#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/75/2227501.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227501_Fobs loop_ _publ_author_name 'Zeng, Wu-Lan' _publ_section_title ; 5-(4-Hydroxybenzylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione ; _journal_coeditor_code HB5605 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2319 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.472 _cell_angle_gamma 90.000 _cell_length_a 13.9001 _cell_length_b 10.2486 _cell_length_c 8.1357 _exptl_crystal_F_000 520.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file hb5605Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wf1046 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 125.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 2096.12 2166.93 86.74 o 4 0 0 35.89 8.21 0.16 o 5 0 0 1096.37 1163.56 26.71 o 6 0 0 179.09 205.17 5.37 o 7 0 0 754.55 828.70 14.50 o 8 0 0 283.52 293.51 3.98 o 9 0 0 468.42 484.24 7.56 o 10 0 0 195.71 188.68 3.08 o 11 0 0 979.29 970.63 24.04 o 12 0 0 332.87 314.97 5.99 o 13 0 0 4.97 5.11 0.64 o 14 0 0 104.14 86.57 1.96 o 15 0 0 20.44 24.69 1.39 o 16 0 0 41.27 39.75 1.00 o 17 0 0 31.31 35.47 0.74 o 2 1 0 859.26 907.99 15.25 o 3 1 0 566.76 611.42 7.04 o 4 1 0 400.57 370.90 14.89 o 5 1 0 2.31 7.17 0.21 o 6 1 0 94.36 84.14 1.02 o 7 1 0 1658.99 1895.32 44.54 o 8 1 0 2.63 5.90 0.28 o 9 1 0 128.30 118.39 1.29 o 10 1 0 0.28 0.40 0.10 o 11 1 0 543.63 528.51 7.13 o 12 1 0 115.54 102.81 3.07 o 13 1 0 92.86 94.59 1.77 o 14 1 0 104.68 103.62 1.23 o 15 1 0 3.51 2.88 0.39 o 16 1 0 4.43 5.27 0.28 o 17 1 0 3.56 5.35 0.29 o 0 2 0 13898.21 7695.26 381.13 o 1 2 0 430.86 401.59 4.79 o 2 2 0 17.06 17.88 0.68 o 3 2 0 411.05 421.58 5.37 o 4 2 0 1345.58 1362.22 45.82 o 5 2 0 895.32 992.68 12.86 o 6 2 0 2679.95 3031.81 54.68 o 7 2 0 714.52 773.06 10.56 o 8 2 0 2.75 5.63 0.36 o 9 2 0 138.52 134.40 1.57 o 10 2 0 182.50 181.16 2.31 o 11 2 0 143.08 135.25 1.55 o 12 2 0 6.12 7.41 0.27 o 13 2 0 84.75 78.77 0.95 o 14 2 0 229.93 216.58 2.80 o 15 2 0 0.51 0.15 0.15 o 16 2 0 51.37 51.77 0.73 o 17 2 0 21.33 22.41 0.56 o 1 3 0 73.04 79.91 0.79 o 2 3 0 147.63 155.35 1.62 o 3 3 0 263.38 231.19 2.25 o 4 3 0 86.07 91.78 0.83 o 5 3 0 1726.79 2026.82 34.15 o 6 3 0 3.32 2.78 0.19 o 7 3 0 11.20 14.35 0.50 o 8 3 0 350.63 377.60 3.92 o 9 3 0 12.01 9.17 0.23 o 10 3 0 98.79 101.44 1.16 o 11 3 0 0.01 0.58 0.35 o 12 3 0 10.39 11.96 0.33 o 13 3 0 180.13 172.45 1.91 o 14 3 0 25.87 27.53 0.52 o 15 3 0 0.52 0.79 0.23 o 16 3 0 2.39 3.02 0.19 o 17 3 0 0.62 0.65 0.24 o 0 4 0 2.55 4.55 0.25 o 1 4 0 6.30 4.85 0.19 o 2 4 0 297.95 267.43 2.88 o 3 4 0 1182.59 1282.40 22.84 o 4 4 0 234.85 253.29 6.36 o 5 4 0 9.24 20.62 0.42 o 6 4 0 13.83 12.33 0.37 o 7 4 0 99.21 105.46 1.17 o 8 4 0 27.86 27.58 0.31 o 9 4 0 13.82 14.57 0.42 o 10 4 0 40.58 36.47 0.44 o 11 4 0 246.70 230.94 3.18 o 12 4 0 27.00 21.49 0.48 o 13 4 0 125.27 119.62 1.58 o 14 4 0 18.24 19.52 0.39 o 15 4 0 0.77 1.12 0.18 o 16 4 0 35.65 36.55 1.09 o 17 4 0 5.10 3.69 0.57 o 1 5 0 21.11 21.45 0.42 o 2 5 0 55.95 54.93 0.69 o 3 5 0 68.70 80.20 0.94 o 4 5 0 81.73 74.79 0.97 o 5 5 0 570.93 578.83 8.57 o 6 5 0 0.71 1.33 0.14 o 7 5 0 131.57 147.30 1.50 o 8 5 0 0.24 0.82 0.13 o 9 5 0 5.37 6.25 0.19 o 10 5 0 6.36 5.74 0.20 o 11 5 0 417.27 395.18 4.70 o 12 5 0 33.30 33.18 0.58 o 13 5 0 13.93 13.10 0.35 o 14 5 0 2.02 3.56 0.53 o 15 5 0 0.22 0.50 0.47 o 16 5 0 3.51 2.14 1.67 o 0 6 0 13.86 12.48 0.39 o 1 6 0 291.60 311.42 3.42 o 2 6 0 107.97 105.58 1.25 o 3 6 0 577.80 597.24 8.38 o 4 6 0 88.60 82.60 1.03 o 5 6 0 14.75 13.43 0.54 o 6 6 0 249.50 247.68 3.28 o 7 6 0 58.02 57.98 0.89 o 8 6 0 7.24 6.80 0.30 o 9 6 0 8.45 7.77 0.42 o 10 6 0 8.11 9.56 0.32 o 11 6 0 312.06 294.14 3.70 o 12 6 0 65.97 64.09 1.03 o 13 6 0 0.56 1.02 0.28 o 14 6 0 0.38 0.82 0.55 o 15 6 0 0.52 1.13 0.57 o 16 6 0 4.68 4.29 0.91 o 1 7 0 9.95 12.62 0.36 o 2 7 0 161.78 144.45 1.81 o 3 7 0 916.84 953.87 15.23 o 4 7 0 173.27 187.21 2.35 o 5 7 0 27.85 24.70 0.58 o 6 7 0 41.63 38.51 0.77 o 7 7 0 6.95 7.55 0.35 o 8 7 0 0.38 1.20 0.28 o 9 7 0 34.99 35.44 0.80 o 10 7 0 35.13 34.76 0.62 o 11 7 0 141.92 128.79 2.25 o 12 7 0 7.30 7.33 0.24 o 13 7 0 25.46 23.36 1.20 o 14 7 0 1.90 2.89 0.74 o 15 7 0 10.87 14.47 1.42 o 0 8 0 6.40 8.38 0.93 o 1 8 0 148.35 148.39 1.78 o 2 8 0 64.98 69.77 0.99 o 3 8 0 12.31 12.33 0.38 o 4 8 0 4.15 5.15 0.28 o 5 8 0 16.50 18.35 0.51 o 6 8 0 46.48 47.70 1.00 o 7 8 0 129.79 128.29 2.07 o 8 8 0 94.49 96.84 1.46 o 9 8 0 91.61 95.52 1.45 o 10 8 0 249.50 244.26 3.47 o 11 8 0 4.83 5.73 0.41 o 12 8 0 17.08 15.39 0.57 o 13 8 0 28.29 31.94 1.58 o 14 8 0 9.72 11.39 1.90 o 1 9 0 48.49 50.56 0.85 o 2 9 0 523.68 541.69 7.55 o 3 9 0 68.15 64.55 1.07 o 4 9 0 12.09 12.24 0.39 o 5 9 0 0.37 0.37 0.22 o 6 9 0 16.25 18.15 0.54 o 7 9 0 40.25 41.50 1.27 o 8 9 0 5.57 6.74 0.44 o 9 9 0 79.54 78.42 1.74 o 10 9 0 49.25 50.56 1.03 o 11 9 0 59.23 56.47 1.10 o 12 9 0 9.66 9.16 1.09 o 13 9 0 2.91 3.91 0.92 o 0 10 0 143.56 157.83 3.04 o 1 10 0 285.79 296.10 4.26 o 2 10 0 1.79 2.31 0.32 o 3 10 0 5.33 5.82 0.36 o 4 10 0 46.60 45.20 0.93 o 5 10 0 13.86 13.41 0.53 o 6 10 0 10.25 11.68 0.66 o 7 10 0 3.12 4.18 0.26 o 8 10 0 9.66 10.54 1.21 o 9 10 0 37.39 34.75 0.81 o 10 10 0 4.47 4.91 0.40 o 11 10 0 8.06 7.51 1.14 o 1 11 0 17.66 17.24 0.58 o 2 11 0 0.00 0.03 0.24 o 3 11 0 30.37 26.62 0.72 o 4 11 0 29.51 34.03 0.86 o 5 11 0 7.19 6.30 0.42 o 6 11 0 15.56 16.57 0.47 o 7 11 0 14.81 13.92 0.75 o 8 11 0 6.87 5.18 0.50 o 9 11 0 8.06 7.41 0.43 o 10 11 0 1.56 1.64 0.49 o 0 12 0 19.18 19.49 1.01 o 1 12 0 1.04 0.73 0.34 o 2 12 0 0.04 0.28 0.37 o 3 12 0 14.02 13.85 0.61 o 4 12 0 0.46 0.63 0.27 o 5 12 0 2.26 1.87 0.33 o 6 12 0 37.46 38.12 1.05 o 7 12 0 0.30 0.47 0.37 o 1 13 0 19.78 21.80 0.79 o 2 13 0 4.10 2.89 0.40 o 3 13 0 20.94 19.62 0.66 o -17 1 1 0.04 0.00 0.14 o -16 1 1 7.39 5.22 0.62 o -15 1 1 26.73 21.35 0.61 o -14 1 1 214.14 233.52 2.62 o -13 1 1 72.21 66.35 0.95 o -12 1 1 1321.52 1286.85 20.37 o -11 1 1 481.67 496.72 6.51 o -10 1 1 25.63 24.17 0.41 o -9 1 1 43.81 41.03 1.05 o -8 1 1 602.10 660.62 7.17 o -7 1 1 963.30 1079.37 13.43 o -6 1 1 912.39 1049.14 11.90 o -5 1 1 6.05 5.60 0.24 o -4 1 1 949.18 981.30 14.57 o -3 1 1 1168.54 1226.03 37.82 o -2 1 1 2400.17 2136.45 60.94 o -1 1 1 2582.08 2349.88 69.39 o 0 1 1 910.87 902.69 15.10 o 1 1 1 2826.16 2824.99 63.49 o 2 1 1 9928.92 8758.73 313.41 o 3 1 1 2.06 4.24 0.12 o 4 1 1 1880.88 1977.94 31.65 o 5 1 1 0.21 0.76 0.13 o 6 1 1 897.29 1146.56 14.40 o 7 1 1 1533.16 1801.80 28.91 o 8 1 1 1515.79 1828.61 29.95 o 9 1 1 14.51 16.98 0.33 o 10 1 1 12.86 6.51 0.17 o 11 1 1 0.74 1.27 0.22 o 12 1 1 32.35 30.51 0.52 o 13 1 1 31.42 33.62 0.56 o 14 1 1 16.38 12.60 0.28 o 15 1 1 7.75 6.22 0.35 o 16 1 1 23.76 24.87 0.39 o 17 1 1 20.29 24.40 0.60 o -17 2 1 21.33 24.41 0.68 o -16 2 1 1.86 3.23 0.39 o -15 2 1 6.98 5.24 0.25 o -14 2 1 35.31 30.74 0.55 o -13 2 1 0.12 0.36 0.13 o -12 2 1 168.78 156.97 1.97 o -11 2 1 53.45 47.93 0.64 o -10 2 1 397.18 384.22 4.76 o -9 2 1 360.35 363.31 4.67 o -8 2 1 0.00 0.18 0.07 o -7 2 1 149.29 155.48 1.47 o -6 2 1 699.96 757.52 42.00 o -5 2 1 513.27 475.74 15.86 o -4 2 1 37.01 39.69 0.34 o -3 2 1 311.26 294.81 3.31 o -2 2 1 736.74 700.76 10.89 o -1 2 1 1831.54 1826.70 30.50 o 0 2 1 7454.31 6085.85 243.68 o 1 2 1 9799.47 7318.13 523.01 o 2 2 1 3470.03 3591.35 73.08 o 3 2 1 291.19 288.12 6.77 o 4 2 1 758.37 836.28 10.45 o 5 2 1 2.44 3.94 0.13 o 6 2 1 760.79 854.05 11.74 o 7 2 1 767.92 839.62 22.01 o 8 2 1 87.80 98.34 1.30 o 9 2 1 31.45 33.22 0.34 o 10 2 1 83.28 75.84 0.73 o 11 2 1 1742.89 1898.08 33.30 o 12 2 1 31.48 27.07 0.63 o 13 2 1 107.49 84.26 1.56 o 14 2 1 15.40 13.82 0.44 o 15 2 1 0.76 0.79 0.13 o 16 2 1 0.62 0.18 0.29 o 17 2 1 1.28 0.29 0.30 o -17 3 1 0.00 0.06 0.20 o -16 3 1 0.33 0.04 0.15 o -15 3 1 32.48 25.54 0.41 o -14 3 1 7.06 8.91 0.31 o -13 3 1 0.03 0.23 0.22 o -12 3 1 296.29 286.43 3.97 o -11 3 1 118.26 107.85 1.60 o -10 3 1 551.96 537.34 7.66 o -9 3 1 30.75 32.31 0.45 o -8 3 1 1.52 1.16 0.12 o -7 3 1 58.87 54.31 0.54 o -6 3 1 296.38 313.68 12.84 o -5 3 1 1.90 2.58 0.29 o -4 3 1 108.27 102.04 1.00 o -3 3 1 1506.87 1596.12 24.23 o -2 3 1 97.04 90.04 1.25 o -1 3 1 95.33 84.72 0.70 o 0 3 1 15705.15 12034.28 408.11 o 1 3 1 1440.90 1530.08 25.51 o 2 3 1 1270.90 1390.20 20.13 o 3 3 1 362.78 365.43 6.38 o 4 3 1 286.48 300.26 4.27 o 5 3 1 9.25 5.20 0.19 o 6 3 1 489.27 497.23 9.99 o 7 3 1 631.25 674.06 11.74 o 8 3 1 72.66 73.62 0.79 o 9 3 1 443.03 439.08 10.32 o 10 3 1 288.98 260.80 2.95 o 11 3 1 135.12 130.83 1.66 o 12 3 1 447.42 421.27 5.41 o 13 3 1 31.02 30.87 1.08 o 14 3 1 1.23 0.12 0.14 o 15 3 1 101.73 93.08 1.83 o 16 3 1 7.48 9.90 0.73 o 17 3 1 11.76 12.24 0.77 o -17 4 1 36.91 44.88 1.82 o -16 4 1 56.49 61.43 0.99 o -15 4 1 3.05 2.51 0.52 o -14 4 1 13.34 14.70 0.58 o -13 4 1 3.69 3.45 0.25 o -12 4 1 147.44 135.11 2.08 o -11 4 1 211.45 219.29 2.80 o -10 4 1 91.12 91.64 1.11 o -9 4 1 16.05 16.07 0.32 o -8 4 1 60.32 53.61 0.93 o -7 4 1 441.76 473.26 20.46 o -6 4 1 980.69 1086.80 16.10 o -5 4 1 55.51 50.16 0.75 o -4 4 1 426.32 403.21 6.55 o -3 4 1 1109.36 1200.45 17.09 o -2 4 1 952.55 1002.71 15.38 o -1 4 1 295.22 279.93 3.01 o 0 4 1 729.59 819.58 10.21 o 1 4 1 92.71 95.10 1.07 o 2 4 1 1627.62 1736.11 31.11 o 3 4 1 1423.65 1619.95 25.60 o 4 4 1 217.89 239.26 2.38 o 5 4 1 576.77 637.46 12.28 o 6 4 1 299.19 294.48 3.10 o 7 4 1 235.62 223.84 2.27 o 8 4 1 107.67 114.36 1.15 o 9 4 1 3.73 2.74 0.18 o 10 4 1 133.69 130.00 1.54 o 11 4 1 81.02 74.37 0.87 o 12 4 1 30.09 30.87 0.88 o 13 4 1 57.00 47.03 0.71 o 14 4 1 3.87 4.54 0.34 o 15 4 1 3.52 1.65 0.32 o 16 4 1 8.38 7.77 0.39 o -16 5 1 5.00 3.47 1.15 o -15 5 1 38.77 38.87 0.89 o -14 5 1 10.38 10.68 0.53 o -13 5 1 43.07 42.94 0.66 o -12 5 1 23.87 23.54 1.11 o -11 5 1 370.58 359.37 5.23 o -10 5 1 441.33 431.70 6.16 o -9 5 1 807.35 837.49 29.66 o -8 5 1 0.94 0.63 0.18 o -7 5 1 34.07 36.39 0.39 o -6 5 1 476.31 453.75 5.86 o -5 5 1 393.30 428.11 5.26 o -4 5 1 257.45 282.33 2.87 o -3 5 1 84.99 84.59 0.83 o -2 5 1 101.63 105.74 1.20 o -1 5 1 282.36 238.62 2.76 o 0 5 1 224.06 241.51 2.73 o 1 5 1 2.37 0.95 0.22 o 2 5 1 283.26 314.34 3.69 o 3 5 1 1032.45 1101.01 17.50 o 4 5 1 199.92 214.11 2.21 o 5 5 1 2.09 0.41 0.18 o 6 5 1 166.35 193.71 1.98 o 7 5 1 128.57 118.20 1.22 o 8 5 1 61.45 61.08 0.70 o 9 5 1 46.20 42.23 0.47 o 10 5 1 12.64 10.26 0.30 o 11 5 1 36.18 34.42 0.47 o 12 5 1 9.42 6.16 0.21 o 13 5 1 47.23 38.13 0.75 o 14 5 1 78.39 80.15 1.47 o 15 5 1 91.69 86.45 1.59 o 16 5 1 0.07 -0.02 0.58 o -16 6 1 1.55 1.25 0.68 o -15 6 1 1.21 0.75 0.36 o -14 6 1 7.93 7.81 0.52 o -13 6 1 0.43 0.92 0.23 o -12 6 1 44.93 43.49 0.80 o -11 6 1 131.29 129.47 4.16 o -10 6 1 96.83 91.88 2.27 o -9 6 1 0.22 0.38 0.09 o -8 6 1 45.34 46.58 0.69 o -7 6 1 50.51 52.59 0.55 o -6 6 1 21.42 28.59 0.41 o -5 6 1 245.50 263.18 2.83 o -4 6 1 112.61 128.84 1.35 o -3 6 1 1.40 3.14 0.49 o -2 6 1 971.89 1061.34 15.37 o -1 6 1 609.46 651.24 9.97 o 0 6 1 315.87 321.59 5.12 o 1 6 1 13.44 14.59 0.35 o 2 6 1 425.83 437.03 5.75 o 3 6 1 104.95 120.02 2.90 o 4 6 1 445.99 450.44 5.84 o 5 6 1 132.21 132.83 1.42 o 6 6 1 65.65 67.33 0.77 o 7 6 1 59.84 55.79 0.74 o 8 6 1 1.38 0.75 0.12 o 9 6 1 7.51 5.61 0.37 o 10 6 1 36.98 34.59 0.59 o 11 6 1 59.22 51.10 1.47 o 12 6 1 17.69 16.25 0.54 o 13 6 1 35.51 36.90 0.78 o 14 6 1 34.17 36.25 1.19 o 15 6 1 11.85 15.32 0.92 o -15 7 1 1.06 0.72 0.79 o -14 7 1 9.87 9.11 0.57 o -13 7 1 20.53 22.89 0.62 o -12 7 1 3.75 4.62 0.32 o -11 7 1 64.05 66.51 1.25 o -10 7 1 7.20 6.04 0.45 o -9 7 1 28.31 25.38 0.77 o -8 7 1 15.93 15.88 0.49 o -7 7 1 29.90 34.73 0.50 o -6 7 1 59.46 60.50 0.75 o -5 7 1 195.62 215.23 2.49 o -4 7 1 0.23 0.24 0.17 o -3 7 1 155.82 158.28 1.76 o -2 7 1 6.51 9.96 0.33 o -1 7 1 216.57 205.78 2.32 o 0 7 1 172.52 169.78 2.06 o 1 7 1 111.50 101.43 1.28 o 2 7 1 42.33 45.05 0.77 o 3 7 1 8.82 9.22 0.35 o 4 7 1 85.75 84.83 1.29 o 5 7 1 41.05 38.72 1.26 o 6 7 1 34.59 38.12 0.65 o 7 7 1 105.20 100.34 2.18 o 8 7 1 9.10 9.58 0.35 o 9 7 1 477.33 462.79 5.93 o 10 7 1 40.22 37.61 0.79 o 11 7 1 29.15 31.67 0.69 o 12 7 1 14.55 14.43 0.41 o 13 7 1 5.94 5.88 0.46 o 14 7 1 33.17 39.48 1.70 o 15 7 1 8.70 10.10 1.30 o -14 8 1 35.15 41.00 1.84 o -13 8 1 4.70 5.62 0.43 o -12 8 1 23.28 22.54 0.60 o -11 8 1 45.60 42.35 0.84 o -10 8 1 28.37 27.13 1.10 o -9 8 1 89.96 79.06 1.65 o -8 8 1 81.35 84.45 1.59 o -7 8 1 8.13 8.23 0.29 o -6 8 1 161.31 159.63 2.17 o -5 8 1 0.01 0.01 0.13 o -4 8 1 69.21 74.22 1.00 o -3 8 1 0.19 0.64 0.35 o -2 8 1 8.01 6.93 0.39 o -1 8 1 460.18 479.10 6.42 o 0 8 1 251.61 243.13 2.97 o 1 8 1 4.50 5.08 0.41 o 2 8 1 136.99 142.94 2.00 o 3 8 1 59.36 64.68 1.13 o 4 8 1 146.26 144.17 2.02 o 5 8 1 269.19 263.67 4.21 o 6 8 1 21.61 21.12 0.52 o 7 8 1 51.19 53.77 0.87 o 8 8 1 49.52 41.71 0.80 o 9 8 1 7.13 4.74 0.34 o 10 8 1 0.06 0.15 0.23 o 11 8 1 32.20 30.55 1.73 o 12 8 1 0.23 0.01 0.24 o 13 8 1 16.46 19.12 1.52 o 14 8 1 0.96 0.57 0.78 o -13 9 1 15.59 13.91 1.28 o -12 9 1 18.74 19.20 0.67 o -11 9 1 3.50 3.84 0.84 o -10 9 1 65.44 67.67 1.56 o -9 9 1 25.50 27.94 0.83 o -8 9 1 30.37 27.14 0.91 o -7 9 1 7.93 6.84 0.31 o -6 9 1 28.68 28.90 0.61 o -5 9 1 6.52 7.86 0.38 o -4 9 1 63.78 62.63 1.10 o -3 9 1 3.40 2.88 0.27 o -2 9 1 0.45 0.64 0.24 o -1 9 1 0.15 1.48 0.53 o 0 9 1 15.51 18.19 0.63 o 1 9 1 40.40 36.35 0.70 o 2 9 1 49.40 55.33 2.84 o 3 9 1 36.11 36.55 0.88 o 4 9 1 6.58 8.98 0.47 o 5 9 1 66.60 63.57 1.32 o 6 9 1 25.88 28.10 0.91 o 7 9 1 66.56 64.84 1.25 o 8 9 1 4.56 3.63 0.38 o 9 9 1 14.93 11.95 0.50 o 10 9 1 3.69 4.21 0.56 o 11 9 1 12.59 13.55 1.76 o 12 9 1 0.15 0.36 0.51 o 13 9 1 5.04 5.64 1.27 o -11 10 1 5.68 6.72 0.42 o -10 10 1 8.17 8.67 1.84 o -9 10 1 109.35 113.68 2.07 o -8 10 1 0.65 0.31 0.29 o -7 10 1 89.79 89.53 2.01 o -6 10 1 13.67 12.49 0.49 o -5 10 1 27.78 27.81 0.59 o -4 10 1 5.63 5.81 0.31 o -3 10 1 11.78 11.59 0.42 o -2 10 1 0.76 0.81 0.30 o -1 10 1 22.14 22.41 0.70 o 0 10 1 28.68 28.94 0.67 o 1 10 1 201.00 210.55 2.87 o 2 10 1 24.33 23.42 0.65 o 3 10 1 75.17 80.52 1.23 o 4 10 1 242.53 243.67 3.37 o 5 10 1 143.82 156.18 2.84 o 6 10 1 12.60 14.16 0.63 o 7 10 1 11.63 11.99 0.46 o 8 10 1 63.50 61.86 1.29 o 9 10 1 24.63 20.31 0.58 o 10 10 1 15.44 16.77 1.16 o 11 10 1 8.65 9.41 1.56 o -10 11 1 1.97 1.27 0.57 o -9 11 1 10.61 10.48 0.55 o -8 11 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