#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/73/2227353.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227353_Fobs loop_ _publ_author_name 'Eshtiagh-Hosseini, Hossein' 'Alfi, Nafiseh' 'Mirzaei, Masoud' 'Fanwick, Philip' 'Fanwick, Phillip E.' _publ_section_title ; Di-\m-hydroxido-bis[aqua(pyridine-2,6-dicarboxylato)iron(III)] monohydrate ; _journal_coeditor_code CV2763 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1450 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.099 _cell_angle_gamma 90.000 _cell_length_a 11.4786 _cell_length_b 21.7080 _cell_length_c 7.3291 _exptl_crystal_F_000 682.00 _reflns_d_resolution_high 0.8633 _[local]_cod_data_source_file cv2763Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' xl in P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 208.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 113.68 137.19 3.49 o 2 0 0 29322.98 36922.91 641.08 o 3 0 0 273.79 357.86 7.59 o 4 0 0 702.83 1171.29 22.04 o 5 0 0 545.99 647.34 18.28 o 6 0 0 22390.19 37424.83 802.70 o 7 0 0 8138.51 10252.45 157.71 o 8 0 0 1578.27 1612.63 42.25 o 10 0 0 368.78 268.80 17.07 o 1 1 0 4283.86 5222.01 55.98 o 2 1 0 179.72 204.02 2.81 o 3 1 0 1551.85 1573.87 22.26 o 4 1 0 87.38 98.84 2.01 o 5 1 0 813.97 964.46 13.88 o 6 1 0 2202.61 3549.15 50.56 o 7 1 0 4732.98 6012.46 85.99 o 8 1 0 613.16 722.63 12.52 o 9 1 0 1872.83 1393.86 36.22 o 10 1 0 16.92 27.04 12.93 o 0 2 0 2984.01 2739.55 41.72 o 1 2 0 9.34 10.35 0.34 o 2 2 0 45.35 60.84 1.06 o 3 2 0 207.18 227.27 3.57 o 4 2 0 90.91 120.77 2.54 o 5 2 0 536.71 691.41 11.11 o 6 2 0 1943.00 2357.75 38.04 o 7 2 0 854.50 947.24 14.38 o 8 2 0 758.27 861.83 24.54 o 9 2 0 552.45 426.51 15.74 o 10 2 0 450.58 427.65 25.34 o 1 3 0 3801.17 3955.71 45.82 o 2 3 0 203.99 256.36 2.96 o 3 3 0 24433.53 29230.27 312.69 o 4 3 0 1063.58 1108.56 16.46 o 5 3 0 577.69 575.50 9.07 o 6 3 0 404.55 619.57 8.99 o 7 3 0 3823.18 3211.39 45.55 o 8 3 0 2575.66 2899.95 67.36 o 11 3 0 2343.92 1920.39 67.21 o 0 4 0 34825.85 31013.62 418.06 o 1 4 0 135.51 149.90 1.97 o 2 4 0 13431.83 16093.20 172.05 o 3 4 0 524.06 560.44 6.45 o 4 4 0 3990.54 4157.91 53.10 o 5 4 0 57.21 60.31 1.78 o 6 4 0 464.22 692.06 11.42 o 7 4 0 884.33 1191.66 21.39 o 8 4 0 12848.15 10662.80 232.51 o 10 4 0 45.03 36.72 9.71 o 1 5 0 11556.16 10999.84 118.23 o 2 5 0 122.45 134.80 1.71 o 3 5 0 1558.63 1609.33 17.14 o 4 5 0 383.64 458.53 7.43 o 5 5 0 156.61 169.51 2.92 o 6 5 0 146.30 216.31 6.03 o 7 5 0 1955.38 2491.42 46.69 o 8 5 0 2179.09 1933.78 47.75 o 10 5 0 188.80 165.03 11.68 o 11 5 0 105.40 84.96 16.12 o 0 6 0 535.46 626.32 8.53 o 1 6 0 74.63 72.29 1.10 o 3 6 0 102.01 101.80 1.74 o 4 6 0 96.36 83.60 1.82 o 5 6 0 1021.49 1450.64 19.61 o 6 6 0 862.29 780.66 14.15 o 7 6 0 106.34 104.57 4.97 o 8 6 0 122.69 109.84 7.89 o 9 6 0 35.47 56.36 8.65 o 10 6 0 898.59 1023.03 28.33 o 11 6 0 651.71 589.72 28.33 o 1 7 0 8973.96 8247.81 72.98 o 2 7 0 85.73 92.89 1.56 o 3 7 0 266.36 321.11 4.44 o 4 7 0 164.85 165.48 3.22 o 5 7 0 15984.61 22331.22 276.58 o 6 7 0 14.91 11.42 2.16 o 7 7 0 5440.50 4615.90 83.52 o 8 7 0 2878.19 2471.50 58.41 o 9 7 0 63.59 54.35 10.85 o 10 7 0 328.00 310.60 15.25 o 0 8 0 43624.57 37549.50 507.23 o 1 8 0 134.33 115.76 1.48 o 2 8 0 1545.73 1708.44 19.38 o 3 8 0 2832.25 2767.12 28.75 o 4 8 0 6604.70 7587.96 88.45 o 5 8 0 46.88 54.24 2.58 o 6 8 0 188.24 195.45 4.36 o 7 8 0 664.13 607.40 14.26 o 8 8 0 6209.26 5521.92 99.98 o 9 8 0 945.78 783.65 19.00 o 10 8 0 267.60 266.87 13.92 o 1 9 0 1708.34 1598.49 14.15 o 2 9 0 54.89 65.96 1.56 o 3 9 0 2846.47 2603.80 27.31 o 4 9 0 658.57 797.69 10.92 o 5 9 0 37.50 51.39 2.84 o 6 9 0 251.86 236.53 5.99 o 7 9 0 1337.69 1267.06 27.01 o 8 9 0 439.67 388.39 12.06 o 9 9 0 3406.84 3272.95 74.23 o 10 9 0 2040.37 1949.48 46.96 o 11 9 0 840.61 906.62 25.98 o 0 10 0 681.00 517.62 6.90 o 1 10 0 481.02 478.86 4.82 o 2 10 0 619.67 623.59 7.43 o 3 10 0 220.14 240.17 3.94 o 4 10 0 1386.69 2041.77 27.16 o 5 10 0 115.69 108.71 3.72 o 6 10 0 55.76 55.72 4.32 o 7 10 0 618.46 572.58 15.89 o 8 10 0 5718.15 5127.08 94.06 o 9 10 0 282.86 288.53 12.29 o 10 10 0 856.98 993.67 38.01 o 11 10 0 31.76 58.37 15.59 o 1 11 0 33268.34 30218.13 275.71 o 2 11 0 78.56 75.78 1.90 o 3 11 0 13465.90 15781.72 214.41 o 4 11 0 241.23 208.84 3.57 o 5 11 0 182.22 254.73 6.49 o 6 11 0 1034.50 896.68 19.38 o 7 11 0 16021.21 14362.15 309.46 o 8 11 0 1473.63 1348.23 33.57 o 9 11 0 902.56 883.56 25.34 o 10 11 0 23.15 60.12 13.31 o 11 11 0 443.72 573.64 21.09 o 1 12 0 419.34 377.58 5.16 o 2 12 0 2596.75 2562.87 27.61 o 3 12 0 1388.46 1433.23 17.30 o 4 12 0 5457.57 4907.88 62.62 o 5 12 0 46.78 40.39 3.94 o 6 12 0 1324.66 1044.87 27.88 o 7 12 0 3888.63 3326.46 74.00 o 8 12 0 878.96 792.57 23.78 o 9 12 0 49.88 66.03 11.34 o 10 12 0 27.53 13.62 10.89 o 11 12 0 491.36 582.63 19.08 o 1 13 0 3334.19 2905.26 31.29 o 2 13 0 140.81 127.14 2.77 o 3 13 0 1807.15 1642.45 18.77 o 4 13 0 7.21 0.46 2.69 o 5 13 0 1285.73 1224.88 22.64 o 6 13 0 35.33 32.62 6.33 o 7 13 0 29.05 39.52 8.04 o 8 13 0 88.06 91.07 10.01 o 9 13 0 1582.19 1656.10 40.43 o 10 13 0 66.69 74.53 11.08 o 11 13 0 17.20 51.70 10.35 o 0 14 0 3040.80 2696.39 51.36 o 1 14 0 79.15 59.59 2.31 o 2 14 0 1179.90 948.19 13.20 o 3 14 0 4.89 8.08 2.77 o 4 14 0 2429.60 2372.24 45.40 o 5 14 0 150.44 143.79 6.56 o 6 14 0 915.23 819.31 19.72 o 7 14 0 1110.15 825.34 26.13 o 8 14 0 1028.40 1027.24 28.60 o 9 14 0 114.25 155.70 10.96 o 10 14 0 12.53 22.68 10.51 o 11 14 0 446.17 542.58 17.30 o 1 15 0 9718.53 8081.64 125.09 o 2 15 0 209.43 182.10 3.83 o 3 15 0 433.78 379.82 7.51 o 4 15 0 1821.37 1699.87 34.78 o 5 15 0 1014.32 819.08 24.05 o 6 15 0 262.84 244.61 14.98 o 7 15 0 4576.42 3589.39 83.06 o 8 15 0 2156.00 2173.00 51.32 o 9 15 0 3595.71 3965.53 73.58 o 10 15 0 198.95 187.26 9.79 o 0 16 0 4094.88 3479.39 79.73 o 1 16 0 50.15 39.67 4.40 o 2 16 0 31.80 36.30 5.50 o 3 16 0 30.16 32.32 4.25 o 4 16 0 1464.51 1301.12 21.16 o 5 16 0 20.59 17.64 6.41 o 6 16 0 97.47 100.17 7.36 o 7 16 0 755.84 726.38 19.04 o 8 16 0 6606.79 7297.50 132.15 o 9 16 0 983.38 1163.82 28.56 o 10 16 0 99.97 100.78 8.50 o 1 17 0 3458.21 3092.21 51.20 o 2 17 0 17.91 19.72 5.58 o 3 17 0 677.86 607.59 12.29 o 4 17 0 70.46 63.53 6.60 o 5 17 0 281.16 246.65 11.83 o 6 17 0 123.33 120.88 9.56 o 7 17 0 48.18 70.02 8.04 o 8 17 0 829.74 912.96 24.88 o 9 17 0 53.69 63.83 8.84 o 0 18 0 7314.70 6385.41 142.58 o 1 18 0 1042.08 906.55 18.81 o 2 18 0 1760.57 1642.79 30.87 o 3 18 0 387.89 335.10 9.44 o 4 18 0 431.67 402.73 10.62 o 5 18 0 1150.52 1194.54 25.64 o 6 18 0 28.47 36.75 7.70 o 8 18 0 1372.08 1658.04 33.83 o 9 18 0 17.86 13.84 7.70 o 1 19 0 5894.84 5245.60 84.92 o 2 19 0 472.30 439.37 12.78 o 3 19 0 411.43 414.07 10.43 o 4 19 0 163.59 140.57 9.71 o 5 19 0 3197.36 3198.76 73.32 o 6 19 0 24.23 17.94 6.64 o 7 19 0 3651.23 4619.09 104.68 o 8 19 0 1242.97 1387.71 30.08 o 0 20 0 1007.72 818.44 25.45 o 1 20 0 1271.61 1108.21 22.11 o 2 20 0 189.33 141.63 8.04 o 3 20 0 1632.93 1418.32 27.27 o 4 20 0 5773.86 5122.37 120.39 o 5 20 0 25.81 30.57 8.91 o 6 20 0 170.19 159.23 7.17 o 7 20 0 893.30 890.65 21.01 o 8 20 0 2456.36 3323.01 77.30 o 1 21 0 77.15 64.63 8.76 o 2 21 0 5.10 6.07 6.60 o 3 21 0 499.42 411.87 12.10 o 4 21 0 68.37 58.18 9.94 o 5 21 0 7.39 9.10 9.18 o 6 21 0 237.09 227.50 11.30 o 7 21 0 1.33 -1.97 3.00 o 0 22 0 2276.34 2325.44 59.44 o 1 22 0 43.76 49.12 9.67 o 2 22 0 47.34 40.09 7.32 o 3 22 0 32.92 32.28 6.26 o 4 22 0 4062.76 3729.84 88.07 o 5 22 0 15.24 40.28 10.85 o 6 22 0 1370.81 1334.77 29.51 o 1 23 0 4905.78 4926.13 80.30 o 2 23 0 20.61 25.87 6.33 o 3 23 0 4206.50 3868.66 73.05 o 4 23 0 949.15 847.68 27.46 o 5 23 0 316.94 340.87 13.43 o 0 24 0 3735.69 4150.70 97.63 o 1 24 0 15.42 26.13 6.60 o 2 24 0 73.97 50.90 6.52 o 3 24 0 124.23 97.17 11.91 o 1 25 0 13.26 4.55 4.93 o -9 1 1 80.98 106.20 8.12 o -8 1 1 662.09 829.51 16.69 o -7 1 1 4987.42 6050.12 60.00 o -6 1 1 708.99 921.91 9.94 o -5 1 1 21713.22 31610.63 303.13 o -4 1 1 921.73 1289.36 13.35 o -3 1 1 10120.13 14416.88 147.13 o -2 1 1 87.10 98.62 1.37 o -1 1 1 4307.82 5161.44 52.49 o 0 1 1 44.77 51.51 0.72 o 1 1 1 9017.16 9379.47 82.61 o 2 1 1 1169.60 1367.61 14.72 o 3 1 1 251.99 334.35 4.51 o 4 1 1 37.35 47.87 1.33 o 5 1 1 655.37 867.93 13.73 o 6 1 1 353.08 389.80 7.36 o 7 1 1 23845.89 27609.63 592.61 o 8 1 1 2010.17 2304.31 45.02 o 9 1 1 4.98 3.53 6.33 o 10 1 1 861.78 704.91 20.56 o 11 1 1 522.86 500.44 20.37 o -10 2 1 192.91 220.33 19.42 o -9 2 1 250.75 205.31 10.54 o -8 2 1 2861.01 3395.91 76.58 o -7 2 1 506.83 483.07 8.08 o -6 2 1 5391.38 8647.55 89.21 o -5 2 1 1040.78 1335.11 16.65 o -3 2 1 1387.11 1590.48 19.23 o -2 2 1 7016.34 8069.39 100.44 o -1 2 1 8.29 12.93 0.49 o 1 2 1 140.37 154.71 1.82 o 2 2 1 33643.58 29302.41 360.82 o 3 2 1 437.08 479.24 5.73 o 4 2 1 9116.33 10324.43 156.57 o 5 2 1 72.71 70.97 1.78 o 6 2 1 1789.02 1880.72 27.54 o 7 2 1 6823.06 7708.65 137.87 o 8 2 1 4736.86 4433.81 82.72 o 9 2 1 660.95 553.99 14.38 o 10 2 1 1364.66 1114.51 29.47 o 11 2 1 2766.62 2177.86 55.49 o -10 3 1 444.95 469.87 23.21 o -9 3 1 88.88 76.35 7.13 o -8 3 1 89.72 84.89 5.95 o -7 3 1 106.83 126.11 5.12 o -6 3 1 68.28 66.41 2.09 o -5 3 1 2829.39 2513.72 32.73 o -4 3 1 1992.49 2741.41 32.51 o -3 3 1 10219.99 11222.75 140.68 o -2 3 1 527.80 550.96 6.56 o -1 3 1 8300.97 9048.16 87.54 o 0 3 1 134.82 138.52 1.48 o 1 3 1 2138.60 2386.84 19.72 o 2 3 1 421.03 515.53 5.95 o 3 3 1 2189.43 2792.35 35.58 o 4 3 1 1006.23 1064.82 12.36 o 5 3 1 626.80 665.01 10.58 o 6 3 1 84.13 97.17 3.00 o 7 3 1 3461.77 3672.68 70.28 o 8 3 1 2298.22 1684.28 40.70 o 9 3 1 746.23 686.82 15.06 o 10 3 1 585.39 460.88 13.12 o 11 3 1 311.48 314.62 22.76 o -10 4 1 923.66 1078.78 39.67 o -8 4 1 1067.23 924.64 21.05 o -7 4 1 6.77 9.94 3.07 o -6 4 1 435.31 496.53 8.31 o -5 4 1 26.31 32.01 0.95 o -4 4 1 1916.57 2692.29 34.36 o -3 4 1 4.58 6.33 0.80 o -2 4 1 10376.42 11995.18 148.87 o -1 4 1 54.80 60.35 0.91 o 0 4 1 737.83 784.00 6.90 o 1 4 1 16.02 16.39 0.57 o 2 4 1 2278.94 2166.55 23.78 o 3 4 1 44.83 39.03 0.95 o 4 4 1 413.82 456.29 5.54 o 5 4 1 208.39 203.87 3.68 o 6 4 1 1407.43 1304.54 20.14 o 7 4 1 44.12 44.79 3.64 o 8 4 1 68.96 58.98 6.75 o 9 4 1 443.48 384.45 10.39 o 10 4 1 33.92 32.39 9.25 o -10 5 1 271.74 237.13 13.20 o -8 5 1 958.58 854.28 24.77 o -7 5 1 2651.43 2365.38 45.06 o -6 5 1 54.37 48.66 2.12 o -5 5 1 8001.77 10498.30 121.75 o -4 5 1 1414.38 1356.04 19.72 o -2 5 1 85.04 88.87 1.59 o -1 5 1 20389.41 19161.93 167.61 o 0 5 1 189.08 200.83 2.12 o 1 5 1 4725.32 5349.45 43.81 o 2 5 1 31.14 28.60 0.83 o 3 5 1 1835.52 2063.35 24.43 o 4 5 1 65.87 65.20 1.52 o 5 5 1 4595.11 4063.58 63.49 o 6 5 1 328.79 276.50 5.80 o 7 5 1 12319.65 12497.81 270.21 o 8 5 1 5003.56 3997.92 89.40 o 9 5 1 2151.11 1729.68 44.42 o 10 5 1 55.86 40.51 12.29 o -11 6 1 2484.71 3138.87 102.75 o -10 6 1 5.79 31.14 11.49 o -9 6 1 114.23 112.61 10.51 o -8 6 1 8617.93 6839.35 151.98 o -7 6 1 2795.19 2569.06 48.02 o -6 6 1 84.38 102.52 3.30 o -5 6 1 3315.57 4157.00 58.71 o -4 6 1 18799.04 17094.37 211.80 o -3 6 1 209.13 267.14 3.64 o -2 6 1 8278.05 8991.57 82.88 o -1 6 1 44.89 50.33 0.95 o 0 6 1 19252.56 21001.57 170.00 o 1 6 1 128.41 157.90 1.86 o 2 6 1 66.40 73.24 1.29 o 3 6 1 284.68 350.66 4.02 o 4 6 1 589.60 714.55 8.72 o 5 6 1 1335.42 1363.55 18.32 o 6 6 1 393.30 320.35 8.23 o 7 6 1 8955.10 7859.49 140.30 o 8 6 1 13299.83 12269.33 264.63 o 9 6 1 1958.70 1943.68 46.54 o 10 6 1 220.76 259.32 13.12 o -11 7 1 609.68 748.87 38.16 o -9 7 1 995.88 932.22 27.84 o -8 7 1 2597.00 2437.71 55.45 o -7 7 1 257.66 255.64 7.62 o -6 7 1 195.52 196.51 4.40 o -5 7 1 1901.32 2245.26 29.93 o -4 7 1 80.89 97.10 2.58 o -3 7 1 4876.49 4327.38 55.15 o -2 7 1 0.69 2.88 0.87 o -1 7 1 14514.26 14216.54 124.90 o 0 7 1 29.08 35.99 0.87 o 1 7 1 249.21 276.35 3.07 o 2 7 1 5.81 6.79 0.87 o 3 7 1 1734.72 2433.31 27.27 o 4 7 1 39.35 45.82 1.29 o 5 7 1 290.41 291.07 6.22 o 6 7 1 24.44 27.16 3.91 o 7 7 1 3265.80 2913.91 47.18 o 8 7 1 2663.29 2461.68 57.16 o 9 7 1 2153.70 2038.09 48.32 o 10 7 1 1398.23 1445.06 31.14 o 11 7 1 2194.98 2155.59 73.32 o 12 7 1 46.26 80.33 19.87 o -11 8 1 488.25 554.15 29.43 o -9 8 1 28.17 9.90 10.01 o -8 8 1 956.49 874.87 19.91 o -7 8 1 358.70 356.19 11.23 o -6 8 1 1762.68 2257.85 41.76 o -5 8 1 813.58 1020.45 13.73 o -4 8 1 981.18 1444.23 19.27 o -3 8 1 868.94 1072.41 14.75 o -2 8 1 18611.78 21926.29 210.24 o -1 8 1 108.44 117.62 1.56 o 0 8 1 1675.24 1751.19 15.13 o 1 8 1 320.03 376.07 3.87 o 2 8 1 857.48 1152.90 12.78 o 3 8 1 325.14 334.12 4.32 o 4 8 1 616.69 619.27 7.43 o 5 8 1 2.71 6.90 2.31 o 6 8 1 7.74 14.53 3.75 o 7 8 1 337.60 293.34 8.88 o 8 8 1 2779.41 2469.68 57.27 o 9 8 1 263.89 265.01 12.33 o 10 8 1 152.67 149.37 11.72 o 11 8 1 774.08 709.62 33.45 o 12 8 1 1166.10 1299.61 49.91 o -11 9 1 2080.88 2476.51 80.98 o -10 9 1 123.18 128.92 12.29 o -9 9 1 101.12 94.18 10.66 o -8 9 1 2340.41 2238.16 51.09 o -7 9 1 11364.40 9861.47 174.78 o -6 9 1 84.90 83.60 3.87 o -5 9 1 5037.26 6061.04 71.88 o -4 9 1 547.37 568.67 8.34 o -3 9 1 6948.94 7362.66 75.48 o -2 9 1 553.99 614.00 5.80 o -1 9 1 35661.14 35458.09 357.82 o 0 9 1 1500.67 1635.13 15.21 o 1 9 1 7944.17 8315.63 90.20 o 2 9 1 34.03 42.03 1.48 o 3 9 1 28877.11 29048.78 310.45 o 4 9 1 792.64 783.39 10.54 o 5 9 1 1105.55 1524.26 28.98 o 6 9 1 183.76 144.32 4.97 o 7 9 1 6454.64 5519.00 85.99 o 8 9 1 5754.61 5383.02 118.87 o 9 9 1 476.60 553.96 17.41 o 10 9 1 2152.48 2307.57 55.11 o 11 9 1 475.48 535.79 29.28 o 12 9 1 899.78 1085.53 46.50 o -10 10 1 60.84 94.52 11.91 o -9 10 1 289.91 280.83 14.03 o -8 10 1 869.33 740.26 18.51 o -7 10 1 2477.71 2134.81 40.96 o -6 10 1 702.95 664.25 11.99 o -5 10 1 1049.67 1154.26 15.48 o -4 10 1 10154.78 11066.90 138.86 o -3 10 1 1307.27 1461.64 18.21 o -2 10 1 54.88 44.30 1.67 o -1 10 1 16.84 17.94 0.99 o 1 10 1 22.80 32.39 1.14 o 2 10 1 2781.34 3412.45 40.89 o 3 10 1 1107.32 1235.28 15.66 o 4 10 1 3195.76 2859.18 32.28 o 5 10 1 1001.51 1239.90 21.05 o 6 10 1 1806.88 1403.46 28.18 o 7 10 1 4596.88 4208.39 77.41 o 8 10 1 9508.16 8835.03 192.53 o 9 10 1 210.66 257.20 12.18 o 10 10 1 427.73 460.46 16.01 o 11 10 1 288.50 333.36 25.00 o 12 10 1 119.68 107.04 25.03 o -11 11 1 48.73 41.91 11.26 o -10 11 1 76.22 93.99 13.20 o -9 11 1 117.89 131.65 15.63 o -8 11 1 133.88 98.92 8.57 o -7 11 1 2263.88 1930.41 37.93 o -6 11 1 652.85 521.49 13.58 o -5 11 1 3005.74 3234.41 52.99 o -4 11 1 115.76 111.40 2.96 o -3 11 1 3417.64 3865.06 43.05 o -2 11 1 11.28 9.56 1.52 o -1 11 1 6040.89 6235.52 58.45 o 0 11 1 11.15 11.68 1.18 o 1 11 1 156.37 123.42 1.90 o 2 11 1 4.23 4.44 1.52 o 3 11 1 238.81 338.21 4.36 o 4 11 1 176.05 163.89 3.38 o 5 11 1 55.52 57.99 3.53 o 6 11 1 197.34 177.36 7.05 o 7 11 1 3507.10 3120.89 58.18 o 8 11 1 902.73 913.94 25.79 o 9 11 1 41.00 40.85 9.79 o 10 11 1 315.20 340.87 14.34 o 11 11 1 495.84 550.96 30.76 o -11 12 1 1213.83 1385.17 34.44 o -9 12 1 49.91 25.18 10.28 o -8 12 1 69.48 56.29 8.69 o -7 12 1 279.08 251.02 9.63 o -6 12 1 174.48 154.83 8.65 o -5 12 1 2182.38 1833.61 35.84 o -4 12 1 3601.67 3624.32 43.92 o -3 12 1 6.19 7.28 2.12 o -2 12 1 2897.38 3561.21 37.66 o -1 12 1 195.88 213.58 3.41 o 0 12 1 10643.64 10603.06 103.02 o 1 12 1 338.82 323.04 3.98 o 2 12 1 3827.38 3805.66 37.82 o 3 12 1 167.29 166.24 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