#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/76/2227636.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227636_Fobs loop_ _publ_author_name 'Li, Fu-An' _publ_section_title ; Tetraaquabis[4-(pyrazin-2-ylsulfanylmethyl-\kN^4^)benzoato]cobalt(II) ; _journal_coeditor_code HY2354 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1323 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.640 _cell_angle_gamma 90.000 _cell_length_a 14.6561 _cell_length_b 11.0666 _cell_length_c 7.9973 _exptl_crystal_F_000 642.00 _reflns_d_resolution_high 0.7587 _[local]_cod_data_source_file hy2354Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' LJB3 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 159.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1854.37 -1.38 1.38 o 2 0 0 59.58 58.18 5.13 o 3 0 0 2878.70 2689.99 71.90 o 4 0 0 2.71 6.04 8.55 o 5 0 0 5170.09 5082.57 176.53 o 6 0 0 1543.79 1532.84 48.74 o 7 0 0 4901.90 5278.21 142.53 o 8 0 0 1480.75 1363.04 37.41 o 9 0 0 36.87 27.51 18.22 o 10 0 0 2658.13 2784.92 68.04 o 11 0 0 1971.37 1853.03 51.16 o 12 0 0 929.46 892.58 33.69 o 13 0 0 1303.03 1294.29 50.77 o 14 0 0 318.01 369.95 27.25 o 15 0 0 282.24 289.59 26.19 o 16 0 0 554.90 584.21 58.61 o 17 0 0 115.72 149.70 40.73 o 18 0 0 906.04 966.43 76.78 o 19 0 0 26.23 1.65 36.60 o 1 1 0 1.12 6.73 1.77 o 2 1 0 50.31 65.61 3.30 o 3 1 0 2306.10 2328.68 35.88 o 4 1 0 1152.86 1079.74 21.65 o 5 1 0 350.66 361.73 18.97 o 6 1 0 638.53 611.10 29.49 o 7 1 0 13.06 21.64 6.45 o 8 1 0 44.32 51.12 8.08 o 9 1 0 55.73 54.16 9.12 o 10 1 0 289.75 279.31 24.35 o 11 1 0 218.47 225.42 14.33 o 12 1 0 1198.10 1176.97 30.13 o 13 1 0 39.11 39.96 11.29 o 14 1 0 46.15 45.31 11.59 o 15 1 0 161.30 182.41 15.94 o 16 1 0 86.19 85.49 17.59 o 17 1 0 1.65 -12.00 22.01 o 18 1 0 5.69 1.19 24.57 o 19 1 0 135.83 121.27 31.61 o 0 2 0 12923.38 13287.08 332.64 o 1 2 0 2109.02 2115.71 40.04 o 2 2 0 4380.50 4210.70 113.87 o 3 2 0 2901.94 2680.32 45.35 o 4 2 0 57.18 43.28 7.37 o 5 2 0 17553.73 16775.13 264.33 o 6 2 0 5364.16 5409.87 90.00 o 7 2 0 1282.64 1180.98 26.10 o 8 2 0 2138.47 2096.95 41.17 o 9 2 0 361.42 343.82 14.83 o 10 2 0 1810.45 1752.94 38.56 o 11 2 0 1385.74 1300.26 36.43 o 12 2 0 1330.65 1362.11 38.13 o 13 2 0 149.71 143.35 20.31 o 14 2 0 2.61 18.47 10.79 o 15 2 0 682.21 741.22 34.18 o 16 2 0 439.81 501.96 28.89 o 17 2 0 1.61 25.80 22.42 o 18 2 0 458.40 497.40 41.96 o 19 2 0 12.89 55.31 35.77 o 1 3 0 347.50 368.13 18.19 o 2 3 0 2871.19 2877.09 55.14 o 3 3 0 624.83 615.01 17.18 o 4 3 0 614.46 666.17 18.41 o 5 3 0 1095.81 1089.74 23.06 o 6 3 0 403.52 405.91 12.72 o 7 3 0 1835.29 1715.90 37.41 o 8 3 0 136.49 148.70 10.68 o 9 3 0 308.34 319.95 14.61 o 10 3 0 269.18 282.92 15.06 o 11 3 0 839.54 797.42 30.52 o 12 3 0 1095.02 1022.48 32.60 o 13 3 0 283.74 261.84 20.14 o 14 3 0 36.65 35.95 16.37 o 15 3 0 39.67 23.47 15.64 o 16 3 0 172.10 172.31 20.90 o 17 3 0 2.01 -21.74 21.74 o 18 3 0 27.86 8.26 34.67 o 0 4 0 7168.42 6816.37 176.10 o 1 4 0 294.25 321.81 12.54 o 2 4 0 647.76 657.41 18.45 o 3 4 0 7410.33 7497.88 137.21 o 4 4 0 1066.43 946.59 24.78 o 5 4 0 12786.47 12200.16 220.76 o 6 4 0 2860.56 2869.01 58.80 o 7 4 0 12.49 -3.32 7.24 o 8 4 0 1740.46 1665.07 45.71 o 9 4 0 315.37 322.02 15.22 o 10 4 0 1720.61 1642.16 41.86 o 11 4 0 146.38 180.40 15.38 o 12 4 0 527.90 509.44 23.32 o 13 4 0 1317.93 1248.57 45.14 o 14 4 0 349.36 332.49 49.81 o 15 4 0 83.74 101.90 31.10 o 16 4 0 121.56 114.20 36.60 o 17 4 0 5.36 -30.27 30.27 o 18 4 0 145.21 247.66 48.71 o 1 5 0 1120.43 1159.90 28.60 o 2 5 0 13.27 14.95 7.42 o 3 5 0 797.02 872.64 23.53 o 4 5 0 177.65 198.79 11.63 o 5 5 0 25.25 32.71 8.46 o 6 5 0 195.58 198.97 12.73 o 7 5 0 2456.66 2336.46 51.61 o 8 5 0 38.20 33.47 11.44 o 9 5 0 6.57 0.86 20.26 o 10 5 0 0.54 -2.09 14.02 o 11 5 0 807.29 708.65 32.32 o 12 5 0 521.31 492.30 28.07 o 13 5 0 386.14 368.68 25.89 o 14 5 0 15.39 29.44 30.54 o 15 5 0 255.17 241.33 43.75 o 16 5 0 157.79 142.82 39.90 o 17 5 0 142.51 186.57 44.30 o 18 5 0 57.13 -27.79 34.40 o 0 6 0 3182.03 3020.70 86.59 o 1 6 0 1482.67 1534.33 35.70 o 2 6 0 6870.06 6963.88 130.22 o 3 6 0 1930.48 1866.11 67.88 o 4 6 0 785.38 778.54 24.25 o 5 6 0 736.23 660.49 23.08 o 6 6 0 866.42 807.29 25.84 o 7 6 0 326.28 333.47 24.89 o 8 6 0 294.01 321.95 36.13 o 9 6 0 850.55 804.85 32.79 o 10 6 0 114.03 135.48 15.58 o 11 6 0 319.41 312.75 23.46 o 12 6 0 309.21 282.17 29.26 o 13 6 0 368.52 404.05 74.16 o 14 6 0 41.92 100.72 34.12 o 15 6 0 328.68 279.58 47.06 o 16 6 0 81.74 108.42 39.63 o 17 6 0 110.17 203.63 47.06 o 1 7 0 59.09 45.98 10.30 o 2 7 0 674.70 621.56 22.56 o 3 7 0 90.90 99.28 11.69 o 4 7 0 584.03 623.87 27.38 o 5 7 0 295.22 309.90 20.22 o 6 7 0 39.59 37.14 13.85 o 7 7 0 993.20 921.17 35.03 o 8 7 0 0.70 21.76 14.57 o 9 7 0 81.08 126.64 21.82 o 10 7 0 569.90 609.55 30.65 o 11 7 0 518.40 489.91 43.89 o 12 7 0 185.99 216.25 28.21 o 13 7 0 3.60 -11.32 20.03 o 14 7 0 20.40 77.88 34.95 o 15 7 0 341.01 285.09 47.88 o 16 7 0 460.51 605.67 65.22 o 0 8 0 145.42 113.10 28.07 o 1 8 0 708.68 677.44 38.11 o 2 8 0 670.84 689.16 35.31 o 3 8 0 536.69 462.07 33.71 o 4 8 0 1373.30 1407.16 53.78 o 5 8 0 405.17 347.09 27.25 o 6 8 0 212.88 219.19 23.54 o 7 8 0 179.30 171.60 22.91 o 8 8 0 376.10 417.44 30.74 o 9 8 0 1390.91 1314.09 54.82 o 10 8 0 279.70 269.76 31.35 o 11 8 0 453.01 450.37 28.46 o 12 8 0 541.63 601.80 40.78 o 13 8 0 22.99 10.30 21.70 o 14 8 0 69.23 148.32 39.08 o 15 8 0 57.36 57.79 38.53 o 16 8 0 14.72 28.34 38.53 o 1 9 0 0.14 11.04 29.72 o 2 9 0 491.19 430.29 30.05 o 3 9 0 203.72 213.41 24.00 o 4 9 0 92.52 114.40 21.81 o 5 9 0 19.09 30.33 18.10 o 6 9 0 1285.84 1225.67 51.08 o 7 9 0 245.94 228.05 25.65 o 8 9 0 1.68 -16.89 16.89 o 9 9 0 39.29 88.65 22.33 o 10 9 0 570.95 509.99 36.83 o 11 9 0 283.98 277.79 24.75 o 12 9 0 163.04 191.27 29.62 o 13 9 0 3.79 -15.56 21.79 o 14 9 0 9.88 -7.15 34.12 o 15 9 0 27.22 -17.34 37.15 o 0 10 0 63.73 94.39 30.54 o 1 10 0 658.77 724.32 39.73 o 2 10 0 4.29 3.13 16.99 o 3 10 0 734.56 709.15 39.68 o 4 10 0 873.00 809.71 80.35 o 5 10 0 63.09 47.16 19.61 o 6 10 0 847.72 814.67 52.70 o 7 10 0 1267.85 1191.16 52.82 o 8 10 0 93.44 70.73 48.98 o 9 10 0 5.42 26.12 21.29 o 10 10 0 185.77 163.13 26.52 o 11 10 0 226.71 181.44 23.28 o 12 10 0 155.13 185.51 25.06 o 13 10 0 8.87 2.70 23.79 o 14 10 0 330.49 413.04 57.51 o 1 11 0 16.13 15.93 36.87 o 2 11 0 0.15 -18.18 18.18 o 3 11 0 35.26 23.22 31.23 o 4 11 0 11.53 -7.29 19.11 o 5 11 0 0.04 3.75 18.68 o 6 11 0 34.66 43.05 20.33 o 7 11 0 29.17 5.73 49.53 o 8 11 0 16.81 20.46 20.80 o 9 11 0 86.68 92.26 25.61 o 10 11 0 15.67 13.35 22.42 o 11 11 0 23.52 -6.92 18.26 o 12 11 0 104.14 120.97 23.92 o 0 12 0 5.64 -25.32 28.62 o 1 12 0 955.11 947.97 58.34 o 2 12 0 234.99 220.58 28.39 o 3 12 0 0.90 -33.49 38.80 o 4 12 0 589.03 603.67 96.73 o 5 12 0 1.13 2.59 19.39 o 6 12 0 271.28 278.17 31.09 o 7 12 0 88.09 71.56 24.98 o 8 12 0 20.16 15.81 25.73 o 9 12 0 247.40 267.88 64.53 o 10 12 0 12.80 -5.88 23.64 o 1 13 0 2.59 34.33 21.95 o 2 13 0 5.17 -17.20 20.72 o 3 13 0 13.53 11.53 22.33 o 4 13 0 63.80 36.10 23.90 o 5 13 0 1.54 18.27 38.39 o 6 13 0 48.97 98.00 26.21 o 7 13 0 51.50 44.85 25.20 o 8 13 0 26.82 23.98 24.57 o 0 14 0 23.62 -29.99 33.02 o 1 14 0 158.10 159.43 35.36 o 2 14 0 161.67 116.44 64.53 o 3 14 0 27.33 -1.41 23.53 o 4 14 0 57.60 49.69 46.23 o 5 14 0 17.10 -0.74 24.22 o -19 1 1 157.35 200.41 33.17 o -18 1 1 170.77 160.48 30.25 o -17 1 1 1.08 -12.51 19.58 o -16 1 1 1019.57 1037.23 53.02 o -15 1 1 381.01 355.03 32.79 o -14 1 1 2257.09 2254.30 62.19 o -13 1 1 4602.50 4401.70 87.40 o -12 1 1 1082.52 1076.15 30.28 o -11 1 1 1243.64 1277.77 29.78 o -10 1 1 466.35 495.13 19.55 o -9 1 1 770.06 760.34 18.28 o -8 1 1 5915.42 5829.27 87.93 o -7 1 1 1059.51 1104.13 21.95 o -6 1 1 5792.24 6097.84 122.61 o -5 1 1 1047.18 927.45 33.30 o -4 1 1 688.11 642.10 21.25 o -3 1 1 5141.15 5165.26 93.76 o -2 1 1 2896.69 3053.56 55.99 o -1 1 1 286.38 260.27 6.99 o 0 1 1 8428.71 8013.24 143.77 o 1 1 1 2320.81 2332.00 49.88 o 2 1 1 5732.46 5590.07 120.98 o 3 1 1 4000.25 3834.15 71.37 o 4 1 1 1990.35 2113.39 42.96 o 5 1 1 2549.06 2500.90 87.86 o 6 1 1 3688.87 4004.55 119.08 o 7 1 1 1288.59 1273.37 31.77 o 8 1 1 1495.68 1392.45 30.76 o 9 1 1 23.84 14.14 8.82 o 10 1 1 3358.66 3476.06 65.01 o 11 1 1 1117.93 1058.85 28.83 o 12 1 1 2.77 -2.23 10.98 o 13 1 1 1376.71 1338.77 38.77 o 14 1 1 95.18 110.83 13.91 o 15 1 1 1406.10 1507.40 42.14 o 16 1 1 8.51 22.01 12.35 o 17 1 1 1.73 -5.08 15.26 o 18 1 1 115.88 73.47 35.50 o 19 1 1 19.38 43.75 37.70 o -19 2 1 5.78 13.29 70.86 o -18 2 1 44.86 18.76 48.02 o -17 2 1 3.83 -13.49 20.88 o -16 2 1 4.76 -2.81 20.64 o -15 2 1 0.71 -4.80 20.00 o -14 2 1 28.32 12.36 43.34 o -13 2 1 2.63 -6.56 21.16 o -12 2 1 601.30 590.10 27.84 o -11 2 1 77.88 71.78 11.31 o -10 2 1 67.83 80.83 13.92 o -9 2 1 25.33 22.34 8.26 o -8 2 1 315.43 380.50 19.22 o -7 2 1 138.21 179.33 11.23 o -6 2 1 136.27 161.66 9.94 o -5 2 1 780.35 732.32 22.63 o -4 2 1 410.72 376.15 13.94 o -3 2 1 154.89 153.66 7.90 o -2 2 1 35.46 50.04 5.02 o -1 2 1 25527.39 26746.48 471.45 o 0 2 1 10955.66 11286.12 177.04 o 1 2 1 2798.04 3026.91 70.86 o 2 2 1 461.94 489.52 12.03 o 3 2 1 1.66 4.65 5.06 o 4 2 1 1375.59 1250.16 29.17 o 5 2 1 2370.15 2394.71 39.43 o 6 2 1 6761.95 7241.68 123.44 o 7 2 1 7.23 13.51 6.99 o 8 2 1 231.08 222.33 12.11 o 9 2 1 2.47 -7.70 7.70 o 10 2 1 9.25 17.65 11.39 o 11 2 1 2356.70 2260.09 47.74 o 12 2 1 170.51 166.78 15.50 o 13 2 1 10.64 6.88 11.98 o 14 2 1 77.39 62.14 14.09 o 15 2 1 23.16 16.85 15.29 o 16 2 1 12.74 1.20 14.09 o 17 2 1 8.14 -12.54 18.12 o 18 2 1 491.64 665.50 66.59 o 19 2 1 4.15 -34.95 34.95 o -18 3 1 452.73 492.96 73.61 o -17 3 1 2.20 2.72 22.76 o -16 3 1 633.31 651.15 43.87 o -15 3 1 67.19 52.42 23.01 o -14 3 1 577.93 553.76 64.12 o -13 3 1 211.01 246.70 33.30 o -12 3 1 230.04 234.22 86.82 o -11 3 1 2847.17 2884.47 74.81 o -10 3 1 1734.89 1661.02 49.13 o -9 3 1 1847.81 1819.43 50.73 o -8 3 1 10422.78 10164.32 187.36 o -7 3 1 38.15 40.99 8.42 o -6 3 1 674.69 578.59 21.55 o -5 3 1 3955.05 3992.80 68.06 o -4 3 1 1735.95 1847.48 41.39 o -3 3 1 4437.05 4526.02 84.14 o -2 3 1 1804.89 1955.67 43.93 o -1 3 1 10502.57 11368.01 202.90 o 0 3 1 114.70 136.31 12.70 o 1 3 1 790.34 854.67 20.75 o 2 3 1 53.93 51.08 8.80 o 3 3 1 7.52 -3.01 5.29 o 4 3 1 30.22 25.53 5.82 o 5 3 1 5423.33 5509.53 91.70 o 6 3 1 62.56 75.95 7.90 o 7 3 1 1574.72 1348.63 27.19 o 8 3 1 1515.06 1340.03 30.72 o 9 3 1 775.89 817.88 31.07 o 10 3 1 4228.07 4248.17 77.78 o 11 3 1 111.61 124.61 13.34 o 12 3 1 136.67 130.88 15.89 o 13 3 1 636.94 676.11 27.68 o 14 3 1 55.77 48.25 14.33 o 15 3 1 1017.60 1025.38 49.06 o 16 3 1 45.31 26.93 18.07 o 17 3 1 3.00 3.28 28.48 o 18 3 1 455.06 535.40 40.09 o -18 4 1 20.92 28.58 25.72 o -17 4 1 120.87 157.57 29.42 o -16 4 1 1.80 10.28 21.75 o -15 4 1 148.83 163.32 29.31 o -14 4 1 9.20 -18.24 18.24 o -13 4 1 59.14 17.05 18.91 o -12 4 1 1.35 -3.78 14.09 o -11 4 1 132.94 129.21 17.58 o -10 4 1 460.50 422.38 23.92 o -9 4 1 62.90 25.95 13.75 o -8 4 1 15.82 -1.24 14.11 o -7 4 1 0.12 -2.74 9.64 o -6 4 1 3571.74 3698.35 74.85 o -5 4 1 705.21 752.02 21.32 o -4 4 1 309.91 281.22 12.03 o -3 4 1 265.54 272.31 11.50 o -2 4 1 743.43 821.32 27.31 o -1 4 1 7346.27 7575.64 137.75 o 0 4 1 15.11 10.36 9.36 o 1 4 1 579.78 686.60 21.91 o 2 4 1 45.61 66.44 8.22 o 3 4 1 786.97 859.69 22.24 o 4 4 1 2237.68 2246.72 61.68 o 5 4 1 124.38 108.68 8.55 o 6 4 1 1168.39 1197.57 26.82 o 7 4 1 38.13 37.97 8.40 o 8 4 1 716.02 667.14 19.37 o 9 4 1 282.74 278.65 15.23 o 10 4 1 131.22 109.67 12.89 o 11 4 1 25.06 31.59 15.23 o 12 4 1 28.15 10.58 11.91 o 13 4 1 0.61 23.98 12.54 o 14 4 1 18.20 49.51 16.25 o 15 4 1 33.76 12.77 27.11 o 16 4 1 103.18 73.16 22.03 o 17 4 1 160.71 208.95 28.50 o 18 4 1 12.56 10.31 19.86 o -18 5 1 166.90 140.34 42.65 o -17 5 1 20.74 15.13 33.02 o -16 5 1 742.96 803.60 56.41 o -15 5 1 42.85 64.67 23.54 o -14 5 1 89.41 62.33 23.31 o -13 5 1 1301.27 1324.10 59.03 o -12 5 1 353.17 345.48 24.18 o -11 5 1 974.45 973.97 38.16 o -10 5 1 895.53 870.40 34.67 o -9 5 1 281.98 283.69 20.55 o -8 5 1 699.24 680.29 24.44 o -7 5 1 381.88 360.04 16.97 o -6 5 1 903.16 863.20 30.36 o -5 5 1 2506.85 2700.34 55.94 o -4 5 1 259.15 244.94 12.35 o -3 5 1 2013.50 1986.76 42.47 o -2 5 1 2206.97 2212.49 46.15 o -1 5 1 1330.24 1320.89 30.58 o 0 5 1 4740.43 4857.03 106.53 o 1 5 1 1676.27 1890.83 82.61 o 2 5 1 440.64 378.45 16.96 o 3 5 1 812.50 826.04 23.10 o 4 5 1 3003.35 2983.67 85.24 o 5 5 1 623.85 558.24 19.66 o 6 5 1 85.79 85.62 10.60 o 7 5 1 509.19 518.49 18.71 o 8 5 1 490.14 408.62 16.84 o 9 5 1 9.02 5.80 10.02 o 10 5 1 1016.23 969.92 31.09 o 11 5 1 342.70 344.01 20.41 o 12 5 1 4.91 -3.47 13.22 o 13 5 1 100.47 100.62 17.72 o 14 5 1 57.75 33.80 15.73 o 15 5 1 596.20 584.45 60.40 o 16 5 1 36.53 -6.33 33.02 o 17 5 1 114.42 205.83 47.33 o 18 5 1 188.37 173.09 47.88 o -17 6 1 54.92 89.98 36.87 o -16 6 1 27.84 56.14 35.22 o -15 6 1 0.19 -8.26 28.62 o -14 6 1 37.11 33.50 22.07 o -13 6 1 225.96 230.26 38.25 o -12 6 1 2.56 -9.12 15.02 o -11 6 1 91.88 111.68 17.94 o -10 6 1 155.56 190.17 19.14 o -9 6 1 249.65 261.16 17.56 o -8 6 1 4.26 -9.29 10.54 o -7 6 1 463.61 455.94 41.57 o -6 6 1 1021.31 1011.16 33.66 o -5 6 1 1379.68 1427.93 35.35 o -4 6 1 60.17 89.70 10.54 o -3 6 1 341.94 412.51 17.03 o -2 6 1 117.75 111.09 10.64 o -1 6 1 6041.75 5799.49 140.90 o 0 6 1 23.15 31.95 10.24 o 1 6 1 194.65 182.57 11.93 o 2 6 1 567.25 551.44 19.41 o 3 6 1 1515.58 1587.97 58.90 o 4 6 1 2331.88 2491.36 66.01 o 5 6 1 113.09 101.87 12.03 o 6 6 1 38.32 39.78 15.01 o 7 6 1 174.06 202.89 15.15 o 8 6 1 399.96 393.40 44.53 o 9 6 1 783.19 742.87 42.07 o 10 6 1 26.26 18.14 15.64 o 11 6 1 4.10 -1.02 17.41 o 12 6 1 469.57 423.93 48.29 o 13 6 1 84.31 97.14 24.61 o 14 6 1 69.30 113.22 35.22 o 15 6 1 19.13 56.91 24.41 o 16 6 1 188.63 223.45 48.16 o 17 6 1 32.94 31.10 38.53 o -16 7 1 92.28 37.42 37.70 o -15 7 1 477.78 446.62 55.31 o -14 7 1 143.89 140.34 35.22 o -13 7 1 156.59 192.35 36.60 o -12 7 1 494.77 529.63 71.41 o -11 7 1 1046.08 1044.75 40.91 o -10 7 1 34.60 17.03 14.57 o -9 7 1 310.88 342.91 23.01 o -8 7 1 352.86 320.91 36.25 o -7 7 1 211.83 218.51 32.43 o -6 7 1 515.35 517.59 32.81 o -5 7 1 1650.00 1652.73 66.48 o -4 7 1 2460.66 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27.79 32.20 o 2 6 9 32.62 -0.55 31.10 o 3 6 9 9.17 26.47 27.38 o 4 6 9 26.44 24.76 17.38 o 5 6 9 93.01 108.78 21.33 o -3 7 9 42.52 47.61 36.32 o -2 7 9 76.76 79.80 37.97 o -1 7 9 29.20 17.61 36.05 o 0 7 9 119.92 124.38 41.00 o 1 7 9 1.30 38.80 37.15 o 2 7 9 94.08 69.62 37.15 o 3 7 9 177.68 104.29 40.45 o -6 0 10 197.63 225.92 29.17 o -5 0 10 50.65 25.32 21.19 o -4 0 10 102.42 116.13 25.32 o -3 0 10 9.92 48.43 22.56 o -2 0 10 90.86 66.87 23.39 o -1 0 10 148.84 165.38 28.07 o 0 0 10 42.30 66.87 23.94 o 1 0 10 14.30 14.58 23.94 o 2 0 10 375.00 367.64 41.00 o 3 0 10 12.12 15.41 24.49 o 4 0 10 8.62 11.01 26.69 o 5 0 10 198.96 171.16 36.87 o -6 1 10 1.57 3.46 19.40 o -5 1 10 0.09 -2.09 13.53 o -4 1 10 3.87 7.27 13.82 o -3 1 10 7.54 0.78 14.15 o -2 1 10 16.88 32.39 15.82 o -1 1 10 53.24 61.41 36.19 o 0 1 10 12.45 15.94 18.85 o 1 1 10 9.04 -5.11 15.75 o 2 1 10 90.23 73.72 18.76 o 3 1 10 7.20 -10.14 17.29 o 4 1 10 65.94 95.06 25.18 o 5 1 10 20.02 -18.68 18.68 o -5 2 10 5.53 8.53 24.77 o -4 2 10 78.05 49.26 27.79 o -3 2 10 48.82 30.27 24.49 o -2 2 10 58.69 35.63 14.29 o -1 2 10 215.53 198.29 19.87 o 0 2 10 10.75 -6.01 14.93 o 1 2 10 1.15 5.46 16.46 o 2 2 10 123.02 100.22 33.98 o 3 2 10 309.50 298.15 27.17 o 4 2 10 198.89 212.33 25.66 o 5 2 10 4.24 15.52 19.32 o -4 3 10 0.71 14.86 25.32 o -3 3 10 55.21 79.25 29.99 o -2 3 10 14.77 56.14 28.07 o -1 3 10 3.43 6.05 24.77 o 0 3 10 51.98 29.72 27.52 o 1 3 10 92.67 96.17 47.61 o 2 3 10 4.05 21.10 32.88 o 3 3 10 0.10 8.20 16.73 o 4 3 10 37.11 30.73 33.71 o -3 4 10 118.13 109.52 33.85 o -2 4 10 3.00 -26.42 26.42 o -1 4 10 143.88 211.89 39.08 o 0 4 10 138.09 98.24 34.95 o 1 4 10 82.17 39.08 30.82 o 2 4 10 36.14 41.44 15.70 o