#------------------------------------------------------------------------------
#$Date: 2010-12-22 21:36:50 +0200 (Wed, 22 Dec 2010) $
#$Revision: 5269 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2227625.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2227625_Fobs
loop_
_publ_author_name
'Ha, Kwang'
_publ_section_title
;
 Bis(acridine-\k<i>N</i>)dibromidoplatinum(II)
;
_journal_coeditor_code           HY2340
_journal_issue                   9
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m1142
_journal_volume                  66
_journal_year                    2010
_space_group_IT_number           15
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.000
_cell_angle_beta                 115.017
_cell_angle_gamma                90.000
_cell_length_a                   16.0256
_cell_length_b                   8.6845
_cell_length_c                   17.0646
_exptl_crystal_F_000             1344.00
_reflns_d_resolution_high        0.8106
_[local]_cod_data_source_file    hy2340Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' [PtBr2(acr)2]'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            529.14
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 103283.16 118891.07 3617.79 o
4 0 0 214136.59 230179.58 3706.56 o
6 0 0 173466.78 176877.77 3000.11 o
8 0 0 121469.34 123698.09 2291.17 o
10 0 0 73042.53 72186.00 2124.51 o
12 0 0 14561.82 13561.55 871.86 o
14 0 0 61272.84 57968.73 3516.13 o
16 0 0 16265.47 14654.24 1155.91 o
1 1 0 181175.94 195275.92 2414.02 o
3 1 0 279990.50 302486.75 3380.06 o
5 1 0 194052.55 205260.97 2668.81 o
7 1 0 135682.23 138540.58 1964.58 o
9 1 0 93476.51 95249.57 1355.38 o
11 1 0 84991.18 85544.40 1752.07 o
13 1 0 18405.83 18776.97 761.96 o
15 1 0 20790.37 21244.91 1040.36 o
17 1 0 12813.25 11285.57 828.33 o
0 2 0 254846.98 274732.03 5504.88 o
2 2 0 208148.16 222386.75 2787.32 o
4 2 0 142282.89 149073.67 1808.64 o
6 2 0 133467.80 139002.83 1955.31 o
8 2 0 79761.20 78201.24 1293.04 o
10 2 0 55324.78 55245.69 1077.53 o
12 2 0 40043.53 38051.48 1068.03 o
14 2 0 27428.74 26731.24 1144.37 o
16 2 0 16499.78 16558.99 968.12 o
1 3 0 118640.59 123248.16 1923.40 o
3 3 0 119496.31 122282.47 1922.75 o
5 3 0 113170.23 117127.66 1536.70 o
7 3 0 54932.02 51963.23 864.95 o
9 3 0 57261.00 57263.77 1083.33 o
11 3 0 36480.75 38388.89 1037.88 o
13 3 0 27891.11 26796.48 1118.07 o
15 3 0 16009.03 14877.68 905.68 o
17 3 0 11648.27 9806.67 1446.84 o
0 4 0 56156.93 54708.04 1525.52 o
2 4 0 69912.43 70897.23 1110.79 o
4 4 0 67747.12 65999.84 1111.11 o
6 4 0 44525.49 43732.19 908.56 o
8 4 0 38864.03 38352.43 751.03 o
10 4 0 31002.68 31327.61 919.93 o
12 4 0 27077.05 27856.54 1655.96 o
14 4 0 19634.39 19728.71 3281.29 o
16 4 0 13920.15 15698.41 2066.52 o
1 5 0 20173.40 19652.74 518.05 o
3 5 0 27893.94 27975.89 560.39 o
5 5 0 29426.57 29159.66 692.26 o
7 5 0 31644.67 29710.27 936.00 o
9 5 0 20266.08 19981.67 748.43 o
11 5 0 22151.64 23014.74 1012.97 o
13 5 0 18069.86 19113.48 1872.56 o
15 5 0 11562.60 12039.04 1119.11 o
0 6 0 14676.78 15186.75 746.38 o
2 6 0 13000.35 13080.84 390.13 o
4 6 0 26993.21 26916.97 732.91 o
6 6 0 6744.75 6126.41 465.49 o
8 6 0 7113.02 7004.19 471.89 o
10 6 0 13298.36 13247.82 669.31 o
12 6 0 13402.96 13207.70 827.38 o
14 6 0 11507.18 12203.48 1108.88 o
1 7 0 5163.64 5687.46 419.51 o
3 7 0 5402.72 5729.60 294.08 o
5 7 0 3113.34 3101.60 352.72 o
7 7 0 18209.15 16823.04 727.15 o
9 7 0 6441.07 6269.50 486.40 o
11 7 0 9295.24 9337.24 702.73 o
13 7 0 7618.97 8363.97 997.20 o
0 8 0 6354.92 6438.87 667.94 o
2 8 0 2295.93 2081.73 252.67 o
4 8 0 3547.93 3453.70 491.65 o
6 8 0 3849.62 3916.18 546.13 o
8 8 0 4673.89 4368.80 479.46 o
10 8 0 7652.79 8822.68 781.07 o
1 9 0 3660.45 3672.47 529.67 o
3 9 0 1965.63 2385.73 448.57 o
5 9 0 2694.14 2547.57 480.12 o
7 9 0 3478.50 4325.44 600.30 o
9 9 0 3550.42 3503.98 2447.36 o
0 10 0 2445.90 3537.64 1043.86 o
2 10 0 2203.30 2121.78 591.15 o
4 10 0 3092.37 1888.96 1332.26 o
6 10 0 1914.36 1085.64 317.12 o
-17 1 1 534.51 292.53 332.58 o
-15 1 1 179.14 151.71 221.52 o
-13 1 1 7022.80 7045.97 486.75 o
-11 1 1 77.71 -20.22 134.50 o
-9 1 1 3334.76 3553.81 182.98 o
-7 1 1 10323.44 10856.69 336.88 o
-5 1 1 847.73 969.20 109.58 o
-3 1 1 1306.65 1409.71 94.68 o
-1 1 1 504.28 642.45 52.16 o
1 1 1 22681.00 24963.52 547.38 o
3 1 1 4140.51 4321.33 175.00 o
5 1 1 83.24 201.70 78.45 o
7 1 1 404.91 486.28 105.03 o
9 1 1 2.56 -70.49 75.96 o
11 1 1 17.17 47.11 114.51 o
13 1 1 1968.03 1891.20 311.28 o
15 1 1 860.24 992.10 342.95 o
17 1 1 115.78 -8.54 376.40 o
-16 2 1 1421.87 1190.27 398.85 o
-14 2 1 1914.50 1897.85 608.68 o
-12 2 1 3184.57 3631.03 359.08 o
-10 2 1 5963.99 6319.31 391.37 o
-8 2 1 6214.05 6028.84 283.36 o
-6 2 1 37896.21 40374.26 672.00 o
-4 2 1 19699.94 19918.09 451.69 o
-2 2 1 23091.95 24050.04 446.35 o
0 2 1 6773.90 6573.63 181.13 o
2 2 1 19003.45 19427.70 532.97 o
4 2 1 1689.15 1706.64 123.64 o
6 2 1 5404.89 6473.81 257.71 o
8 2 1 573.94 585.26 120.37 o
10 2 1 25.33 -42.96 106.98 o
12 2 1 792.90 845.25 282.43 o
14 2 1 1086.07 894.50 331.87 o
16 2 1 674.18 352.07 404.45 o
-17 3 1 1302.56 225.58 378.52 o
-15 3 1 4336.56 3689.86 539.78 o
-13 3 1 4925.60 5741.72 569.20 o
-11 3 1 8952.58 8775.45 445.82 o
-9 3 1 16425.45 16675.41 510.95 o
-7 3 1 27600.15 27578.51 570.03 o
-5 3 1 15101.89 14131.63 357.70 o
-3 3 1 23355.49 24068.64 507.21 o
-1 3 1 26179.89 27577.23 524.95 o
1 3 1 11555.90 11442.07 357.65 o
3 3 1 5675.30 5810.67 197.32 o
5 3 1 5013.19 5185.14 213.31 o
7 3 1 349.29 371.83 99.16 o
9 3 1 571.87 648.07 128.78 o
11 3 1 460.58 601.57 201.67 o
13 3 1 1423.07 1590.27 358.17 o
15 3 1 2215.47 1960.62 418.11 o
-16 4 1 1381.86 527.74 486.32 o
-14 4 1 9272.08 7521.22 898.47 o
-12 4 1 6813.98 6940.74 470.42 o
-10 4 1 12875.79 13444.64 623.57 o
-8 4 1 15942.56 16185.12 455.31 o
-6 4 1 21277.43 20086.12 479.05 o
-4 4 1 28233.07 27313.71 607.63 o
-2 4 1 3687.38 3180.54 174.09 o
0 4 1 36556.41 37218.80 677.64 o
2 4 1 9503.58 9165.92 460.52 o
4 4 1 4028.99 4055.12 240.47 o
6 4 1 237.63 266.87 83.22 o
8 4 1 233.38 80.18 125.21 o
10 4 1 38.86 4.91 152.64 o
12 4 1 3147.15 3807.03 481.63 o
14 4 1 1601.77 1375.22 632.44 o
16 4 1 1490.78 1445.88 553.29 o
-15 5 1 3937.00 3015.83 695.54 o
-13 5 1 4015.30 4717.49 771.31 o
-11 5 1 8994.56 9390.59 642.74 o
-9 5 1 13138.80 12724.23 582.93 o
-7 5 1 11724.42 11730.53 447.92 o
-5 5 1 23572.55 23328.80 761.77 o
-3 5 1 18760.02 18593.20 445.82 o
-1 5 1 11348.50 11064.16 360.30 o
1 5 1 7711.45 7312.72 526.01 o
3 5 1 4958.56 4964.35 237.01 o
5 5 1 1792.39 1620.81 183.40 o
7 5 1 20.60 -28.87 135.01 o
9 5 1 320.17 400.08 228.92 o
11 5 1 11.50 -139.40 204.60 o
13 5 1 1627.82 1142.80 480.27 o
15 5 1 1523.92 1742.45 576.59 o
-14 6 1 2920.22 1973.20 643.96 o
-12 6 1 3949.59 3695.30 529.02 o
-10 6 1 5022.50 4721.48 463.64 o
-8 6 1 10597.17 10487.64 553.48 o
-6 6 1 4668.05 4703.45 311.67 o
-4 6 1 12325.31 12986.14 463.14 o
-2 6 1 8488.43 8509.19 317.37 o
0 6 1 7403.19 7269.58 290.87 o
2 6 1 4126.65 3715.18 256.46 o
4 6 1 385.81 308.63 126.85 o
6 6 1 6926.77 6542.60 441.95 o
8 6 1 431.21 430.63 207.99 o
10 6 1 167.00 168.47 233.71 o
12 6 1 163.36 284.29 258.74 o
14 6 1 407.34 262.23 434.33 o
-13 7 1 1549.82 662.67 1324.35 o
-11 7 1 4739.91 4540.02 581.60 o
-9 7 1 9487.95 9379.81 615.32 o
-7 7 1 131.68 -156.94 156.94 o
-5 7 1 4590.93 4736.66 391.08 o
-3 7 1 3024.70 3290.17 241.19 o
-1 7 1 1879.99 2102.52 347.80 o
1 7 1 674.71 706.89 165.29 o
3 7 1 560.09 639.00 197.62 o
5 7 1 6552.96 6465.54 452.80 o
7 7 1 37.38 180.93 194.16 o
9 7 1 9.36 -22.19 198.02 o
11 7 1 33.31 -219.06 219.06 o
13 7 1 292.28 14.52 398.19 o
-12 8 1 48.73 -296.23 385.92 o
-10 8 1 1073.93 1088.99 343.01 o
-8 8 1 438.22 318.22 252.58 o
-6 8 1 1710.28 1969.86 401.09 o
-4 8 1 784.19 1233.57 344.18 o
-2 8 1 884.53 843.56 198.82 o
0 8 1 1492.56 1265.09 272.76 o
2 8 1 53.62 163.71 234.76 o
4 8 1 9.69 9.57 233.28 o
6 8 1 31.54 126.46 207.51 o
8 8 1 7.82 -115.66 191.90 o
10 8 1 52.01 92.18 258.80 o
-9 9 1 7.29 -27.43 307.37 o
-7 9 1 86.02 84.35 275.09 o
-5 9 1 1.21 60.65 272.67 o
-3 9 1 14.84 -26.18 244.88 o
-1 9 1 769.89 541.06 220.98 o
1 9 1 279.50 197.33 257.89 o
3 9 1 72.27 -68.49 255.27 o
5 9 1 5.31 126.96 289.62 o
7 9 1 13.47 226.58 291.52 o
9 9 1 12.98 7.86 318.88 o
-6 10 1 304.00 689.10 315.24 o
-4 10 1 166.52 -67.14 290.68 o
-2 10 1 92.77 67.69 361.71 o
0 10 1 36.30 -123.46 473.37 o
2 10 1 282.63 327.80 491.26 o
4 10 1 3.66 -205.05 301.48 o
-18 0 2 4346.90 3869.00 1029.73 o
-16 0 2 6106.11 5890.08 809.16 o
-14 0 2 1659.29 1946.68 464.12 o
-12 0 2 4481.15 4867.87 559.67 o
-10 0 2 4303.67 5393.67 565.12 o
-8 0 2 5215.86 5206.86 605.39 o
-6 0 2 7121.02 6807.88 438.96 o
-4 0 2 7444.88 7162.16 400.01 o
-2 0 2 72601.78 70487.23 2662.22 o
0 0 2 154823.83 168717.88 4880.59 o
2 0 2 113244.08 127618.30 3823.20 o
4 0 2 119564.09 137119.14 4264.29 o
6 0 2 100509.60 110034.59 3111.46 o
8 0 2 86898.98 89522.96 1858.73 o
10 0 2 68041.07 67931.96 1884.45 o
12 0 2 33249.70 34560.05 1461.81 o
14 0 2 53911.69 54132.04 2056.39 o
16 0 2 33619.00 31831.42 2383.43 o
-17 1 2 4097.86 4097.17 576.27 o
-15 1 2 2813.74 3254.82 634.17 o
-13 1 2 749.76 723.42 223.71 o
-11 1 2 6533.44 6244.37 405.83 o
-9 1 2 9694.85 10216.53 351.22 o
-7 1 2 38998.05 41662.07 1020.41 o
-5 1 2 10373.76 10294.67 240.68 o
-3 1 2 31850.97 32035.29 483.74 o
-1 1 2 117194.94 126091.94 1619.92 o
1 1 2 31750.15 33647.07 692.08 o
3 1 2 53432.88 57418.94 1128.41 o
5 1 2 81062.74 86728.65 1845.97 o
7 1 2 103507.41 104967.31 1782.86 o
9 1 2 90061.95 88450.53 1485.95 o
11 1 2 53377.46 52403.56 1093.80 o
13 1 2 53497.14 53638.37 1647.94 o
15 1 2 37572.86 37268.41 1425.83 o
-18 2 2 3498.64 2100.35 1007.85 o
-16 2 2 3525.09 3160.58 528.15 o
-14 2 2 5001.01 4927.58 470.42 o
-12 2 2 10054.56 10216.50 539.70 o
-10 2 2 15536.59 16395.68 508.81 o
-8 2 2 3057.61 2774.15 212.10 o
-6 2 2 32985.38 33056.36 583.33 o
-4 2 2 31920.64 31790.42 530.62 o
-2 2 2 33835.16 33790.93 578.74 o
0 2 2 74881.21 80492.05 1287.27 o
2 2 2 52166.57 51268.31 1112.79 o
4 2 2 152693.38 163898.92 2851.51 o
6 2 2 37128.96 36193.67 774.68 o
8 2 2 72872.23 71130.43 1227.22 o
10 2 2 53094.50 52414.16 1065.29 o
12 2 2 42196.95 39638.60 1343.04 o
14 2 2 33918.86 32431.80 1293.00 o
16 2 2 18785.16 19794.08 1303.19 o
-17 3 2 6115.79 6380.28 847.85 o
-15 3 2 9904.88 9853.77 743.30 o
-13 3 2 7712.06 7804.31 749.59 o
-11 3 2 14890.73 14504.17 517.83 o
-9 3 2 11898.00 11741.85 377.74 o
-7 3 2 33636.62 32971.09 640.90 o
-5 3 2 32101.08 31930.08 650.19 o
-3 3 2 58110.66 58956.89 955.33 o
-1 3 2 44914.42 44517.30 744.84 o
1 3 2 60559.29 60911.51 1088.25 o
3 3 2 60260.94 60962.55 1093.98 o
5 3 2 56136.70 54851.25 1087.75 o
7 3 2 48295.00 48843.34 981.16 o
9 3 2 38607.76 36294.57 1121.45 o
11 3 2 35407.60 34886.32 1006.40 o
13 3 2 23907.77 22690.15 1037.85 o
15 3 2 20117.45 20322.78 1903.30 o
-16 4 2 7472.94 8364.77 1203.70 o
-14 4 2 20025.20 19393.06 1287.92 o
-12 4 2 16387.24 16160.64 679.89 o
-10 4 2 23822.56 23518.42 600.52 o
-8 4 2 29450.72 28618.50 635.93 o
-6 4 2 34464.21 33762.06 739.60 o
-4 4 2 44561.91 44684.02 843.93 o
-2 4 2 33037.17 33261.26 592.95 o
0 4 2 60441.64 61732.53 1186.00 o
2 4 2 48611.67 49663.98 1001.76 o
4 4 2 41783.34 41033.96 1403.25 o
6 4 2 35415.12 33630.76 1058.65 o
8 4 2 25835.63 24031.69 743.01 o
10 4 2 21413.21 23943.07 982.58 o
12 4 2 20669.47 20531.08 956.41 o
14 4 2 14224.82 15367.02 1600.68 o
-15 5 2 9251.97 9727.12 1216.77 o
-13 5 2 24170.24 24551.09 1486.49 o
-11 5 2 22530.92 23066.33 1165.76 o
-9 5 2 31880.72 31979.77 932.58 o
-7 5 2 40698.60 41085.57 907.26 o
-5 5 2 51644.45 49987.21 984.61 o
-3 5 2 60287.93 59988.26 954.61 o
-1 5 2 15393.48 14173.09 456.91 o
1 5 2 36140.68 34820.12 912.44 o
3 5 2 28473.94 27561.58 720.23 o
5 5 2 22225.21 22734.03 876.49 o
7 5 2 19707.15 20112.76 739.59 o
9 5 2 12710.86 12865.39 737.89 o
11 5 2 22322.86 20640.07 979.87 o
13 5 2 6810.92 7640.24 1832.14 o
-14 6 2 22577.08 24446.68 1537.17 o
-12 6 2 23546.68 23351.55 1075.97 o
-10 6 2 34637.89 33913.01 1049.64 o
-8 6 2 19417.43 19894.51 753.73 o
-6 6 2 36542.81 36382.68 866.79 o
-4 6 2 39819.15 39146.30 875.67 o
-2 6 2 34233.42 33551.27 670.92 o
0 6 2 34310.00 32845.03 896.23 o
2 6 2 27850.02 27441.44 997.36 o
4 6 2 34353.11 32403.09 1136.79 o
6 6 2 8081.01 7990.03 491.48 o
8 6 2 7359.91 8161.39 524.62 o
10 6 2 6102.99 5895.81 570.02 o
12 6 2 5403.06 4900.11 611.13 o
-13 7 2 16656.23 18250.42 1740.39 o
-11 7 2 27010.34 29014.92 1223.74 o
-9 7 2 25469.08 25583.52 931.26 o
-7 7 2 46122.05 47845.51 1271.20 o
-5 7 2 29781.73 30985.73 1404.60 o
-3 7 2 29446.94 29974.40 769.58 o
-1 7 2 26795.53 25806.04 721.07 o
1 7 2 18782.30 19052.07 871.74 o
3 7 2 12221.34 11585.80 756.02 o
5 7 2 7836.28 8054.44 505.41 o
7 7 2 12079.13 12521.81 779.74 o
9 7 2 6153.28 6223.89 529.57 o
11 7 2 4001.21 3352.33 623.79 o
-12 8 2 14280.48 16512.81 1142.71 o
-10 8 2 25164.29 26830.06 1198.71 o
-8 8 2 27628.71 26976.34 996.38 o
-6 8 2 18984.16 18949.42 956.41 o
-4 8 2 22461.41 22595.37 1015.42 o
-2 8 2 22350.74 22211.72 698.81 o
0 8 2 21201.31 19984.38 953.63 o
2 8 2 10149.77 10556.34 726.21 o
4 8 2 10904.51 9665.95 711.96 o
6 8 2 6303.19 6980.60 529.20 o
8 8 2 6299.09 6134.67 550.47 o
10 8 2 2886.41 1608.68 1043.68 o
-9 9 2 13887.65 15317.08 958.15 o
-7 9 2 17993.49 18648.55 1012.60 o
-5 9 2 14814.15 15577.84 1094.19 o
-3 9 2 15098.78 15951.60 903.59 o
-1 9 2 15987.88 16139.11 725.10 o
1 9 2 12984.75 13164.53 841.56 o
3 9 2 7668.50 7831.31 781.49 o
5 9 2 6004.74 7155.07 711.27 o
7 9 2 6123.38 7452.35 955.45 o
-6 10 2 8547.46 9079.26 934.53 o
-4 10 2 11178.24 9683.11 1398.89 o
-2 10 2 10491.07 10698.88 1038.18 o
0 10 2 7505.64 8378.26 570.28 o
2 10 2 7923.13 10814.98 1167.20 o
4 10 2 5126.10 5320.32 845.89 o
-17 1 3 866.85 954.94 325.27 o
-15 1 3 24.02 -194.14 194.14 o
-13 1 3 520.01 667.00 217.91 o
-11 1 3 356.98 278.56 155.31 o
-9 1 3 253.74 267.52 84.57 o
-7 1 3 2315.37 2480.49 177.66 o
-5 1 3 1122.67 1151.92 100.10 o
-3 1 3 1376.94 1435.18 123.22 o
-1 1 3 33.64 159.16 82.66 o
1 1 3 5212.77 5235.55 317.49 o
3 1 3 5224.11 5202.11 257.31 o
5 1 3 1401.36 1749.74 204.45 o
7 1 3 3992.07 4270.36 273.78 o
9 1 3 5590.82 5511.75 307.91 o
11 1 3 545.01 535.12 157.82 o
13 1 3 180.95 223.56 241.80 o
15 1 3 5.18 -319.13 319.13 o
-18 2 3 606.98 222.11 369.96 o
-16 2 3 1250.01 490.78 312.41 o
-14 2 3 1142.19 1097.95 267.10 o
-12 2 3 2154.63 2232.60 316.98 o
-10 2 3 4401.04 4442.45 272.59 o
-8 2 3 9.64 63.20 67.81 o
-6 2 3 941.27 1014.71 115.94 o
-4 2 3 2073.88 2295.28 159.45 o
-2 2 3 3244.88 3541.56 177.28 o
0 2 3 14121.45 14486.32 389.98 o
2 2 3 27830.49 29030.27 798.08 o
4 2 3 1235.57 745.18 212.39 o
6 2 3 4104.84 3873.71 228.57 o
8 2 3 8325.96 8102.52 372.63 o
10 2 3 3817.66 3914.04 388.92 o
12 2 3 3067.66 3269.26 455.70 o
14 2 3 770.54 1119.11 330.33 o
16 2 3 2085.51 1406.66 1113.90 o
-17 3 3 1639.91 1481.14 477.62 o
-15 3 3 748.88 778.08 325.84 o
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