#------------------------------------------------------------------------------ #$Date: 2010-12-22 21:36:50 +0200 (Wed, 22 Dec 2010) $ #$Revision: 5269 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2227663.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227663_Fobs loop_ _publ_author_name 'bin Shawkataly, Omar' 'Khan, Imthyaz Ahmed' 'Sirat, Siti Syaida' 'Yeap, Chin Sing' 'Fun, Hoong-Kun' _publ_section_title ; Bis([\m-bis(diphenylphosphino)methane-1:2\k^2^P:P']nonacarbonyl-1\k^3^C,2\k^3^C,3\k^3^C-{tris[4-(methylsulfanyl)phenyl]arsine-3\kAs}-triangulo-triruthenium(0)) dichloromethane monosolvate ; _journal_coeditor_code IS2583 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1150 _journal_page_last m1151 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 94.539 _cell_angle_beta 98.228 _cell_angle_gamma 103.212 _cell_length_a 10.8077 _cell_length_b 12.6180 _cell_length_c 20.9478 _exptl_crystal_F_000 1418.00 _reflns_d_resolution_high 0.6167 _[local]_cod_data_source_file is2583Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' iak20c_0m in P-1 (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 310.09 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 46.19 141.67 7.22 o 3 0 0 202.27 164.61 6.60 o 4 0 0 5992.20 6138.52 46.13 o 5 0 0 4613.38 5311.23 37.88 o 6 0 0 65.23 131.72 5.09 o 7 0 0 4307.45 4417.19 44.51 o 8 0 0 1345.49 1171.18 16.29 o 9 0 0 3723.49 3628.74 46.47 o 10 0 0 22.15 -6.37 11.55 o 11 0 0 7.41 1.70 12.75 o 12 0 0 2058.27 2235.24 35.89 o 13 0 0 4432.56 4448.99 66.54 o 14 0 0 38.60 110.43 25.01 o 15 0 0 740.00 756.43 41.23 o 16 0 0 349.85 271.94 28.67 o -17 1 0 483.82 406.94 60.81 o -16 1 0 529.46 484.06 31.58 o -15 1 0 802.48 767.20 34.38 o -14 1 0 296.12 254.67 29.54 o -13 1 0 13.67 -2.13 15.67 o -12 1 0 1074.41 1130.99 25.01 o -11 1 0 425.90 464.91 22.21 o -10 1 0 5371.88 5245.50 78.74 o -9 1 0 1313.73 1258.87 18.37 o -8 1 0 20.51 38.83 4.34 o -7 1 0 2722.45 2593.59 21.79 o -6 1 0 5315.76 5151.15 34.67 o -5 1 0 4630.10 4648.54 33.63 o -4 1 0 5687.12 5350.59 38.47 o -3 1 0 2680.05 3083.96 35.58 o -2 1 0 14443.40 15478.57 95.92 o -1 1 0 17137.40 17944.82 202.60 o 0 1 0 57035.42 48448.01 2295.26 o 1 1 0 16257.82 16897.91 100.61 o 2 1 0 8.11 1.42 2.34 o 3 1 0 22714.63 23493.78 143.73 o 4 1 0 1000.07 984.99 11.23 o 5 1 0 609.35 628.52 8.53 o 6 1 0 344.47 370.32 8.07 o 7 1 0 1486.89 1609.74 17.00 o 8 1 0 886.46 976.98 14.75 o 9 1 0 1649.75 1706.04 26.81 o 10 1 0 281.09 221.45 19.72 o 11 1 0 1117.21 1066.15 31.17 o 12 1 0 5184.75 5401.48 61.30 o 13 1 0 5266.11 5290.73 128.89 o 14 1 0 1271.02 1320.29 47.90 o 15 1 0 73.80 57.64 27.48 o 16 1 0 269.17 194.10 33.34 o -17 2 0 397.18 381.96 36.92 o -16 2 0 84.69 75.71 26.53 o -15 2 0 745.74 731.74 33.73 o -14 2 0 715.19 666.85 30.54 o -13 2 0 3223.63 3318.66 63.27 o -12 2 0 155.12 162.32 13.15 o -11 2 0 4656.89 4687.32 74.99 o -10 2 0 8689.49 8896.94 92.94 o -9 2 0 45.29 45.48 7.24 o -8 2 0 2971.71 2900.94 22.82 o -7 2 0 3027.53 2963.92 21.73 o -6 2 0 11611.42 11623.66 64.88 o -5 2 0 30047.59 29161.85 156.60 o -4 2 0 4511.10 5288.03 32.02 o -3 2 0 12426.22 12783.78 80.54 o -2 2 0 1095.22 1295.91 10.47 o -1 2 0 34452.27 36493.95 180.40 o 0 2 0 48.13 94.18 2.93 o 1 2 0 5271.65 5156.08 32.72 o 2 2 0 16306.40 17780.60 120.64 o 3 2 0 40384.21 41738.80 224.17 o 4 2 0 6686.13 6888.22 45.67 o 5 2 0 10662.18 10292.17 62.77 o 6 2 0 5231.20 5106.28 31.11 o 7 2 0 2273.49 2147.87 23.86 o 8 2 0 9884.58 9947.46 70.52 o 9 2 0 1232.97 1283.82 25.85 o 10 2 0 363.98 308.10 15.77 o 11 2 0 345.34 260.66 16.84 o 12 2 0 6032.13 6369.44 79.95 o 13 2 0 901.53 908.45 56.89 o 14 2 0 275.75 193.18 29.40 o 15 2 0 3.19 -15.26 24.91 o 16 2 0 58.95 50.69 29.81 o -17 3 0 15.02 100.28 29.44 o -16 3 0 24.53 2.30 27.08 o -15 3 0 2714.70 2840.00 65.17 o -14 3 0 12.79 31.61 20.37 o -13 3 0 438.92 415.63 21.63 o -12 3 0 16.45 39.88 10.46 o -11 3 0 11149.18 10940.17 114.95 o -10 3 0 791.42 900.51 21.29 o -9 3 0 210.31 220.54 11.82 o -8 3 0 46.54 60.66 5.10 o -7 3 0 21580.44 21406.19 101.58 o -6 3 0 9260.53 10118.79 50.22 o -5 3 0 741.47 961.95 10.91 o -4 3 0 10445.18 10946.92 54.03 o -3 3 0 1097.71 1088.20 10.26 o -2 3 0 9553.12 10088.92 54.02 o -1 3 0 35531.29 37921.57 208.33 o 0 3 0 84.17 52.89 3.75 o 1 3 0 50970.78 54160.20 292.20 o 2 3 0 72899.41 74467.66 362.89 o 3 3 0 4330.54 4115.55 26.04 o 4 3 0 12817.83 12877.20 69.40 o 5 3 0 3800.78 4001.55 24.65 o 6 3 0 10227.67 10588.51 51.90 o 7 3 0 1264.51 1186.69 16.79 o 8 3 0 5157.21 4910.51 46.14 o 9 3 0 40.04 39.88 9.27 o 10 3 0 730.31 702.78 23.09 o 11 3 0 544.89 428.93 25.13 o 12 3 0 4471.95 4814.03 73.96 o 13 3 0 7.25 -8.84 21.84 o 14 3 0 9.79 0.80 24.41 o 15 3 0 3.57 -23.63 26.54 o 16 3 0 131.71 123.74 33.95 o -17 4 0 2423.46 2386.56 71.88 o -16 4 0 126.67 105.13 31.37 o -15 4 0 3456.87 3650.09 69.78 o -14 4 0 30.34 22.18 20.75 o -13 4 0 83.78 68.38 17.14 o -12 4 0 1525.08 1581.50 29.02 o -11 4 0 10892.10 11604.28 90.27 o -10 4 0 985.17 994.35 18.96 o -9 4 0 1727.74 1642.67 18.89 o -8 4 0 4342.89 4248.88 34.12 o -7 4 0 2575.10 2385.02 16.09 o -6 4 0 1570.14 1428.09 12.54 o -5 4 0 3041.93 2748.12 18.07 o -4 4 0 214.01 282.77 6.47 o -3 4 0 195.55 207.11 5.09 o -2 4 0 3331.69 3128.03 20.50 o -1 4 0 10968.66 11163.55 63.88 o 0 4 0 288.29 256.65 5.93 o 1 4 0 15552.05 16342.28 81.72 o 2 4 0 58549.70 59414.69 275.77 o 3 4 0 150.08 175.85 5.69 o 4 4 0 373.76 416.06 8.10 o 5 4 0 5137.83 5109.61 30.67 o 6 4 0 7165.98 7459.60 51.22 o 7 4 0 600.14 621.49 23.35 o 8 4 0 1868.27 1716.64 29.97 o 9 4 0 487.64 462.30 19.22 o 10 4 0 1066.90 1007.18 42.44 o 11 4 0 572.43 426.30 29.89 o 12 4 0 470.62 392.28 41.33 o 13 4 0 1652.85 1775.61 54.13 o 14 4 0 1326.20 1382.25 52.35 o 15 4 0 68.71 118.03 31.29 o -17 5 0 2642.70 2797.64 78.15 o -16 5 0 260.15 362.13 38.29 o -15 5 0 240.39 166.47 30.56 o -14 5 0 414.44 404.45 46.44 o -13 5 0 36.12 16.13 19.24 o -12 5 0 2009.01 2037.83 41.32 o -11 5 0 319.82 309.57 19.43 o -10 5 0 1584.59 1700.98 26.93 o -9 5 0 3546.05 3556.55 34.91 o -8 5 0 9777.18 9968.86 62.54 o -7 5 0 150.89 144.79 6.39 o -6 5 0 728.94 613.30 10.03 o -5 5 0 559.10 526.15 7.18 o -4 5 0 2128.11 2032.95 14.19 o -3 5 0 5038.34 4486.36 25.33 o -2 5 0 341.95 377.83 6.88 o -1 5 0 7428.79 7505.07 39.42 o 0 5 0 10639.54 10714.10 55.21 o 1 5 0 38070.02 38097.36 180.73 o 2 5 0 15280.18 14130.74 70.70 o 3 5 0 89.88 134.45 5.71 o 4 5 0 1625.73 1814.11 16.03 o 5 5 0 222.01 206.95 7.90 o 6 5 0 36.04 43.81 9.39 o 7 5 0 683.47 672.77 18.72 o 8 5 0 1024.95 1048.55 21.59 o 9 5 0 1160.36 1144.46 27.96 o 10 5 0 223.01 252.79 21.53 o 11 5 0 96.07 57.51 21.03 o 12 5 0 1701.54 1635.11 58.45 o 13 5 0 2015.18 2017.17 68.08 o 14 5 0 2872.79 2997.88 72.73 o 15 5 0 946.36 979.53 65.46 o -17 6 0 244.06 222.41 43.46 o -16 6 0 922.10 809.55 46.74 o -15 6 0 401.25 474.31 48.35 o -14 6 0 631.17 529.14 36.88 o -13 6 0 36.64 17.72 16.34 o -12 6 0 1205.42 1216.54 29.49 o -11 6 0 1427.23 1401.60 38.55 o -10 6 0 3413.86 3237.04 38.01 o -9 6 0 3604.95 3919.53 41.27 o -8 6 0 4389.39 4155.14 41.37 o -7 6 0 4852.66 4833.59 37.39 o -6 6 0 15537.42 15601.60 77.32 o -5 6 0 10473.32 10319.29 53.43 o -4 6 0 4704.48 4805.75 27.16 o -3 6 0 22185.13 20882.95 90.82 o -2 6 0 4900.80 5203.83 30.62 o -1 6 0 1345.69 1503.11 13.89 o 0 6 0 3557.92 3786.89 27.59 o 1 6 0 14915.24 14817.40 71.94 o 2 6 0 1012.06 1004.08 12.31 o 3 6 0 4860.89 4856.17 31.34 o 4 6 0 4122.18 4045.18 29.64 o 5 6 0 3322.19 3252.41 40.12 o 6 6 0 1628.75 1534.66 25.80 o 7 6 0 1722.73 1671.76 29.85 o 8 6 0 141.99 192.70 13.76 o 9 6 0 32.73 62.96 14.11 o 10 6 0 1401.19 1358.01 38.40 o 11 6 0 17.90 15.28 20.77 o 12 6 0 845.29 666.66 44.32 o 13 6 0 955.10 965.81 53.61 o 14 6 0 3368.58 3468.79 79.80 o -17 7 0 65.86 25.13 38.01 o -16 7 0 1230.90 1419.96 65.35 o -15 7 0 79.00 56.89 27.59 o -14 7 0 921.44 883.38 53.18 o -13 7 0 5710.99 5616.28 74.37 o -12 7 0 637.85 663.86 27.15 o -11 7 0 68.47 84.19 13.62 o -10 7 0 18.29 -4.99 8.94 o -9 7 0 18270.10 17479.27 122.47 o -8 7 0 2169.69 2048.86 28.57 o -7 7 0 1066.19 928.51 23.05 o -6 7 0 4116.07 4232.07 27.64 o -5 7 0 13654.04 13973.86 64.94 o -4 7 0 152.86 137.20 5.75 o -3 7 0 5615.27 5973.22 31.98 o -2 7 0 4551.80 4323.39 24.68 o -1 7 0 1.65 8.91 3.95 o 0 7 0 4704.67 4615.81 27.39 o 1 7 0 191.37 222.66 6.94 o 2 7 0 499.52 495.63 10.66 o 3 7 0 4496.32 4257.85 36.36 o 4 7 0 1779.67 1828.47 23.08 o 5 7 0 377.82 367.60 16.12 o 6 7 0 75.66 41.87 13.29 o 7 7 0 12467.84 11912.55 105.41 o 8 7 0 428.88 404.91 17.60 o 9 7 0 1960.82 2041.90 36.49 o 10 7 0 5385.91 5418.16 77.59 o 11 7 0 937.68 896.66 39.49 o 12 7 0 395.65 390.16 62.17 o 13 7 0 128.99 132.75 35.19 o 14 7 0 2639.15 2749.29 73.85 o -17 8 0 23.20 -15.14 34.28 o -16 8 0 3717.76 3979.12 99.81 o -15 8 0 560.82 537.59 45.88 o -14 8 0 303.68 354.92 27.96 o -13 8 0 2322.14 2333.54 54.98 o -12 8 0 489.11 545.28 25.43 o -11 8 0 42.39 49.68 14.49 o -10 8 0 4650.43 4468.58 48.64 o -9 8 0 5773.99 5801.07 58.95 o -8 8 0 1217.75 1217.03 24.41 o -7 8 0 2940.76 3010.22 28.82 o -6 8 0 1168.11 1183.99 16.79 o -5 8 0 6497.98 6214.71 35.33 o -4 8 0 1674.38 1745.02 15.43 o -3 8 0 257.48 230.60 6.63 o -2 8 0 2093.71 2094.97 16.75 o -1 8 0 6124.01 6514.29 34.53 o 0 8 0 448.87 413.50 8.51 o 1 8 0 10702.56 10416.24 58.58 o 2 8 0 2693.12 2856.27 24.23 o 3 8 0 9667.95 9882.39 67.73 o 4 8 0 6098.24 5706.58 50.61 o 5 8 0 4748.69 4712.14 46.52 o 6 8 0 20.93 23.37 12.03 o 7 8 0 1580.11 1480.80 31.78 o 8 8 0 1615.57 1653.23 34.70 o 9 8 0 3244.05 3423.11 49.87 o 10 8 0 472.32 449.40 37.18 o 11 8 0 200.48 126.73 27.11 o 12 8 0 81.05 59.20 31.17 o 13 8 0 663.94 723.95 52.86 o -16 9 0 904.17 623.31 65.29 o -15 9 0 1707.47 1874.30 92.51 o -14 9 0 4002.87 3987.73 90.09 o -13 9 0 1307.42 1239.48 44.25 o -12 9 0 272.71 193.82 22.50 o -11 9 0 4.41 2.74 15.81 o -10 9 0 8406.99 8491.40 79.78 o -9 9 0 1798.46 1737.62 30.78 o -8 9 0 1840.59 2045.57 40.80 o -7 9 0 266.93 290.44 11.39 o -6 9 0 167.82 159.13 8.54 o -5 9 0 2798.44 2529.43 22.79 o -4 9 0 15347.98 14783.32 68.81 o -3 9 0 2289.98 2393.99 19.77 o -2 9 0 83.42 96.47 6.00 o -1 9 0 4644.49 4617.87 29.12 o 0 9 0 195.40 160.32 7.24 o 1 9 0 6836.35 6865.97 42.43 o 2 9 0 5552.93 5129.57 41.11 o 3 9 0 10030.89 10225.07 78.51 o 4 9 0 2059.32 1854.36 27.93 o 5 9 0 616.78 598.76 17.27 o 6 9 0 1433.33 1318.99 31.70 o 7 9 0 34.90 7.13 14.18 o 8 9 0 61.09 70.21 15.71 o 9 9 0 1725.93 1707.60 39.96 o 10 9 0 50.25 3.68 21.91 o 11 9 0 1330.03 1280.22 62.44 o 12 9 0 49.80 81.09 32.92 o 13 9 0 15.73 35.30 34.89 o -16 10 0 1232.69 1107.42 76.94 o -15 10 0 54.36 58.98 32.42 o -14 10 0 305.13 277.66 36.82 o -13 10 0 155.29 134.43 29.69 o -12 10 0 1341.98 1291.89 39.85 o -11 10 0 1577.95 1626.51 42.57 o -10 10 0 303.24 289.70 19.25 o -9 10 0 466.49 505.05 23.98 o -8 10 0 1872.80 1971.96 24.46 o -7 10 0 1284.97 1207.28 21.29 o -6 10 0 113.78 83.82 10.35 o -5 10 0 1156.64 1203.30 17.17 o -4 10 0 16104.30 16128.36 81.36 o -3 10 0 281.32 223.22 8.71 o -2 10 0 1196.88 1177.91 14.50 o -1 10 0 3806.83 3723.00 26.61 o 0 10 0 1224.10 1220.27 24.16 o 1 10 0 313.07 308.29 11.03 o 2 10 0 912.70 1011.01 21.67 o 3 10 0 10189.59 9746.54 91.82 o 4 10 0 364.35 332.38 15.13 o 5 10 0 2778.51 2795.94 36.78 o 6 10 0 33.59 50.11 14.03 o 7 10 0 205.00 160.05 19.84 o 8 10 0 707.33 604.27 34.12 o 9 10 0 603.87 582.42 28.38 o 10 10 0 768.38 865.23 30.45 o 11 10 0 1073.35 1050.96 71.90 o 12 10 0 344.52 393.89 44.83 o -16 11 0 618.88 679.74 65.60 o -15 11 0 34.50 42.45 31.47 o -14 11 0 402.09 264.70 37.49 o -13 11 0 1081.34 1259.72 54.71 o -12 11 0 1116.38 1070.12 44.02 o -11 11 0 2140.69 1971.78 54.00 o -10 11 0 4622.21 4663.75 70.11 o -9 11 0 2709.16 2765.55 38.66 o -8 11 0 3885.83 3853.06 45.82 o -7 11 0 2084.16 2053.64 24.15 o -6 11 0 2150.32 2202.52 24.83 o -5 11 0 1277.48 1242.54 19.10 o -4 11 0 12763.44 12487.42 70.38 o -3 11 0 622.07 576.23 12.81 o -2 11 0 441.65 452.85 11.52 o -1 11 0 3211.64 3323.34 28.40 o 0 11 0 1983.48 2042.17 25.60 o 1 11 0 801.42 812.51 17.05 o 2 11 0 40.83 25.21 9.96 o 3 11 0 68.89 69.07 11.26 o 4 11 0 2.44 4.78 10.47 o 5 11 0 4682.70 4650.02 51.85 o 6 11 0 95.22 84.46 18.84 o 7 11 0 111.19 111.19 19.91 o 8 11 0 182.64 269.58 23.96 o 9 11 0 1998.01 2105.82 48.06 o 10 11 0 466.95 412.73 25.62 o 11 11 0 1027.92 959.56 59.36 o -16 12 0 0.09 1.23 33.39 o -15 12 0 437.66 447.32 45.27 o -14 12 0 1076.27 1156.09 56.80 o -13 12 0 423.96 376.66 39.58 o -12 12 0 1860.72 1887.39 63.36 o -11 12 0 668.05 667.61 38.02 o -10 12 0 1237.59 1228.09 37.19 o -9 12 0 736.18 713.12 26.26 o -8 12 0 6614.06 6554.98 59.98 o -7 12 0 2838.10 2882.21 31.20 o -6 12 0 1632.41 1546.51 22.01 o -5 12 0 868.41 930.80 17.73 o -4 12 0 2412.01 2310.02 25.31 o -3 12 0 3022.93 3019.67 30.31 o -2 12 0 33.99 35.16 8.75 o -1 12 0 61.89 60.51 9.66 o 0 12 0 7232.58 7123.58 60.52 o 1 12 0 51.75 72.58 12.11 o 2 12 0 1020.15 906.54 23.25 o 3 12 0 1884.81 1867.51 32.01 o 4 12 0 1189.13 1226.96 27.15 o 5 12 0 997.30 982.04 37.34 o 6 12 0 3.78 -1.70 19.60 o 7 12 0 2547.04 2607.05 61.26 o 8 12 0 4635.06 4943.87 74.82 o 9 12 0 923.76 910.50 65.03 o 10 12 0 5.18 16.95 20.02 o 11 12 0 1631.44 1561.06 73.56 o -15 13 0 1853.51 2095.21 75.95 o -14 13 0 451.62 392.77 48.89 o -13 13 0 201.14 185.75 36.15 o -12 13 0 1327.65 1324.00 57.54 o -11 13 0 57.97 42.39 26.56 o -10 13 0 817.07 821.22 29.94 o -9 13 0 2631.64 2604.03 36.98 o -8 13 0 5842.18 5832.07 56.33 o -7 13 0 38.06 48.62 10.11 o -6 13 0 1003.96 991.67 19.30 o -5 13 0 27.25 23.85 9.30 o -4 13 0 21.01 13.87 8.78 o -3 13 0 105.02 78.09 10.63 o -2 13 0 1508.97 1603.39 36.53 o -1 13 0 4.24 15.75 10.49 o 0 13 0 5371.19 5245.34 51.31 o 1 13 0 80.97 82.24 13.53 o 2 13 0 167.13 152.17 15.04 o 3 13 0 194.32 155.67 15.36 o 4 13 0 8681.79 8600.02 83.28 o 5 13 0 1518.82 1600.82 37.15 o 6 13 0 77.99 110.82 21.70 o 7 13 0 246.09 249.26 26.17 o 8 13 0 911.35 947.93 37.87 o 9 13 0 404.51 290.41 27.70 o 10 13 0 4.29 34.30 21.05 o -15 14 0 632.72 476.99 48.37 o -14 14 0 1175.91 1181.96 61.25 o -13 14 0 1.42 -16.44 31.03 o -12 14 0 151.29 136.74 34.38 o -11 14 0 264.16 227.30 34.68 o -10 14 0 523.12 512.60 33.57 o -9 14 0 771.28 686.88 22.32 o -8 14 0 2162.04 2219.52 40.36 o -7 14 0 1618.23 1730.67 29.61 o -6 14 0 6256.96 6196.80 58.13 o -5 14 0 1054.68 1116.02 31.93 o -4 14 0 937.43 868.14 20.25 o -3 14 0 326.58 328.06 14.84 o -2 14 0 5090.81 5192.00 48.91 o -1 14 0 66.98 80.19 11.77 o 0 14 0 136.97 158.19 14.70 o 1 14 0 1773.88 1723.28 32.81 o 2 14 0 1949.13 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