#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:49:16 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181196 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/75/2227572.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227572_Fobs loop_ _publ_author_name 'Wei, Wen-Bin' 'Tian, Shuo' 'Zhou, Hao' 'Sun, Jie' 'Wang, Hai-Bo' _publ_section_title ; 5-Chloroindoline-2,3-dione ; _journal_coeditor_code HB5688 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3024 _journal_volume 66 _journal_year 2010 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 24.7060 _cell_length_b 5.6890 _cell_length_c 5.2090 _exptl_crystal_F_000 368.00 _reflns_d_resolution_high 0.7837 _cod_data_source_file hb5688Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' X in Pna2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 97.22 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 296.75 339.67 2.34 o 4 0 0 5.44 5.34 0.86 o 6 0 0 1618.03 1631.30 8.83 o 8 0 0 260.34 304.26 8.11 o 10 0 0 233.73 199.72 4.17 o 12 0 0 2332.29 2489.03 21.26 o 14 0 0 301.83 296.42 6.34 o 16 0 0 62.32 56.21 3.38 o 18 0 0 228.94 249.09 6.88 o 20 0 0 17.44 17.86 3.10 o 22 0 0 56.30 57.87 4.19 o 24 0 0 41.76 49.41 4.84 o 26 0 0 419.06 423.40 30.21 o 28 0 0 6.96 0.78 4.22 o 30 0 0 13.33 15.73 3.79 o 1 1 0 2399.12 2275.44 37.05 o 2 1 0 1997.87 1821.50 34.15 o 3 1 0 1731.29 1786.81 8.50 o 4 1 0 495.21 467.44 5.06 o 5 1 0 312.96 326.55 4.19 o 6 1 0 69.53 82.07 2.44 o 7 1 0 729.16 722.95 15.03 o 8 1 0 1717.34 1751.67 11.22 o 9 1 0 115.85 124.99 3.83 o 10 1 0 25.80 26.64 1.94 o 11 1 0 42.04 54.97 2.89 o 12 1 0 1452.91 1569.39 12.81 o 13 1 0 1524.16 1616.31 20.79 o 14 1 0 640.08 640.13 9.40 o 15 1 0 418.29 429.41 7.99 o 16 1 0 176.68 187.74 5.82 o 17 1 0 263.11 243.81 11.38 o 18 1 0 563.77 539.92 10.12 o 19 1 0 459.02 443.27 18.42 o 20 1 0 63.18 56.34 5.21 o 21 1 0 32.05 31.46 5.68 o 22 1 0 49.79 50.42 4.54 o 23 1 0 144.88 133.21 6.71 o 24 1 0 116.47 111.01 9.47 o 25 1 0 136.56 126.78 7.26 o 26 1 0 0.21 -0.48 4.34 o 27 1 0 28.99 24.03 3.62 o 28 1 0 0.50 -1.81 3.37 o 29 1 0 22.63 16.23 3.89 o 30 1 0 9.54 10.09 13.96 o 31 1 0 19.04 22.93 4.25 o 0 2 0 399.95 457.09 8.20 o 1 2 0 4169.68 2060.56 1899.46 o 2 2 0 2561.76 1486.08 1413.98 o 3 2 0 7.44 3.70 1.33 o 4 2 0 279.05 310.06 5.82 o 5 2 0 1636.33 1669.37 11.63 o 6 2 0 375.01 378.51 8.57 o 7 2 0 867.17 824.57 8.81 o 8 2 0 3.92 3.59 1.57 o 9 2 0 267.67 272.63 5.53 o 10 2 0 104.23 103.48 3.81 o 11 2 0 1114.25 1176.32 11.94 o 12 2 0 37.40 38.52 2.91 o 13 2 0 0.43 3.65 4.15 o 14 2 0 115.86 107.96 4.29 o 15 2 0 2.73 2.90 1.74 o 16 2 0 84.91 90.64 4.08 o 17 2 0 1.52 -1.75 1.99 o 18 2 0 45.96 36.59 3.68 o 19 2 0 24.25 20.40 2.85 o 20 2 0 77.09 67.79 4.58 o 21 2 0 0.20 -2.16 2.74 o 22 2 0 106.86 97.39 6.85 o 23 2 0 8.62 2.91 4.15 o 24 2 0 87.40 81.56 8.01 o 25 2 0 2.07 -2.44 3.45 o 26 2 0 8.53 7.35 4.15 o 27 2 0 149.47 160.22 14.31 o 28 2 0 1.66 -3.66 3.66 o 29 2 0 38.68 34.29 6.67 o 30 2 0 53.81 49.58 5.89 o 1 3 0 20.82 23.55 2.29 o 2 3 0 102.09 115.37 3.90 o 3 3 0 508.19 555.07 14.48 o 4 3 0 140.42 127.91 4.14 o 5 3 0 340.12 340.31 11.38 o 6 3 0 184.02 197.77 5.23 o 7 3 0 7.26 7.15 1.78 o 8 3 0 1.77 2.84 1.41 o 9 3 0 186.57 183.75 5.20 o 10 3 0 31.50 31.09 2.92 o 11 3 0 1.50 4.33 5.86 o 12 3 0 394.82 393.55 20.68 o 13 3 0 404.45 395.33 8.62 o 14 3 0 1239.76 1250.88 15.21 o 15 3 0 11.23 13.05 3.17 o 16 3 0 125.69 110.42 5.57 o 17 3 0 20.47 15.19 3.04 o 18 3 0 10.48 7.60 2.66 o 19 3 0 55.20 48.60 4.30 o 20 3 0 121.19 136.51 6.13 o 21 3 0 13.39 10.86 3.25 o 22 3 0 73.60 59.93 5.79 o 23 3 0 0.55 -0.91 3.50 o 24 3 0 39.17 47.82 4.54 o 25 3 0 8.81 12.39 3.72 o 26 3 0 91.51 104.22 6.51 o 27 3 0 2.62 -4.14 4.14 o 28 3 0 56.27 59.60 7.21 o 0 4 0 9.17 20.48 3.31 o 1 4 0 1.98 3.11 3.74 o 2 4 0 299.57 281.90 8.72 o 3 4 0 501.04 502.36 12.44 o 4 4 0 163.54 164.94 5.68 o 5 4 0 17.45 15.62 2.51 o 6 4 0 287.81 287.60 12.74 o 7 4 0 2.49 2.17 3.12 o 8 4 0 108.10 98.78 11.20 o 9 4 0 414.75 392.07 8.91 o 10 4 0 339.31 345.54 8.49 o 11 4 0 63.74 60.58 4.03 o 12 4 0 246.16 228.13 7.27 o 13 4 0 16.87 26.22 7.07 o 14 4 0 6.29 4.72 2.48 o 15 4 0 21.98 30.65 5.83 o 16 4 0 20.87 34.03 3.54 o 17 4 0 5.06 2.64 2.57 o 18 4 0 1.09 3.82 2.57 o 19 4 0 45.10 49.20 4.45 o 20 4 0 9.05 13.38 2.73 o 21 4 0 1.86 -0.71 2.83 o 22 4 0 1.84 -0.30 3.99 o 23 4 0 17.73 27.65 7.40 o 24 4 0 21.02 22.40 4.56 o 25 4 0 2.55 -1.18 3.11 o 26 4 0 6.69 3.41 3.98 o 1 5 0 211.62 210.49 7.05 o 2 5 0 31.39 28.53 3.49 o 3 5 0 115.03 124.21 5.61 o 4 5 0 17.33 14.70 3.16 o 5 5 0 17.06 16.44 2.48 o 6 5 0 10.99 7.23 3.74 o 7 5 0 1.70 1.05 2.52 o 8 5 0 135.09 114.05 7.71 o 9 5 0 19.35 13.62 3.09 o 10 5 0 22.23 14.32 3.26 o 11 5 0 140.41 139.88 7.17 o 12 5 0 87.15 91.95 8.23 o 13 5 0 11.65 18.08 3.43 o 14 5 0 75.63 66.19 5.21 o 15 5 0 152.08 155.65 7.29 o 16 5 0 0.51 3.80 3.09 o 17 5 0 6.84 17.15 3.13 o 18 5 0 8.11 6.67 3.27 o 19 5 0 0.17 -3.20 3.20 o 20 5 0 0.91 -0.57 3.38 o 21 5 0 59.35 62.84 11.46 o 22 5 0 0.08 5.45 3.41 o 0 6 0 0.01 6.55 3.86 o 1 6 0 50.02 48.01 4.58 o 2 6 0 147.79 131.87 6.62 o 3 6 0 0.43 -3.10 3.10 o 4 6 0 0.15 -0.53 3.55 o 5 6 0 5.43 3.49 3.07 o 6 6 0 34.32 30.56 3.42 o 7 6 0 5.69 6.58 3.02 o 8 6 0 122.58 131.99 11.30 o 9 6 0 33.92 53.78 4.83 o 10 6 0 0.78 -1.48 3.21 o 11 6 0 71.84 69.23 5.70 o 12 6 0 52.85 53.36 5.35 o 13 6 0 0.91 -1.30 3.31 o 14 6 0 11.43 18.55 4.55 o 15 6 0 112.38 119.43 12.49 o 16 6 0 6.27 6.41 7.76 o 17 6 0 3.74 5.44 3.74 o 1 7 0 37.68 39.47 5.20 o 2 7 0 4.68 6.33 3.41 o 3 7 0 0.12 4.90 2.81 o 4 7 0 3.54 9.02 3.44 o 5 7 0 12.30 17.07 3.99 o 6 7 0 22.77 26.15 4.09 o 7 7 0 40.89 36.39 4.79 o 8 7 0 6.74 6.38 3.98 o 2 0 1 673.12 697.13 11.22 o 4 0 1 9452.28 8626.88 82.06 o 6 0 1 2249.26 2351.24 11.57 o 8 0 1 951.96 948.47 8.28 o 10 0 1 249.31 257.28 6.51 o 12 0 1 1018.24 1035.19 10.58 o 14 0 1 999.49 1013.68 11.46 o 16 0 1 611.02 609.30 9.76 o 18 0 1 1360.96 1387.67 15.53 o 20 0 1 330.86 323.15 8.50 o 22 0 1 148.84 133.67 6.21 o 24 0 1 121.83 125.17 6.30 o 26 0 1 41.25 43.71 4.41 o 28 0 1 60.93 61.37 5.52 o 30 0 1 44.75 46.36 5.35 o 0 1 1 1180.06 1197.00 10.78 o 1 1 1 759.61 768.61 7.69 o 2 1 1 277.49 281.59 4.40 o 3 1 1 4371.07 3996.07 67.64 o 4 1 1 3556.39 3335.57 62.14 o 5 1 1 4464.45 4064.05 64.94 o 6 1 1 8160.51 7800.42 140.67 o 7 1 1 474.81 504.13 6.64 o 8 1 1 337.58 366.45 5.48 o 9 1 1 254.45 236.84 4.66 o 10 1 1 436.90 426.36 9.94 o 11 1 1 531.10 563.70 13.70 o 12 1 1 179.68 199.09 5.16 o 13 1 1 112.26 103.10 4.01 o 14 1 1 137.67 131.58 7.34 o 15 1 1 146.33 138.17 4.81 o 16 1 1 35.71 31.46 3.94 o 17 1 1 72.48 71.78 4.00 o 18 1 1 76.72 72.11 4.40 o 19 1 1 19.50 15.21 2.90 o 20 1 1 95.04 89.53 7.58 o 21 1 1 106.94 106.34 5.58 o 22 1 1 81.67 69.52 5.31 o 23 1 1 203.90 198.84 7.77 o 24 1 1 61.94 58.87 4.92 o 25 1 1 1.69 4.29 4.49 o 26 1 1 20.32 19.44 3.67 o 27 1 1 4.96 6.16 3.95 o 28 1 1 32.05 42.98 11.00 o 29 1 1 26.67 25.12 5.46 o 30 1 1 9.46 11.94 13.87 o 1 2 1 109.09 102.82 3.00 o 2 2 1 256.25 268.47 4.77 o 3 2 1 401.37 412.82 5.89 o 4 2 1 81.49 90.00 2.86 o 5 2 1 99.11 94.73 3.08 o 6 2 1 448.46 484.30 6.78 o 7 2 1 1030.96 1116.98 23.83 o 8 2 1 352.00 397.62 6.53 o 9 2 1 1516.50 1543.91 13.17 o 10 2 1 82.50 75.83 3.42 o 11 2 1 448.87 443.62 17.66 o 12 2 1 10.61 9.20 2.01 o 13 2 1 296.25 259.38 6.43 o 14 2 1 36.54 40.49 3.15 o 15 2 1 346.21 337.26 8.26 o 16 2 1 64.77 63.84 3.95 o 17 2 1 228.18 168.70 112.61 o 18 2 1 3.22 0.51 4.43 o 19 2 1 515.46 555.83 11.06 o 20 2 1 263.26 274.80 8.37 o 21 2 1 6.57 3.39 3.09 o 22 2 1 63.00 60.17 4.99 o 23 2 1 135.39 148.76 6.95 o 24 2 1 49.22 46.64 7.69 o 25 2 1 107.34 109.79 15.39 o 26 2 1 8.68 2.46 3.86 o 27 2 1 4.31 5.45 3.33 o 28 2 1 29.45 31.45 4.53 o 29 2 1 15.74 23.15 5.79 o 0 3 1 878.84 881.74 14.73 o 1 3 1 420.34 439.85 7.38 o 2 3 1 434.19 438.19 7.41 o 3 3 1 354.24 401.34 7.12 o 4 3 1 979.44 944.43 13.11 o 5 3 1 487.07 483.05 7.98 o 6 3 1 195.89 191.82 5.20 o 7 3 1 109.33 103.96 4.12 o 8 3 1 588.43 569.99 9.61 o 9 3 1 7.25 6.72 2.06 o 10 3 1 184.75 179.69 5.71 o 11 3 1 97.72 107.00 4.57 o 12 3 1 168.11 155.08 5.62 o 13 3 1 23.18 24.08 2.52 o 14 3 1 19.69 26.13 2.86 o 15 3 1 20.68 22.83 4.15 o 16 3 1 232.77 224.74 7.67 o 17 3 1 39.14 33.84 4.40 o 18 3 1 89.56 87.02 5.22 o 19 3 1 7.32 7.60 6.10 o 20 3 1 16.06 14.93 3.52 o 21 3 1 19.39 14.24 3.07 o 22 3 1 21.09 19.12 3.66 o 23 3 1 16.52 17.66 3.54 o 24 3 1 2.38 2.73 3.19 o 25 3 1 6.89 0.11 5.25 o 26 3 1 40.50 45.14 7.83 o 27 3 1 27.77 35.80 4.64 o 28 3 1 27.44 35.28 7.60 o 1 4 1 66.60 62.79 3.69 o 2 4 1 35.60 35.91 2.88 o 3 4 1 102.37 101.67 6.85 o 4 4 1 36.23 41.80 3.03 o 5 4 1 99.21 92.60 4.54 o 6 4 1 8.46 12.05 5.09 o 7 4 1 34.66 34.14 3.41 o 8 4 1 492.13 459.99 9.59 o 9 4 1 253.29 251.20 15.57 o 10 4 1 194.12 196.48 6.59 o 11 4 1 33.84 34.72 3.59 o 12 4 1 42.44 38.86 4.12 o 13 4 1 102.91 97.20 6.99 o 14 4 1 131.45 125.04 5.78 o 15 4 1 20.83 17.99 3.44 o 16 4 1 26.67 27.26 3.66 o 17 4 1 143.07 159.21 7.26 o 18 4 1 90.58 79.38 5.81 o 19 4 1 6.34 14.63 3.30 o 20 4 1 74.33 84.41 7.66 o 21 4 1 71.56 90.76 5.89 o 22 4 1 14.61 8.18 3.76 o 23 4 1 17.56 18.29 3.93 o 24 4 1 60.30 54.46 5.92 o 25 4 1 8.83 9.66 6.56 o 0 5 1 76.80 75.85 6.17 o 1 5 1 77.90 76.87 4.71 o 2 5 1 8.43 9.87 3.02 o 3 5 1 222.00 223.11 9.80 o 4 5 1 53.73 57.42 4.21 o 5 5 1 174.44 168.44 6.70 o 6 5 1 83.20 78.46 5.02 o 7 5 1 47.71 50.16 4.62 o 8 5 1 182.76 178.56 13.07 o 9 5 1 43.07 42.79 4.40 o 10 5 1 100.26 87.52 5.61 o 11 5 1 56.91 51.96 4.37 o 12 5 1 26.65 34.72 3.84 o 13 5 1 10.76 23.42 6.43 o 14 5 1 72.43 67.51 5.19 o 15 5 1 36.16 47.54 4.63 o 16 5 1 7.74 8.84 3.17 o 17 5 1 1.63 -2.34 3.30 o 18 5 1 16.53 9.42 4.33 o 19 5 1 14.18 19.72 8.07 o 20 5 1 0.14 -3.41 3.43 o 21 5 1 7.17 4.36 4.03 o 22 5 1 24.27 32.96 10.26 o 1 6 1 2.85 0.11 2.93 o 2 6 1 84.66 83.07 5.74 o 3 6 1 41.69 43.38 4.20 o 4 6 1 40.67 42.20 4.96 o 5 6 1 60.81 65.42 5.38 o 6 6 1 62.97 58.58 7.10 o 7 6 1 16.09 19.60 3.79 o 8 6 1 15.49 17.57 5.20 o 9 6 1 11.27 16.81 3.71 o 10 6 1 37.93 38.43 5.67 o 11 6 1 3.27 3.43 6.63 o 12 6 1 20.65 21.26 5.09 o 13 6 1 48.63 45.20 7.52 o 14 6 1 27.17 32.01 4.77 o 15 6 1 12.39 21.47 4.05 o 16 6 1 31.49 40.33 5.03 o 17 6 1 18.34 23.39 5.79 o 0 7 1 3.39 5.89 4.48 o 1 7 1 9.00 11.41 5.03 o 2 7 1 25.29 26.84 4.49 o 3 7 1 7.39 3.34 6.61 o 4 7 1 10.02 13.59 4.07 o 5 7 1 8.00 5.56 6.42 o 6 7 1 6.42 8.33 3.67 o 0 0 2 1605.25 1636.60 15.48 o 2 0 2 3493.86 3649.72 71.42 o 4 0 2 981.12 958.66 8.72 o 6 0 2 501.06 503.22 8.75 o 8 0 2 1033.47 1080.40 17.01 o 10 0 2 1347.94 1336.40 12.37 o 12 0 2 558.40 574.51 8.76 o 14 0 2 927.82 914.82 21.04 o 16 0 2 56.59 53.29 3.85 o 18 0 2 304.49 313.16 8.18 o 20 0 2 197.93 217.90 7.21 o 22 0 2 11.57 20.71 4.33 o 24 0 2 57.53 56.35 4.71 o 26 0 2 3.98 0.02 3.69 o 28 0 2 117.52 110.51 7.36 o 30 0 2 16.47 20.25 4.24 o 1 1 2 308.78 300.92 5.58 o 2 1 2 704.05 770.29 7.96 o 3 1 2 447.06 473.15 6.34 o 4 1 2 239.48 275.47 13.37 o 5 1 2 138.47 152.59 3.82 o 6 1 2 71.58 75.80 2.82 o 7 1 2 299.87 320.13 5.72 o 8 1 2 492.29 511.68 7.55 o 9 1 2 1622.76 1701.31 13.80 o 10 1 2 872.06 862.60 15.90 o 11 1 2 381.35 407.81 16.01 o 12 1 2 91.81 96.37 3.97 o 13 1 2 95.40 88.34 3.96 o 14 1 2 115.23 114.36 4.60 o 15 1 2 309.99 303.89 7.35 o 16 1 2 99.38 88.85 5.12 o 17 1 2 335.52 337.07 8.72 o 18 1 2 92.06 76.67 8.94 o 19 1 2 179.34 180.94 6.94 o 20 1 2 188.86 204.10 7.32 o 21 1 2 73.05 62.99 7.17 o 22 1 2 119.69 128.63 16.46 o 23 1 2 162.28 156.11 7.46 o 24 1 2 77.87 77.50 6.15 o 25 1 2 54.37 56.81 5.48 o 26 1 2 2.15 -3.60 3.91 o 27 1 2 19.60 24.05 4.17 o 28 1 2 31.41 40.35 4.91 o 29 1 2 19.17 26.73 4.43 o 0 2 2 729.53 797.54 12.97 o 1 2 2 694.38 632.31 9.44 o 2 2 2 407.63 418.28 6.83 o 3 2 2 929.31 940.13 10.13 o 4 2 2 147.32 151.72 4.44 o 5 2 2 1431.89 1457.59 29.71 o 6 2 2 380.44 411.70 16.04 o 7 2 2 283.08 286.48 9.17 o 8 2 2 480.87 482.04 8.03 o 9 2 2 671.62 607.31 9.31 o 10 2 2 760.62 770.47 10.58 o 11 2 2 294.82 286.77 13.49 o 12 2 2 418.74 420.06 8.43 o 13 2 2 36.63 35.93 3.90 o 14 2 2 126.98 128.81 9.17 o 15 2 2 187.00 186.10 6.14 o 16 2 2 141.18 128.59 5.42 o 17 2 2 39.96 32.60 3.61 o 18 2 2 34.62 31.78 3.66 o 19 2 2 35.96 36.95 3.89 o 20 2 2 9.06 8.24 9.07 o 21 2 2 41.50 39.67 8.41 o 22 2 2 105.12 95.86 6.22 o 23 2 2 86.38 98.47 6.28 o 24 2 2 1.81 -0.73 3.43 o 25 2 2 8.72 7.96 3.73 o 26 2 2 12.87 11.44 3.30 o 27 2 2 16.83 21.68 4.00 o 28 2 2 29.74 34.01 4.73 o 1 3 2 474.42 490.12 8.45 o 2 3 2 110.49 108.45 4.30 o 3 3 2 185.29 202.87 5.58 o 4 3 2 229.73 228.40 5.96 o 5 3 2 38.38 37.41 6.68 o 6 3 2 104.35 106.53 4.29 o 7 3 2 27.38 33.48 2.85 o 8 3 2 78.62 78.91 3.80 o 9 3 2 102.21 99.02 4.57 o 10 3 2 28.38 29.39 3.05 o 11 3 2 147.64 150.31 7.05 o 12 3 2 212.54 206.16 6.62 o 13 3 2 206.93 199.60 8.19 o 14 3 2 252.70 225.94 8.00 o 15 3 2 166.16 156.50 7.76 o 16 3 2 74.14 78.97 5.26 o 17 3 2 44.90 40.03 4.08 o 18 3 2 160.25 182.20 7.16 o 19 3 2 105.54 90.31 6.03 o 20 3 2 77.64 73.41 5.60 o 21 3 2 12.08 10.65 4.58 o 22 3 2 42.65 46.38 5.85 o 23 3 2 21.37 21.18 4.34 o 24 3 2 36.72 32.83 7.58 o 25 3 2 5.39 -0.33 3.79 o 26 3 2 33.93 31.88 5.01 o 27 3 2 15.21 20.76 7.32 o 0 4 2 220.28 203.48 9.33 o 1 4 2 18.56 19.22 2.78 o 2 4 2 45.93 50.24 6.26 o 3 4 2 305.12 302.57 8.03 o 4 4 2 299.78 284.35 9.16 o 5 4 2 186.18 187.60 6.51 o 6 4 2 183.53 180.20 9.25 o 7 4 2 136.50 145.19 5.90 o 8 4 2 241.79 215.65 7.23 o 9 4 2 24.98 22.38 3.44 o 10 4 2 113.03 106.74 5.53 o 11 4 2 102.44 105.85 7.07 o 12 4 2 23.88 31.18 6.64 o 13 4 2 30.47 35.90 3.56 o 14 4 2 12.17 7.45 3.78 o 15 4 2 15.75 7.80 3.44 o 16 4 2 19.84 16.62 3.49 o 17 4 2 108.30 105.52 6.44 o 18 4 2 13.53 18.99 4.41 o 19 4 2 2.59 3.09 3.09 o 20 4 2 38.46 37.18 4.48 o 21 4 2 6.14 5.90 3.65 o 22 4 2 50.07 59.48 6.10 o 23 4 2 14.31 19.91 4.19 o 24 4 2 12.63 7.18 4.22 o 1 5 2 123.59 113.99 5.78 o 2 5 2 36.65 35.78 3.97 o 3 5 2 34.20 35.87 3.76 o 4 5 2 233.96 219.05 10.41 o 5 5 2 23.44 24.54 3.33 o 6 5 2 65.88 64.85 4.92 o 7 5 2 71.40 62.51 5.23 o 8 5 2 123.50 116.86 6.44 o 9 5 2 17.79 17.91 3.28 o 10 5 2 44.20 34.63 8.19 o 11 5 2 43.65 37.44 4.70 o 12 5 2 17.47 13.53 3.69 o 13 5 2 53.58 53.17 4.90 o 14 5 2 18.39 23.76 5.09 o 15 5 2 49.32 63.18 5.16 o 16 5 2 13.83 13.05 3.93 o 17 5 2 25.36 23.01 4.22 o 18 5 2 3.73 6.35 3.69 o 19 5 2 61.32 81.39 6.57 o 20 5 2 20.42 19.93 5.13 o 0 6 2 88.85 87.94 8.16 o 1 6 2 51.09 45.73 4.92 o 2 6 2 22.38 28.65 3.63 o 3 6 2 7.02 6.37 3.19 o 4 6 2 5.16 6.59 6.42 o 5 6 2 13.38 15.95 4.31 o 6 6 2 16.58 16.89 3.58 o 7 6 2 33.22 34.83 4.37 o 8 6 2 9.23 16.57 3.08 o 9 6 2 2.89 1.96 3.15 o 10 6 2 3.93 4.46 3.47 o 11 6 2 5.24 7.42 3.33 o 12 6 2 33.25 36.70 4.61 o 13 6 2 6.02 1.44 4.02 o 14 6 2 0.20 3.46 2.93 o 15 6 2 4.62 -2.62 5.68 o 2 0 3 787.69 921.07 29.19 o 4 0 3 292.69 283.45 6.06 o 6 0 3 192.73 197.28 5.18 o 8 0 3 69.74 70.15 3.51 o 10 0 3 214.01 202.97 5.86 o 12 0 3 474.78 477.58 9.20 o 14 0 3 1433.96 1474.15 16.82 o 16 0 3 106.39 100.47 5.11 o 18 0 3 7.20 6.14 2.23 o 20 0 3 177.73 183.11 16.95 o 22 0 3 68.19 63.43 5.37 o 24 0 3 124.51 127.97 7.07 o 26 0 3 51.67 50.96 5.43 o 28 0 3 73.48 87.16 6.52 o 0 1 3 428.33 436.51 10.64 o 1 1 3 580.16 599.17 8.73 o 2 1 3 135.70 136.20 4.44 o 3 1 3 130.82 112.78 4.10 o 4 1 3 687.78 684.04 9.45 o 5 1 3 596.25 609.48 18.83 o 6 1 3 41.36 48.38 3.00 o 7 1 3 116.03 111.59 4.35 o 8 1 3 682.60 700.07 10.22 o 9 1 3 508.25 465.34 16.85 o 10 1 3 25.35 29.66 4.65 o 11 1 3 269.05 265.52 7.00 o 12 1 3 15.05 16.12 2.51 o 13 1 3 10.26 8.86 2.20 o 14 1 3 49.40 50.03 3.72 o 15 1 3 17.24 18.27 3.08 o 16 1 3 313.70 303.98 8.56 o 17 1 3 5.34 6.25 2.94 o 18 1 3 173.43 174.59 6.99 o 19 1 3 1.48 1.64 4.02 o 20 1 3 21.47 22.63 7.03 o 21 1 3 7.77 7.48 3.42 o 22 1 3 20.07 27.89 3.99 o 23 1 3 20.87 18.90 3.95 o 24 1 3 6.67 6.06 4.80 o 25 1 3 4.44 5.95 3.51 o 26 1 3 28.68 26.90 5.18 o 27 1 3 60.53 46.17 7.20 o 1 2 3 97.47 101.36 4.08 o 2 2 3 10.26 11.04 2.09 o 3 2 3 210.43 216.70 18.51 o 4 2 3 80.27 81.70 3.78 o 5 2 3 395.76 389.25 8.18 o 6 2 3 32.38 33.65 2.94 o 7 2 3 15.12 14.80 2.13 o 8 2 3 24.01 27.73 3.05 o 9 2 3 321.36 327.89 7.80 o 10 2 3 37.98 34.68 3.48 o 11 2 3 9.12 7.99 2.29 o 12 2 3 395.98 381.04 9.03 o 13 2 3 452.46 441.26 18.07 o 14 2 3 63.51 64.28 4.46 o 15 2 3 206.49 204.84 15.45 o 16 2 3 80.75 82.84 6.73 o 17 2 3 140.74 139.77 10.10 o 18 2 3 58.21 53.71 4.85 o 19 2 3 36.01 36.85 5.52 o 20 2 3 9.57 10.97 5.55 o 21 2 3 91.55 98.06 6.16 o 22 2 3 5.46 4.84 5.80 o 23 2 3 95.15 100.67 7.05 o 24 2 3 41.96 42.70 5.66 o 25 2 3 6.96 6.51 3.67 o 26 2 3 36.28 37.10 6.93 o 0 3 3 1317.18 1306.19 21.92 o 1 3 3 73.03 64.80 6.16 o 2 3 3 350.74 328.08 8.03 o 3 3 3 52.29 46.14 3.43 o 4 3 3 38.43 36.36 4.15 o 5 3 3 34.43 37.85 3.20 o 6 3 3 268.50 284.03 12.76 o 7 3 3 33.57 33.62 3.45 o 8 3 3 22.22 24.52 3.04 o 9 3 3 266.07 270.67 10.59 o 10 3 3 194.24 177.33 16.64 o 11 3 3 173.41 155.93 6.30 o 12 3 3 52.88 52.04 7.16 o 13 3 3 7.17 2.70 2.84 o 14 3 3 193.19 188.60 7.48 o 15 3 3 286.21 270.31 8.94 o 16 3 3 55.74 42.25 4.73 o 17 3 3 90.11 79.56 5.60 o 18 3 3 4.56 -3.31 3.55 o 19 3 3 13.13 7.08 4.29 o 20 3 3 21.42 14.89 3.69 o 21 3 3 6.63 3.17 3.26 o 22 3 3 9.89 12.64 3.99 o 23 3 3 42.27 44.54 5.35 o 24 3 3 13.49 16.15 5.00 o 1 4 3 214.67 214.90 10.51 o 2 4 3 166.13 177.24 15.36 o 3 4 3 50.93 54.84 4.13 o 4 4 3 212.26 197.33 10.78 o 5 4 3 18.73 19.60 3.19 o 6 4 3 31.25 28.06 5.46 o 7 4 3 78.72 81.39 4.94 o 8 4 3 3.92 7.82 2.59 o 9 4 3 106.59 96.28 5.42 o 10 4 3 105.18 89.81 5.80 o 11 4 3 61.82 57.48 4.64 o 12 4 3 15.52 17.01 3.54 o 13 4 3 2.16 2.51 5.75 o 14 4 3 39.34 44.63 4.40 o 15 4 3 61.41 57.30 5.59 o 16 4 3 38.65 39.96 6.37 o 17 4 3 31.16 25.47 4.68 o 18 4 3 40.39 39.55 5.60 o 19 4 3 28.87 30.68 4.56 o 20 4 3 20.06 16.67 4.04 o 21 4 3 0.29 -2.58 4.16 o 22 4 3 41.36 51.86 5.73 o 0 5 3 25.19 32.28 5.57 o 1 5 3 87.55 102.65 5.83 o 2 5 3 4.04 2.12 5.84 o 3 5 3 44.56 49.38 4.52 o 4 5 3 9.50 5.73 2.97 o 5 5 3 8.52 8.10 5.77 o 6 5 3 19.30 18.63 3.54 o 7 5 3 88.21 88.02 6.16 o 8 5 3 0.15 2.54 2.86 o 9 5 3 4.08 4.21 4.05 o 10 5 3 11.29 14.61 3.68 o 11 5 3 16.05 24.52 4.09 o 12 5 3 54.69 55.41 6.67 o 13 5 3 9.73 9.79 3.55 o 14 5 3 18.27 15.67 4.91 o 15 5 3 2.06 6.24 2.95 o 16 5 3 6.92 14.54 5.52 o 17 5 3 0.64 6.05 3.47 o 1 6 3 41.39 39.63 5.26 o 2 6 3 39.34 44.07 8.83 o 3 6 3 16.04 14.22 6.54 o 4 6 3 5.39 5.91 3.61 o 5 6 3 10.72 9.61 4.09 o 6 6 3 4.71 6.54 3.51 o 7 6 3 23.05 16.94 3.90 o 8 6 3 0.96 4.13 5.10 o 9 6 3 4.94 2.61 3.60 o 10 6 3 5.22 3.21 4.23 o 0 0 4 10.34 11.25 3.17 o 2 0 4 308.85 301.65 10.89 o 4 0 4 497.37 488.16 29.15 o 6 0 4 550.48 530.65 10.05 o 8 0 4 52.60 53.92 3.63 o 10 0 4 437.08 454.43 23.57 o 12 0 4 399.36 391.75 9.71 o 14 0 4 165.37 162.00 6.65 o 16 0 4 3.49 2.45 3.72 o 18 0 4 6.98 6.11 3.12 o 20 0 4 65.23 71.59 5.65 o 22 0 4 4.45 5.67 2.88 o 24 0 4 33.91 34.36 4.49 o 1 1 4 44.95 50.18 3.30 o 2 1 4 40.81 43.45 3.16 o 3 1 4 5.63 1.46 1.91 o 4 1 4 182.17 191.17 17.88 o 5 1 4 8.66 10.12 2.10 o 6 1 4 12.10 12.32 2.56 o 7 1 4 68.08 62.11 4.09 o 8 1 4 227.99 239.83 10.22 o 9 1 4 402.78 381.45 9.31 o 10 1 4 85.03 78.60 12.54 o 11 1 4 131.75 142.67 6.06 o 12 1 4 3.88 4.60 4.95 o 13 1 4 15.48 14.47 3.40 o 14 1 4 98.38 100.78 5.56 o 15 1 4 74.85 74.25 5.16 o 16 1 4 23.76 28.36 6.98 o 17 1 4 79.19 83.54 6.23 o 18 1 4 62.01 60.32 5.34 o 19 1 4 60.39 70.41 5.74 o 20 1 4 67.01 75.53 5.49 o 21 1 4 8.68 5.32 3.98 o 22 1 4 24.68 36.27 4.58 o 23 1 4 42.16 38.76 5.34 o 24 1 4 18.80 24.16 5.11 o 0 2 4 377.44 361.01 12.07 o 1 2 4 118.57 107.60 5.15 o 2 2 4 23.39 21.39 2.89 o 3 2 4 318.10 307.11 8.21 o 4 2 4 70.10 68.10 4.51 o 5 2 4 405.21 393.87 9.56 o 6 2 4 93.46 92.10 6.07 o 7 2 4 21.76 17.97 3.18 o 8 2 4 201.97 192.66 8.55 o 9 2 4 46.38 40.49 4.47 o 10 2 4 115.68 112.63 5.73 o 11 2 4 69.33 60.26 4.86 o 12 2 4 154.92 170.70 11.86 o 13 2 4 21.91 27.07 3.46 o 14 2 4 22.37 17.38 3.67 o 15 2 4 39.45 37.29 4.34 o 16 2 4 26.88 30.63 4.04 o 17 2 4 1.29 0.28 2.96 o 18 2 4 11.48 13.19 5.59 o 19 2 4 14.06 11.98 3.70 o 20 2 4 34.16 45.37 12.80 o 21 2 4 11.06 17.25 3.87 o 22 2 4 1.33 0.66 4.01 o 23 2 4 63.42 89.20 10.33 o 1 3 4 86.56 80.36 4.83 o 2 3 4 84.46 83.25 4.69 o 3 3 4 115.47 102.09 5.40 o 4 3 4 111.73 122.67 6.34 o 5 3 4 71.34 75.84 4.93 o 6 3 4 126.33 134.16 6.14 o 7 3 4 33.00 30.44 3.75 o 8 3 4 16.88 16.67 2.95 o 9 3 4 22.25 19.30 9.75 o 10 3 4 52.16 45.21 5.96 o 11 3 4 65.29 61.33 5.04 o 12 3 4 59.66 61.35 4.89 o 13 3 4 38.90 48.30 5.05 o 14 3 4 3.46 8.71 3.29 o 15 3 4 63.46 69.64 5.70 o 16 3 4 70.40 81.23 6.33 o 17 3 4 24.86 19.44 4.67 o 18 3 4 129.71 137.83 7.96 o 19 3 4 72.63 68.54 6.84 o 20 3 4 71.91 85.75 6.95 o 21 3 4 8.62 5.62 4.59 o 0 4 4 125.62 140.12 9.32 o 1 4 4 8.77 6.38 3.07 o 2 4 4 5.54 5.85 3.02 o 3 4 4 59.04 65.90 10.05 o 4 4 4 93.32 100.30 5.99 o 5 4 4 105.50 109.77 6.08 o 6 4 4 68.72 68.90 5.63 o 7 4 4 22.27 23.36 8.06 o 8 4 4 27.14 33.67 11.40 o 9 4 4 0.96 -2.82 2.82 o 10 4 4 2.68 8.34 3.32 o 11 4 4 6.37 6.04 3.08 o 12 4 4 29.47 27.07 4.67 o 13 4 4 21.86 24.68 6.03 o 14 4 4 1.61 1.27 3.45 o 15 4 4 28.59 26.73 8.32 o 16 4 4 3.14 5.37 4.97 o 17 4 4 36.42 34.20 5.16 o 18 4 4 34.17 34.66 5.67 o 1 5 4 15.42 12.27 3.58 o 2 5 4 6.17 5.23 4.87 o 3 5 4 3.63 1.81 3.74 o 4 5 4 33.12 35.45 4.52 o 5 5 4 20.19 20.55 4.21 o 6 5 4 34.99 52.28 5.16 o 7 5 4 2.31 2.27 3.36 o 8 5 4 0.89 2.24 3.17 o 9 5 4 22.86 32.37 6.40 o 10 5 4 19.35 31.65 6.19 o 11 5 4 8.97 1.53 3.97 o 12 5 4 7.84 11.69 3.33 o 2 0 5 2.89 2.50 2.77 o 4 0 5 155.85 141.10 11.55 o 6 0 5 4.80 4.61 2.81 o 8 0 5 165.39 166.91 7.41 o 10 0 5 22.70 22.97 4.67 o 12 0 5 77.27 83.19 6.11 o 14 0 5 138.44 141.88 12.39 o 16 0 5 17.12 20.30 4.29 o 18 0 5 60.71 68.42 5.79 o 20 0 5 35.55 30.98 5.41 o 0 1 5 252.94 251.75 11.98 o 1 1 5 69.58 64.99 4.92 o 2 1 5 0.88 1.12 2.56 o 3 1 5 200.67 182.75 7.53 o 4 1 5 113.92 119.67 6.15 o 5 1 5 72.10 65.33 7.06 o 6 1 5 202.69 188.55 7.78 o 7 1 5 131.45 123.80 6.70 o 8 1 5 5.24 4.39 3.85 o 9 1 5 52.10 47.18 4.68 o 10 1 5 81.52 78.66 5.89 o 11 1 5 56.86 51.18 6.50 o 12 1 5 7.45 8.57 3.23 o 13 1 5 4.42 3.28 3.60 o 14 1 5 16.14 11.96 4.17 o 15 1 5 8.63 8.76 3.45 o 16 1 5 2.74 5.38 3.22 o 17 1 5 11.13 14.28 3.75 o 18 1 5 44.80 41.09 6.89 o 19 1 5 2.02 0.00 5.65 o 20 1 5 3.59 3.15 4.15 o 1 2 5 33.97 31.61 7.51 o 2 2 5 11.38 13.46 5.67 o 3 2 5 21.82 23.21 3.40 o 4 2 5 124.61 114.01 7.26 o 5 2 5 5.02 4.17 2.94 o 6 2 5 47.94 48.00 4.57 o 7 2 5 53.11 59.03 5.58 o 8 2 5 161.56 162.80 7.57 o 9 2 5 103.01 107.11 6.61 o 10 2 5 68.94 71.33 6.24 o 11 2 5 29.17 29.46 4.23 o 12 2 5 14.51 13.80 3.65 o 13 2 5 46.47 55.70 5.10 o 14 2 5 6.40 5.58 3.88 o 15 2 5 64.41 79.20 6.63 o 16 2 5 30.11 39.66 10.10 o 17 2 5 17.85 18.01 5.48 o 18 2 5 4.72 4.35 4.61 o 0 3 5 47.60 56.11 7.53 o 1 3 5 42.02 42.36 4.62 o 2 3 5 67.68 72.71 5.36 o 3 3 5 7.02 0.29 3.47 o 4 3 5 44.62 41.60 4.72 o 5 3 5 31.50 33.64 4.56 o 6 3 5 72.98 74.88 15.00 o 7 3 5 14.18 11.66 4.53 o 8 3 5 34.44 39.18 4.77 o 9 3 5 14.90 14.15 3.88 o 10 3 5 8.77 10.89 3.39 o 11 3 5 29.72 32.21 4.76 o 12 3 5 20.86 27.56 5.42 o 13 3 5 7.70 7.85 4.09 o 14 3 5 4.37 2.66 3.92 o 15 3 5 8.81 15.30 3.93 o 16 3 5 38.79 52.12 12.20 o 1 4 5 3.76 2.36 3.10 o 2 4 5 13.87 12.79 6.02 o 3 4 5 24.25 29.54 4.48 o 4 4 5 1.85 3.12 3.48 o 5 4 5 15.36 17.46 4.37 o 6 4 5 3.61 11.68 5.40 o 7 4 5 1.82 -0.65 3.76 o 8 4 5 24.32 21.45 4.15 o 9 4 5 3.10 3.48 3.10 o 10 4 5 15.22 17.66 4.33 o 11 4 5 20.52 26.07 5.64 o 0 0 6 601.80 557.25 20.27 o 2 0 6 12.19 6.33 3.80 o 4 0 6 23.77 27.24 4.86 o 6 0 6 85.62 88.47 6.14 o 8 0 6 5.43 5.43 3.45 o 10 0 6 23.13 17.31 3.82 o 12 0 6 64.40 78.39 6.24 o 1 1 6 16.10 14.23 4.10 o 2 1 6 13.10 23.14 9.79 o 3 1 6 16.74 14.53 3.52 o 4 1 6 22.88 23.26 4.26 o 5 1 6 8.81 9.72 3.39 o 6 1 6 10.14 11.77 3.76 o 7 1 6 28.48 27.59 10.20 o 8 1 6 9.70 3.91 4.07 o 9 1 6 15.84 19.46 4.09 o 10 1 6 4.64 -3.57 4.14 o 11 1 6 4.18 3.32 3.70 o 12 1 6 29.57 24.41 5.00 o 0 2 6 50.55 51.84 7.57 o 1 2 6 73.63 71.06 8.82 o 2 2 6 42.61 34.30 10.40 o 3 2 6 0.25 -3.08 3.75 o 4 2 6 4.42 3.80 3.50 o 5 2 6 41.31 41.76 5.69 o 6 2 6 4.13 5.79 4.55 o 7 2 6 31.84 29.21 5.61 o 8 2 6 8.52 9.86 4.45 o 9 2 6 12.29 12.73 5.49 o 10 2 6 16.07 20.87 4.93 o 1 3 6 5.97 6.25 4.63 o 2 3 6 62.10 64.73 5.75 o 3 3 6 6.28 4.44 3.70 o