Crystallography Open Database

Information card for entry 2227673

Preview

Coordinates	2227673.cif
Structure factors	2227673.hkl
Original IUCr paper	HTML

Structure parameters

Chemical name	<i>catena</i>-Poly[[(tetrahydrofuran-κ<i>O</i>)lithium(I)]- bis(μ-trimethylsilanolato-κ^2^<i>O</i>:<i>O</i>)-gallium(III)- bis(μ-trimethylsilanolato-κ^2^<i>O</i>:<i>O</i>)- [(tetrahydrofuran-κ<i>O</i>)lithium(I)]-μ-bromido]
Formula	C20 H52 Br Ga Li2 O6 Si4
Calculated formula	C20 H52 Br Ga Li2 O6 Si4
Title of publication	<i>catena</i>-Poly[[(tetrahydrofuran-κ<i>O</i>)lithium(I)]-bis(μ-trimethylsilanolato-κ^2^<i>O</i>:<i>O</i>)-gallium(III)-bis(μ-trimethylsilanolato-κ^2^<i>O</i>:<i>O</i>)-[(tetrahydrofuran-κ<i>O</i>)lithium(I)]-μ-bromido]
Authors of publication	Grubba, Rafał; Baranowska, Katarzyna; Pikies, Jerzy
Journal of publication	Acta Crystallographica Section E
Year of publication	2010
Journal volume	66
Journal issue	10
Pages of publication	m1242
a	25.802 ± 0.008 Å
b	9.761 ± 0.002 Å
c	18.689 ± 0.006 Å
α	90°
β	130.81 ± 0.02°
γ	90°
Cell volume	3563 ± 2 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0325
Residual factor for significantly intense reflections	0.0308
Weighted residual factors for significantly intense reflections	0.0828
Weighted residual factors for all reflections included in the refinement	0.0841
Goodness-of-fit parameter for all reflections included in the refinement	1.048
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	Yes

Version history

Revision	Date	Message	Files
181197 (current)	2016-04-03	hkl/2/22/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/22/76.	2227673.cif 2227673.hkl
176789	2016-02-20	cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/22.	2227673.cif 2227673.hkl
120072	2014-07-11	Adding DOIs to range 2 structures.	2227673.cif 2227673.hkl
88064	2013-08-29	Adding _cod_database_fobs_code data item to all COD CIFs that have Fobs deposited and did not have this data item yet.	2227673.cif 2227673.hkl
26848	2011-09-28	cif/2/, hkl/2/, html/ Reorganising CIFs of the range 2* into the "prefix-directory" tree.	2227673.cif 2227673.hkl
5269	2010-12-22	hkl/ Adding Fobs data for the recent IUCr-published structres.	2227673.cif 2227673.hkl
4710	2010-12-18	../uploads/cif-deposit/cod/cif Adding structures of 2227673 via cif-deposit CGI script.	2227673.cif