#------------------------------------------------------------------------------ #$Date: 2010-12-22 21:36:50 +0200 (Wed, 22 Dec 2010) $ #$Revision: 5269 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2227626.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227626_Fobs loop_ _publ_author_name 'bin Shawkataly, Omar' 'Ghani, Syed Sauban' 'Jothiramalingam, Rajabathar' 'Yeap, Chin Sing' 'Fun, Hoong-Kun' _publ_section_title ; Undecacarbonyl-1\k^3^C,2\k^4^C,3\k^4^C-[tris(2-chloroethyl) phosphite-1\kP]-triangulo-triruthenium(0) ; _journal_coeditor_code HY2343 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1191 _journal_page_last m1192 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 109.442 _cell_angle_beta 93.791 _cell_angle_gamma 90.763 _cell_length_a 7.8592 _cell_length_b 12.5979 _cell_length_c 14.8393 _exptl_crystal_F_000 848.00 _reflns_d_resolution_high 0.6190 _[local]_cod_data_source_file hy2343Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ssg15m in P-1 (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 277.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2802.76 3037.12 119.50 o 2 0 0 5846.35 5995.83 235.16 o 3 0 0 2451.24 2808.93 125.45 o 5 0 0 13159.44 13251.08 524.19 o 6 0 0 6230.18 6630.11 287.97 o 7 0 0 6119.10 6040.24 273.27 o 8 0 0 176.43 218.83 23.09 o 9 0 0 149.22 184.68 25.24 o 10 0 0 4483.54 4557.55 175.48 o 11 0 0 4041.85 4210.19 169.79 o 12 0 0 561.47 608.10 37.42 o -12 1 0 10.03 8.77 21.44 o -11 1 0 1692.80 1829.36 89.49 o -10 1 0 88.27 92.90 22.61 o -9 1 0 3907.81 3996.11 150.96 o -7 1 0 473.01 565.45 47.91 o -6 1 0 5991.62 6508.12 272.71 o -5 1 0 859.50 793.56 51.78 o -4 1 0 16171.60 16931.83 650.41 o -3 1 0 1367.52 1450.63 73.66 o -2 1 0 146.78 160.33 15.54 o -1 1 0 18103.17 20787.92 652.44 o 0 1 0 9471.17 10327.16 249.80 o 1 1 0 35560.00 36041.84 1335.70 o 2 1 0 13479.94 14243.42 543.19 o 3 1 0 4340.44 4635.20 197.35 o 4 1 0 952.10 4.39 10.93 o 5 1 0 9279.46 10205.33 415.54 o 6 1 0 6665.60 7120.29 309.13 o 7 1 0 4657.77 4957.85 140.86 o 8 1 0 18.24 13.76 12.05 o 9 1 0 38.68 26.37 16.21 o 10 1 0 4301.99 4172.07 166.46 o 11 1 0 55.75 47.84 16.14 o 12 1 0 2048.30 2023.54 105.54 o -12 2 0 278.09 263.10 38.05 o -11 2 0 143.87 114.39 26.28 o -10 2 0 1854.06 1924.11 89.73 o -9 2 0 64.22 71.96 19.42 o -7 2 0 546.94 498.78 74.79 o -6 2 0 32.61 27.43 15.67 o -5 2 0 3989.49 4179.05 227.97 o -4 2 0 11960.07 12389.19 490.82 o -3 2 0 4870.40 5521.96 161.09 o -2 2 0 3886.99 4552.51 188.71 o -1 2 0 746.54 1008.46 54.75 o 0 2 0 7575.34 8661.41 214.69 o 1 2 0 12756.08 14875.14 568.58 o 2 2 0 4270.55 4011.42 562.69 o 3 2 0 2255.45 2044.43 47.49 o 4 2 0 5058.10 5400.99 146.20 o 5 2 0 439.13 433.63 21.39 o 6 2 0 8099.00 8503.27 227.99 o 7 2 0 2.90 0.71 10.13 o 8 2 0 4097.46 4136.10 159.05 o 9 2 0 391.39 363.93 38.01 o 10 2 0 0.20 -10.08 12.22 o 11 2 0 2648.07 2431.78 117.96 o 12 2 0 576.91 649.44 62.70 o -12 3 0 178.45 162.89 33.45 o -11 3 0 4.86 13.84 21.27 o -10 3 0 211.87 177.91 30.64 o -9 3 0 1483.69 1530.74 73.65 o -8 3 0 3671.28 3705.03 138.40 o -7 3 0 615.00 584.22 43.35 o -6 3 0 35.79 42.38 12.73 o -5 3 0 2325.72 2363.94 81.17 o -4 3 0 1588.30 1773.52 54.69 o -3 3 0 6635.05 6618.00 113.36 o -1 3 0 4433.21 4851.39 123.78 o 0 3 0 2208.41 2510.45 74.15 o 1 3 0 88.66 72.49 19.74 o 2 3 0 23559.85 24296.90 464.00 o 3 3 0 1608.06 1689.99 44.55 o 4 3 0 972.85 932.22 28.99 o 5 3 0 259.47 296.79 18.53 o 6 3 0 4230.06 4173.59 98.67 o 7 3 0 1290.84 1364.29 43.73 o 8 3 0 5355.64 5123.20 196.07 o 9 3 0 286.79 269.49 36.72 o 10 3 0 10.30 -17.08 17.08 o 11 3 0 198.12 226.02 40.33 o 12 3 0 365.37 369.02 52.68 o -12 4 0 194.26 180.90 36.46 o -11 4 0 644.21 655.22 55.59 o -10 4 0 176.30 129.80 28.92 o -9 4 0 237.93 262.71 33.05 o -8 4 0 29.90 35.71 15.38 o -7 4 0 952.26 879.42 47.64 o -6 4 0 607.51 694.23 42.81 o -5 4 0 1588.70 1559.51 42.88 o -4 4 0 921.52 1073.11 45.46 o -3 4 0 800.38 797.77 36.83 o -2 4 0 2623.55 2636.24 63.83 o -1 4 0 16243.95 10381.61 338.10 o 0 4 0 1402.77 1593.42 35.80 o 1 4 0 2301.98 2420.30 55.12 o 2 4 0 349.73 396.43 14.55 o 3 4 0 880.32 973.67 32.88 o 4 4 0 1624.45 1692.12 86.64 o 5 4 0 1.32 2.60 6.26 o 6 4 0 1037.89 1118.16 69.17 o 7 4 0 1577.07 1597.69 105.01 o 8 4 0 46.26 27.42 16.76 o 9 4 0 1313.79 1309.61 78.23 o 10 4 0 805.77 810.78 62.70 o 11 4 0 62.72 117.92 32.29 o 12 4 0 394.17 391.60 56.24 o -12 5 0 7.23 13.12 26.17 o -11 5 0 125.94 152.02 34.71 o -10 5 0 9.35 -10.54 20.40 o -9 5 0 2489.25 2668.19 120.01 o -8 5 0 112.50 161.37 27.05 o -7 5 0 14.06 11.77 14.50 o -6 5 0 1764.13 1819.25 78.79 o -5 5 0 691.89 678.12 75.43 o -4 5 0 1191.10 1137.34 91.97 o -3 5 0 3276.32 3117.53 95.26 o -2 5 0 86.34 98.79 8.95 o -1 5 0 397.47 402.89 21.53 o 0 5 0 2308.35 2397.26 51.00 o 1 5 0 5662.79 6142.95 106.53 o 2 5 0 2363.99 2417.39 46.95 o 3 5 0 332.51 312.19 23.53 o 4 5 0 1022.41 897.35 124.03 o 5 5 0 560.53 638.63 42.17 o 6 5 0 27.66 59.40 17.62 o 7 5 0 2866.25 2916.33 117.57 o 8 5 0 2490.01 2365.21 118.46 o 9 5 0 608.73 556.80 57.23 o 10 5 0 106.74 79.68 28.95 o 11 5 0 37.84 42.91 29.15 o 12 5 0 101.98 116.11 38.13 o -12 6 0 559.32 626.72 68.43 o -11 6 0 157.26 166.81 40.06 o -10 6 0 71.39 102.14 31.24 o -9 6 0 4134.20 4314.07 180.39 o -8 6 0 991.25 949.92 62.29 o -7 6 0 624.82 629.73 48.16 o -6 6 0 11.32 -6.17 12.55 o -5 6 0 186.44 211.75 14.30 o -4 6 0 12288.09 12321.51 316.35 o -3 6 0 978.30 1021.54 84.66 o -2 6 0 5579.50 5431.49 101.78 o -1 6 0 10.76 8.99 6.04 o 0 6 0 2194.65 2310.40 46.41 o 1 6 0 5627.92 5601.01 90.55 o 2 6 0 7687.57 7883.70 115.41 o 3 6 0 2881.74 2979.90 56.73 o 4 6 0 70.51 22.84 22.61 o 5 6 0 343.15 338.67 39.01 o 6 6 0 2421.94 2383.56 69.29 o 7 6 0 748.77 779.63 101.20 o 8 6 0 386.59 344.48 39.24 o 9 6 0 658.77 607.63 63.79 o 10 6 0 126.21 121.12 34.20 o 11 6 0 464.17 434.64 59.41 o -11 7 0 712.11 803.49 79.40 o -10 7 0 926.74 839.67 68.66 o -9 7 0 89.22 87.19 28.27 o -8 7 0 4792.18 4625.78 193.73 o -7 7 0 54.06 31.75 20.94 o -6 7 0 3.72 25.80 15.75 o -5 7 0 1617.15 1720.43 51.57 o -4 7 0 1226.68 1104.60 52.29 o -3 7 0 33843.91 34727.02 687.80 o -2 7 0 720.00 733.45 20.53 o -1 7 0 2663.02 2596.64 50.76 o 0 7 0 15.75 4.19 7.93 o 1 7 0 1422.93 1347.61 38.42 o 2 7 0 10286.92 10129.96 146.95 o 3 7 0 11603.08 11787.73 168.33 o 4 7 0 131.20 119.01 17.29 o 5 7 0 1241.14 1164.38 46.08 o 6 7 0 404.70 372.13 30.86 o 7 7 0 3444.74 3237.52 122.30 o 8 7 0 3739.23 3599.41 134.74 o 9 7 0 65.55 109.20 33.57 o 10 7 0 101.78 61.39 31.65 o 11 7 0 75.67 66.58 35.30 o -11 8 0 94.23 118.52 42.02 o -10 8 0 730.57 693.62 72.92 o -9 8 0 1975.66 1819.00 107.59 o -8 8 0 3817.73 4031.63 181.51 o -7 8 0 5027.40 5005.95 210.46 o -6 8 0 1224.35 1239.86 63.41 o -5 8 0 1925.46 1935.99 60.02 o -4 8 0 4613.48 4555.46 201.63 o -3 8 0 7136.23 7184.75 165.98 o -2 8 0 6670.69 6524.26 98.71 o -1 8 0 29053.64 29180.50 436.07 o 0 8 0 2182.96 2227.68 39.30 o 1 8 0 24.23 21.91 8.03 o 2 8 0 18132.10 18220.36 281.61 o 3 8 0 58.06 47.12 10.42 o 4 8 0 6397.56 6534.50 158.11 o 5 8 0 139.47 127.98 20.03 o 6 8 0 785.04 777.05 46.10 o 7 8 0 3229.46 3099.19 142.75 o 8 8 0 30.25 53.37 23.35 o 9 8 0 4284.31 4454.52 207.12 o 10 8 0 346.23 302.72 54.88 o 11 8 0 282.80 264.36 54.98 o -11 9 0 370.79 358.12 60.75 o -10 9 0 910.72 833.08 83.90 o -9 9 0 464.10 431.74 59.85 o -8 9 0 307.90 262.96 46.92 o -7 9 0 8148.69 8489.86 331.71 o -6 9 0 214.37 159.80 18.24 o -5 9 0 6386.35 6446.70 152.79 o -4 9 0 350.93 320.11 28.21 o -3 9 0 328.51 305.65 34.58 o -2 9 0 6828.18 6743.74 109.39 o -1 9 0 67.67 80.12 12.96 o 0 9 0 6736.26 6841.53 94.26 o 1 9 0 175.03 174.14 14.78 o 2 9 0 141.71 180.33 15.51 o 3 9 0 4657.91 4879.08 84.03 o 4 9 0 2927.21 3150.37 80.12 o 5 9 0 7344.76 7268.62 177.06 o 6 9 0 290.26 325.35 31.73 o 7 9 0 267.05 220.76 26.27 o 8 9 0 743.01 733.41 82.45 o 9 9 0 1218.42 1086.22 90.04 o 10 9 0 553.02 544.65 74.81 o -11 10 0 1651.75 1736.53 121.81 o -10 10 0 51.95 8.02 33.32 o -9 10 0 213.42 188.44 45.77 o -8 10 0 793.58 792.44 81.88 o -7 10 0 26.75 20.29 26.43 o -6 10 0 9576.17 9692.82 216.02 o -5 10 0 6733.59 6917.57 206.12 o -4 10 0 1876.52 1911.22 67.89 o -3 10 0 12.21 21.77 21.11 o -2 10 0 153.40 150.03 14.06 o -1 10 0 4397.71 4629.18 81.36 o 0 10 0 3618.05 3793.68 65.86 o 1 10 0 483.29 539.83 24.40 o 2 10 0 95.60 97.59 13.67 o 3 10 0 1645.33 1679.50 42.35 o 4 10 0 4218.41 4182.65 85.06 o 5 10 0 9195.74 8957.10 214.91 o 6 10 0 334.39 308.83 32.70 o 7 10 0 291.18 269.46 30.49 o 8 10 0 1592.53 1517.72 92.53 o 9 10 0 199.94 263.40 55.48 o 10 10 0 2334.98 2116.57 141.74 o -10 11 0 547.91 494.50 72.97 o -9 11 0 604.88 627.87 79.80 o -8 11 0 71.04 88.14 36.73 o -7 11 0 519.65 467.48 67.02 o -6 11 0 1815.61 1657.72 68.30 o -5 11 0 2660.91 2686.10 86.69 o -4 11 0 5368.23 5525.67 145.32 o -3 11 0 95.37 119.75 13.58 o -2 11 0 90.92 84.85 12.53 o -1 11 0 2245.72 2308.60 51.53 o 0 11 0 2.66 4.58 11.66 o 1 11 0 10889.93 10861.02 181.57 o 2 11 0 2.65 1.81 9.90 o 3 11 0 0.27 -7.39 10.16 o 4 11 0 3970.01 4053.00 83.22 o 5 11 0 496.64 493.06 42.68 o 6 11 0 2822.93 2828.60 96.41 o 7 11 0 474.10 453.23 40.72 o 8 11 0 426.50 405.22 65.32 o 9 11 0 387.34 302.02 62.11 o 10 11 0 355.34 464.40 77.25 o -10 12 0 263.00 266.71 59.56 o -9 12 0 70.30 53.04 38.64 o -8 12 0 257.16 291.65 58.77 o -7 12 0 210.84 180.35 49.61 o -6 12 0 1204.25 1237.55 61.20 o -5 12 0 509.32 505.27 41.64 o -4 12 0 76.80 28.39 22.78 o -3 12 0 551.81 564.94 45.57 o -2 12 0 174.10 146.30 15.33 o -1 12 0 31.94 31.95 12.37 o 0 12 0 989.06 1030.44 46.85 o 1 12 0 626.80 579.81 32.86 o 2 12 0 7.79 -4.12 12.55 o 3 12 0 249.62 250.52 21.48 o 4 12 0 12.26 17.48 13.32 o 5 12 0 1314.18 1108.98 62.72 o 6 12 0 1238.76 1228.74 108.75 o 7 12 0 184.05 126.97 27.47 o 8 12 0 137.23 121.96 25.38 o 9 12 0 81.92 82.12 43.54 o -9 13 0 53.11 67.18 43.47 o -8 13 0 139.85 180.77 53.63 o -7 13 0 1495.34 1351.54 111.14 o -6 13 0 8.52 5.08 19.70 o -5 13 0 814.84 810.09 60.07 o -4 13 0 129.02 137.24 27.75 o -3 13 0 334.35 297.97 38.89 o -2 13 0 85.99 72.52 14.15 o -1 13 0 1463.10 1401.91 52.30 o 0 13 0 0.14 0.02 13.27 o 1 13 0 20.48 23.78 14.93 o 2 13 0 764.16 734.72 38.89 o 3 13 0 773.33 781.95 40.38 o 4 13 0 286.21 317.62 25.17 o 5 13 0 27.78 34.50 21.94 o 6 13 0 660.44 591.59 51.47 o 7 13 0 373.09 305.84 39.42 o 8 13 0 43.59 12.15 23.92 o -8 14 0 5.82 -1.63 36.47 o -7 14 0 3.19 -5.95 34.99 o -6 14 0 1390.29 1312.84 73.11 o -5 14 0 710.96 699.08 53.57 o -4 14 0 625.32 615.44 52.02 o -3 14 0 306.39 294.43 58.15 o -2 14 0 322.53 303.17 34.60 o -1 14 0 884.24 970.65 51.13 o 0 14 0 1927.79 1817.50 56.02 o 1 14 0 782.04 829.16 47.33 o 2 14 0 25.97 6.73 15.93 o 3 14 0 5.71 14.25 16.91 o 4 14 0 769.16 767.78 60.66 o 5 14 0 518.86 480.11 62.61 o 6 14 0 11.80 27.17 23.90 o 7 14 0 8.64 -11.08 24.33 o 8 14 0 4.86 -15.88 25.32 o -8 15 0 258.79 277.27 70.71 o -7 15 0 62.89 135.96 55.74 o -6 15 0 713.74 666.55 67.60 o -5 15 0 124.15 120.71 34.50 o -4 15 0 3070.01 3222.68 114.75 o -3 15 0 164.43 191.47 58.11 o -2 15 0 8.65 -8.76 17.07 o -1 15 0 2214.10 2248.59 97.39 o 0 15 0 138.56 131.95 21.86 o 1 15 0 1318.03 1320.88 56.56 o 2 15 0 841.42 921.52 47.12 o 3 15 0 37.42 14.36 18.31 o 4 15 0 647.67 621.31 86.08 o 5 15 0 0.21 7.93 30.53 o 6 15 0 980.41 1040.78 111.98 o 7 15 0 347.98 318.02 64.09 o -7 16 0 7.01 30.37 45.56 o -6 16 0 181.48 228.20 40.40 o -5 16 0 2310.20 2519.11 113.92 o -4 16 0 949.01 896.17 118.02 o -3 16 0 1682.98 1606.28 106.98 o -2 16 0 178.40 212.57 27.70 o -1 16 0 399.14 403.36 33.37 o 0 16 0 1724.85 1719.08 64.99 o 1 16 0 3581.48 3390.04 96.98 o 2 16 0 1491.87 1492.63 58.70 o 3 16 0 763.19 760.16 43.84 o 4 16 0 107.24 133.02 30.13 o 5 16 0 211.28 191.56 45.36 o 6 16 0 866.46 789.76 103.00 o -6 17 0 146.24 133.97 36.65 o -5 17 0 413.45 320.49 64.95 o -4 17 0 332.27 289.59 63.72 o -3 17 0 3228.89 3448.04 184.19 o -2 17 0 2.02 14.36 19.39 o -1 17 0 52.96 62.88 20.05 o 0 17 0 756.01 756.44 59.03 o 1 17 0 421.65 397.74 43.79 o 2 17 0 4003.53 4097.16 145.88 o 3 17 0 129.70 159.03 31.75 o 4 17 0 848.87 792.10 75.72 o 5 17 0 311.63 294.75 71.66 o -4 18 0 1493.96 1750.28 135.55 o -3 18 0 281.51 271.42 68.69 o -2 18 0 2087.62 2150.40 125.77 o -1 18 0 234.44 242.18 34.46 o 0 18 0 59.13 26.42 31.18 o 1 18 0 1322.48 1231.15 141.89 o 2 18 0 427.27 407.45 53.68 o 3 18 0 1477.03 1404.37 93.40 o -2 19 0 1182.11 1264.11 97.24 o -1 19 0 243.99 317.52 39.38 o 0 19 0 907.33 879.40 70.78 o 1 19 0 298.09 255.37 46.74 o -2 -19 1 1150.80 1161.07 98.20 o -1 -19 1 25.01 45.55 33.73 o 0 -19 1 0.61 6.95 24.80 o 1 -19 1 250.21 288.05 38.03 o 2 -19 1 69.67 114.65 69.91 o 3 -19 1 1028.52 1256.33 136.69 o -4 -18 1 43.55 70.47 39.67 o -3 -18 1 506.58 456.04 44.99 o -2 -18 1 666.87 696.23 64.93 o -1 -18 1 1140.44 1030.54 76.76 o 0 -18 1 37.31 33.48 23.59 o 1 -18 1 1.95 -20.45 21.88 o 2 -18 1 1703.44 1480.68 188.07 o 3 -18 1 1241.61 1226.97 131.75 o 4 -18 1 661.89 668.30 94.48 o 5 -18 1 327.30 358.50 67.66 o -5 -17 1 762.46 597.32 94.00 o -4 -17 1 40.27 32.57 33.28 o -3 -17 1 1188.17 1163.31 63.10 o -2 -17 1 782.77 668.80 43.69 o -1 -17 1 4382.99 4277.40 115.40 o 0 -17 1 128.59 98.90 30.20 o 1 -17 1 35.47 7.40 18.23 o 2 -17 1 464.96 499.05 38.42 o 3 -17 1 78.55 67.78 40.90 o 4 -17 1 3348.57 3701.02 202.32 o 5 -17 1 55.61 85.87 44.60 o 6 -17 1 444.25 429.07 51.48 o -6 -16 1 28.13 32.90 44.15 o -5 -16 1 1759.16 1688.57 101.68 o -4 -16 1 126.11 99.14 28.58 o -3 -16 1 609.29 591.29 38.98 o -2 -16 1 3751.49 3683.69 92.51 o -1 -16 1 318.95 301.15 38.49 o 0 -16 1 2643.97 2462.98 126.18 o 1 -16 1 787.57 801.85 42.61 o 2 -16 1 788.61 829.24 65.21 o 3 -16 1 1130.72 1088.93 93.16 o 4 -16 1 1275.01 1443.63 96.95 o 5 -16 1 1124.29 1120.51 82.57 o 6 -16 1 113.28 81.95 31.69 o 7 -16 1 371.98 386.83 38.03 o -7 -15 1 71.00 81.49 32.62 o -6 -15 1 1275.41 1060.11 110.77 o -5 -15 1 505.40 531.60 67.49 o -4 -15 1 735.00 685.89 58.88 o -3 -15 1 16.26 21.30 18.46 o -2 -15 1 721.38 689.22 40.87 o -1 -15 1 1288.15 1374.34 58.91 o 0 -15 1 4082.35 4022.17 92.83 o 1 -15 1 659.28 624.90 39.18 o 2 -15 1 976.39 956.08 49.73 o 3 -15 1 389.55 346.01 53.53 o 4 -15 1 467.55 545.42 51.40 o 5 -15 1 2516.52 2534.14 110.33 o 6 -15 1 21.90 37.34 26.06 o 7 -15 1 1116.69 1146.00 58.13 o 8 -15 1 538.65 484.61 86.07 o -8 -14 1 51.10 34.95 25.99 o -7 -14 1 4.17 -7.87 22.91 o -6 -14 1 315.98 338.25 43.84 o -5 -14 1 144.10 196.38 33.55 o -4 -14 1 1585.07 1407.97 118.28 o -3 -14 1 16.70 3.66 16.29 o -2 -14 1 167.40 170.90 22.62 o -1 -14 1 891.60 829.42 42.29 o 0 -14 1 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