#------------------------------------------------------------------------------ #$Date: 2010-12-22 21:36:50 +0200 (Wed, 22 Dec 2010) $ #$Revision: 5269 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2227643.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227643_Fobs loop_ _publ_author_name 'Wang, Peng' 'Wan, Rong' 'Yu, Peng' 'He, Qiu' 'Zhang, Jian-qiang' _publ_section_title ; 1-(3-Chloropyridin-2-yl)hydrazine ; _journal_coeditor_code IM2217 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2599 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.460 _cell_angle_gamma 90.000 _cell_length_a 11.6370 _cell_length_b 3.9060 _cell_length_c 13.9460 _exptl_crystal_F_000 296.00 _reflns_d_resolution_high 0.8322 _[local]_cod_data_source_file im2217Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I' _shelx_refln_list_code 4 _shelx_f_calc_maximum 99.29 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 111.21 110.64 2.87 o 2 0 0 3799.43 3472.04 23.25 o 3 0 0 4693.50 4830.98 32.60 o 4 0 0 121.69 133.56 5.34 o 5 0 0 298.99 313.79 8.95 o 6 0 0 806.71 814.44 16.33 o 7 0 0 202.51 201.96 8.92 o 8 0 0 313.03 317.66 12.15 o 9 0 0 61.18 58.66 6.16 o 10 0 0 284.28 301.22 13.99 o 11 0 0 15.64 12.44 3.93 o 12 0 0 10.69 12.17 3.02 o 13 0 0 128.92 124.79 10.46 o 1 1 0 845.91 886.09 40.16 o 2 1 0 2598.94 2728.48 31.56 o 3 1 0 35.06 37.33 1.60 o 4 1 0 3585.79 3407.57 27.64 o 5 1 0 7.06 6.90 2.04 o 6 1 0 228.73 240.55 6.19 o 7 1 0 633.48 640.31 16.78 o 8 1 0 2.24 3.29 1.56 o 9 1 0 312.52 324.69 9.14 o 10 1 0 261.74 262.69 11.70 o 11 1 0 249.36 262.50 9.61 o 12 1 0 91.17 86.82 5.93 o 13 1 0 2.48 1.83 2.45 o 0 2 0 135.80 162.27 3.41 o 1 2 0 130.33 128.08 3.96 o 2 2 0 466.28 469.23 7.78 o 3 2 0 561.50 540.71 8.81 o 4 2 0 364.25 380.86 14.80 o 5 2 0 284.69 284.46 7.76 o 6 2 0 266.02 266.85 13.74 o 7 2 0 255.11 255.66 7.92 o 8 2 0 66.94 70.91 4.40 o 9 2 0 54.48 51.12 5.00 o 10 2 0 0.85 1.11 1.57 o 11 2 0 176.18 180.44 11.18 o 12 2 0 4.75 8.01 2.54 o 1 3 0 30.04 33.04 9.40 o 2 3 0 42.38 43.50 8.79 o 3 3 0 9.66 7.43 2.05 o 4 3 0 16.58 14.00 2.54 o 5 3 0 118.91 122.14 5.57 o 6 3 0 8.32 10.10 2.03 o 7 3 0 109.48 107.25 6.05 o 8 3 0 35.76 30.24 3.57 o 9 3 0 6.41 7.06 1.84 o 10 3 0 17.76 16.08 2.88 o 0 4 0 1.51 0.92 2.50 o 1 4 0 1.07 0.61 3.87 o 2 4 0 3.10 6.23 3.09 o 3 4 0 18.13 17.05 3.05 o 4 4 0 14.01 13.17 3.50 o 5 4 0 4.74 1.58 2.23 o 6 4 0 1.89 4.84 2.42 o 7 4 0 38.14 33.99 6.62 o -13 1 1 0.30 0.27 2.81 o -12 1 1 0.03 1.61 2.07 o -11 1 1 104.67 89.81 7.89 o -10 1 1 324.15 334.22 23.65 o -9 1 1 4.12 4.32 2.26 o -8 1 1 2.04 1.87 1.52 o -7 1 1 6.61 7.99 1.75 o -6 1 1 103.28 108.83 6.67 o -5 1 1 616.66 638.26 15.18 o -4 1 1 35.09 35.89 2.08 o -3 1 1 213.00 213.97 4.34 o -2 1 1 353.42 364.76 8.21 o -1 1 1 1207.28 1252.33 48.95 o 0 1 1 3272.55 3260.47 63.49 o 1 1 1 6388.02 6520.49 68.27 o 2 1 1 2.85 5.44 0.81 o 3 1 1 2.15 2.55 0.99 o 4 1 1 363.04 385.95 19.26 o 5 1 1 45.58 53.67 2.95 o 6 1 1 10.64 8.95 1.69 o 7 1 1 69.03 65.89 4.45 o 8 1 1 15.44 15.68 4.02 o 9 1 1 109.19 119.29 5.93 o 10 1 1 52.89 49.25 4.28 o 11 1 1 91.17 99.82 8.75 o 12 1 1 3.85 2.70 2.07 o 13 1 1 0.77 0.56 2.55 o -12 2 1 1.08 2.13 2.35 o -11 2 1 1.60 4.48 2.89 o -10 2 1 26.64 22.17 3.36 o -9 2 1 79.70 78.73 5.11 o -8 2 1 0.23 0.84 3.63 o -7 2 1 118.39 136.00 6.31 o -6 2 1 8.24 7.47 2.09 o -5 2 1 2.08 1.00 1.47 o -4 2 1 42.08 35.68 2.62 o -3 2 1 450.27 425.20 7.66 o -2 2 1 11.09 11.21 1.45 o -1 2 1 454.76 462.49 10.00 o 0 2 1 265.93 258.94 3.89 o 1 2 1 74.37 72.28 3.13 o 2 2 1 7.12 5.05 1.06 o 3 2 1 8.94 7.99 1.30 o 4 2 1 0.86 3.26 1.72 o 5 2 1 470.85 483.84 9.43 o 6 2 1 242.47 218.38 6.85 o 7 2 1 53.73 56.13 3.62 o 8 2 1 79.91 69.80 4.34 o 9 2 1 20.29 19.08 3.83 o 10 2 1 109.24 103.81 6.20 o 11 2 1 77.14 73.96 5.46 o 12 2 1 60.14 59.32 4.78 o -10 3 1 19.20 18.05 3.60 o -9 3 1 5.89 6.76 2.69 o -8 3 1 45.10 48.08 4.56 o -7 3 1 3.88 3.63 3.98 o -6 3 1 31.01 34.84 3.57 o -5 3 1 196.87 205.67 7.58 o -4 3 1 20.30 22.27 3.44 o -3 3 1 32.42 28.56 2.80 o -2 3 1 240.57 236.31 7.39 o -1 3 1 39.95 38.83 3.19 o 0 3 1 193.24 206.84 4.71 o 1 3 1 153.22 147.40 5.62 o 2 3 1 78.36 78.00 4.27 o 3 3 1 190.56 198.00 8.35 o 4 3 1 36.85 34.84 4.07 o 5 3 1 139.64 147.70 6.24 o 6 3 1 131.82 134.27 6.00 o 7 3 1 4.81 8.26 2.33 o 8 3 1 230.87 205.97 8.23 o 9 3 1 5.49 11.19 2.37 o 10 3 1 37.83 33.76 3.78 o -7 4 1 52.02 44.20 5.34 o -6 4 1 87.43 95.91 7.27 o -5 4 1 0.75 2.47 4.57 o -4 4 1 177.51 169.31 8.06 o -3 4 1 44.26 50.41 10.86 o -2 4 1 66.21 65.52 5.62 o -1 4 1 220.81 208.24 11.06 o 0 4 1 7.87 8.09 1.96 o 1 4 1 36.51 36.66 4.92 o 2 4 1 52.96 55.05 4.36 o 3 4 1 0.37 2.22 4.68 o 4 4 1 36.46 40.49 4.52 o 5 4 1 25.15 20.80 3.58 o 6 4 1 14.44 14.44 3.35 o -13 0 2 91.51 82.73 7.84 o -12 0 2 39.03 37.51 4.71 o -11 0 2 124.15 121.84 9.20 o -10 0 2 2407.77 2383.62 36.48 o -9 0 2 494.84 491.42 15.69 o -8 0 2 682.28 641.97 16.47 o -7 0 2 786.77 809.63 17.48 o -6 0 2 9.24 7.09 1.88 o -5 0 2 1262.62 1302.68 18.03 o -4 0 2 1586.09 1548.46 17.87 o -3 0 2 570.53 604.97 9.43 o -2 0 2 608.30 656.84 8.65 o -1 0 2 2506.30 2655.37 17.84 o 0 0 2 461.41 457.41 5.15 o 1 0 2 1191.94 1301.37 12.02 o 2 0 2 140.86 138.99 4.44 o 3 0 2 5317.08 5433.46 37.00 o 4 0 2 1088.86 1085.48 16.09 o 5 0 2 4049.88 4155.36 37.93 o 6 0 2 365.16 354.96 11.04 o 7 0 2 123.34 135.42 7.65 o 8 0 2 752.34 784.38 19.26 o 9 0 2 45.38 49.52 5.54 o 10 0 2 12.28 9.94 4.44 o 11 0 2 166.44 170.29 9.97 o 12 0 2 0.49 0.59 1.61 o 13 0 2 27.25 31.50 4.31 o -13 1 2 9.86 10.48 3.91 o -12 1 2 109.35 118.82 5.98 o -11 1 2 13.72 15.68 2.24 o -10 1 2 1.36 1.13 2.10 o -9 1 2 245.65 249.68 16.80 o -8 1 2 238.06 216.13 6.87 o -7 1 2 89.32 80.80 3.96 o -6 1 2 2044.79 1959.94 42.63 o -5 1 2 104.18 105.48 6.73 o -4 1 2 394.44 396.17 6.79 o -3 1 2 1912.24 1738.25 72.84 o -2 1 2 680.78 665.42 7.16 o -1 1 2 3385.17 3417.08 123.63 o 0 1 2 1101.24 1102.93 17.55 o 1 1 2 9859.23 9263.42 142.01 o 2 1 2 591.94 553.97 18.38 o 3 1 2 14.77 16.92 1.49 o 4 1 2 1173.17 1146.62 12.12 o 5 1 2 125.82 126.08 3.79 o 6 1 2 29.07 34.12 2.69 o 7 1 2 610.43 612.45 11.60 o 8 1 2 4.29 3.59 1.42 o 9 1 2 5.91 7.31 2.00 o 10 1 2 18.80 22.08 3.27 o 11 1 2 7.63 6.63 2.54 o 12 1 2 5.51 4.46 2.63 o -12 2 2 10.66 11.37 3.32 o -11 2 2 15.22 15.58 2.64 o -10 2 2 13.52 12.07 2.91 o -9 2 2 14.14 14.76 2.76 o -8 2 2 138.02 153.04 6.49 o -7 2 2 66.70 60.92 3.87 o -6 2 2 304.56 337.15 8.38 o -5 2 2 211.01 208.61 6.17 o -4 2 2 59.34 56.10 3.17 o -3 2 2 1038.90 1022.43 12.12 o -2 2 2 98.24 98.46 6.02 o -1 2 2 80.26 82.77 3.27 o 0 2 2 127.27 123.91 3.27 o 1 2 2 2445.04 2525.15 38.90 o 2 2 2 18.50 17.31 1.78 o 3 2 2 514.82 509.37 11.10 o 4 2 2 276.47 261.24 6.83 o 5 2 2 10.69 6.94 1.66 o 6 2 2 209.70 195.64 10.52 o 7 2 2 23.66 24.61 3.29 o 8 2 2 45.30 53.42 7.52 o 9 2 2 194.48 190.32 14.71 o 10 2 2 29.39 26.24 3.59 o 11 2 2 113.61 114.57 6.63 o -10 3 2 0.98 0.60 2.61 o -9 3 2 5.59 10.35 3.85 o -8 3 2 2.17 2.15 1.83 o -7 3 2 15.20 18.89 2.74 o -6 3 2 18.49 17.84 2.70 o -5 3 2 49.53 59.32 4.14 o -4 3 2 88.35 87.33 4.72 o -3 3 2 247.49 245.60 7.82 o -2 3 2 15.09 17.12 3.52 o -1 3 2 142.64 139.47 5.74 o 0 3 2 104.05 110.54 5.76 o 1 3 2 12.57 16.36 2.32 o 2 3 2 73.36 75.29 6.58 o 3 3 2 16.11 13.99 2.64 o 4 3 2 5.23 3.25 2.06 o 5 3 2 66.34 64.53 4.54 o 6 3 2 24.89 22.47 3.30 o 7 3 2 58.07 61.89 4.47 o 8 3 2 23.31 23.86 3.34 o 9 3 2 14.75 14.18 4.07 o -7 4 2 8.63 8.48 3.28 o -6 4 2 2.05 4.38 2.12 o -5 4 2 14.29 13.03 3.20 o -4 4 2 2.11 3.36 2.11 o -3 4 2 11.09 14.11 2.98 o -2 4 2 121.13 116.43 7.16 o -1 4 2 19.28 14.19 3.07 o 0 4 2 15.32 11.84 2.18 o 1 4 2 1.25 0.58 2.82 o 2 4 2 76.36 60.35 5.45 o 3 4 2 1.42 4.67 2.70 o 4 4 2 41.68 35.61 6.46 o 5 4 2 1.84 3.58 2.52 o 6 4 2 41.83 41.21 4.44 o -13 1 3 15.67 9.63 2.70 o -12 1 3 20.57 24.54 2.96 o -11 1 3 64.31 67.86 4.67 o -10 1 3 7.71 11.85 2.31 o -9 1 3 782.97 754.00 13.74 o -8 1 3 53.26 50.43 3.48 o -7 1 3 0.27 1.96 0.96 o -6 1 3 8.59 12.65 3.61 o -5 1 3 194.35 167.57 5.44 o -4 1 3 36.91 29.37 1.92 o -3 1 3 220.66 217.70 4.55 o -2 1 3 4.72 4.79 0.94 o -1 1 3 461.62 441.46 5.89 o 0 1 3 2042.88 2066.91 18.14 o 1 1 3 781.96 821.74 11.26 o 2 1 3 237.16 242.15 4.88 o 3 1 3 2.41 0.92 1.26 o 4 1 3 477.47 455.15 18.92 o 5 1 3 150.65 187.15 9.72 o 6 1 3 479.07 496.38 9.94 o 7 1 3 0.02 1.53 1.74 o 8 1 3 1.46 0.71 2.00 o 9 1 3 151.41 141.15 6.86 o 10 1 3 41.55 45.19 9.35 o 11 1 3 9.44 6.05 2.57 o 12 1 3 4.74 2.99 3.60 o -12 2 3 1.74 1.34 4.59 o -11 2 3 43.77 42.49 4.11 o -10 2 3 10.25 10.02 2.82 o -9 2 3 35.50 37.76 4.00 o -8 2 3 51.71 55.96 4.82 o -7 2 3 3.60 6.37 1.98 o -6 2 3 3.00 3.53 1.42 o -5 2 3 412.98 393.33 8.48 o -4 2 3 614.48 586.45 10.97 o -3 2 3 128.01 116.41 4.23 o -2 2 3 215.53 241.96 5.93 o -1 2 3 509.85 514.21 8.13 o 0 2 3 1680.47 1648.39 12.03 o 1 2 3 209.91 226.15 5.66 o 2 2 3 1636.97 1676.17 48.61 o 3 2 3 125.26 128.30 4.57 o 4 2 3 58.76 52.43 3.59 o 5 2 3 78.53 77.56 4.21 o 6 2 3 3.76 3.92 2.19 o 7 2 3 59.69 62.12 4.38 o 8 2 3 15.19 8.60 2.58 o 9 2 3 115.86 88.55 12.35 o 10 2 3 94.81 92.68 6.05 o 11 2 3 25.81 19.52 4.17 o -10 3 3 55.79 48.06 5.68 o -9 3 3 14.88 16.61 5.42 o -8 3 3 30.36 25.37 4.01 o -7 3 3 97.31 104.55 6.20 o -6 3 3 2.05 4.78 5.45 o -5 3 3 163.28 171.86 6.65 o -4 3 3 203.40 200.93 9.62 o -3 3 3 25.50 31.56 3.07 o -2 3 3 756.79 781.00 30.46 o -1 3 3 0.36 0.36 1.59 o 0 3 3 184.39 187.87 5.66 o 1 3 3 2.37 4.62 1.72 o 2 3 3 367.23 369.50 9.77 o 3 3 3 171.69 183.85 8.60 o 4 3 3 109.75 111.76 5.65 o 5 3 3 3.35 4.84 5.66 o 6 3 3 196.34 194.25 7.98 o 7 3 3 7.29 10.37 2.41 o 8 3 3 11.00 11.86 3.17 o 9 3 3 43.21 42.85 4.70 o -7 4 3 0.08 2.60 2.60 o -6 4 3 40.46 50.92 4.98 o -5 4 3 27.03 26.35 3.67 o -4 4 3 19.48 20.33 3.95 o -3 4 3 5.07 5.14 2.79 o -2 4 3 24.75 27.40 4.65 o -1 4 3 55.12 59.32 5.23 o 0 4 3 52.09 52.90 5.26 o 1 4 3 26.77 21.70 4.23 o 2 4 3 292.48 231.19 138.18 o 3 4 3 10.82 7.30 3.47 o 4 4 3 119.65 125.55 7.00 o 5 4 3 57.70 55.33 5.48 o 6 4 3 0.93 1.80 3.34 o -13 0 4 17.36 25.85 4.98 o -12 0 4 25.52 18.50 5.10 o -11 0 4 70.09 71.32 7.06 o -10 0 4 0.43 1.84 2.16 o -9 0 4 8.33 4.93 3.20 o -8 0 4 4.29 8.35 1.96 o -7 0 4 1187.45 1228.84 21.66 o -6 0 4 14.65 14.34 2.34 o -5 0 4 5290.80 4976.04 40.60 o -4 0 4 22.82 17.58 2.52 o -3 0 4 166.53 150.29 5.38 o -2 0 4 7793.40 7382.78 44.48 o -1 0 4 1.17 0.28 1.25 o 0 0 4 12.30 9.84 1.16 o 1 0 4 3972.74 3794.00 28.02 o 2 0 4 114.20 115.46 4.76 o 3 0 4 378.14 334.79 9.03 o 4 0 4 65.25 63.98 4.52 o 5 0 4 1.01 0.60 1.12 o 6 0 4 10.97 5.11 2.57 o 7 0 4 471.53 471.35 15.10 o 8 0 4 110.93 110.37 7.99 o 9 0 4 20.11 25.30 4.18 o 10 0 4 226.71 225.72 12.12 o 11 0 4 31.73 32.42 5.00 o 12 0 4 68.97 72.44 7.68 o -13 1 4 30.98 28.07 3.39 o -12 1 4 55.87 49.90 4.55 o -11 1 4 133.23 129.40 6.64 o -10 1 4 1.66 1.99 2.22 o -9 1 4 842.64 820.03 14.38 o -8 1 4 1.65 0.36 1.83 o -7 1 4 53.43 55.08 4.57 o -6 1 4 615.23 529.21 11.06 o -5 1 4 85.04 84.79 3.05 o -4 1 4 13.49 12.51 1.56 o -3 1 4 1889.82 1881.10 39.62 o -2 1 4 36.57 42.54 1.69 o -1 1 4 3.07 1.25 0.68 o 0 1 4 124.17 122.32 2.54 o 1 1 4 462.44 452.62 6.68 o 2 1 4 480.72 464.90 8.80 o 3 1 4 574.19 591.05 12.45 o 4 1 4 343.53 308.34 14.04 o 5 1 4 843.36 827.24 21.39 o 6 1 4 11.74 11.15 2.18 o 7 1 4 134.81 134.81 6.02 o 8 1 4 349.71 346.98 10.25 o 9 1 4 1.41 0.81 2.01 o 10 1 4 127.21 124.93 7.80 o 11 1 4 91.85 89.26 6.54 o 12 1 4 20.39 23.40 5.74 o -12 2 4 0.25 0.06 1.89 o -11 2 4 0.36 1.28 2.65 o -10 2 4 70.70 75.92 5.46 o -9 2 4 340.03 320.70 10.54 o -8 2 4 142.78 161.72 6.60 o -7 2 4 224.92 225.07 7.40 o -6 2 4 107.78 117.47 5.05 o -5 2 4 137.86 118.83 4.83 o -4 2 4 395.12 397.83 8.32 o -3 2 4 21.16 22.54 2.21 o -2 2 4 344.11 332.86 7.15 o -1 2 4 672.69 680.29 9.91 o 0 2 4 638.58 656.95 12.74 o 1 2 4 567.46 579.23 9.46 o 2 2 4 416.02 439.35 8.69 o 3 2 4 1.57 1.89 1.44 o 4 2 4 436.28 440.87 24.98 o 5 2 4 0.01 1.48 2.70 o 6 2 4 243.82 238.70 7.86 o 7 2 4 122.80 127.29 21.46 o 8 2 4 49.65 42.84 6.03 o 9 2 4 91.88 88.16 5.75 o 10 2 4 0.88 1.34 2.21 o 11 2 4 0.06 0.43 1.84 o -10 3 4 12.39 7.12 3.97 o -9 3 4 1.11 1.97 2.61 o -8 3 4 48.53 54.43 5.77 o -7 3 4 0.64 2.44 2.02 o -6 3 4 12.11 9.72 2.55 o -5 3 4 27.32 27.02 8.31 o -4 3 4 97.54 92.70 5.25 o -3 3 4 78.50 82.36 4.69 o -2 3 4 0.64 1.00 2.12 o -1 3 4 213.97 230.63 8.03 o 0 3 4 409.69 404.96 7.17 o 1 3 4 1.56 4.23 4.50 o 2 3 4 402.27 411.34 19.44 o 3 3 4 382.72 372.09 10.54 o 4 3 4 12.24 13.38 5.67 o 5 3 4 149.79 148.04 9.10 o 6 3 4 57.24 57.75 4.49 o 7 3 4 2.26 2.94 1.83 o 8 3 4 20.00 23.59 3.38 o 9 3 4 0.00 0.02 1.97 o -7 4 4 10.81 10.01 3.58 o -6 4 4 14.12 18.30 3.76 o -5 4 4 1.90 1.70 2.44 o -4 4 4 41.87 43.02 5.34 o -3 4 4 28.05 26.29 4.10 o -2 4 4 30.18 33.08 3.83 o -1 4 4 1.54 4.00 3.37 o 0 4 4 0.50 1.28 1.72 o 1 4 4 49.54 50.94 5.73 o 2 4 4 176.85 184.04 8.98 o 3 4 4 148.71 155.42 9.00 o 4 4 4 29.07 20.19 4.18 o 5 4 4 1.84 0.79 2.61 o -13 1 5 2.81 3.21 2.25 o -12 1 5 0.42 1.63 1.39 o -11 1 5 11.93 11.18 2.30 o -10 1 5 203.51 199.73 7.72 o -9 1 5 14.09 11.00 2.55 o -8 1 5 58.10 54.89 3.61 o -7 1 5 20.70 18.78 2.12 o -6 1 5 345.85 410.53 15.86 o -5 1 5 5.09 5.45 1.50 o -4 1 5 1215.42 1238.16 54.32 o -3 1 5 27.09 27.83 1.96 o -2 1 5 3.72 4.93 0.94 o -1 1 5 1235.80 1233.15 19.96 o 0 1 5 569.46 592.49 9.39 o 1 1 5 130.41 131.10 3.86 o 2 1 5 34.53 43.43 1.86 o 3 1 5 37.67 39.29 2.83 o 4 1 5 357.24 347.25 15.91 o 5 1 5 93.77 104.91 4.74 o 6 1 5 68.20 63.26 4.47 o 7 1 5 0.02 1.36 1.34 o 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