#------------------------------------------------------------------------------ #$Date: 2010-12-22 21:36:50 +0200 (Wed, 22 Dec 2010) $ #$Revision: 5269 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2227728.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227728_Fobs loop_ _publ_author_name 'Archana, R.' 'Yamuna, E.' 'Rajendra Prasad, K. J.' 'Thiruvalluvar, A.' 'Butcher, R. J.' _publ_section_title ; 8-Methyl-2,3,4,9-tetrahydro-1H-carbazol-1-one ; _journal_coeditor_code JJ2046 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2299 _journal_page_last o2300 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.960 _cell_angle_gamma 90.000 _cell_length_a 10.5245 _cell_length_b 7.1564 _cell_length_c 13.5870 _exptl_crystal_F_000 424.00 _reflns_d_resolution_high 0.8014 _[local]_cod_data_source_file jj2046Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ot-c in P 21/n Z=4 C13H13N1O1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 62.75 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1251.91 1117.75 13.26 o 4 0 0 2649.03 2411.14 36.92 o 6 0 0 65.31 88.79 1.67 o 8 0 0 1172.46 1210.36 7.59 o 10 0 0 125.67 130.03 2.78 o 12 0 0 8.62 8.89 0.68 o 1 1 0 647.89 613.47 1.71 o 2 1 0 108.79 106.85 1.36 o 3 1 0 191.23 211.79 1.18 o 4 1 0 567.84 614.32 8.26 o 5 1 0 1401.35 1545.27 6.61 o 6 1 0 0.00 1.28 1.12 o 7 1 0 256.76 285.08 6.46 o 8 1 0 52.96 60.44 0.93 o 9 1 0 160.13 152.85 8.32 o 10 1 0 60.84 68.75 5.53 o 11 1 0 23.04 31.88 1.55 o 12 1 0 59.03 81.71 4.74 o 0 2 0 108.74 74.08 0.63 o 1 2 0 63.19 60.17 3.02 o 2 2 0 47.48 48.81 0.32 o 3 2 0 368.94 382.94 3.49 o 4 2 0 36.94 36.01 1.04 o 5 2 0 176.44 189.08 3.42 o 6 2 0 223.15 253.69 8.06 o 7 2 0 261.13 262.12 6.86 o 8 2 0 304.57 281.10 2.51 o 9 2 0 121.89 108.58 1.59 o 10 2 0 9.53 8.09 0.85 o 11 2 0 2.01 3.03 0.67 o 12 2 0 25.82 36.16 1.14 o 1 3 0 70.26 71.42 0.65 o 2 3 0 429.27 495.58 3.14 o 3 3 0 439.67 501.47 3.82 o 4 3 0 160.33 169.20 2.36 o 5 3 0 47.98 44.29 1.32 o 6 3 0 163.75 165.83 5.63 o 7 3 0 741.39 710.68 17.51 o 8 3 0 102.91 82.77 2.19 o 9 3 0 534.72 501.71 7.06 o 10 3 0 0.26 0.23 0.72 o 11 3 0 22.68 28.35 1.16 o 12 3 0 12.76 15.02 0.70 o 0 4 0 109.42 127.97 1.29 o 1 4 0 435.17 467.72 3.82 o 2 4 0 492.11 554.79 4.36 o 3 4 0 51.01 55.44 1.54 o 4 4 0 94.52 128.36 7.86 o 5 4 0 31.63 34.21 1.82 o 6 4 0 23.01 18.23 0.81 o 7 4 0 315.53 281.75 11.02 o 8 4 0 31.67 24.97 0.83 o 9 4 0 104.40 102.42 1.49 o 10 4 0 69.01 61.98 1.06 o 11 4 0 0.86 2.33 0.52 o 1 5 0 35.12 41.96 1.57 o 2 5 0 119.69 127.30 1.64 o 3 5 0 40.49 39.18 0.90 o 4 5 0 120.45 121.54 1.55 o 5 5 0 656.32 532.36 4.60 o 6 5 0 24.85 22.55 1.06 o 7 5 0 126.28 133.84 8.03 o 8 5 0 85.78 70.22 3.38 o 9 5 0 17.34 14.79 1.29 o 10 5 0 0.23 0.66 0.60 o 0 6 0 958.65 976.05 22.21 o 1 6 0 118.31 117.78 1.68 o 2 6 0 38.18 40.50 1.01 o 3 6 0 6.42 6.57 0.67 o 4 6 0 318.57 295.82 3.55 o 5 6 0 2.54 4.21 0.60 o 6 6 0 38.27 33.04 1.22 o 7 6 0 13.43 11.03 0.78 o 8 6 0 10.95 11.04 0.69 o 9 6 0 133.95 153.01 1.77 o 1 7 0 71.42 65.55 1.36 o 2 7 0 393.35 357.92 2.93 o 3 7 0 88.54 81.61 1.38 o 4 7 0 13.02 8.67 0.70 o 5 7 0 45.73 34.82 1.16 o 6 7 0 0.43 0.01 0.47 o 7 7 0 0.10 0.76 0.39 o 8 7 0 148.17 160.98 1.54 o 0 8 0 29.57 29.20 1.09 o 1 8 0 178.90 169.14 2.06 o 2 8 0 3.69 4.39 0.40 o 3 8 0 1.68 2.82 0.35 o 4 8 0 13.05 10.49 0.74 o 5 8 0 4.69 5.36 0.29 o -11 0 1 111.13 94.84 2.28 o -9 0 1 789.48 713.38 6.26 o -7 0 1 154.28 131.50 2.26 o -5 0 1 38.21 41.04 3.59 o -3 0 1 1.11 2.59 0.53 o 1 0 1 848.47 760.62 6.38 o 3 0 1 1251.77 1148.51 3.92 o 5 0 1 850.94 921.36 4.69 o 7 0 1 75.17 65.49 1.63 o 9 0 1 115.69 116.89 2.68 o 11 0 1 94.92 98.65 4.38 o -12 1 1 27.68 37.17 0.97 o -11 1 1 141.80 153.16 5.94 o -10 1 1 291.68 284.77 10.43 o -9 1 1 612.88 563.83 13.05 o -8 1 1 80.94 87.64 1.44 o -7 1 1 240.09 253.00 2.20 o -6 1 1 6.01 1.04 0.30 o -5 1 1 41.36 53.37 0.92 o -4 1 1 633.05 635.89 2.43 o -3 1 1 1433.66 1353.36 1.75 o -2 1 1 468.56 448.11 4.75 o -1 1 1 300.36 315.13 0.88 o 0 1 1 3938.03 2970.32 16.97 o 1 1 1 462.33 432.23 1.13 o 2 1 1 130.40 127.95 3.98 o 3 1 1 570.80 551.11 2.65 o 4 1 1 1370.58 1285.62 19.73 o 5 1 1 11.80 11.17 0.43 o 6 1 1 5.97 6.47 0.38 o 7 1 1 135.86 138.66 2.37 o 8 1 1 409.01 393.70 3.82 o 9 1 1 49.26 43.41 1.06 o 10 1 1 22.19 15.31 1.25 o 11 1 1 15.06 17.14 0.69 o 12 1 1 134.54 150.62 2.25 o -12 2 1 7.19 6.75 0.68 o -11 2 1 46.91 53.24 1.70 o -10 2 1 0.07 -0.16 0.81 o -9 2 1 55.50 57.26 2.82 o -8 2 1 14.37 24.40 3.05 o -7 2 1 208.71 218.46 8.32 o -6 2 1 655.78 709.59 6.65 o -5 2 1 290.10 307.08 9.75 o -4 2 1 785.63 779.33 3.52 o -3 2 1 30.16 37.04 0.51 o -2 2 1 1968.97 1869.78 15.44 o -1 2 1 635.88 602.26 2.48 o 0 2 1 347.70 317.59 5.89 o 1 2 1 273.86 301.28 1.17 o 2 2 1 526.80 504.08 6.19 o 3 2 1 829.78 878.24 7.68 o 4 2 1 1240.56 1242.02 4.23 o 5 2 1 84.54 110.89 1.28 o 6 2 1 1.75 1.08 0.36 o 7 2 1 104.61 104.60 1.46 o 8 2 1 99.78 80.88 2.16 o 9 2 1 531.81 468.17 3.29 o 10 2 1 79.90 86.93 2.30 o 11 2 1 0.65 0.26 0.63 o 12 2 1 21.66 30.19 1.38 o -12 3 1 85.71 102.11 1.59 o -11 3 1 30.59 33.24 1.24 o -10 3 1 118.49 113.67 1.52 o -9 3 1 32.14 40.80 1.00 o -8 3 1 465.27 449.26 3.18 o -7 3 1 92.97 100.96 4.38 o -6 3 1 446.27 427.32 2.92 o -5 3 1 63.75 72.86 1.65 o -4 3 1 321.05 385.45 9.17 o -3 3 1 28.38 33.40 0.98 o -2 3 1 1668.69 1918.18 3.88 o -1 3 1 19.14 24.82 0.37 o 0 3 1 35.74 55.84 0.46 o 1 3 1 525.32 590.18 22.60 o 2 3 1 230.73 240.86 6.38 o 3 3 1 190.95 214.02 2.22 o 4 3 1 580.11 583.79 2.91 o 5 3 1 964.44 1032.14 17.83 o 6 3 1 18.52 15.16 0.80 o 7 3 1 4.11 6.18 0.51 o 8 3 1 481.23 415.00 3.10 o 9 3 1 71.08 60.36 1.24 o 10 3 1 38.79 42.25 1.59 o 11 3 1 10.76 9.49 0.79 o 12 3 1 5.95 3.87 0.48 o -11 4 1 49.34 56.70 1.24 o -10 4 1 0.03 0.66 0.39 o -9 4 1 0.64 0.39 0.44 o -8 4 1 12.51 15.61 2.16 o -7 4 1 166.02 150.16 7.96 o -6 4 1 84.44 87.22 5.09 o -5 4 1 16.18 13.98 1.74 o -4 4 1 14.47 18.60 0.90 o -3 4 1 76.54 98.67 3.05 o -2 4 1 62.24 71.03 1.66 o -1 4 1 137.79 149.77 1.27 o 0 4 1 0.10 2.79 0.40 o 1 4 1 318.00 389.19 8.90 o 2 4 1 1.86 2.21 0.35 o 3 4 1 947.08 949.88 25.56 o 4 4 1 49.11 44.69 0.98 o 5 4 1 271.68 263.55 3.02 o 6 4 1 5.90 5.50 0.47 o 7 4 1 869.11 763.88 11.57 o 8 4 1 14.19 15.90 1.16 o 9 4 1 2.21 4.22 0.99 o 10 4 1 6.36 8.11 0.73 o 11 4 1 0.68 1.07 0.52 o -10 5 1 0.05 0.05 0.41 o -9 5 1 1.16 0.42 0.40 o -8 5 1 29.42 21.73 0.99 o -7 5 1 34.88 23.57 1.07 o -6 5 1 85.39 74.01 1.80 o -5 5 1 536.31 450.16 4.25 o -4 5 1 322.43 303.63 4.78 o -3 5 1 20.21 19.42 0.75 o -2 5 1 17.58 21.65 0.63 o -1 5 1 389.06 369.85 2.62 o 0 5 1 160.36 187.74 1.79 o 1 5 1 60.72 56.94 1.27 o 2 5 1 7.32 8.66 0.75 o 3 5 1 89.25 85.64 1.28 o 4 5 1 16.68 13.02 0.57 o 5 5 1 139.39 112.30 2.15 o 6 5 1 201.09 201.47 8.05 o 7 5 1 92.24 87.53 2.06 o 8 5 1 0.00 0.22 0.50 o 9 5 1 7.77 7.98 0.48 o 10 5 1 55.38 70.52 1.31 o -9 6 1 51.53 61.56 2.38 o -8 6 1 104.96 117.80 1.85 o -7 6 1 59.32 45.30 1.32 o -6 6 1 41.68 40.18 1.32 o -5 6 1 385.58 330.71 3.68 o -4 6 1 26.36 25.44 1.15 o -3 6 1 797.45 718.19 4.54 o -2 6 1 70.89 64.33 1.27 o -1 6 1 0.03 -0.02 0.55 o 0 6 1 34.36 37.39 0.78 o 1 6 1 649.84 696.27 12.96 o 2 6 1 148.55 147.33 1.81 o 3 6 1 56.72 49.22 3.16 o 4 6 1 57.11 50.86 1.48 o 5 6 1 936.57 792.17 5.65 o 6 6 1 72.99 58.64 1.56 o 7 6 1 41.07 34.88 1.18 o 8 6 1 4.43 2.95 0.47 o 9 6 1 11.18 9.14 0.50 o -8 7 1 51.76 59.47 0.97 o -7 7 1 10.62 11.30 0.61 o -6 7 1 63.44 55.48 1.34 o -5 7 1 15.37 16.41 0.85 o -4 7 1 48.67 41.45 1.30 o -3 7 1 13.56 12.67 0.60 o -2 7 1 205.79 203.65 1.78 o -1 7 1 174.20 164.91 1.64 o 0 7 1 922.49 880.42 7.44 o 1 7 1 26.37 27.83 1.40 o 2 7 1 2.85 1.25 0.35 o 3 7 1 65.55 60.14 2.54 o 4 7 1 173.11 172.06 2.48 o 5 7 1 8.94 9.09 0.68 o 6 7 1 2.20 2.88 0.46 o 7 7 1 5.14 5.25 0.46 o 8 7 1 15.82 16.36 0.52 o -5 8 1 19.17 18.97 0.96 o -4 8 1 5.50 5.33 0.33 o -3 8 1 4.05 3.40 0.53 o -2 8 1 13.47 11.33 0.50 o -1 8 1 1.43 1.52 0.29 o 0 8 1 67.67 68.68 1.64 o 1 8 1 3.28 3.45 0.37 o 2 8 1 19.93 25.50 0.92 o 3 8 1 59.61 63.70 3.55 o 4 8 1 70.53 70.85 2.42 o 5 8 1 0.68 1.90 0.32 o -12 0 2 6.37 9.94 0.73 o -10 0 2 41.85 25.93 1.29 o -8 0 2 432.71 436.89 4.52 o -6 0 2 1317.56 1351.82 6.47 o -4 0 2 2681.93 2587.32 6.87 o 0 0 2 777.85 744.32 6.04 o 4 0 2 651.83 638.61 6.28 o 6 0 2 508.64 527.11 2.61 o 8 0 2 255.30 291.42 3.94 o 10 0 2 38.34 35.11 1.44 o 12 0 2 61.58 80.31 1.47 o -13 1 2 11.15 16.95 0.61 o -12 1 2 9.49 11.66 0.87 o -11 1 2 5.89 6.66 0.59 o -10 1 2 81.21 74.64 2.38 o -9 1 2 257.09 226.46 4.73 o -8 1 2 521.24 516.35 15.09 o -7 1 2 81.62 80.57 1.75 o -6 1 2 37.97 33.17 1.43 o -5 1 2 856.80 909.68 4.34 o -4 1 2 16.08 24.99 0.64 o -3 1 2 2349.03 2186.78 18.57 o -2 1 2 893.96 840.50 2.98 o -1 1 2 166.55 193.28 6.48 o 2 1 2 896.30 798.25 9.85 o 3 1 2 3.69 3.99 0.28 o 4 1 2 161.88 157.90 3.59 o 5 1 2 391.84 453.14 4.59 o 6 1 2 551.22 587.34 2.38 o 7 1 2 145.33 142.76 3.96 o 8 1 2 41.35 42.40 1.52 o 9 1 2 102.60 105.56 3.42 o 10 1 2 127.15 123.47 1.74 o 11 1 2 12.31 13.13 1.01 o 12 1 2 1.81 1.62 0.40 o -12 2 2 2.68 2.88 0.52 o -11 2 2 15.41 18.46 1.08 o -10 2 2 22.09 25.10 1.54 o -9 2 2 19.97 21.59 0.62 o -8 2 2 510.69 496.23 2.62 o -7 2 2 223.68 219.27 3.26 o -6 2 2 9.53 7.15 0.54 o -5 2 2 1380.69 1596.89 5.63 o -4 2 2 0.66 2.07 0.24 o -3 2 2 1294.26 1389.50 9.75 o -2 2 2 58.90 55.73 0.54 o -1 2 2 408.34 425.58 1.68 o 0 2 2 911.55 881.93 9.93 o 1 2 2 183.31 218.28 4.32 o 2 2 2 0.51 1.08 0.14 o 3 2 2 0.23 0.23 0.10 o 4 2 2 77.61 91.53 1.58 o 5 2 2 32.71 47.81 0.90 o 6 2 2 8.85 5.95 0.40 o 7 2 2 28.89 26.90 0.63 o 8 2 2 589.15 562.73 4.02 o 9 2 2 412.73 409.40 16.43 o 10 2 2 347.84 330.08 13.77 o 11 2 2 17.65 13.40 0.93 o 12 2 2 39.05 45.57 2.78 o -12 3 2 6.92 9.12 0.59 o -11 3 2 4.34 5.64 0.66 o -10 3 2 32.51 24.68 1.22 o -9 3 2 3.65 4.68 0.50 o -8 3 2 46.09 37.43 2.21 o -7 3 2 262.53 264.86 2.80 o -6 3 2 14.35 15.59 1.81 o -5 3 2 61.56 58.67 3.69 o -4 3 2 483.02 593.88 4.59 o -3 3 2 1367.18 1530.34 25.40 o -2 3 2 6.94 5.45 0.42 o -1 3 2 383.04 440.77 6.16 o 0 3 2 83.21 95.38 3.29 o 1 3 2 114.80 121.04 0.99 o 2 3 2 1184.50 1172.36 8.85 o 3 3 2 433.67 477.24 3.55 o 4 3 2 126.71 151.64 3.81 o 5 3 2 342.68 338.35 2.45 o 6 3 2 344.42 345.99 2.61 o 7 3 2 51.73 50.36 0.90 o 8 3 2 79.69 66.35 1.40 o 9 3 2 64.61 51.35 1.15 o 10 3 2 34.24 29.41 1.33 o 11 3 2 4.22 4.59 0.63 o 12 3 2 0.18 0.07 0.44 o -11 4 2 16.43 19.19 0.73 o -10 4 2 6.59 8.12 0.42 o -9 4 2 8.50 3.49 0.46 o -8 4 2 409.10 382.60 2.89 o -7 4 2 91.95 92.44 3.30 o -6 4 2 403.44 369.11 3.69 o -5 4 2 55.86 53.32 1.05 o -4 4 2 41.29 50.38 1.54 o -3 4 2 100.97 105.76 1.85 o -2 4 2 577.81 676.19 14.93 o -1 4 2 490.27 519.01 3.56 o 0 4 2 11.04 11.93 0.65 o 1 4 2 80.88 96.32 2.13 o 2 4 2 10.74 13.08 0.51 o 3 4 2 161.23 160.42 2.55 o 4 4 2 141.70 146.51 2.58 o 5 4 2 93.17 90.33 1.78 o 6 4 2 0.67 0.66 0.49 o 7 4 2 128.12 123.62 1.71 o 8 4 2 47.31 46.21 1.12 o 9 4 2 3.97 3.33 0.46 o 10 4 2 13.90 15.87 0.90 o 11 4 2 16.02 18.37 0.77 o -10 5 2 9.99 12.36 0.39 o -9 5 2 8.32 8.75 0.62 o -8 5 2 101.14 93.86 1.86 o -7 5 2 1.08 0.60 0.60 o -6 5 2 3.19 3.39 0.59 o -5 5 2 33.80 23.54 1.05 o -4 5 2 307.53 293.72 6.44 o -3 5 2 207.74 207.08 2.09 o -2 5 2 1.79 3.74 0.48 o -1 5 2 131.15 136.76 2.41 o 0 5 2 14.75 19.73 0.62 o 1 5 2 7.98 3.44 0.89 o 2 5 2 224.78 216.66 2.86 o 3 5 2 108.94 111.80 1.43 o 4 5 2 216.00 217.23 2.02 o 5 5 2 111.59 109.57 3.76 o 6 5 2 30.12 22.86 1.29 o 7 5 2 53.15 46.69 1.57 o 8 5 2 27.80 20.78 0.70 o 9 5 2 22.05 26.89 1.43 o 10 5 2 3.89 5.00 0.54 o -9 6 2 11.26 18.05 0.71 o -8 6 2 11.19 8.69 0.61 o -7 6 2 0.36 0.43 0.49 o -6 6 2 2.24 1.41 0.55 o -5 6 2 37.83 37.79 1.32 o -4 6 2 2.49 4.34 0.63 o -3 6 2 254.45 219.73 3.45 o -2 6 2 1.24 0.78 0.47 o -1 6 2 44.27 43.51 1.08 o 0 6 2 64.60 66.28 1.09 o 1 6 2 10.01 10.58 0.52 o 2 6 2 190.70 169.30 7.11 o 3 6 2 335.17 304.44 7.56 o 4 6 2 4.00 4.23 0.64 o 5 6 2 4.87 6.68 0.64 o 6 6 2 73.75 65.25 1.62 o 7 6 2 4.10 4.07 0.56 o 8 6 2 93.05 96.71 1.63 o -8 7 2 1.86 1.26 0.44 o -7 7 2 94.35 104.36 1.56 o -6 7 2 51.23 45.62 1.22 o -5 7 2 55.91 45.90 1.32 o -4 7 2 143.77 136.88 2.32 o -3 7 2 0.69 0.32 0.62 o -2 7 2 186.63 173.77 2.81 o -1 7 2 72.26 68.04 1.21 o 0 7 2 2.13 0.98 0.38 o 1 7 2 2.40 3.16 0.38 o 2 7 2 44.38 43.67 0.84 o 3 7 2 138.31 148.87 2.52 o 4 7 2 45.86 50.63 1.35 o 5 7 2 34.75 40.81 1.19 o 6 7 2 51.64 54.37 1.23 o 7 7 2 2.41 3.53 0.40 o -5 8 2 9.25 9.87 0.35 o -4 8 2 0.02 -0.30 0.31 o -3 8 2 0.34 0.29 0.34 o -2 8 2 1.19 0.77 0.47 o -1 8 2 6.11 3.68 0.34 o 0 8 2 23.58 25.98 0.56 o 1 8 2 226.87 212.91 1.82 o 2 8 2 60.14 66.08 2.30 o 3 8 2 10.23 12.71 0.66 o 4 8 2 34.62 35.90 0.95 o 5 8 2 13.31 16.94 0.56 o -11 0 3 36.59 34.58 1.42 o -9 0 3 1442.20 1183.83 7.97 o -7 0 3 404.69 404.71 4.00 o -5 0 3 860.51 1048.50 3.66 o -3 0 3 657.43 670.07 3.46 o -1 0 3 26.53 22.81 0.50 o 3 0 3 960.14 902.83 3.00 o 5 0 3 623.34 636.49 4.17 o 7 0 3 72.70 75.88 1.51 o 9 0 3 36.82 40.92 1.51 o 11 0 3 132.33 157.09 1.73 o -12 1 3 9.35 9.95 0.72 o -11 1 3 33.49 37.30 1.03 o -10 1 3 21.87 13.70 0.91 o -9 1 3 107.29 95.12 1.64 o -8 1 3 3.81 7.92 3.50 o -7 1 3 212.11 211.51 3.06 o -6 1 3 21.87 27.40 0.66 o -5 1 3 2.38 2.59 0.61 o -4 1 3 54.92 60.01 0.89 o -3 1 3 20.77 35.58 0.57 o -2 1 3 1116.70 1095.21 3.20 o -1 1 3 3.98 2.49 0.73 o 2 1 3 554.60 551.63 6.83 o 3 1 3 253.43 231.77 2.53 o 4 1 3 826.53 813.45 2.85 o 5 1 3 2.27 1.81 0.20 o 6 1 3 13.53 26.65 0.66 o 7 1 3 23.56 23.68 0.56 o 8 1 3 201.42 213.88 2.47 o 9 1 3 840.03 822.98 5.44 o 10 1 3 105.28 103.14 2.33 o 11 1 3 16.49 14.78 0.66 o 12 1 3 21.00 25.50 0.70 o -12 2 3 139.67 179.85 5.39 o -11 2 3 0.92 0.67 0.52 o -10 2 3 19.84 18.60 1.03 o -9 2 3 27.22 24.99 1.22 o -8 2 3 32.55 30.79 0.93 o -7 2 3 4.36 3.95 0.88 o -6 2 3 5.98 4.08 0.71 o -5 2 3 0.83 3.84 0.54 o -4 2 3 2804.08 3132.20 66.16 o -3 2 3 38.41 31.02 1.02 o -2 2 3 115.72 135.95 0.50 o -1 2 3 2.36 2.09 0.10 o 0 2 3 194.46 236.18 4.68 o 1 2 3 207.26 231.15 1.44 o 2 2 3 263.25 272.78 3.11 o 3 2 3 156.33 163.20 6.28 o 4 2 3 639.10 650.13 10.25 o 5 2 3 506.07 505.30 2.83 o 6 2 3 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