3067.00 2953.70 86.26 o 27 1 0 14.54 15.44 5.28 o 29 1 0 265.43 226.33 11.65 o 31 1 0 0.38 4.12 2.71 o 33 1 0 182.87 176.82 13.27 o 35 1 0 798.84 733.53 25.54 o 37 1 0 36.47 18.62 10.81 o 39 1 0 100.62 88.40 46.04 o 0 2 0 64009.02 69587.31 4031.85 o 2 2 0 22750.66 25402.09 229.08 o 4 2 0 12537.56 12977.01 134.45 o 6 2 0 68214.55 74062.23 2807.29 o 8 2 0 13197.29 15181.25 142.70 o 10 2 0 42165.80 48796.66 489.14 o 12 2 0 8144.41 8681.34 117.37 o 14 2 0 13101.86 14987.60 148.42 o 16 2 0 474.33 398.23 14.27 o 18 2 0 3.27 3.08 3.90 o 20 2 0 781.00 756.30 22.80 o 22 2 0 614.81 567.90 16.93 o 24 2 0 1258.50 1187.04 40.41 o 26 2 0 1271.38 1171.23 35.22 o 28 2 0 163.72 150.42 14.23 o 30 2 0 1648.16 1609.22 36.50 o 32 2 0 767.12 810.06 34.73 o 34 2 0 1854.68 1950.84 79.14 o 36 2 0 35.24 30.80 12.78 o 38 2 0 478.55 530.30 25.96 o 1 3 0 3037.29 3107.96 33.82 o 3 3 0 4548.82 4218.46 136.16 o 5 3 0 2478.47 2625.56 19.48 o 7 3 0 17484.00 19744.65 194.98 o 9 3 0 28152.46 33325.11 428.64 o 11 3 0 202.83 175.59 9.54 o 13 3 0 2713.93 2831.96 27.96 o 15 3 0 1030.12 1101.52 29.05 o 17 3 0 281.36 215.78 9.61 o 19 3 0 550.16 536.53 17.00 o 21 3 0 265.54 243.17 8.61 o 23 3 0 597.71 494.66 21.33 o 25 3 0 103.37 71.50 10.48 o 27 3 0 641.38 632.98 23.97 o 29 3 0 399.54 368.30 14.04 o 31 3 0 1133.58 1096.69 48.23 o 33 3 0 1388.50 1515.12 41.17 o 35 3 0 2.99 7.98 5.93 o 37 3 0 300.76 267.97 55.36 o 0 4 0 59.53 30.61 9.76 o 2 4 0 120.07 118.79 7.45 o 4 4 0 5943.01 5595.11 200.07 o 6 4 0 10034.03 11034.33 127.50 o 8 4 0 15.64 43.57 8.68 o 10 4 0 8398.10 9081.92 73.33 o 12 4 0 7179.38 7560.74 124.83 o 14 4 0 592.94 521.19 17.98 o 16 4 0 5272.29 5417.51 69.20 o 18 4 0 546.43 479.76 17.41 o 20 4 0 3074.64 3299.83 49.38 o 22 4 0 37.44 19.21 5.48 o 24 4 0 10.67 34.50 7.52 o 26 4 0 79.65 110.36 9.52 o 28 4 0 174.40 158.86 11.58 o 30 4 0 203.03 185.58 22.88 o 32 4 0 19.75 20.47 11.19 o 34 4 0 73.77 61.74 14.43 o 36 4 0 714.90 758.41 43.12 o 1 5 0 1449.38 1426.20 39.15 o 3 5 0 7463.54 7542.99 174.23 o 5 5 0 2163.87 2451.91 53.53 o 7 5 0 6824.48 6978.53 62.36 o 9 5 0 469.30 564.33 20.90 o 11 5 0 209.73 186.30 10.25 o 13 5 0 5695.88 5606.98 187.17 o 15 5 0 942.68 1018.88 31.45 o 17 5 0 6011.92 6076.18 85.50 o 19 5 0 17.73 5.85 5.92 o 21 5 0 1972.55 1929.84 56.51 o 23 5 0 1344.09 1492.26 38.75 o 25 5 0 567.80 586.53 25.79 o 27 5 0 1387.05 1444.32 55.61 o 29 5 0 81.57 70.23 16.90 o 31 5 0 785.84 768.50 39.66 o 33 5 0 133.31 122.07 31.82 o 35 5 0 204.66 135.43 41.40 o 0 6 0 717.72 767.55 35.89 o 2 6 0 385.58 405.93 16.43 o 4 6 0 2412.87 2648.63 36.74 o 6 6 0 85.76 104.17 18.95 o 8 6 0 2070.54 2078.10 35.37 o 10 6 0 300.54 306.02 12.80 o 12 6 0 386.73 387.64 15.82 o 14 6 0 0.74 9.03 5.60 o 16 6 0 130.77 137.89 16.55 o 18 6 0 80.92 100.44 20.83 o 20 6 0 112.91 118.05 21.82 o 22 6 0 1.31 8.68 5.46 o 24 6 0 459.67 424.32 24.61 o 26 6 0 482.95 452.12 26.46 o 28 6 0 131.88 134.14 29.39 o 30 6 0 80.06 65.45 16.34 o 32 6 0 26.50 27.95 10.71 o 34 6 0 6.85 12.29 9.81 o 1 7 0 1782.14 1733.68 44.31 o 3 7 0 4654.58 4899.18 69.13 o 5 7 0 217.75 209.34 20.15 o 7 7 0 2506.73 2396.49 50.86 o 9 7 0 300.50 227.76 18.69 o 11 7 0 2119.26 2067.84 35.33 o 13 7 0 601.96 680.47 29.13 o 15 7 0 60.39 50.24 10.58 o 17 7 0 1731.33 1723.14 44.41 o 19 7 0 984.08 1059.22 31.37 o 21 7 0 815.12 769.86 36.83 o 23 7 0 1055.31 1061.25 43.39 o 25 7 0 39.40 42.58 11.31 o 27 7 0 1199.79 1208.88 48.94 o 29 7 0 21.79 27.69 14.07 o 31 7 0 1285.08 1311.34 59.77 o 0 8 0 35.46 44.95 13.24 o 2 8 0 340.01 329.66 23.68 o 4 8 0 9.71 16.51 7.16 o 6 8 0 72.51 84.45 17.11 o 8 8 0 2.70 5.16 7.06 o 10 8 0 751.80 795.96 31.28 o 12 8 0 6.72 11.95 6.32 o 14 8 0 628.51 642.05 29.04 o 16 8 0 113.21 133.51 24.95 o 18 8 0 173.06 143.01 13.76 o 20 8 0 683.87 631.26 26.28 o 22 8 0 9.36 17.65 7.18 o 24 8 0 291.07 267.32 27.56 o 26 8 0 91.69 86.02 22.94 o 28 8 0 2.45 8.10 8.11 o 1 9 0 675.61 639.38 29.15 o 3 9 0 257.39 266.23 15.16 o 5 9 0 238.23 238.10 27.01 o 7 9 0 388.86 364.08 22.23 o 9 9 0 30.04 31.38 9.22 o 11 9 0 1548.53 1611.92 56.71 o 13 9 0 65.69 94.66 21.34 o 15 9 0 798.52 763.15 24.26 o 17 9 0 550.00 488.25 24.52 o 19 9 0 255.22 261.11 20.04 o 21 9 0 286.54 265.49 23.18 o 23 9 0 109.57 103.47 41.68 o 0 10 0 86.79 80.85 23.08 o 2 10 0 106.09 92.90 19.54 o 4 10 0 518.32 531.84 19.57 o 6 10 0 0.22 6.32 5.47 o 8 10 0 1149.87 1121.89 40.25 o 10 10 0 1443.82 1499.55 52.26 o 12 10 0 0.03 16.75 9.72 o 14 10 0 1969.45 2016.49 87.69 o 16 10 0 74.80 62.97 19.72 o 18 10 0 217.43 176.21 20.86 o 1 11 0 256.16 248.53 24.17 o 3 11 0 39.35 39.93 11.96 o 5 11 0 64.37 56.39 15.46 o 7 11 0 72.14 67.13 21.15 o 9 11 0 40.19 44.98 14.39 o 11 11 0 0.56 9.30 11.37 o -39 1 1 7.93 4.22 10.87 o -37 1 1 218.18 180.71 19.97 o -35 1 1 183.43 190.61 13.57 o -33 1 1 464.43 468.82 21.63 o -31 1 1 1436.03 1398.56 32.68 o -29 1 1 863.47 855.40 32.52 o -27 1 1 607.24 580.59 23.77 o -25 1 1 24.75 37.93 8.51 o -23 1 1 246.75 227.36 11.25 o -21 1 1 1595.00 1581.66 34.20 o -19 1 1 3357.11 3095.20 30.58 o -17 1 1 751.98 730.73 20.65 o -15 1 1 3533.43 3741.08 23.93 o -13 1 1 1.45 44.21 4.35 o -11 1 1 1113.65 970.76 8.14 o -9 1 1 17411.74 17930.90 140.63 o -7 1 1 3831.25 3680.67 49.27 o -5 1 1 15685.79 15709.85 117.14 o -3 1 1 1936.43 1994.10 22.08 o -1 1 1 5959.45 6119.02 61.56 o 1 1 1 116.07 109.37 2.23 o 3 1 1 16107.39 16853.82 117.88 o 5 1 1 12877.88 14478.31 114.65 o 7 1 1 2758.43 2355.05 19.89 o 9 1 1 997.73 799.90 6.91 o 11 1 1 260.56 381.88 8.27 o 13 1 1 1142.19 1062.73 20.27 o 15 1 1 15845.47 18927.64 219.01 o 17 1 1 345.51 288.02 10.28 o 19 1 1 6.02 24.17 5.12 o 21 1 1 3080.15 3081.24 44.09 o 23 1 1 4199.22 4235.61 61.11 o 25 1 1 614.82 641.28 17.74 o 27 1 1 2451.52 2389.83 50.01 o 29 1 1 31.86 25.20 6.98 o 31 1 1 3.61 8.19 6.30 o 33 1 1 628.14 592.89 25.65 o 35 1 1 11.40 13.08 8.36 o 37 1 1 350.01 326.25 18.74 o -40 2 1 365.39 322.38 43.76 o -38 2 1 222.11 224.40 23.89 o -36 2 1 49.33 47.49 15.76 o -34 2 1 80.48 66.87 18.22 o -32 2 1 1820.55 1686.11 45.96 o -30 2 1 181.55 159.39 10.62 o -28 2 1 230.50 220.18 15.90 o -26 2 1 89.97 95.17 12.55 o -24 2 1 4295.86 4488.41 63.86 o -22 2 1 1556.81 1373.58 30.05 o -20 2 1 124.63 122.20 6.76 o -18 2 1 108.07 77.21 6.80 o -16 2 1 513.53 566.90 14.84 o -14 2 1 4108.78 4051.87 209.03 o -12 2 1 3776.84 4076.98 26.89 o -10 2 1 294.05 209.33 4.50 o -8 2 1 10404.59 12047.53 115.50 o -6 2 1 1095.63 1091.35 7.46 o -4 2 1 5066.73 4803.44 73.88 o -2 2 1 984.55 907.54 6.62 o 0 2 1 4134.63 4060.67 44.30 o 2 2 1 49709.26 53983.79 459.41 o 4 2 1 37124.59 41010.52 545.40 o 6 2 1 616.06 466.59 9.58 o 8 2 1 448.57 494.61 11.30 o 10 2 1 17.03 6.48 2.65 o 12 2 1 979.68 1018.37 20.39 o 14 2 1 1949.22 2000.23 45.79 o 16 2 1 5.39 6.05 3.57 o 18 2 1 1329.21 1219.67 45.82 o 20 2 1 322.43 284.96 11.09 o 22 2 1 3592.00 3646.32 56.25 o 24 2 1 100.86 113.74 9.06 o 26 2 1 28.35 28.40 6.41 o 28 2 1 29.39 33.58 7.37 o 30 2 1 21.23 30.82 8.87 o 32 2 1 1.95 6.92 7.12 o 34 2 1 34.01 22.88 8.20 o 36 2 1 346.33 331.83 22.71 o 38 2 1 90.99 62.99 23.97 o -39 3 1 158.16 98.03 43.12 o -37 3 1 7.07 7.73 7.92 o -35 3 1 1706.37 1724.78 65.39 o -33 3 1 16.01 19.42 7.99 o -31 3 1 5.71 14.19 6.24 o -29 3 1 58.85 62.40 9.80 o -27 3 1 1.20 2.98 4.73 o -25 3 1 7.82 15.45 4.64 o -23 3 1 94.59 95.14 10.58 o -21 3 1 3.47 11.21 3.95 o -19 3 1 116.89 111.22 11.41 o -17 3 1 20.69 19.08 4.93 o -15 3 1 581.57 613.20 16.48 o -13 3 1 2372.88 1981.62 42.12 o -11 3 1 8981.23 9829.80 129.56 o -9 3 1 3201.01 3256.85 51.98 o -7 3 1 1036.45 840.40 27.47 o -5 3 1 3074.49 3157.81 79.61 o -3 3 1 16575.41 17538.81 221.99 o -1 3 1 2888.23 3259.22 59.23 o 1 3 1 465.05 337.89 7.63 o 3 3 1 1764.95 1923.17 20.57 o 5 3 1 1391.28 1432.24 27.68 o 7 3 1 368.43 307.01 9.34 o 9 3 1 1307.16 1469.65 30.46 o 11 3 1 3516.26 3461.87 32.19 o 13 3 1 4250.36 4211.41 79.44 o 15 3 1 54.31 76.23 14.80 o 17 3 1 2306.15 2206.16 32.68 o 19 3 1 303.61 294.52 12.84 o 21 3 1 1665.05 1628.78 38.01 o 23 3 1 422.84 433.21 18.94 o 25 3 1 491.43 406.38 18.95 o 27 3 1 1051.85 1034.11 40.69 o 29 3 1 149.19 136.67 17.00 o 31 3 1 612.54 628.63 22.37 o 33 3 1 3.89 7.39 7.74 o 35 3 1 196.59 159.16 47.95 o 37 3 1 626.95 663.93 43.85 o -38 4 1 0.95 4.01 8.51 o -36 4 1 47.39 42.88 13.54 o -34 4 1 298.52 315.51 24.89 o -32 4 1 51.12 62.14 16.26 o -30 4 1 1713.01 1521.70 62.59 o -28 4 1 694.30 656.86 31.39 o -26 4 1 2591.20 2768.50 63.65 o -24 4 1 0.56 3.37 3.55 o -22 4 1 2255.08 1843.31 39.14 o -20 4 1 943.62 795.94 22.18 o -18 4 1 1504.39 1352.70 32.02 o -16 4 1 185.05 143.62 7.44 o -14 4 1 773.95 736.80 22.90 o -12 4 1 1220.40 1320.11 34.66 o -10 4 1 6520.19 6847.82 63.72 o -8 4 1 2323.64 2269.03 25.11 o -6 4 1 10185.36 11348.65 114.48 o -4 4 1 5937.21 5877.16 86.36 o -2 4 1 5024.90 5855.57 63.39 o 0 4 1 620.83 909.31 20.73 o 2 4 1 14551.49 16834.42 108.89 o 4 4 1 3.14 5.07 4.48 o 6 4 1 28.05 61.12 12.95 o 8 4 1 1386.60 1494.14 38.55 o 10 4 1 1983.51 2117.33 53.06 o 12 4 1 4.92 10.58 4.28 o 14 4 1 2286.25 2054.29 29.46 o 16 4 1 27.78 56.92 11.73 o 18 4 1 649.51 533.15 16.78 o 20 4 1 532.87 601.07 23.29 o 22 4 1 1036.62 891.14 28.63 o 24 4 1 64.95 21.75 5.90 o 26 4 1 927.87 944.77 41.76 o 28 4 1 859.93 864.11 29.94 o 30 4 1 1161.46 1294.16 58.27 o 32 4 1 57.69 77.51 19.58 o 34 4 1 131.04 134.08 47.97 o 36 4 1 6.43 19.93 7.96 o -35 5 1 684.58 754.92 39.93 o -33 5 1 848.94 920.98 39.68 o -31 5 1 563.25 568.60 31.35 o -29 5 1 66.87 66.11 14.79 o -27 5 1 692.85 678.73 32.13 o -25 5 1 281.79 265.64 18.48 o -23 5 1 134.46 101.09 12.50 o -21 5 1 506.82 380.18 18.81 o -19 5 1 27.89 21.08 5.67 o -17 5 1 1681.61 1673.92 39.72 o -15 5 1 1685.98 1613.86 26.54 o -13 5 1 28.11 33.29 7.35 o -11 5 1 18.11 25.84 5.81 o -9 5 1 27.95 40.27 9.14 o -7 5 1 735.19 883.28 29.57 o -5 5 1 2138.52 2093.98 53.43 o -3 5 1 460.85 445.46 14.07 o -1 5 1 818.46 864.62 24.45 o 1 5 1 5203.81 5485.51 109.91 o 3 5 1 563.70 727.23 21.63 o 5 5 1 470.39 421.37 17.62 o 7 5 1 2078.08 2113.38 30.43 o 9 5 1 3245.92 3455.76 46.48 o 11 5 1 4575.00 4811.22 59.06 o 13 5 1 3355.55 3427.45 45.69 o 15 5 1 10.00 11.53 4.82 o 17 5 1 2254.06 2187.78 46.06 o 19 5 1 2128.66 2013.55 29.31 o 21 5 1 0.11 5.27 5.21 o 23 5 1 937.54 822.07 30.72 o 25 5 1 726.63 688.36 31.59 o 27 5 1 699.20 687.70 44.08 o 29 5 1 51.31 41.72 11.93 o 31 5 1 133.72 119.88 23.58 o 33 5 1 311.57 324.55 32.52 o -34 6 1 869.54 966.04 46.26 o -32 6 1 364.20 379.82 27.70 o -30 6 1 753.04 779.12 37.20 o -28 6 1 439.08 435.27 20.80 o -26 6 1 76.41 94.44 21.86 o -24 6 1 708.70 719.02 34.73 o -22 6 1 186.63 204.03 12.55 o -20 6 1 1486.92 1595.86 46.69 o -18 6 1 2887.00 2708.63 48.90 o -16 6 1 5743.36 6056.52 115.51 o -14 6 1 599.02 588.28 23.34 o -12 6 1 1080.64 965.96 25.60 o -10 6 1 1364.18 1381.29 39.25 o -8 6 1 4071.96 4036.58 53.37 o -6 6 1 65.12 80.12 15.68 o -4 6 1 3725.61 3548.71 48.16 o -2 6 1 114.28 154.41 17.26 o 0 6 1 1522.65 1513.08 25.98 o 2 6 1 220.90 262.01 14.31 o 4 6 1 2611.25 2550.25 36.29 o 6 6 1 6162.07 6113.54 75.58 o 8 6 1 10590.75 10430.76 121.02 o 10 6 1 4044.65 4094.00 61.93 o 12 6 1 491.76 496.14 20.92 o 14 6 1 307.39 306.19 15.12 o 16 6 1 1419.12 1405.17 43.29 o 18 6 1 282.85 272.48 18.16 o 20 6 1 415.79 472.21 20.51 o 22 6 1 102.66 85.21 17.16 o 24 6 1 616.63 622.51 31.49 o 26 6 1 368.11 406.46 23.37 o 28 6 1 1384.54 1501.51 59.62 o 30 6 1 1280.61 1347.21 68.60 o 32 6 1 2250.48 2425.42 99.66 o -31 7 1 186.45 191.15 45.36 o -29 7 1 465.96 485.83 24.64 o -27 7 1 960.43 978.75 42.42 o -25 7 1 0.02 10.36 7.15 o -23 7 1 15.14 16.83 5.73 o -21 7 1 843.29 841.50 31.44 o -19 7 1 549.57 525.55 24.59 o -17 7 1 3566.26 3623.22 80.72 o -15 7 1 2585.96 2605.00 55.41 o -13 7 1 2133.70 2136.42 42.97 o -11 7 1 2536.90 2586.86 46.94 o -9 7 1 2.51 9.26 5.94 o -7 7 1 1705.82 1752.37 41.35 o -5 7 1 128.98 161.36 20.59 o -3 7 1 25.49 43.37 8.91 o -1 7 1 2898.90 2926.18 49.57 o 1 7 1 99.20 139.60 24.84 o 3 7 1 827.96 822.14 31.23 o 5 7 1 47.02 59.85 11.58 o 7 7 1 31.76 40.77 8.57 o 9 7 1 2863.38 2848.26 51.46 o 11 7 1 8109.89 8320.11 116.77 o 13 7 1 16.45 21.80 5.89 o 15 7 1 143.52 140.34 24.31 o 17 7 1 1911.94 1802.45 37.56 o 19 7 1 269.98 222.31 13.65 o 21 7 1 29.31 27.82 7.41 o 23 7 1 1152.59 1197.11 52.76 o 25 7 1 472.18 501.42 27.48 o 27 7 1 84.70 73.92 17.84 o 29 7 1 9.48 11.04 10.27 o -28 8 1 519.94 557.85 28.52 o -26 8 1 948.57 982.75 53.58 o -24 8 1 67.24 68.86 16.44 o -22 8 1 74.26 99.40 21.84 o -20 8 1 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2090.71 2281.70 83.69 o 26 4 6 7.18 12.19 6.54 o 28 4 6 1488.81 1513.46 65.96 o -37 5 6 18.91 8.93 6.25 o -35 5 6 749.38 814.00 30.98 o -33 5 6 1339.59 1333.49 34.44 o -31 5 6 1513.65 1599.79 60.11 o -29 5 6 825.72 766.82 35.28 o -27 5 6 348.65 375.30 21.85 o -25 5 6 112.31 128.86 13.76 o -23 5 6 3022.50 3099.54 71.60 o -21 5 6 2007.22 1965.97 49.78 o -19 5 6 5312.74 5565.81 118.29 o -17 5 6 3229.73 3171.71 77.17 o -15 5 6 2756.47 2818.18 54.59 o -13 5 6 139.56 174.20 14.75 o -11 5 6 1056.68 979.99 29.16 o -9 5 6 4525.36 4862.90 57.70 o -7 5 6 2504.30 2476.72 34.54 o -5 5 6 0.95 7.93 4.74 o -3 5 6 440.67 428.78 15.89 o -1 5 6 3169.83 3029.16 41.13 o 1 5 6 3486.31 3197.42 48.18 o 3 5 6 9960.89 9792.25 134.00 o 5 5 6 2615.43 2449.24 52.70 o 7 5 6 7958.06 7975.06 151.48 o 9 5 6 13.28 24.25 7.01 o 11 5 6 332.31 292.39 19.01 o 13 5 6 3740.84 3847.04 94.47 o 15 5 6 897.59 916.16 41.10 o 17 5 6 1826.08 1921.47 59.27 o 19 5 6 546.87 535.77 21.21 o 21 5 6 101.76 113.82 25.40 o 23 5 6 1705.39 1842.09 65.24 o 25 5 6 427.22 459.83 20.85 o 27 5 6 1272.67 1292.23 56.28 o -36 6 6 587.01 624.20 32.09 o -34 6 6 2.10 8.28 7.65 o -32 6 6 89.63 86.40 19.57 o -30 6 6 169.27 191.68 35.73 o -28 6 6 521.69 470.84 24.73 o -26 6 6 88.64 69.74 18.41 o -24 6 6 27.74 32.41 9.21 o -22 6 6 921.53 861.71 36.81 o -20 6 6 28.17 30.93 9.57 o -18 6 6 2031.66 1925.10 46.29 o -16 6 6 1546.18 1576.45 52.46 o -14 6 6 97.38 70.71 13.70 o -12 6 6 338.03 348.36 15.98 o -10 6 6 218.50 157.34 13.45 o -8 6 6 996.21 1036.58 37.29 o -6 6 6 430.17 369.06 16.92 o -4 6 6 1.54 15.59 4.38 o -2 6 6 0.01 7.94 5.55 o 0 6 6 4772.68 4798.14 102.25 o 2 6 6 874.96 849.64 28.25 o 4 6 6 792.60 745.19 25.59 o 6 6 6 1589.21 1588.82 32.91 o 8 6 6 210.31 194.70 18.73 o 10 6 6 152.37 153.13 28.03 o 12 6 6 62.79 83.90 16.88 o 14 6 6 21.65 25.48 7.34 o 16 6 6 266.96 311.55 17.96 o 18 6 6 799.45 855.01 26.08 o 20 6 6 9.39 15.49 6.72 o 22 6 6 474.44 461.43 22.89 o 24 6 6 0.01 8.33 6.29 o -33 7 6 625.83 555.25 24.31 o -31 7 6 687.27 701.00 39.02 o -29 7 6 479.52 511.68 20.25 o -27 7 6 1501.98 1447.50 37.09 o -25 7 6 108.59 113.76 25.67 o -23 7 6 1928.98 1994.00 73.33 o -21 7 6 482.41 451.62 25.17 o -19 7 6 1271.99 1306.86 36.79 o -17 7 6 1355.91 1353.32 36.02 o -15 7 6 30.95 62.64 13.51 o -13 7 6 827.18 865.62 32.88 o -11 7 6 2191.87 2048.76 44.20 o -9 7 6 1877.85 1751.75 41.23 o -7 7 6 2725.36 2775.28 57.04 o -5 7 6 750.94 655.88 28.12 o -3 7 6 5123.92 5531.57 110.98 o -1 7 6 620.71 575.88 27.90 o 1 7 6 2153.33 2028.75 49.42 o 3 7 6 2269.92 2297.12 57.58 o 5 7 6 70.34 91.74 18.68 o 7 7 6 1010.64 1061.23 24.75 o 9 7 6 3.41 10.28 7.72 o 11 7 6 438.33 457.01 25.68 o 13 7 6 928.49 944.35 40.08 o 15 7 6 957.28 960.79 29.37 o 17 7 6 2162.93 2319.77 77.62 o 19 7 6 6.08 11.45 8.49 o 21 7 6 678.12 649.44 34.49 o -30 8 6 298.56 271.90 25.59 o -28 8 6 91.63 82.33 22.30 o -26 8 6 122.99 103.24 27.31 o -24 8 6 188.02 181.49 38.85 o -22 8 6 678.35 698.37 24.67 o -20 8 6 14.51 15.80 10.23 o -18 8 6 939.49 945.34 39.89 o -16 8 6 258.38 222.37 21.42 o -14 8 6 1.11 -0.15 10.52 o -12 8 6 81.77 84.22 17.35 o -10 8 6 4805.32 4988.61 72.28 o -8 8 6 55.75 62.08 14.16 o -6 8 6 3266.88 3271.76 60.64 o -4 8 6 310.06 367.55 21.98 o -2 8 6 567.33 571.34 26.21 o 0 8 6 2769.48 2800.27 76.86 o 2 8 6 6.41 16.99 4.87 o 4 8 6 275.43 285.07 20.87 o 6 8 6 172.15 167.97 22.82 o 8 8 6 62.54 69.79 15.73 o 10 8 6 361.26 365.62 19.29 o 12 8 6 2942.07 3053.78 99.95 o 14 8 6 1412.36 1416.08 50.02 o 16 8 6 320.68 332.85 18.75 o 18 8 6 54.17 50.10 14.75 o -25 9 6 397.79 364.49 25.33 o -23 9 6 135.05 131.12 34.61 o -21 9 6 553.86 549.37 26.98 o -19 9 6 9.59 18.22 10.03 o -17 9 6 2328.59 2378.56 80.87 o -15 9 6 2.67 6.21 8.54 o -13 9 6 3932.70 4072.24 85.52 o -11 9 6 28.62 43.57 11.49 o -9 9 6 5.39 9.20 9.18 o -7 9 6 391.86 290.19 44.52 o -5 9 6 164.13 171.39 32.53 o -3 9 6 1900.41 1930.14 64.49 o -1 9 6 222.85 213.03 22.56 o 1 9 6 45.77 42.09 10.20 o 3 9 6 904.05 865.72 24.81 o 5 9 6 340.37 357.79 16.59 o 7 9 6 844.16 899.64 34.68 o 9 9 6 120.41 113.09 34.77 o 11 9 6 1196.67 1243.48 57.42 o 13 9 6 158.56 125.12 28.55 o -18 10 6 271.36 248.54 26.20 o -16 10 6 769.78 765.98 36.84 o -14 10 6 116.93 110.45 31.46 o -12 10 6 1187.41 1218.44 56.92 o -10 10 6 4168.13 4328.15 162.61 o -8 10 6 55.74 65.33 23.51 o -6 10 6 3431.92 3508.41 90.53 o -4 10 6 390.43 465.29 189.09 o -2 10 6 110.93 96.13 25.33 o 0 10 6 2255.89 2268.40 89.85 o 2 10 6 27.68 21.56 7.53 o 4 10 6 524.77 489.66 21.77 o 6 10 6 699.54 746.24 35.23 o 8 10 6 0.17 7.93 7.82 o -43 1 7 51.25 31.89 14.06 o -41 1 7 42.56 34.00 12.36 o -39 1 7 478.11 492.06 20.71 o -37 1 7 505.10 475.17 20.38 o -35 1 7 7.99 12.18 7.78 o -33 1 7 3113.59 3111.22 76.67 o -31 1 7 1151.62 1058.12 41.52 o -29 1 7 419.28 432.72 18.92 o -27 1 7 8985.94 9211.71 204.33 o -25 1 7 1087.96 1072.88 36.07 o -23 1 7 2667.36 2696.53 80.81 o -21 1 7 3698.47 3750.37 154.75 o -19 1 7 1687.02 1464.33 36.33 o -17 1 7 7615.94 7308.59 413.45 o -15 1 7 3545.95 3494.71 33.15 o -13 1 7 1425.05 1253.31 27.24 o -11 1 7 10194.66 10788.94 128.60 o -9 1 7 17.52 11.69 3.32 o -7 1 7 1975.80 2116.96 51.29 o -5 1 7 10599.63 12090.09 121.66 o -3 1 7 9507.52 9549.64 152.21 o -1 1 7 1036.00 1178.81 25.59 o 1 1 7 628.05 672.24 15.64 o 3 1 7 2845.93 2564.05 28.29 o 5 1 7 144.04 119.37 8.07 o 7 1 7 2899.08 2748.27 64.92 o 9 1 7 3211.85 2965.18 56.83 o 11 1 7 430.30 393.42 14.51 o 13 1 7 55.17 56.06 13.27 o 15 1 7 71.28 57.28 14.90 o 17 1 7 2787.52 2807.12 79.91 o 19 1 7 72.59 100.78 22.83 o 21 1 7 1289.75 1390.62 63.70 o 23 1 7 653.86 681.56 30.25 o 25 1 7 108.99 123.85 24.55 o 27 1 7 27.15 32.53 11.22 o 29 1 7 77.90 56.20 25.91 o -42 2 7 508.36 579.19 42.71 o -40 2 7 1.96 6.46 6.99 o -38 2 7 832.27 841.46 38.31 o -36 2 7 20.27 20.43 6.05 o -34 2 7 29.04 34.16 8.89 o -32 2 7 293.58 314.71 18.25 o -30 2 7 421.51 402.99 20.77 o -28 2 7 8.22 14.68 5.44 o -26 2 7 14530.00 14536.34 213.54 o -24 2 7 2278.76 2162.15 50.20 o -22 2 7 13.55 16.45 5.32 o -20 2 7 10.00 7.37 4.45 o -18 2 7 2697.96 2853.83 44.99 o -16 2 7 72.73 66.45 6.37 o -14 2 7 916.71 949.59 23.51 o -12 2 7 1334.17 1460.03 31.21 o -10 2 7 622.53 583.08 19.15 o -8 2 7 4553.51 5023.70 90.10 o -6 2 7 186.38 168.50 8.40 o -4 2 7 2955.88 3007.60 46.82 o -2 2 7 17271.82 19905.40 209.30 o 0 2 7 882.96 985.12 24.39 o 2 2 7 1649.99 1747.00 23.32 o 4 2 7 478.88 425.77 12.77 o 6 2 7 1812.47 2028.41 30.07 o 8 2 7 0.15 2.81 5.26 o 10 2 7 222.95 215.14 8.74 o 12 2 7 4.62 6.79 3.76 o 14 2 7 634.55 626.08 33.89 o 16 2 7 1523.57 1428.93 42.50 o 18 2 7 35.51 36.88 10.48 o 20 2 7 309.96 285.39 21.69 o 22 2 7 1733.84 1860.20 77.77 o 24 2 7 1126.61 1105.48 50.67 o 26 2 7 32.55 33.30 11.40 o 28 2 7 457.47 483.61 21.35 o -41 3 7 145.93 114.18 28.86 o -39 3 7 972.45 1058.02 54.96 o -37 3 7 690.79 642.37 26.50 o -35 3 7 212.63 239.32 23.79 o -33 3 7 904.78 967.85 38.68 o -31 3 7 212.77 221.81 14.35 o -29 3 7 118.46 102.82 20.49 o -27 3 7 1279.92 1284.12 51.91 o -25 3 7 2984.89 2741.97 47.63 o -23 3 7 3510.53 3536.24 76.38 o -21 3 7 4959.42 4953.94 74.98 o -19 3 7 9.48 12.65 5.84 o -17 3 7 7665.13 7795.07 92.73 o -15 3 7 579.51 530.82 18.67 o -13 3 7 1671.93 1555.11 33.12 o -11 3 7 1112.83 1006.52 25.13 o -9 3 7 1507.69 1419.02 32.44 o -7 3 7 1973.82 1915.57 24.75 o -5 3 7 433.50 440.01 13.57 o -3 3 7 132.35 147.81 4.32 o -1 3 7 5843.82 6053.24 131.54 o 1 3 7 198.99 194.98 8.63 o 3 3 7 1454.82 1433.58 20.73 o 5 3 7 1991.51 1807.12 30.23 o 7 3 7 304.03 292.80 13.28 o 9 3 7 95.77 80.96 9.30 o 11 3 7 708.58 638.45 26.50 o 13 3 7 52.14 42.16 10.13 o 15 3 7 66.10 76.08 9.83 o 17 3 7 9.28 14.32 6.39 o 19 3 7 10.52 14.39 8.28 o 21 3 7 14.58 13.96 7.26 o 23 3 7 126.07 135.36 23.18 o 25 3 7 1471.17 1507.67 56.34 o 27 3 7 90.66 71.98 22.87 o -40 4 7 923.54 963.65 45.82 o -38 4 7 33.13 43.93 10.82 o -36 4 7 43.21 38.47 10.47 o -34 4 7 89.34 133.51 30.71 o -32 4 7 482.36 444.89 29.23 o -30 4 7 30.54 25.11 8.96 o -28 4 7 423.87 436.92 24.86 o -26 4 7 1144.06 1175.73 50.10 o -24 4 7 2694.20 2856.60 50.64 o -22 4 7 28.12 29.96 8.04 o -20 4 7 2767.78 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