#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/76/2227633.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227633_Fobs loop_ _publ_author_name 'Liu, Hai-Yan' 'Liu, Li-Xin' 'Sha, Jing-Quan' 'Yu, Lian-Sheng' _publ_section_title ; catena-Poly[[(5-carboxy-2H-1,2,3-triazole-4-carboxylato-\k^2^N^3^,O^4^)sodium]-di-\m-aqua-\k^4^O:O] ; _journal_coeditor_code HY2351 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1336 _journal_page_last m1337 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.647 _cell_angle_gamma 90.000 _cell_length_a 6.8706 _cell_length_b 10.6280 _cell_length_c 11.5585 _exptl_crystal_F_000 440.00 _reflns_d_resolution_high 0.8113 _[local]_cod_data_source_file hy2351Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' aaa in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 261.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2373.38 2580.58 64.66 o 4 0 0 2.35 7.40 1.20 o 6 0 0 0.36 0.83 0.87 o 8 0 0 29.15 25.99 2.85 o 1 1 0 307.44 297.01 4.57 o 2 1 0 17.25 25.01 0.78 o 3 1 0 41.40 48.53 1.67 o 4 1 0 425.69 454.49 9.32 o 5 1 0 3.53 2.19 0.61 o 6 1 0 128.39 128.58 4.03 o 7 1 0 129.85 129.71 4.67 o 8 1 0 34.13 32.47 2.19 o 0 2 0 704.07 669.47 12.13 o 1 2 0 15.25 11.76 0.35 o 2 2 0 610.34 674.23 8.81 o 3 2 0 5271.35 4947.86 71.80 o 4 2 0 816.20 809.10 15.52 o 5 2 0 4.06 5.40 0.80 o 6 2 0 302.14 305.41 7.37 o 7 2 0 75.66 80.14 3.23 o 8 2 0 1.63 1.18 0.82 o 1 3 0 2035.78 1985.87 25.14 o 2 3 0 420.68 461.31 8.83 o 3 3 0 121.88 118.58 1.78 o 4 3 0 3.86 5.95 0.59 o 5 3 0 87.95 97.73 5.06 o 6 3 0 21.86 23.57 1.56 o 7 3 0 0.15 0.00 0.60 o 8 3 0 6.06 6.81 1.95 o 0 4 0 34.10 12.28 1.58 o 1 4 0 48.32 79.36 1.37 o 2 4 0 562.48 578.67 7.80 o 3 4 0 1660.36 1686.88 21.84 o 4 4 0 1097.88 1202.70 16.06 o 5 4 0 56.92 53.13 1.75 o 6 4 0 180.96 186.90 5.41 o 7 4 0 45.81 48.11 4.82 o 8 4 0 37.64 40.70 2.78 o 1 5 0 45.09 49.42 1.04 o 2 5 0 390.40 400.85 5.63 o 3 5 0 524.75 514.88 7.38 o 4 5 0 7.52 9.17 0.60 o 5 5 0 4.82 4.97 0.74 o 6 5 0 0.72 1.34 0.75 o 7 5 0 106.37 97.12 3.86 o 0 6 0 398.12 352.39 14.38 o 1 6 0 28.29 30.24 0.82 o 2 6 0 25.47 27.51 0.82 o 3 6 0 600.99 624.86 12.82 o 4 6 0 87.03 91.32 2.51 o 5 6 0 10.79 11.97 1.07 o 6 6 0 61.18 65.22 2.40 o 7 6 0 6.81 8.23 1.35 o 1 7 0 139.56 129.24 2.25 o 2 7 0 4.85 9.51 0.69 o 3 7 0 170.43 173.10 5.81 o 4 7 0 45.11 46.62 1.74 o 5 7 0 0.05 0.00 0.44 o 6 7 0 5.63 6.21 0.92 o 7 7 0 15.08 16.47 1.76 o 0 8 0 71.52 69.86 2.15 o 1 8 0 91.64 92.53 2.21 o 2 8 0 179.40 192.02 3.88 o 3 8 0 75.76 74.23 2.51 o 4 8 0 52.64 50.24 1.87 o 5 8 0 1.82 1.51 0.61 o 6 8 0 204.94 213.01 5.11 o 1 9 0 187.49 172.08 3.55 o 2 9 0 62.59 62.55 1.91 o 3 9 0 268.97 250.56 5.05 o 4 9 0 21.40 22.26 2.16 o 5 9 0 181.01 174.55 4.32 o 6 9 0 0.20 0.20 0.59 o 0 10 0 302.00 287.39 9.43 o 1 10 0 450.70 440.64 9.50 o 2 10 0 0.88 2.78 0.72 o 3 10 0 98.47 105.02 2.88 o 4 10 0 3.83 5.66 1.12 o 5 10 0 4.72 4.51 0.86 o 1 11 0 142.51 146.61 4.20 o 2 11 0 1.39 0.49 0.55 o 3 11 0 0.62 0.22 0.52 o 4 11 0 3.65 3.54 0.94 o 0 12 0 54.65 64.17 3.74 o 1 12 0 58.50 66.28 4.27 o 2 12 0 1.03 0.52 0.58 o 3 12 0 60.15 55.86 2.60 o 1 13 0 1.27 0.98 0.72 o -7 0 1 56.65 50.06 3.53 o -5 0 1 1.01 1.31 0.78 o -3 0 1 130.65 152.17 5.08 o -1 0 1 100.87 115.16 4.00 o 1 0 1 878.53 831.44 21.28 o 3 0 1 279.48 265.66 8.00 o 5 0 1 414.52 443.43 13.47 o 7 0 1 6.83 5.56 1.50 o -8 1 1 32.35 27.31 3.03 o -7 1 1 7.58 9.03 1.23 o -6 1 1 345.03 344.52 8.06 o -5 1 1 163.57 174.07 4.60 o -4 1 1 505.19 503.73 10.18 o -3 1 1 188.60 201.75 4.47 o -2 1 1 7676.58 7141.13 178.02 o -1 1 1 2222.33 2133.95 26.83 o 0 1 1 1396.87 1312.55 21.40 o 1 1 1 13.55 20.21 0.57 o 2 1 1 114.66 132.24 2.49 o 3 1 1 65.73 78.94 2.27 o 4 1 1 1867.85 1810.11 33.06 o 5 1 1 0.03 2.96 3.44 o 6 1 1 124.78 131.29 4.94 o 7 1 1 22.39 23.49 3.04 o 8 1 1 138.08 141.68 4.83 o -8 2 1 22.20 22.46 2.90 o -7 2 1 51.65 52.92 2.55 o -6 2 1 1.20 2.88 1.18 o -5 2 1 53.73 59.31 2.29 o -4 2 1 14.53 19.25 1.15 o -3 2 1 69.35 70.38 1.37 o -2 2 1 113.15 105.47 1.50 o -1 2 1 64.31 70.33 1.07 o 0 2 1 9.68 4.79 0.24 o 1 2 1 0.56 1.02 0.42 o 2 2 1 638.91 676.48 11.90 o 3 2 1 1.42 1.88 0.34 o 4 2 1 192.91 180.27 4.42 o 5 2 1 308.52 323.66 7.37 o 6 2 1 135.38 136.71 4.18 o 7 2 1 8.38 7.43 1.16 o 8 2 1 4.31 4.31 1.07 o -8 3 1 12.48 11.76 1.58 o -7 3 1 229.33 234.30 9.50 o -6 3 1 20.12 21.81 1.50 o -5 3 1 11.01 11.73 1.03 o -4 3 1 546.91 575.25 8.15 o -3 3 1 2025.23 1958.89 22.34 o -2 3 1 2366.55 2307.52 29.11 o -1 3 1 0.01 2.10 0.58 o 0 3 1 4999.64 3993.66 58.53 o 1 3 1 1090.27 1046.57 13.45 o 2 3 1 583.07 635.79 9.77 o 3 3 1 756.67 809.03 12.53 o 4 3 1 118.93 128.58 2.86 o 5 3 1 433.32 438.63 9.36 o 6 3 1 77.60 78.40 2.96 o 7 3 1 93.77 97.19 3.60 o 8 3 1 0.01 0.87 1.18 o -8 4 1 2.70 2.63 0.97 o -7 4 1 1.60 3.26 0.96 o -6 4 1 24.09 24.23 1.73 o -5 4 1 17.48 19.17 1.02 o -4 4 1 10.83 10.20 0.61 o -3 4 1 26.88 30.86 0.88 o -2 4 1 90.57 94.02 2.41 o -1 4 1 271.02 281.00 3.90 o 0 4 1 29.46 34.90 0.76 o 1 4 1 657.31 671.45 10.32 o 2 4 1 46.59 52.19 1.17 o 3 4 1 0.64 1.26 0.61 o 4 4 1 38.73 40.27 1.22 o 5 4 1 26.07 26.41 1.25 o 6 4 1 16.03 17.59 1.40 o 7 4 1 114.97 112.43 6.16 o -7 5 1 32.93 37.22 2.96 o -6 5 1 3.63 4.84 1.00 o -5 5 1 74.04 80.34 2.63 o -4 5 1 87.67 100.10 2.57 o -3 5 1 1610.75 1562.30 20.28 o -2 5 1 995.42 1008.83 13.19 o -1 5 1 3517.27 3327.20 41.98 o 0 5 1 2239.51 2153.25 27.34 o 1 5 1 1847.80 1669.33 21.35 o 2 5 1 832.77 922.87 12.20 o 3 5 1 41.92 55.42 3.15 o 4 5 1 7.85 12.02 0.70 o 5 5 1 39.21 45.64 1.47 o 6 5 1 10.42 10.96 1.33 o 7 5 1 95.22 99.36 3.99 o -7 6 1 0.25 0.63 0.73 o -6 6 1 18.02 19.00 1.65 o -5 6 1 53.48 51.62 1.92 o -4 6 1 181.80 173.32 3.79 o -3 6 1 68.08 73.37 3.19 o -2 6 1 336.22 358.53 6.11 o -1 6 1 0.13 0.63 0.26 o 0 6 1 248.69 276.68 4.02 o 1 6 1 659.60 687.04 9.21 o 2 6 1 80.82 78.17 1.60 o 3 6 1 236.92 247.90 5.81 o 4 6 1 18.39 20.87 1.51 o 5 6 1 33.88 35.77 1.64 o 6 6 1 15.56 15.19 1.27 o 7 6 1 13.57 13.33 1.64 o -7 7 1 72.53 77.15 3.47 o -6 7 1 162.32 168.47 4.28 o -5 7 1 21.53 20.71 1.27 o -4 7 1 632.32 656.51 19.15 o -3 7 1 190.42 205.96 4.14 o -2 7 1 634.28 642.06 10.36 o -1 7 1 31.49 39.16 1.25 o 0 7 1 1759.69 1686.78 21.72 o 1 7 1 220.23 244.33 3.76 o 2 7 1 989.08 1036.34 13.78 o 3 7 1 47.77 48.26 1.91 o 4 7 1 568.09 571.93 9.89 o 5 7 1 188.70 195.25 4.53 o 6 7 1 1.35 2.29 1.48 o 7 7 1 44.37 46.11 2.75 o -6 8 1 29.36 31.39 1.71 o -5 8 1 26.22 24.48 1.43 o -4 8 1 71.72 69.39 2.20 o -3 8 1 75.66 82.47 2.28 o -2 8 1 275.81 276.09 5.13 o -1 8 1 2.74 2.55 0.45 o 0 8 1 274.74 279.81 7.19 o 1 8 1 278.27 294.32 4.64 o 2 8 1 19.72 17.79 0.94 o 3 8 1 199.64 184.92 5.69 o 4 8 1 0.02 0.25 0.45 o 5 8 1 16.58 15.60 1.24 o 6 8 1 148.12 144.23 4.00 o -6 9 1 15.12 16.48 1.76 o -5 9 1 226.09 224.21 5.08 o -4 9 1 391.03 387.94 8.53 o -3 9 1 14.38 14.28 0.99 o -2 9 1 198.74 195.83 4.04 o -1 9 1 151.97 134.28 2.99 o 0 9 1 303.17 283.62 6.42 o 1 9 1 113.21 113.37 3.29 o 2 9 1 391.72 403.90 8.28 o 3 9 1 828.40 800.56 13.16 o 4 9 1 34.35 32.14 1.87 o 5 9 1 84.17 81.49 2.74 o 6 9 1 13.69 12.20 1.28 o -5 10 1 338.89 333.48 6.89 o -4 10 1 0.03 0.00 0.46 o -3 10 1 267.35 266.04 5.39 o -2 10 1 2.37 5.83 1.83 o -1 10 1 74.48 69.50 2.68 o 0 10 1 10.51 10.31 1.01 o 1 10 1 155.70 156.34 5.59 o 2 10 1 0.08 0.42 0.54 o 3 10 1 737.14 692.26 35.89 o 4 10 1 0.78 0.56 0.49 o 5 10 1 50.26 50.12 2.15 o -4 11 1 0.33 0.75 0.58 o -3 11 1 7.94 9.07 1.12 o -2 11 1 236.62 259.52 6.44 o -1 11 1 130.17 121.21 3.69 o 0 11 1 230.97 259.38 6.34 o 1 11 1 0.15 0.71 0.54 o 2 11 1 0.47 2.81 0.76 o 3 11 1 0.07 0.18 0.54 o 4 11 1 12.48 11.85 1.35 o -3 12 1 19.13 19.65 1.57 o -2 12 1 27.72 26.32 1.71 o -1 12 1 2.77 3.12 0.78 o 0 12 1 13.61 10.77 1.16 o 1 12 1 157.65 154.40 4.53 o 2 12 1 0.67 1.01 0.64 o 3 12 1 16.69 14.87 1.43 o 0 13 1 13.78 20.88 1.60 o -8 0 2 12.81 11.84 2.07 o -6 0 2 85.81 92.66 4.65 o -4 0 2 2079.97 2343.53 59.83 o -2 0 2 68468.67 18957.46 480.48 o 0 0 2 6822.66 3210.53 59.24 o 2 0 2 4229.40 4146.62 103.36 o 4 0 2 542.58 490.57 14.15 o 6 0 2 34.61 37.16 2.83 o 8 0 2 110.48 109.60 5.90 o -8 1 2 6.46 7.50 1.26 o -7 1 2 1.68 1.75 0.71 o -6 1 2 110.46 108.08 3.58 o -5 1 2 0.94 0.33 0.49 o -4 1 2 23.84 23.43 1.31 o -3 1 2 7.69 11.27 1.16 o -2 1 2 1231.81 1299.11 16.52 o -1 1 2 721.68 707.39 8.12 o 0 1 2 461.20 497.82 6.40 o 1 1 2 125.22 128.19 2.76 o 2 1 2 164.30 144.46 2.68 o 3 1 2 16.05 28.71 1.24 o 4 1 2 752.18 757.16 14.69 o 5 1 2 129.77 139.78 4.26 o 6 1 2 181.42 180.53 5.08 o 7 1 2 22.93 25.58 1.86 o 8 1 2 1.98 1.76 0.89 o -8 2 2 33.12 30.98 3.26 o -7 2 2 19.29 18.90 2.01 o -6 2 2 148.32 152.35 4.61 o -5 2 2 567.40 572.77 11.71 o -4 2 2 77.23 75.71 1.82 o -3 2 2 939.72 874.15 11.43 o -2 2 2 49.08 50.99 0.87 o -1 2 2 654.23 716.05 8.31 o 0 2 2 88.71 77.13 1.24 o 1 2 2 10511.32 7565.11 352.73 o 2 2 2 738.42 730.55 11.18 o 3 2 2 2.92 1.29 0.34 o 4 2 2 1691.94 1632.16 29.96 o 5 2 2 83.12 84.13 2.98 o 6 2 2 5.79 5.94 0.97 o 7 2 2 61.57 62.10 2.85 o 8 2 2 3.11 1.99 0.89 o -8 3 2 24.50 25.00 2.04 o -7 3 2 7.85 10.13 1.32 o -6 3 2 0.87 1.12 0.63 o -5 3 2 60.85 62.85 1.90 o -4 3 2 62.98 62.50 1.36 o -3 3 2 216.03 218.29 4.50 o -2 3 2 15.31 19.38 0.46 o -1 3 2 974.03 994.71 14.84 o 0 3 2 147.96 180.13 2.96 o 1 3 2 16.66 24.94 0.93 o 2 3 2 7.58 7.68 0.77 o 3 3 2 1066.68 1138.54 17.31 o 4 3 2 32.38 35.22 1.33 o 5 3 2 0.90 0.94 0.61 o 6 3 2 32.68 34.66 1.91 o 7 3 2 35.30 33.39 2.07 o 8 3 2 0.44 1.67 0.87 o -8 4 2 39.27 35.95 2.37 o -7 4 2 59.15 59.27 2.81 o -6 4 2 365.15 382.75 9.01 o -5 4 2 52.46 55.88 5.83 o -4 4 2 65.19 71.30 1.80 o -3 4 2 235.11 210.85 7.35 o -2 4 2 3.59 1.38 0.37 o -1 4 2 306.21 359.34 7.24 o 0 4 2 2297.83 2211.29 27.99 o 1 4 2 4869.86 4290.27 53.98 o 2 4 2 2188.73 2343.37 47.21 o 3 4 2 139.75 143.13 3.14 o 4 4 2 390.85 420.86 7.29 o 5 4 2 23.19 21.51 1.17 o 6 4 2 124.39 129.44 4.01 o 7 4 2 70.29 82.23 3.28 o -7 5 2 6.76 6.26 1.14 o -6 5 2 5.10 7.23 1.10 o -5 5 2 242.66 244.88 5.55 o -4 5 2 5.08 4.99 0.60 o -3 5 2 23.92 23.09 1.00 o -2 5 2 124.08 129.84 2.62 o -1 5 2 662.46 685.05 9.05 o 0 5 2 1008.46 1044.03 13.53 o 1 5 2 31.21 23.06 0.71 o 2 5 2 162.57 179.57 2.49 o 3 5 2 0.67 0.75 0.28 o 4 5 2 1.19 1.44 0.37 o 5 5 2 375.45 385.99 7.10 o 6 5 2 48.75 48.62 2.54 o 7 5 2 165.06 160.46 5.34 o -7 6 2 24.09 26.30 2.92 o -6 6 2 65.04 67.99 2.94 o -5 6 2 182.80 196.08 4.35 o -4 6 2 13.26 12.81 0.91 o -3 6 2 1.39 3.67 1.99 o -2 6 2 63.53 51.97 1.48 o -1 6 2 169.31 157.75 2.49 o 0 6 2 393.17 388.67 5.44 o 1 6 2 1078.54 1102.46 14.42 o 2 6 2 1.56 1.35 0.29 o 3 6 2 1.67 1.51 0.60 o 4 6 2 229.01 244.39 6.15 o 5 6 2 98.12 100.12 3.78 o 6 6 2 203.03 196.28 4.83 o 7 6 2 23.71 23.80 2.05 o -7 7 2 0.03 0.80 0.76 o -6 7 2 4.28 4.80 1.09 o -5 7 2 37.25 43.13 1.77 o -4 7 2 179.40 186.37 4.04 o -3 7 2 46.77 47.72 1.57 o -2 7 2 344.91 343.43 6.01 o -1 7 2 107.46 106.56 2.36 o 0 7 2 45.59 36.49 1.18 o 1 7 2 255.02 262.06 4.01 o 2 7 2 80.56 84.08 2.44 o 3 7 2 0.72 2.42 0.49 o 4 7 2 71.97 67.25 2.19 o 5 7 2 38.82 36.86 1.73 o 6 7 2 20.30 22.02 1.56 o -6 8 2 1.90 3.15 0.95 o -5 8 2 8.61 8.61 0.94 o -4 8 2 87.99 97.48 3.80 o -3 8 2 162.37 157.90 3.48 o -2 8 2 8.81 9.08 0.73 o -1 8 2 9.07 9.90 0.70 o 0 8 2 99.01 109.49 2.46 o 1 8 2 432.09 397.58 6.74 o 2 8 2 97.52 83.67 2.19 o 3 8 2 49.80 49.24 2.81 o 4 8 2 718.59 699.74 17.75 o 5 8 2 0.01 0.88 0.71 o 6 8 2 48.42 48.67 2.22 o -6 9 2 0.10 0.30 0.81 o -5 9 2 100.32 92.39 3.57 o -4 9 2 2.56 2.07 0.59 o -3 9 2 40.27 39.53 1.57 o -2 9 2 55.35 51.33 1.70 o -1 9 2 23.72 20.82 1.02 o 0 9 2 215.62 216.21 4.20 o 1 9 2 891.33 802.08 44.60 o 2 9 2 21.86 21.66 2.59 o 3 9 2 55.71 47.03 1.76 o 4 9 2 31.57 30.15 1.54 o 5 9 2 1.67 2.28 0.67 o -5 10 2 41.10 45.29 2.51 o -4 10 2 2.32 3.52 0.71 o -3 10 2 292.43 286.79 7.11 o -2 10 2 231.66 223.39 4.59 o -1 10 2 432.38 416.16 7.36 o 0 10 2 0.49 1.12 0.59 o 1 10 2 133.14 133.28 3.85 o 2 10 2 27.10 29.47 1.69 o 3 10 2 0.27 0.67 0.59 o 4 10 2 45.17 43.37 2.27 o 5 10 2 30.63 34.49 2.62 o -4 11 2 2.06 0.78 0.76 o -3 11 2 31.87 34.31 2.06 o -2 11 2 3.64 3.31 0.79 o -1 11 2 20.19 20.55 1.73 o 0 11 2 0.01 0.34 0.56 o 1 11 2 57.42 55.32 2.35 o 2 11 2 16.26 16.03 1.34 o 3 11 2 64.69 64.13 2.76 o 4 11 2 13.37 15.90 1.53 o -3 12 2 13.53 17.87 2.16 o -2 12 2 30.78 37.55 2.01 o -1 12 2 91.80 98.60 3.37 o 0 12 2 7.48 5.22 0.89 o 1 12 2 122.42 113.03 3.74 o 2 12 2 36.46 34.04 1.99 o 3 12 2 79.03 78.70 3.22 o -7 0 3 0.00 0.00 0.83 o -5 0 3 45.46 51.65 3.09 o -3 0 3 130.19 129.20 4.51 o -1 0 3 1170.45 1201.96 17.61 o 1 0 3 1847.68 1768.76 31.34 o 3 0 3 1581.17 1619.72 41.58 o 5 0 3 143.78 138.87 5.65 o 7 0 3 70.67 69.01 4.29 o -8 1 3 12.88 11.44 2.11 o -7 1 3 41.93 39.49 2.17 o -6 1 3 240.28 240.61 6.17 o -5 1 3 16.51 19.58 1.05 o -4 1 3 3004.86 3077.80 44.75 o -3 1 3 2028.77 1633.45 321.15 o -2 1 3 0.06 3.19 0.29 o -1 1 3 364.46 343.64 4.10 o 0 1 3 1520.55 1624.51 20.42 o 1 1 3 34.90 32.39 1.21 o 2 1 3 1092.58 993.83 14.98 o 3 1 3 38.12 36.65 1.45 o 4 1 3 973.84 989.21 18.76 o 5 1 3 46.42 43.53 1.97 o 6 1 3 171.46 170.38 4.89 o 7 1 3 240.09 238.53 6.51 o 8 1 3 20.67 20.78 1.89 o -8 2 3 14.26 12.95 1.50 o -7 2 3 41.71 46.63 3.60 o -6 2 3 0.87 1.09 0.57 o -5 2 3 11.74 9.66 0.85 o -4 2 3 250.30 260.11 4.00 o -3 2 3 57.63 55.89 1.19 o -2 2 3 5.76 3.48 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