Crystallography Open Database

Information card for entry 2227325

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Structure parameters

Chemical name	Bis[<i>N</i>'-(2-oxo-1<i>H</i>-indol-3-ylidene)thiophene-2-carbohydrazidato- κ^3^<i>O</i>,<i>N</i>',<i>O</i>']zinc(II) <i>N</i>,<i>N</i>-dimethylformide monosolvate monohydrate
Formula	C29 H25 N7 O6 S2 Zn
Calculated formula	C29 H25 N7 O6 S2 Zn
Title of publication	Bis[<i>N</i>'-(2-oxo-1<i>H</i>-indol-3-ylidene)thiophene-2-carbohydrazidato-κ^3^<i>O</i>,<i>N</i>',<i>O</i>']zinc(II) <i>N</i>,<i>N</i>-dimethylformide monosolvate monohydrate
Authors of publication	Abdul Halim, Siti Nadiah; Ali, Hapipah Mohd; Ng, Seik Weng
Journal of publication	Acta Crystallographica Section E
Year of publication	2010
Journal volume	66
Journal issue	11
Pages of publication	m1438
a	11.525 ± 0.0008 Å
b	12.0656 ± 0.0008 Å
c	13.4643 ± 0.0009 Å
α	105.913 ± 0.001°
β	100.531 ± 0.001°
γ	114.754 ± 0.001°
Cell volume	1537.25 ± 0.18 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	295 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1468
Residual factor for significantly intense reflections	0.0593
Weighted residual factors for significantly intense reflections	0.1433
Weighted residual factors for all reflections included in the refinement	0.1819
Goodness-of-fit parameter for all reflections included in the refinement	0.978
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	Yes

Version history

Revision	Date	Message	Files
181194 (current)	2016-04-03	hkl/2/22/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/22/73.	2227325.cif 2227325.hkl
176789	2016-02-20	cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/22.	2227325.cif 2227325.hkl
120072	2014-07-11	Adding DOIs to range 2 structures.	2227325.cif 2227325.hkl
88064	2013-08-29	Adding _cod_database_fobs_code data item to all COD CIFs that have Fobs deposited and did not have this data item yet.	2227325.cif 2227325.hkl
26848	2011-09-28	cif/2/, hkl/2/, html/ Reorganising CIFs of the range 2* into the "prefix-directory" tree.	2227325.cif 2227325.hkl
5269	2010-12-22	hkl/ Adding Fobs data for the recent IUCr-published structres.	2227325.cif 2227325.hkl
4362	2010-12-17	../uploads/cif-deposit/cod/cif Adding structures of 2227325 via cif-deposit CGI script.	2227325.cif