#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/75/2227570.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227570_Fobs loop_ _publ_author_name 'Fejfarov\'a, Karla' 'Khalaji, Aliakbar Dehno' 'Du\E)-N-(2,4-Dimethoxybenzylidene)-4-ethoxyaniline ; _journal_coeditor_code HB5685 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2874 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90 _cell_angle_beta 90.9091(10) _cell_angle_gamma 90 _cell_length_a 8.45360(10) _cell_length_b 9.6531(2) _cell_length_c 18.0561(3) _exptl_crystal_F_000 608 _reflns_d_resolution_high 0.8390 _[local]_cod_data_source_file hb5685Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 175.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1318.71 1364.02 6.38 o 2 0 0 12732.14 12477.87 64.75 o 3 0 0 4396.25 4407.20 20.99 o 4 0 0 43.57 50.52 1.81 o 5 0 0 1898.23 1983.80 6.00 o 6 0 0 1537.71 1471.26 5.72 o 7 0 0 6.33 8.83 0.95 o 8 0 0 3.30 5.75 1.33 o 9 0 0 4.19 5.14 1.11 o 1 1 0 96.32 84.47 1.52 o 2 1 0 301.66 267.74 1.62 o 3 1 0 19.01 15.47 0.64 o 4 1 0 127.62 172.34 1.87 o 5 1 0 550.47 577.67 2.16 o 6 1 0 763.80 803.14 2.48 o 7 1 0 28.17 28.96 0.79 o 8 1 0 23.76 18.26 1.05 o 9 1 0 38.63 40.84 1.21 o 0 2 0 1797.37 2015.37 6.70 o 1 2 0 2845.46 2753.03 6.29 o 2 2 0 105.79 107.18 1.24 o 3 2 0 538.77 599.01 3.78 o 4 2 0 585.40 563.42 2.92 o 5 2 0 63.05 65.20 0.79 o 6 2 0 156.34 165.00 1.27 o 7 2 0 86.31 93.43 1.14 o 8 2 0 0.87 0.89 0.79 < 9 2 0 14.49 12.99 0.92 o 1 3 0 1044.81 1159.95 3.72 o 2 3 0 109.99 119.56 1.49 o 3 3 0 207.89 228.45 2.38 o 4 3 0 793.40 785.45 2.89 o 5 3 0 88.44 91.77 0.95 o 6 3 0 3.47 2.41 0.57 o 7 3 0 21.31 26.52 0.79 o 8 3 0 1.22 1.33 0.67 < 9 3 0 5.27 3.75 0.70 o 0 4 0 9251.24 9917.22 27.06 o 1 4 0 1.02 4.16 0.92 o 2 4 0 61.37 60.75 1.49 o 3 4 0 1113.37 1122.20 3.97 o 4 4 0 190.45 197.08 1.43 o 5 4 0 179.31 177.10 1.43 o 6 4 0 92.65 80.03 1.14 o 7 4 0 48.89 45.70 1.14 o 8 4 0 3.69 2.38 0.73 o 9 4 0 5.75 4.70 0.73 o 1 5 0 4698.87 5133.62 18.80 o 2 5 0 7.42 6.26 0.89 o 3 5 0 234.83 257.48 2.06 o 4 5 0 409.32 415.08 2.38 o 5 5 0 269.07 275.10 1.91 o 6 5 0 33.65 33.44 1.05 o 7 5 0 13.31 14.39 1.14 o 8 5 0 7.22 6.32 0.73 o 9 5 0 0.82 1.56 1.21 < 0 6 0 5549.24 5777.95 14.51 o 1 6 0 1899.82 2000.38 4.95 o 2 6 0 124.51 107.88 1.33 o 3 6 0 18.91 20.80 0.98 o 4 6 0 1.04 -0.38 1.02 < 5 6 0 124.49 127.88 1.49 o 6 6 0 17.91 15.21 0.86 o 7 6 0 16.89 13.37 0.95 o 8 6 0 82.29 84.76 1.17 o 1 7 0 6.36 5.37 0.60 o 2 7 0 133.53 137.09 1.68 o 3 7 0 334.08 330.20 2.38 o 4 7 0 218.26 234.99 2.48 o 5 7 0 522.99 540.11 4.13 o 6 7 0 0.62 1.27 0.83 < 7 7 0 47.95 52.87 0.92 o 0 8 0 1021.06 1042.87 7.30 o 1 8 0 768.22 790.44 4.13 o 2 8 0 1221.55 1205.33 5.78 o 3 8 0 1032.85 1065.13 5.21 o 4 8 0 83.88 83.99 1.43 o 5 8 0 332.23 323.31 2.76 o 6 8 0 40.34 45.60 1.30 o 7 8 0 0.30 1.02 1.37 < 1 9 0 13.68 18.48 1.14 o 2 9 0 26.60 27.25 1.37 o 3 9 0 16.38 16.29 1.24 o 4 9 0 36.37 37.69 1.97 o 5 9 0 144.89 141.50 1.94 o 6 9 0 0.84 -0.35 0.73 < 0 10 0 888.23 871.74 5.72 o 1 10 0 120.99 119.97 1.94 o 2 10 0 216.35 214.99 2.16 o 3 10 0 34.37 30.71 1.05 o 4 10 0 19.67 17.91 1.02 o 1 11 0 146.74 129.25 2.10 o 2 11 0 41.13 34.23 1.30 o -9 1 1 0.52 1.40 0.79 < -8 1 1 149.17 143.92 1.59 o -7 1 1 2.05 0.92 0.54 < -6 1 1 948.22 986.41 2.99 o -5 1 1 1.36 1.71 0.44 o -4 1 1 59.92 69.23 2.32 o -3 1 1 19.52 10.42 0.86 o -2 1 1 11179.02 11099.79 58.75 o -1 1 1 530.72 540.08 2.32 o 0 1 1 4.88 6.22 0.38 o 1 1 1 614.08 589.87 3.18 o 2 1 1 1168.97 1122.45 3.43 o 3 1 1 12.25 18.23 0.67 o 4 1 1 5150.09 5584.62 19.59 o 5 1 1 9.61 9.40 0.51 o 6 1 1 18.15 15.62 0.57 o 7 1 1 16.95 16.04 0.73 o 8 1 1 11.32 8.19 0.73 o 9 1 1 35.07 30.93 1.14 o -9 2 1 2.07 3.11 0.79 o -8 2 1 104.86 110.10 1.43 o -7 2 1 106.29 115.24 1.17 o -6 2 1 129.91 129.88 1.17 o -5 2 1 196.19 186.03 1.40 o -4 2 1 989.75 1008.51 3.91 o -3 2 1 995.69 1053.32 6.99 o -2 2 1 125.85 101.94 1.24 o -1 2 1 30848.08 30671.83 62.94 o 0 2 1 12722.98 13284.63 50.65 o 1 2 1 13692.18 13801.21 54.65 o 2 2 1 2847.20 2834.23 8.54 o 3 2 1 878.72 849.06 3.65 o 4 2 1 2863.06 3124.06 7.24 o 5 2 1 137.12 166.69 1.11 o 6 2 1 242.46 238.52 1.68 o 7 2 1 204.25 193.65 1.62 o 8 2 1 171.57 150.71 1.52 o 9 2 1 139.55 140.20 1.81 o -9 3 1 18.00 16.20 0.83 o -8 3 1 1.00 1.78 0.73 < -7 3 1 1.95 2.89 0.57 o -6 3 1 61.47 67.93 0.92 o -5 3 1 30.71 31.06 0.70 o -4 3 1 0.00 0.95 0.54 < -3 3 1 60.36 66.66 1.30 o -2 3 1 164.27 165.96 1.68 o -1 3 1 2782.73 2973.83 7.72 o 0 3 1 22660.18 22946.99 95.11 o 1 3 1 857.69 947.28 3.94 o 2 3 1 833.94 802.51 3.84 o 3 3 1 425.15 420.61 2.76 o 4 3 1 1360.36 1373.99 3.97 o 5 3 1 175.03 191.84 1.43 o 6 3 1 136.24 134.93 1.40 o 7 3 1 1.60 2.35 0.64 o 8 3 1 112.79 113.81 1.33 o 9 3 1 96.22 100.95 1.49 o -9 4 1 0.78 0.89 0.70 < -8 4 1 9.45 10.42 0.89 o -7 4 1 107.73 110.80 1.49 o -6 4 1 0.16 0.32 0.70 < -5 4 1 155.23 169.93 1.37 o -4 4 1 20.66 17.85 0.67 o -3 4 1 1.49 2.79 0.70 o -2 4 1 667.54 667.16 4.06 o -1 4 1 2785.34 2958.71 11.69 o 0 4 1 186.69 233.34 3.11 o 1 4 1 15.35 13.72 1.02 o 2 4 1 167.85 173.45 3.18 o 3 4 1 437.78 436.33 2.19 o 4 4 1 633.53 686.60 2.86 o 5 4 1 207.18 221.53 1.65 o 6 4 1 52.88 53.35 1.08 o 7 4 1 21.75 20.07 0.95 o 8 4 1 23.57 24.10 1.02 o 9 4 1 164.20 169.74 1.91 o -9 5 1 0.56 1.49 1.17 < -8 5 1 1.87 1.43 0.67 < -7 5 1 23.09 22.90 0.89 o -6 5 1 7.39 7.81 0.86 o -5 5 1 68.67 69.70 1.17 o -4 5 1 34.02 33.15 1.08 o -3 5 1 356.61 356.65 2.60 o -2 5 1 726.36 757.70 3.87 o -1 5 1 1622.09 1727.21 10.86 o 0 5 1 18.15 17.82 1.40 o 1 5 1 26.03 29.91 1.59 o 2 5 1 28.92 22.90 0.86 o 3 5 1 17.70 17.94 0.79 o 4 5 1 15.95 16.80 0.83 o 5 5 1 309.09 293.78 2.00 o 6 5 1 51.56 49.41 1.14 o 7 5 1 1.08 0.98 0.98 < 8 5 1 38.31 28.55 0.89 o -8 6 1 0.61 0.29 0.64 < -7 6 1 69.85 69.23 1.52 o -6 6 1 51.93 51.41 1.02 o -5 6 1 24.21 24.77 0.95 o -4 6 1 1193.34 1190.18 4.48 o -3 6 1 22.94 28.14 1.11 o -2 6 1 574.64 555.76 2.89 o -1 6 1 567.57 567.96 2.92 o 0 6 1 509.80 513.34 2.70 o 1 6 1 2409.61 2450.42 5.14 o 2 6 1 460.82 477.48 2.45 o 3 6 1 1330.09 1377.55 4.92 o 4 6 1 256.51 252.78 2.19 o 5 6 1 3.76 7.27 0.95 o 6 6 1 120.07 121.91 1.65 o 7 6 1 93.96 91.55 1.14 o 8 6 1 11.36 12.00 0.89 o -7 7 1 3.87 4.03 0.73 o -6 7 1 87.09 89.52 1.33 o -5 7 1 0.19 0.19 0.70 < -4 7 1 81.64 88.31 1.59 o -3 7 1 143.04 136.52 2.16 o -2 7 1 12.87 11.02 1.21 o -1 7 1 11.85 15.94 0.83 o 0 7 1 167.00 194.76 1.62 o 1 7 1 208.50 229.88 2.10 o 2 7 1 33.46 33.82 1.14 o 3 7 1 183.03 176.69 1.81 o 4 7 1 469.02 495.49 3.52 o 5 7 1 4.84 4.80 1.11 o 6 7 1 20.91 19.37 1.11 o 7 7 1 5.83 6.13 0.79 o -7 8 1 138.99 148.81 3.08 o -6 8 1 0.00 -0.64 0.73 < -5 8 1 46.45 46.36 1.17 o -4 8 1 0.00 3.05 0.86 o -3 8 1 124.34 126.93 1.87 o -2 8 1 45.18 44.81 1.56 o -1 8 1 3225.18 3340.80 7.02 o 0 8 1 200.77 211.43 1.84 o 1 8 1 128.11 132.77 1.65 o 2 8 1 62.29 58.43 1.56 o 3 8 1 7.78 8.22 0.92 o 4 8 1 16.88 19.05 1.49 o 5 8 1 1.40 1.87 1.17 < 6 8 1 10.65 11.08 0.86 o 7 8 1 26.18 31.98 1.87 o -6 9 1 0.71 0.35 0.86 < -5 9 1 77.46 77.96 1.46 o -4 9 1 22.97 19.97 1.33 o -3 9 1 78.56 77.77 1.84 o -2 9 1 2.03 2.60 1.08 < -1 9 1 662.93 672.85 3.65 o 0 9 1 633.88 620.51 3.59 o 1 9 1 60.18 68.31 1.27 o 2 9 1 62.97 67.58 1.43 o 3 9 1 276.70 271.55 2.79 o 4 9 1 75.53 77.90 1.87 o 5 9 1 79.49 73.04 1.49 o 6 9 1 25.24 28.71 0.98 o -4 10 1 76.07 72.12 1.52 o -3 10 1 13.55 8.35 0.86 o -2 10 1 420.73 374.21 3.84 o -1 10 1 177.27 182.85 2.95 o 0 10 1 6.63 7.81 0.95 o 1 10 1 302.43 312.00 2.89 o 2 10 1 33.37 30.04 1.05 o 3 10 1 31.50 32.49 1.24 o 4 10 1 18.31 18.55 0.89 o -2 11 1 141.47 127.88 2.95 o -1 11 1 183.78 161.48 2.35 o 0 11 1 4.90 2.22 1.43 < 1 11 1 10.13 8.32 1.14 o 2 11 1 85.60 67.29 2.29 o -9 0 2 1.60 1.37 1.08 < -8 0 2 721.83 759.45 4.19 o -7 0 2 27.15 28.20 1.14 o -6 0 2 66.39 55.92 1.08 o -5 0 2 4.48 4.13 0.64 o -4 0 2 193.06 178.88 2.57 o -3 0 2 6785.60 6912.08 34.17 o -2 0 2 9146.55 8633.42 37.34 o -1 0 2 6503.25 6495.13 50.43 o 0 0 2 2346.60 2375.61 8.38 o 1 0 2 1122.74 1162.40 6.64 o 2 0 2 952.61 835.76 3.08 o 3 0 2 3237.08 3298.88 7.81 o 4 0 2 2603.57 2855.50 6.16 o 5 0 2 7.98 3.46 0.70 o 6 0 2 8.36 5.68 0.67 o 7 0 2 2.18 0.70 1.02 < 8 0 2 516.13 501.17 4.67 o 9 0 2 29.26 27.75 1.40 o -9 1 2 112.08 122.96 1.52 o -8 1 2 268.79 266.88 1.84 o -7 1 2 600.30 591.49 2.48 o -6 1 2 68.64 67.55 0.86 o -5 1 2 203.39 212.83 1.33 o -4 1 2 759.99 775.13 4.95 o -3 1 2 307.87 302.98 2.35 o -2 1 2 17205.12 16411.34 51.73 o -1 1 2 1352.57 1469.07 4.19 o 0 1 2 4.72 2.51 0.44 o 1 1 2 484.20 453.89 3.21 o 2 1 2 936.52 818.67 2.06 o 3 1 2 467.68 430.93 1.91 o 4 1 2 62.20 62.46 0.86 o 5 1 2 199.00 216.58 1.37 o 6 1 2 170.92 159.29 1.30 o 7 1 2 46.96 43.00 0.98 o 8 1 2 110.49 102.83 1.43 o 9 1 2 360.67 333.09 2.41 o -9 2 2 1.02 2.54 0.73 o -8 2 2 3.95 5.62 0.67 o -7 2 2 6.91 10.10 0.64 o -6 2 2 39.13 37.66 0.79 o -5 2 2 20.73 26.58 0.57 o -4 2 2 610.21 593.68 3.40 o -3 2 2 548.57 534.52 3.94 o -2 2 2 8051.78 7948.76 20.20 o -1 2 2 758.32 769.45 2.89 o 0 2 2 8.13 8.29 0.54 o 1 2 2 318.24 286.09 1.75 o 2 2 2 1345.99 1289.45 3.94 o 3 2 2 129.09 134.14 1.43 o 4 2 2 1458.28 1553.57 4.22 o 5 2 2 61.29 58.02 0.73 o 6 2 2 1.27 2.16 0.73 < 7 2 2 27.70 22.23 0.73 o 8 2 2 1.70 1.84 0.67 < 9 2 2 3.50 3.49 0.95 o -9 3 2 7.02 7.40 0.76 o -8 3 2 20.05 16.29 0.73 o -7 3 2 112.30 113.65 1.17 o -6 3 2 3.96 4.70 0.64 o -5 3 2 122.89 125.69 1.11 o -4 3 2 89.51 86.38 1.17 o -3 3 2 604.97 630.87 3.56 o -2 3 2 0.88 2.60 0.70 o -1 3 2 3077.67 3234.29 8.54 o 0 3 2 3556.75 3611.20 9.69 o 1 3 2 489.63 485.80 4.03 o 2 3 2 157.00 166.15 1.75 o 3 3 2 848.13 939.03 3.68 o 4 3 2 760.93 794.60 2.51 o 5 3 2 273.27 292.89 1.71 o 6 3 2 191.16 183.11 1.87 o 7 3 2 203.04 192.25 1.68 o 8 3 2 0.02 1.33 0.73 < 9 3 2 41.45 37.54 1.11 o -9 4 2 7.24 3.24 0.79 o -8 4 2 21.65 22.32 1.08 o -7 4 2 84.36 85.96 1.11 o -6 4 2 315.77 309.68 1.91 o -5 4 2 18.77 17.28 0.60 o -4 4 2 63.38 62.24 0.95 o -3 4 2 4.39 5.05 0.67 o -2 4 2 129.49 151.98 2.29 o -1 4 2 291.17 288.66 3.84 o 0 4 2 236.57 277.10 3.14 o 1 4 2 14.29 17.12 1.24 o 2 4 2 1869.80 1881.23 11.65 o 3 4 2 1078.89 1158.40 3.56 o 4 4 2 609.38 669.58 2.51 o 5 4 2 139.55 143.35 1.43 o 6 4 2 17.37 18.51 0.83 o 7 4 2 2.06 0.86 0.76 < 8 4 2 4.67 3.78 0.86 o 9 4 2 27.37 31.25 0.92 o -9 5 2 2.83 3.08 1.17 < -8 5 2 25.84 25.25 1.02 o -7 5 2 16.55 15.50 0.76 o -6 5 2 6.38 6.32 0.79 o -5 5 2 41.44 38.81 0.92 o -4 5 2 152.11 150.78 1.62 o -3 5 2 56.02 55.83 1.24 o -2 5 2 479.42 499.62 3.59 o -1 5 2 922.95 1014.51 5.97 o 0 5 2 1445.22 1691.49 8.16 o 1 5 2 84.14 83.20 2.22 o 2 5 2 251.68 270.78 1.91 o 3 5 2 536.68 514.23 2.32 o 4 5 2 31.83 36.36 0.98 o 5 5 2 172.39 174.31 1.68 o 6 5 2 8.77 7.68 0.95 o 7 5 2 11.01 6.92 0.79 o 8 5 2 53.88 49.44 1.11 o -8 6 2 0.08 0.48 0.67 < -7 6 2 0.97 1.75 0.76 < -6 6 2 40.37 41.95 1.02 o -5 6 2 13.92 14.07 1.05 o -4 6 2 1002.78 1033.63 4.22 o -3 6 2 10.70 13.27 1.02 o -2 6 2 704.37 739.31 4.00 o -1 6 2 110.37 128.23 1.43 o 0 6 2 465.01 461.03 2.38 o 1 6 2 562.71 594.85 3.08 o 2 6 2 138.35 142.97 1.43 o 3 6 2 933.88 957.67 3.56 o 4 6 2 141.80 155.67 1.94 o 5 6 2 0.34 1.43 1.05 < 6 6 2 22.98 23.34 1.05 o 7 6 2 41.57 41.92 0.89 o 8 6 2 80.19 81.10 1.40 o -7 7 2 66.88 64.88 1.30 o -6 7 2 184.36 185.17 1.65 o -5 7 2 225.18 234.65 1.75 o -4 7 2 303.74 291.11 2.57 o -3 7 2 1021.75 1082.34 4.60 o -2 7 2 184.83 182.57 2.29 o -1 7 2 699.36 732.29 3.68 o 0 7 2 27.74 26.26 0.92 o 1 7 2 365.87 381.52 2.67 o 2 7 2 42.15 38.33 1.30 o 3 7 2 162.97 167.83 1.91 o 4 7 2 83.51 82.47 1.71 o 5 7 2 18.53 17.97 1.14 o 6 7 2 102.73 102.29 1.62 o 7 7 2 18.73 19.69 1.02 o -7 8 2 21.72 17.75 1.49 o -6 8 2 8.36 7.30 0.79 o -5 8 2 411.93 426.01 2.79 o -4 8 2 230.55 248.24 2.13 o -3 8 2 74.90 80.72 1.43 o -2 8 2 300.39 300.98 2.64 o -1 8 2 906.93 896.76 3.97 o 0 8 2 232.22 234.33 2.13 o 1 8 2 117.28 125.06 1.52 o 2 8 2 633.82 655.73 3.84 o 3 8 2 78.76 85.17 1.68 o 4 8 2 2.94 2.83 1.05 < 5 8 2 128.80 135.44 2.06 o 6 8 2 17.21 18.35 1.08 o 7 8 2 40.29 46.08 2.06 o -6 9 2 47.28 48.81 1.91 o -5 9 2 19.59 18.39 0.89 o -4 9 2 239.28 249.51 3.02 o -3 9 2 2.94 3.65 0.98 o -2 9 2 36.35 40.62 2.19 o -1 9 2 27.25 33.79 1.37 o 0 9 2 12.43 15.37 1.11 o 1 9 2 1.19 1.59 0.76 < 2 9 2 29.22 29.95 1.11 o 3 9 2 426.48 405.14 2.76 o 4 9 2 11.01 12.54 1.05 o 5 9 2 10.37 12.16 0.95 o 6 9 2 11.60 13.46 1.05 o -4 10 2 31.65 28.83 0.95 o -3 10 2 7.00 5.78 0.83 o -2 10 2 114.80 96.86 2.38 o -1 10 2 431.04 414.04 4.29 o 0 10 2 12.58 10.35 1.30 o 1 10 2 74.34 66.43 1.49 o 2 10 2 0.41 0.06 0.76 < 3 10 2 1.74 3.46 0.89 o 4 10 2 108.68 109.72 2.06 o -2 11 2 84.88 77.48 2.38 o -1 11 2 620.09 588.38 4.38 o 0 11 2 34.68 37.73 1.84 o 1 11 2 3.20 4.48 1.59 < 2 11 2 95.17 102.22 2.60 o -9 1 3 10.89 9.97 0.79 o -8 1 3 53.21 57.80 1.05 o -7 1 3 227.74 218.89 1.65 o -6 1 3 0.04 1.27 0.44 < -5 1 3 990.06 950.49 2.64 o -4 1 3 857.23 848.52 5.30 o -3 1 3 1501.71 1503.05 4.76 o -2 1 3 831.88 736.45 2.86 o -1 1 3 871.01 885.71 3.65 o 0 1 3 1243.78 1177.45 3.27 o 1 1 3 1518.35 1416.80 4.13 o 2 1 3 509.88 442.14 1.71 o 3 1 3 6.09 7.18 0.44 o 4 1 3 1.77 1.02 0.51 < 5 1 3 112.03 115.37 0.95 o 6 1 3 217.16 214.96 1.37 o 7 1 3 12.27 15.47 0.79 o 8 1 3 95.63 83.52 1.33 o 9 1 3 16.18 13.66 0.89 o -9 2 3 19.18 16.99 0.73 o -8 2 3 5.13 5.68 0.70 o -7 2 3 74.06 74.28 1.05 o -6 2 3 364.97 366.43 2.10 o -5 2 3 369.66 385.01 1.78 o -4 2 3 1052.77 1006.29 5.11 o -3 2 3 31.66 29.09 0.83 o -2 2 3 778.61 785.96 3.46 o -1 2 3 42.56 33.25 0.86 o 0 2 3 490.45 481.39 2.38 o 1 2 3 43.68 52.33 0.79 o 2 2 3 921.95 876.18 3.02 o 3 2 3 414.05 443.31 2.54 o 4 2 3 46.65 60.59 0.73 o 5 2 3 230.52 264.18 1.37 o 6 2 3 0.89 0.79 0.64 < 7 2 3 1.22 0.32 0.67 < 8 2 3 55.94 56.84 0.95 o 9 2 3 75.54 64.02 1.37 o -9 3 3 16.04 13.75 0.76 o -8 3 3 6.68 4.86 0.57 o -7 3 3 174.00 168.62 1.46 o -6 3 3 1.32 1.14 0.64 < -5 3 3 749.67 693.90 2.48 o -4 3 3 1986.79 1908.76 4.35 o -3 3 3 1260.66 1288.91 5.49 o -2 3 3 909.96 938.39 3.87 o -1 3 3 265.65 241.28 2.41 o 0 3 3 3409.36 3449.95 9.84 o 1 3 3 57.15 69.04 2.10 o 2 3 3 2273.81 2326.42 5.46 o 3 3 3 56.43 51.83 1.14 o 4 3 3 2.24 2.41 0.44 o 5 3 3 0.24 1.81 0.54 o 6 3 3 0.33 0.83 0.86 < 7 3 3 13.12 10.67 0.76 o 8 3 3 978.01 961.76 4.06 o 9 3 3 78.52 80.44 1.21 o -9 4 3 74.69 83.14 1.40 o -8 4 3 26.64 25.15 0.89 o -7 4 3 60.63 67.32 0.95 o -6 4 3 3.55 2.00 0.70 < -5 4 3 1.67 1.43 0.51 < -4 4 3 421.86 398.41 1.94 o -3 4 3 696.97 740.52 2.86 o -2 4 3 333.38 388.85 3.91 o -1 4 3 29.24 32.11 1.11 o 0 4 3 277.18 298.35 3.21 o 1 4 3 556.49 607.75 6.22 o 2 4 3 525.31 519.24 5.56 o 3 4 3 175.17 203.68 1.21 o 4 4 3 7.68 4.89 0.64 o 5 4 3 15.41 10.83 0.70 o 6 4 3 3.11 3.87 0.89 o 7 4 3 32.48 29.22 0.92 o 8 4 3 33.38 29.95 0.98 o 9 4 3 0.22 1.46 0.76 < -8 5 3 12.20 9.05 0.83 o -7 5 3 18.25 16.89 0.73 o -6 5 3 526.63 539.57 2.45 o -5 5 3 0.33 -0.16 0.73 < -4 5 3 332.17 306.13 2.38 o -3 5 3 54.44 51.22 1.17 o -2 5 3 77.43 67.07 1.68 o -1 5 3 334.80 372.94 2.64 o 0 5 3 1274.33 1378.24 5.49 o 1 5 3 10.10 7.21 0.98 o 2 5 3 112.62 104.83 1.40 o 3 5 3 512.49 544.33 2.54 o 4 5 3 92.78 91.01 1.33 o 5 5 3 20.53 21.88 0.98 o 6 5 3 13.33 14.64 0.83 o 7 5 3 350.94 369.10 2.38 o 8 5 3 52.89 51.95 1.14 o -8 6 3 14.47 13.46 0.86 o -7 6 3 68.29 71.23 1.21 o -6 6 3 345.60 353.70 2.25 o -5 6 3 615.58 657.00 3.40 o -4 6 3 43.55 42.90 1.02 o -3 6 3 9.62 11.31 0.92 o -2 6 3 209.85 232.99 2.38 o -1 6 3 14.03 15.40 0.98 o 0 6 3 0.47 0.25 0.73 < 1 6 3 225.05 239.09 2.00 o 2 6 3 12.88 14.32 1.02 o 3 6 3 13.07 18.20 0.89 o 4 6 3 14.90 13.56 1.27 o 5 6 3 0.00 -1.02 1.08 < 6 6 3 47.98 47.82 0.98 o 7 6 3 3.13 2.79 0.73 o 8 6 3 24.78 30.26 0.89 o -7 7 3 0.09 0.19 0.76 < -6 7 3 13.97 14.80 0.73 o -5 7 3 261.33 271.80 1.91 o -4 7 3 2.65 2.38 0.95 < -3 7 3 426.59 434.58 2.95 o -2 7 3 8.37 9.88 1.30 o -1 7 3 14.30 13.88 1.14 o 0 7 3 137.41 144.68 1.49 o 1 7 3 0.66 1.17 0.89 < 2 7 3 24.06 23.34 1.30 o 3 7 3 238.18 225.63 2.38 o 4 7 3 85.62 87.93 1.94 o 5 7 3 0.00 0.25 1.05 < 6 7 3 16.49 17.02 1.08 o 7 7 3 1.27 -0.57 0.79 < -6 8 3 2.31 1.97 0.70 < -5 8 3 29.42 30.39 0.98 o -4 8 3 55.40 51.60 1.24 o -3 8 3 127.23 122.58 1.71 o -2 8 3 29.43 28.77 1.08 o -1 8 3 28.46 32.07 1.21 o 0 8 3 0.05 -0.10 0.76 < 1 8 3 204.19 213.59 2.06 o 2 8 3 158.45 173.52 1.94 o 3 8 3 15.57 13.31 0.98 o 4 8 3 9.36 8.89 0.98 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90.51 96.86 1.65 o 2 0 4 1069.31 1080.50 4.06 o 3 0 4 750.50 698.70 3.18 o 4 0 4 1424.02 1344.39 5.14 o 5 0 4 194.80 227.82 1.78 o 6 0 4 2.11 0.51 0.67 < 7 0 4 100.91 78.91 1.59 o 8 0 4 404.31 399.14 4.19 o 9 0 4 22.45 18.67 1.24 o -9 1 4 13.54 16.67 0.83 o -8 1 4 46.09 46.05 1.02 o -7 1 4 402.12 392.89 2.19 o -6 1 4 329.84 300.03 1.59 o -5 1 4 1716.53 1627.50 3.33 o -4 1 4 0.45 1.68 0.76 < -3 1 4 620.85 616.51 3.18 o -2 1 4 502.93 488.41 2.51 o -1 1 4 10.37 8.45 0.83 o 0 1 4 706.53 697.52 2.48 o 1 1 4 2679.76 2603.07 6.35 o 2 1 4 134.15 131.37 0.95 o 3 1 4 326.45 301.62 1.84 o 4 1 4 3.37 5.68 0.44 o 5 1 4 45.92 48.52 0.64 o 6 1 4 115.16 106.76 1.08 o 7 1 4 30.61 25.40 0.76 o 8 1 4 40.26 37.03 0.92 o 9 1 4 3.16 7.24 0.73 o -9 2 4 21.95 21.94 0.76 o -8 2 4 74.99 78.72 1.08 o -7 2 4 88.37 88.12 1.08 o -6 2 4 322.55 313.65 1.78 o -5 2 4 427.67 440.36 1.97 o -4 2 4 1306.94 1292.44 3.91 o -3 2 4 643.31 660.84 4.41 o -2 2 4 674.46 660.84 2.79 o -1 2 4 92.06 94.47 1.14 o 0 2 4 643.05 625.21 2.73 o 1 2 4 171.60 171.86 1.49 o 2 2 4 199.79 199.87 1.37 o 3 2 4 6.65 5.43 0.67 o 4 2 4 6.02 7.68 0.44 o 5 2 4 45.39 43.66 0.73 o 6 2 4 112.04 100.89 1.08 o 7 2 4 27.15 21.21 0.79 o 8 2 4 3.44 4.67 0.67 o 9 2 4 40.31 42.71 1.21 o -9 3 4 113.92 111.40 1.65 o -8 3 4 95.81 98.09 1.30 o -7 3 4 48.29 42.78 0.89 o -6 3 4 62.91 58.65 0.95 o -5 3 4 32.60 31.57 0.70 o -4 3 4 2128.12 2103.11 4.38 o -3 3 4 246.95 237.57 2.76 o -2 3 4 552.86 585.90 3.21 o -1 3 4 12.17 11.78 0.79 o 0 3 4 1167.69 1143.15 6.32 o 1 3 4 1055.28 1011.27 5.78 o 2 3 4 576.67 587.26 3.56 o 3 3 4 394.56 434.49 2.83 o 4 3 4 12.55 12.58 0.54 o 5 3 4 15.31 19.56 0.60 o 6 3 4 3.60 3.62 0.57 o 7 3 4 52.45 59.54 1.14 o 8 3 4 103.81 95.17 1.46 o 9 3 4 61.43 65.23 1.24 o -9 4 4 44.27 54.78 1.71 o -8 4 4 189.20 194.98 1.62 o -7 4 4 105.31 94.63 1.11 o -6 4 4 1598.74 1612.19 4.19 o -5 4 4 161.11 160.21 1.21 o -4 4 4 75.41 79.61 0.98 o -3 4 4 980.03 1036.36 3.14 o -2 4 4 313.81 323.59 2.73 o -1 4 4 29.75 24.80 1.05 o 0 4 4 1828.48 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0.92 o 4 6 4 32.61 32.87 1.17 o 5 6 4 37.82 41.51 1.17 o 6 6 4 83.64 77.45 1.27 o 7 6 4 199.21 194.95 1.71 o 8 6 4 73.12 72.12 1.84 o -7 7 4 58.60 55.32 1.05 o -6 7 4 848.42 902.82 3.24 o -5 7 4 3.06 2.70 0.67 o -4 7 4 9.03 8.16 0.70 o -3 7 4 44.61 47.35 1.30 o -2 7 4 2.02 1.33 0.79 < -1 7 4 11.72 9.62 1.05 o 0 7 4 153.20 154.62 1.71 o 1 7 4 16.67 18.67 0.98 o 2 7 4 195.01 203.49 2.00 o 3 7 4 1.87 1.62 1.02 < 4 7 4 3.26 2.64 0.92 < 5 7 4 0.06 0.19 0.73 < 6 7 4 9.81 6.48 0.98 o 7 7 4 3.72 2.22 0.70 o -6 8 4 275.19 268.50 1.97 o -5 8 4 25.85 25.82 0.92 o -4 8 4 7.09 8.38 0.98 o -3 8 4 42.41 41.19 1.21 o -2 8 4 7.77 7.08 0.92 o -1 8 4 0.50 0.64 1.05 < 0 8 4 44.97 48.27 1.40 o 1 8 4 155.00 152.43 1.68 o 2 8 4 30.23 28.71 1.05 o 3 8 4 0.74 0.73 0.89 < 4 8 4 63.22 59.45 1.40 o 5 8 4 83.89 86.19 1.78 o 6 8 4 47.81 54.75 1.17 o -5 9 4 256.20 245.47 2.25 o -4 9 4 175.37 174.40 2.54 o -3 9 4 61.10 62.72 1.65 o -2 9 4 29.72 32.80 1.11 o -1 9 4 0.01 1.08 0.83 < 0 9 4 45.55 47.92 1.52 o 1 9 4 97.47 97.75 1.43 o 2 9 4 1.98 1.91 0.73 < 3 9 4 131.35 141.41 1.78 o 4 9 4 0.55 0.83 0.76 < 5 9 4 1.55 0.95 0.79 < -4 10 4 0.09 0.76 0.86 < -3 10 4 2.29 2.51 0.98 < -2 10 4 273.60 288.12 3.02 o -1 10 4 1.00 1.65 0.98 < 0 10 4 68.79 67.23 2.00 o 1 10 4 33.38 35.98 1.68 o 2 10 4 83.14 76.69 1.21 o 3 10 4 34.26 29.88 0.98 o 4 10 4 153.44 165.80 1.84 o -1 11 4 2.85 0.79 0.92 < 0 11 4 35.17 32.99 1.37 o 1 11 4 0.45 -2.86 1.49 < -9 1 5 11.83 14.00 0.79 o -8 1 5 18.51 16.93 0.83 o -7 1 5 1085.23 1124.16 3.84 o -6 1 5 253.64 252.49 1.59 o -5 1 5 403.78 403.43 1.71 o -4 1 5 52.28 51.16 0.86 o -3 1 5 174.48 170.82 1.78 o -2 1 5 44.56 47.25 0.86 o -1 1 5 26.25 25.63 0.92 o 0 1 5 633.13 584.03 2.29 o 1 1 5 164.65 139.25 1.40 o 2 1 5 491.13 452.78 1.94 o 3 1 5 0.34 0.70 0.51 < 4 1 5 4.96 5.34 0.41 o 5 1 5 0.78 0.48 0.44 < 6 1 5 12.46 12.42 0.60 o 7 1 5 2.50 2.03 0.64 o 8 1 5 6.77 7.65 0.70 o 9 1 5 0.46 0.51 0.76 < -9 2 5 57.68 56.94 0.98 o -8 2 5 65.71 66.66 1.17 o -7 2 5 1651.86 1641.34 4.16 o -6 2 5 988.01 966.84 3.24 o -5 2 5 48.23 55.38 0.89 o -4 2 5 171.06 185.33 1.30 o -3 2 5 562.65 584.63 3.24 o -2 2 5 63.60 63.26 1.08 o -1 2 5 1796.80 1723.50 5.05 o 0 2 5 0.25 0.13 0.48 < 1 2 5 76.29 60.97 0.95 o 2 2 5 82.27 77.96 1.05 o 3 2 5 238.05 224.48 1.65 o 4 2 5 4.70 1.11 0.38 < 5 2 5 1139.87 1107.27 2.89 o 6 2 5 829.19 815.78 3.05 o 7 2 5 128.35 128.10 1.30 o 8 2 5 3.59 3.97 0.79 o 9 2 5 49.20 53.25 1.21 o -9 3 5 78.01 85.01 1.24 o -8 3 5 78.46 72.66 1.08 o -7 3 5 1006.02 1026.80 3.52 o -6 3 5 1446.36 1374.78 3.81 o -5 3 5 145.07 136.74 1.27 o -4 3 5 566.55 515.08 2.13 o -3 3 5 13.04 8.61 0.70 o -2 3 5 3379.22 3637.31 7.94 o -1 3 5 1939.98 2040.77 6.86 o 0 3 5 310.67 325.72 2.89 o 1 3 5 195.02 206.54 2.45 o 2 3 5 210.43 181.14 1.84 o 3 3 5 93.12 97.81 0.83 o 4 3 5 668.08 638.71 1.97 o 5 3 5 157.75 154.84 1.14 o 6 3 5 310.08 308.83 1.97 o 7 3 5 35.68 37.57 0.92 o 8 3 5 0.00 0.95 0.79 < 9 3 5 20.55 22.80 0.83 o -9 4 5 39.47 47.13 1.52 o -8 4 5 108.68 116.51 1.37 o -7 4 5 608.58 612.35 2.60 o -6 4 5 1137.95 1118.89 3.49 o -5 4 5 15.52 14.83 0.70 o -4 4 5 68.27 68.31 0.92 o -3 4 5 62.94 58.84 0.83 o -2 4 5 141.12 173.58 1.75 o -1 4 5 533.42 575.55 4.32 o 0 4 5 341.42 337.15 3.62 o 1 4 5 232.26 224.04 3.27 o 2 4 5 0.32 1.24 0.60 < 3 4 5 387.63 367.42 1.78 o 4 4 5 135.38 130.93 1.11 o 5 4 5 50.07 51.25 0.86 o 6 4 5 81.32 81.26 1.08 o 7 4 5 52.34 51.60 1.17 o 8 4 5 12.09 10.92 0.83 o 9 4 5 7.17 6.54 1.59 o -8 5 5 140.84 144.24 1.68 o -7 5 5 34.31 42.49 1.11 o -6 5 5 53.01 51.98 1.05 o -5 5 5 29.00 28.61 0.95 o -4 5 5 16.29 15.88 0.76 o -3 5 5 327.89 349.86 2.06 o -2 5 5 105.86 102.60 1.24 o -1 5 5 16.53 11.56 0.73 o 0 5 5 131.50 146.90 1.65 o 1 5 5 154.77 141.41 1.40 o 2 5 5 409.62 437.34 2.35 o 3 5 5 152.78 139.41 1.43 o 4 5 5 18.44 22.48 0.89 o 5 5 5 0.22 0.16 0.79 < 6 5 5 123.20 116.23 1.33 o 7 5 5 1.49 2.99 0.83 o 8 5 5 5.11 5.37 0.73 o -8 6 5 208.93 251.89 3.11 o -7 6 5 830.55 865.64 3.56 o -6 6 5 212.39 226.64 1.78 o -5 6 5 478.78 503.65 2.67 o -4 6 5 28.98 25.85 1.05 o -3 6 5 11.65 12.26 0.86 o -2 6 5 48.88 58.43 1.17 o -1 6 5 620.94 665.38 3.11 o 0 6 5 327.29 325.85 2.16 o 1 6 5 125.11 142.30 1.52 o 2 6 5 172.11 157.70 1.71 o 3 6 5 116.15 122.80 1.43 o 4 6 5 0.69 1.05 0.98 < 5 6 5 167.11 179.33 1.71 o 6 6 5 146.46 132.61 1.62 o 7 6 5 11.01 10.67 0.79 o 8 6 5 11.97 10.16 1.14 o -7 7 5 335.38 347.54 2.32 o -6 7 5 19.41 17.75 0.73 o -5 7 5 458.38 481.77 2.70 o -4 7 5 5.89 6.22 0.70 o -3 7 5 5.78 7.11 1.08 o -2 7 5 222.57 227.47 2.22 o -1 7 5 71.34 71.96 1.49 o 0 7 5 27.73 24.26 1.21 o 1 7 5 7.82 6.73 0.95 o 2 7 5 0.56 0.64 0.98 < 3 7 5 8.72 6.57 1.14 o 4 7 5 9.62 9.53 1.05 o 5 7 5 39.93 43.63 1.14 o 6 7 5 11.26 10.73 0.89 o 7 7 5 28.95 25.02 0.83 o -6 8 5 471.13 487.20 2.29 o -5 8 5 179.87 185.26 1.71 o -4 8 5 2.69 3.56 0.98 o -3 8 5 69.93 72.02 1.65 o -2 8 5 255.19 271.90 2.45 o -1 8 5 70.32 88.28 1.68 o 0 8 5 0.02 0.19 0.86 < 1 8 5 18.67 17.12 0.89 o 2 8 5 0.86 2.16 0.83 < 3 8 5 1.30 3.84 0.92 o 4 8 5 44.85 31.88 1.14 o 5 8 5 58.82 57.86 1.17 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445.82 2.45 o 0 3 11 26.17 29.41 0.70 o 1 3 11 131.89 141.19 1.11 o 2 3 11 734.43 727.09 2.45 o 3 3 11 0.58 1.24 0.60 < 4 3 11 2490.37 2551.69 4.92 o 5 3 11 401.53 415.24 2.19 o 6 3 11 13.16 14.54 0.92 o 7 3 11 7.30 9.84 0.73 o 8 3 11 2.80 3.75 1.05 o -7 4 11 1.87 0.29 0.73 < -6 4 11 0.64 1.30 0.70 < -5 4 11 17.95 20.07 0.98 o -4 4 11 17.73 21.18 0.92 o -3 4 11 3.66 4.80 0.83 o -2 4 11 54.21 53.83 0.95 o -1 4 11 30.51 28.55 0.83 o 0 4 11 258.48 251.48 1.62 o 1 4 11 7.47 8.03 0.60 o 2 4 11 72.06 72.37 1.02 o 3 4 11 437.30 433.85 2.29 o 4 4 11 106.37 115.37 1.43 o 5 4 11 72.66 72.88 1.17 o 6 4 11 13.35 11.08 0.86 o 7 4 11 46.93 48.87 0.98 o -7 5 11 31.61 28.74 0.79 o -6 5 11 79.21 78.56 1.33 o -5 5 11 13.28 13.02 0.98 o -4 5 11 110.37 105.24 1.68 o -3 5 11 79.08 78.34 1.46 o -2 5 11 62.20 56.65 1.21 o -1 5 11 201.96 212.13 1.78 o 0 5 11 91.56 88.66 1.14 o 1 5 11 159.52 161.23 1.59 o 2 5 11 202.52 208.83 1.71 o 3 5 11 525.23 546.30 2.70 o 4 5 11 18.18 17.75 0.89 o 5 5 11 5.26 5.02 0.86 o 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102.45 1.43 o -3 4 12 7.46 8.10 0.89 o -2 4 12 2.27 2.41 0.76 o -1 4 12 2.68 2.99 0.83 o 0 4 12 318.68 324.17 2.00 o 1 4 12 794.83 814.99 3.52 o 2 4 12 752.70 763.38 3.11 o 3 4 12 26.94 26.20 0.89 o 4 4 12 351.68 378.15 2.22 o 5 4 12 7.04 6.19 0.76 o 6 4 12 59.44 60.75 1.21 o 7 4 12 264.67 277.04 1.91 o -7 5 12 1.20 0.38 0.98 < -6 5 12 2.56 1.62 0.67 < -5 5 12 32.68 32.52 1.08 o -4 5 12 13.08 14.67 0.98 o -3 5 12 34.14 33.95 1.17 o -2 5 12 96.04 90.44 1.43 o -1 5 12 1.99 3.78 0.98 o 0 5 12 55.81 50.81 1.08 o 1 5 12 1691.61 1737.09 4.95 o 2 5 12 356.10 359.95 2.25 o 3 5 12 1057.19 1100.54 3.94 o 4 5 12 17.02 15.02 0.86 o 5 5 12 0.02 0.22 0.86 < 6 5 12 163.90 196.54 1.65 o -6 6 12 0.86 -0.10 0.64 < -5 6 12 183.20 188.38 2.03 o -4 6 12 43.27 40.17 1.14 o -3 6 12 3.66 6.16 0.98 o -2 6 12 3.50 2.00 0.92 < -1 6 12 7.49 6.83 0.70 o 0 6 12 96.84 100.16 1.49 o 1 6 12 245.77 246.24 1.87 o 2 6 12 60.87 64.12 1.27 o 3 6 12 3.58 4.48 0.73 o 4 6 12 1.67 1.11 0.83 < 5 6 12 48.79 52.62 1.24 o 6 6 12 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