#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/76/2227615.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227615_Fobs loop_ _publ_author_name 'Guo, Hang-Ming' _publ_section_title ; Bis{[6-methoxy-2-(4-methylphenyl)iminiomethyl]phenolate-\k^2^O,O'}tris(nitrato-\k^2^O,O')europium(III) ; _journal_coeditor_code HG2728 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1445 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 98.165 _cell_angle_beta 101.665 _cell_angle_gamma 106.681 _cell_length_a 9.7603 _cell_length_b 10.0250 _cell_length_c 18.4227 _exptl_crystal_F_000 823.83 _reflns_d_resolution_high 0.7652 _[local]_cod_data_source_file hg2728Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' J in P1 New: P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 347.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 9426.51 11428.62 139.11 o 2 0 0 15040.65 15841.96 216.55 o 3 0 0 32.46 47.73 9.55 o 4 0 0 15005.63 15483.15 219.26 o 5 0 0 773.06 772.93 32.96 o 6 0 0 457.71 513.30 33.76 o 7 0 0 39.21 45.27 19.96 o 8 0 0 234.97 221.98 43.64 o 9 0 0 304.69 287.01 38.82 o 10 0 0 704.42 503.14 59.52 o 11 0 0 622.43 525.78 63.18 o -12 1 0 2.20 -12.23 37.74 o -11 1 0 35.54 30.82 35.08 o -10 1 0 214.98 207.05 42.55 o -9 1 0 679.83 699.66 46.65 o -8 1 0 1218.99 1317.96 55.21 o -7 1 0 2645.08 2702.55 123.08 o -6 1 0 3164.95 3127.57 64.78 o -5 1 0 4001.74 3886.19 69.12 o -4 1 0 4727.72 5057.71 80.21 o -3 1 0 1060.52 1198.46 34.78 o -2 1 0 3962.27 4051.35 82.18 o -1 1 0 8614.68 8685.30 137.87 o 0 1 0 6435.86 5741.02 81.77 o 1 1 0 3037.85 2681.56 63.78 o 2 1 0 383.94 360.41 15.37 o 3 1 0 95.66 111.38 11.14 o 4 1 0 4089.43 4176.98 63.34 o 5 1 0 4056.49 4165.45 66.23 o 6 1 0 1815.61 1773.10 62.30 o 7 1 0 1711.05 1812.06 68.31 o 8 1 0 1522.33 1543.34 70.35 o 9 1 0 1356.01 1279.52 112.88 o 10 1 0 711.82 695.45 73.16 o 11 1 0 373.38 352.96 89.08 o -12 2 0 396.25 221.99 81.28 o -11 2 0 520.94 506.85 48.91 o -10 2 0 1108.49 1109.93 63.56 o -9 2 0 1310.79 1442.94 57.47 o -8 2 0 2279.69 2326.46 67.03 o -7 2 0 1863.88 1976.71 56.17 o -6 2 0 1175.04 1230.93 28.48 o -5 2 0 867.94 859.50 40.03 o -4 2 0 1102.85 1155.25 31.51 o -3 2 0 480.56 477.19 30.59 o -2 2 0 2750.46 2920.45 64.74 o -1 2 0 209.63 236.40 13.64 o 0 2 0 16448.98 16069.12 198.93 o 1 2 0 5395.24 4769.76 80.50 o 2 2 0 3403.84 3410.19 58.50 o 3 2 0 12455.69 12573.46 152.78 o 4 2 0 13612.96 14319.17 149.45 o 5 2 0 5744.28 5750.75 89.54 o 6 2 0 2229.06 2204.20 84.31 o 7 2 0 2567.34 2507.15 71.11 o 8 2 0 661.05 657.27 54.84 o 9 2 0 328.51 266.21 54.38 o 10 2 0 5.14 0.43 42.66 o 11 2 0 5.85 70.40 50.96 o -12 3 0 356.55 353.09 84.78 o -11 3 0 137.80 63.43 57.31 o -10 3 0 3.36 76.54 53.94 o -9 3 0 0.04 13.36 42.82 o -8 3 0 256.75 314.63 51.19 o -7 3 0 764.30 824.31 29.20 o -6 3 0 2339.50 2451.04 47.50 o -5 3 0 2524.31 2849.95 51.73 o -4 3 0 6629.42 6951.39 104.80 o -3 3 0 9854.36 9244.72 119.14 o -2 3 0 17653.14 16595.60 207.01 o -1 3 0 11368.47 10708.98 159.82 o 0 3 0 4347.17 4162.39 67.59 o 1 3 0 4301.04 4223.02 79.69 o 2 3 0 5389.29 5448.53 79.49 o 3 3 0 3274.55 3344.93 53.32 o 4 3 0 193.65 168.20 20.76 o 5 3 0 28.14 65.66 19.58 o 6 3 0 839.01 820.19 39.47 o 7 3 0 306.28 294.59 41.91 o 8 3 0 751.53 668.06 68.16 o 9 3 0 525.32 384.42 113.93 o 10 3 0 413.23 365.51 68.05 o -12 4 0 53.31 99.63 73.54 o -11 4 0 187.62 79.78 56.68 o -10 4 0 419.38 467.45 75.79 o -9 4 0 836.14 961.37 82.40 o -8 4 0 2795.47 3136.54 106.69 o -7 4 0 2446.94 2685.39 88.69 o -6 4 0 2115.80 2262.28 48.25 o -5 4 0 5155.89 5407.65 88.47 o -4 4 0 5490.24 5404.00 77.03 o -3 4 0 6678.68 6609.46 96.05 o -2 4 0 947.62 906.06 26.04 o -1 4 0 173.96 180.72 12.73 o 0 4 0 232.53 299.63 17.29 o 1 4 0 3309.04 3501.93 66.89 o 2 4 0 1220.17 1185.46 29.55 o 3 4 0 1437.10 1419.88 32.21 o 4 4 0 2279.95 2389.39 66.43 o 5 4 0 332.20 416.93 37.43 o 6 4 0 3959.22 3923.98 99.01 o 7 4 0 2090.82 1995.59 104.45 o 8 4 0 1250.68 1028.00 149.14 o 9 4 0 443.97 449.68 72.84 o -12 5 0 392.40 350.96 82.90 o -11 5 0 393.32 514.15 80.03 o -10 5 0 502.65 587.31 77.66 o -9 5 0 874.21 957.00 82.40 o -8 5 0 293.98 272.10 41.29 o -7 5 0 184.14 248.75 51.56 o -6 5 0 24.87 29.58 13.16 o -5 5 0 348.55 421.73 16.72 o -4 5 0 490.93 398.36 21.31 o -3 5 0 3325.86 3036.96 59.38 o -2 5 0 4653.77 4436.18 80.05 o -1 5 0 3526.80 3481.69 51.63 o 0 5 0 2606.13 2626.52 47.66 o 1 5 0 4163.12 4091.67 57.23 o 2 5 0 5241.29 5061.68 67.79 o 3 5 0 2401.64 2392.42 53.22 o 4 5 0 2098.95 2029.02 84.14 o 5 5 0 3219.23 3235.98 88.92 o 6 5 0 464.13 464.80 41.78 o 7 5 0 130.90 158.41 31.96 o 8 5 0 13.24 -8.45 48.91 o 9 5 0 0.52 22.90 58.39 o -12 6 0 29.87 54.19 66.55 o -11 6 0 27.90 -12.98 57.81 o -10 6 0 38.95 46.70 54.19 o -9 6 0 1.20 -19.15 35.71 o -8 6 0 401.32 431.46 50.57 o -7 6 0 1577.32 1582.20 54.53 o -6 6 0 670.31 591.80 37.22 o -5 6 0 3595.19 3627.97 130.71 o -4 6 0 3914.87 3945.21 77.18 o -3 6 0 3609.01 3373.10 75.82 o -2 6 0 6079.62 5866.77 84.53 o -1 6 0 465.12 374.41 20.58 o 0 6 0 1120.66 992.57 28.66 o 1 6 0 341.71 319.88 21.05 o 2 6 0 657.41 623.12 32.50 o 3 6 0 371.15 315.89 43.86 o 4 6 0 1.07 -1.50 22.47 o 5 6 0 1.97 3.08 25.97 o 6 6 0 258.78 287.72 42.83 o 7 6 0 662.43 753.83 57.61 o 8 6 0 257.70 145.61 66.99 o -12 7 0 208.43 230.60 73.91 o -11 7 0 154.97 68.17 60.05 o -10 7 0 884.85 1074.94 178.48 o -9 7 0 788.74 876.33 74.79 o -8 7 0 1045.03 1024.59 75.76 o -7 7 0 1062.73 1031.83 50.25 o -6 7 0 1626.91 1629.55 79.99 o -5 7 0 1849.18 1767.21 66.95 o -4 7 0 380.98 323.10 35.93 o -3 7 0 144.85 82.05 17.81 o -2 7 0 33.62 11.85 16.18 o -1 7 0 2.03 -12.29 12.29 o 0 7 0 692.23 710.93 35.19 o 1 7 0 1324.39 1274.35 45.29 o 2 7 0 2847.21 2785.69 84.80 o 3 7 0 1750.96 1983.26 95.11 o 4 7 0 782.36 768.32 69.23 o 5 7 0 875.77 848.58 155.69 o 6 7 0 707.82 714.56 71.31 o 7 7 0 487.12 393.41 111.81 o -11 8 0 73.94 73.04 69.17 o -10 8 0 87.95 114.29 47.37 o -9 8 0 161.55 233.84 52.22 o -8 8 0 199.41 214.74 30.16 o -7 8 0 81.52 99.97 26.65 o -6 8 0 0.76 -11.32 23.03 o -5 8 0 204.52 217.67 33.10 o -4 8 0 825.70 837.58 43.92 o -3 8 0 585.42 505.87 40.91 o -2 8 0 1097.30 1144.05 42.55 o -1 8 0 1887.98 1934.04 56.09 o 0 8 0 2323.84 2314.78 63.30 o 1 8 0 1737.23 1973.47 68.19 o 2 8 0 1998.43 2091.32 79.22 o 3 8 0 922.10 974.42 77.28 o 4 8 0 528.20 490.47 67.67 o 5 8 0 88.53 54.56 59.80 o 6 8 0 0.46 57.93 59.06 o -11 9 0 16.02 25.28 50.87 o -10 9 0 80.51 55.89 53.87 o -9 9 0 145.83 158.57 63.18 o -8 9 0 171.12 146.83 35.93 o -7 9 0 384.78 430.01 42.63 o -6 9 0 904.82 951.25 59.84 o -5 9 0 732.51 729.99 55.62 o -4 9 0 308.64 317.96 33.22 o -3 9 0 870.24 957.14 40.39 o -2 9 0 781.40 857.05 41.11 o -1 9 0 506.23 574.53 47.27 o 0 9 0 122.01 138.30 29.54 o 1 9 0 1.67 21.19 31.31 o 2 9 0 8.14 11.64 33.57 o 3 9 0 31.92 -28.05 43.71 o 4 9 0 159.28 146.53 55.70 o 5 9 0 117.57 79.91 73.66 o -10 10 0 327.83 346.33 110.99 o -9 10 0 246.67 262.70 60.02 o -8 10 0 162.31 217.51 41.26 o -7 10 0 196.44 188.52 38.08 o -6 10 0 184.61 190.17 39.65 o -5 10 0 7.26 8.48 29.21 o -4 10 0 45.06 28.54 25.49 o -3 10 0 16.14 4.26 19.13 o -2 10 0 7.20 20.29 21.29 o -1 10 0 363.12 329.96 54.12 o 0 10 0 115.51 94.87 42.66 o 1 10 0 469.50 569.01 107.43 o 2 10 0 491.12 425.10 67.70 o 3 10 0 484.19 335.13 67.39 o 4 10 0 487.95 608.22 84.75 o -9 11 0 31.04 17.34 30.60 o -8 11 0 1.26 21.12 32.87 o -7 11 0 9.64 23.23 33.83 o -6 11 0 370.59 353.67 51.85 o -5 11 0 90.62 39.12 35.51 o -4 11 0 88.62 81.12 47.97 o -3 11 0 266.62 290.10 52.35 o -2 11 0 558.47 671.28 103.21 o -1 11 0 301.48 280.98 54.02 o 0 11 0 303.57 229.11 71.92 o 1 11 0 208.52 189.15 75.41 o 2 11 0 163.44 123.69 58.82 o -8 12 0 53.57 6.97 36.62 o -7 12 0 115.24 132.73 45.92 o -6 12 0 219.95 238.71 97.56 o -5 12 0 179.94 187.26 48.39 o -4 12 0 71.10 92.61 46.08 o -3 12 0 99.10 171.36 53.28 o -2 12 0 54.44 44.76 57.75 o -1 12 0 4.41 18.73 52.31 o 0 12 0 3.37 67.92 62.55 o 4 -13 1 112.76 161.33 57.11 o 0 -12 1 179.31 163.43 71.54 o 1 -12 1 196.44 222.99 67.67 o 2 -12 1 258.72 311.39 46.69 o 3 -12 1 93.74 116.95 47.85 o 4 -12 1 98.54 180.23 61.25 o 5 -12 1 28.46 27.43 39.48 o 6 -12 1 155.73 133.39 45.15 o 7 -12 1 41.87 82.34 49.19 o 8 -12 1 0.05 -36.58 36.58 o -3 -11 1 346.70 446.45 78.46 o -2 -11 1 181.11 170.81 60.05 o -1 -11 1 137.43 178.29 77.66 o 0 -11 1 64.23 109.12 66.30 o 1 -11 1 3.62 -17.21 37.52 o 2 -11 1 0.04 -12.63 26.05 o 3 -11 1 42.36 21.83 23.74 o 4 -11 1 7.29 14.00 28.88 o 5 -11 1 242.48 205.70 45.37 o 6 -11 1 198.68 168.89 43.50 o 7 -11 1 248.04 248.41 44.84 o 8 -11 1 145.83 169.96 43.92 o 9 -11 1 142.50 99.98 35.69 o -4 -10 1 8.48 -35.89 90.14 o -3 -10 1 10.88 -24.35 48.51 o -2 -10 1 74.35 -14.04 46.11 o -1 -10 1 60.71 53.66 35.45 o 0 -10 1 141.59 130.72 44.43 o 1 -10 1 404.67 418.95 40.42 o 2 -10 1 688.69 706.62 41.55 o 3 -10 1 985.25 1048.43 43.30 o 4 -10 1 296.93 288.63 36.22 o 5 -10 1 374.54 388.79 98.70 o 6 -10 1 706.10 727.05 85.69 o 7 -10 1 224.68 223.96 52.80 o 8 -10 1 54.82 27.20 28.17 o 9 -10 1 29.54 -3.26 28.05 o 10 -10 1 13.27 90.21 53.99 o -5 -9 1 188.54 84.53 68.29 o -4 -9 1 519.17 413.78 66.89 o -3 -9 1 627.06 701.24 75.13 o -2 -9 1 499.79 472.35 49.34 o -1 -9 1 927.19 828.19 57.45 o 0 -9 1 591.20 617.89 44.09 o 1 -9 1 457.95 538.92 37.82 o 2 -9 1 283.64 280.67 36.82 o 3 -9 1 435.59 449.52 29.42 o 4 -9 1 249.10 237.00 32.91 o 5 -9 1 34.71 11.69 25.91 o 6 -9 1 2.03 22.04 25.98 o 7 -9 1 85.24 84.38 52.92 o 8 -9 1 66.86 58.52 33.22 o 9 -9 1 98.34 105.73 45.94 o 10 -9 1 215.18 174.18 55.64 o 11 -9 1 119.25 77.96 61.80 o -6 -8 1 503.47 451.10 84.15 o -5 -8 1 636.58 672.21 97.89 o -4 -8 1 365.86 357.97 135.22 o -3 -8 1 419.04 463.60 60.16 o -2 -8 1 224.24 178.63 52.08 o -1 -8 1 241.66 240.26 43.43 o 0 -8 1 198.55 205.64 23.13 o 1 -8 1 458.06 484.55 33.17 o 2 -8 1 811.22 809.76 47.77 o 3 -8 1 424.89 421.53 50.04 o 4 -8 1 1487.77 1503.91 84.00 o 5 -8 1 1556.85 1636.69 77.78 o 6 -8 1 949.65 1045.28 58.38 o 7 -8 1 312.85 359.88 40.30 o 8 -8 1 457.55 424.92 79.91 o 9 -8 1 284.17 381.28 61.18 o 10 -8 1 611.54 574.43 149.89 o 11 -8 1 54.07 73.04 66.05 o -7 -7 1 15.50 11.45 46.82 o -6 -7 1 89.84 135.09 45.57 o -5 -7 1 41.94 57.72 40.05 o -4 -7 1 440.48 538.49 78.91 o -3 -7 1 552.72 605.23 59.45 o -2 -7 1 13.17 16.86 25.34 o -1 -7 1 1684.44 1626.29 46.96 o 0 -7 1 2320.78 2334.89 65.54 o 1 -7 1 1905.16 1942.69 49.46 o 2 -7 1 1527.61 1636.56 70.55 o 3 -7 1 3172.94 3178.08 72.34 o 4 -7 1 2507.45 2375.71 77.50 o 5 -7 1 744.10 687.34 45.61 o 6 -7 1 563.89 579.50 42.27 o 7 -7 1 31.07 -1.54 21.30 o 8 -7 1 9.10 30.37 22.78 o 9 -7 1 26.82 106.57 45.83 o 10 -7 1 1.47 53.22 41.01 o 11 -7 1 0.89 -26.34 57.18 o 12 -7 1 152.59 129.35 76.29 o -8 -6 1 234.31 174.04 64.12 o -7 -6 1 345.02 298.57 43.02 o -6 -6 1 1045.37 1033.87 58.65 o -5 -6 1 1776.46 1755.15 96.65 o -4 -6 1 2490.76 2574.02 100.23 o -3 -6 1 2863.62 2886.76 63.57 o -2 -6 1 3578.29 3713.37 71.75 o -1 -6 1 1742.32 1716.52 48.35 o 0 -6 1 389.86 350.83 20.88 o 1 -6 1 1827.85 1720.99 36.72 o 2 -6 1 1075.32 964.84 28.73 o 3 -6 1 540.40 465.18 32.43 o 4 -6 1 0.69 7.79 15.00 o 5 -6 1 2209.61 2266.79 58.12 o 6 -6 1 55.96 59.74 16.27 o 7 -6 1 709.96 806.73 43.17 o 8 -6 1 345.49 408.64 52.97 o 9 -6 1 1407.37 1693.74 98.76 o 10 -6 1 291.08 208.01 66.92 o 11 -6 1 530.71 486.93 84.65 o 12 -6 1 169.21 235.72 74.54 o -9 -5 1 730.24 533.21 215.56 o -8 -5 1 1077.11 1257.29 114.18 o -7 -5 1 1598.44 1586.12 91.65 o -6 -5 1 488.13 440.12 39.46 o -5 -5 1 628.67 676.48 52.48 o -4 -5 1 178.85 124.56 26.89 o -3 -5 1 6.41 9.95 12.84 o -2 -5 1 142.58 161.12 15.45 o -1 -5 1 1476.17 1544.57 38.63 o 0 -5 1 4780.66 4808.27 70.30 o 1 -5 1 2993.11 2746.85 44.47 o 2 -5 1 7408.41 7103.64 82.46 o 3 -5 1 10019.47 9887.12 139.50 o 4 -5 1 4192.11 4155.02 71.94 o 5 -5 1 1303.13 1417.92 37.14 o 6 -5 1 1678.64 1818.37 57.40 o 7 -5 1 1797.22 1948.90 59.60 o 8 -5 1 1151.29 1347.73 76.08 o 9 -5 1 28.52 40.33 50.07 o 10 -5 1 22.64 133.09 61.93 o 11 -5 1 57.36 83.15 63.43 o 12 -5 1 0.50 29.96 64.42 o -10 -4 1 325.35 297.68 68.13 o -9 -4 1 84.22 113.49 55.39 o -8 -4 1 291.93 304.34 51.00 o -7 -4 1 22.46 39.34 30.46 o -6 -4 1 318.44 343.64 32.84 o -5 -4 1 1242.45 1238.90 50.45 o -4 -4 1 1917.28 1915.20 58.24 o -3 -4 1 3720.78 3814.32 61.78 o -2 -4 1 4070.61 3744.96 67.54 o -1 -4 1 2848.88 2529.57 47.44 o 0 -4 1 5698.70 5352.20 76.57 o 1 -4 1 14934.37 14583.01 157.80 o 2 -4 1 17861.92 18013.22 187.80 o 3 -4 1 4318.46 4473.52 76.05 o 4 -4 1 1837.98 1853.64 35.93 o 5 -4 1 331.59 284.58 22.56 o 6 -4 1 929.12 915.31 43.59 o 7 -4 1 221.69 219.92 33.71 o 8 -4 1 33.07 33.16 20.42 o 9 -4 1 561.05 527.63 77.28 o 10 -4 1 242.76 296.15 72.17 o 11 -4 1 307.28 299.77 76.16 o 12 -4 1 414.83 370.19 84.40 o -10 -3 1 55.01 77.47 49.69 o -9 -3 1 441.44 319.63 58.76 o -8 -3 1 1188.41 1210.62 73.34 o -7 -3 1 2634.44 2676.27 107.71 o -6 -3 1 2836.00 2841.42 116.96 o -5 -3 1 3480.33 3585.67 78.21 o -4 -3 1 8196.46 7834.70 119.78 o -3 -3 1 8288.30 7942.92 104.71 o -2 -3 1 5373.96 5469.35 98.20 o -1 -3 1 2719.11 2735.84 58.76 o 0 -3 1 3531.61 3460.84 59.10 o 1 -3 1 426.63 436.43 18.30 o 2 -3 1 2591.54 2920.82 49.97 o 3 -3 1 9028.18 9657.25 126.43 o 4 -3 1 2345.32 2385.18 42.62 o 5 -3 1 2854.00 2797.14 64.27 o 6 -3 1 4700.23 4429.13 91.86 o 7 -3 1 5230.77 5325.89 109.80 o 8 -3 1 1912.93 2081.67 146.70 o 9 -3 1 1599.19 1699.36 70.89 o 10 -3 1 1000.86 1059.17 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