#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/77/2227730.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227730_Fobs loop_ _publ_author_name 'Yang, Ting-Hai' 'Zhuang, Wei' 'Wei, Wei' 'Yang, Yong-Bing' 'Chen, Qiang' _publ_section_title ; [Amino(iminio)methyl]phosphonate ; _journal_coeditor_code JJ2049 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2326 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 99.570 _cell_angle_beta 90.784 _cell_angle_gamma 101.546 _cell_length_a 4.8559 _cell_length_b 5.9102 _cell_length_c 8.1012 _exptl_crystal_F_000 128.00 _reflns_d_resolution_high 0.8110 _[local]_cod_data_source_file jj2049Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 3 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 40.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 739.18 716.98 32.23 o 2 0 0 304.56 325.77 5.40 o 3 0 0 130.91 130.40 2.17 o 4 0 0 230.34 249.76 6.04 o 5 0 0 20.57 21.97 0.67 o -5 1 0 17.02 15.56 0.50 o -4 1 0 288.76 306.93 7.39 o -3 1 0 125.11 93.28 2.29 o -2 1 0 141.78 200.66 4.81 o -1 1 0 383.07 410.94 9.88 o 1 1 0 110.14 112.27 1.97 o 2 1 0 1.60 3.02 0.11 o 3 1 0 87.88 94.67 1.59 o 4 1 0 7.08 6.86 0.19 o 5 1 0 78.91 79.58 1.41 o -5 2 0 3.43 2.43 0.16 o -4 2 0 91.54 92.42 2.30 o -3 2 0 349.90 385.77 9.23 o -2 2 0 35.40 60.62 1.49 o -1 2 0 483.82 497.74 11.95 o 0 2 0 1150.90 1239.76 78.27 o 1 2 0 667.65 699.67 12.76 o 2 2 0 89.79 104.99 1.29 o 3 2 0 15.83 19.36 0.38 o 4 2 0 134.50 132.99 2.25 o 5 2 0 145.95 136.63 2.34 o -5 3 0 86.09 84.37 1.56 o -4 3 0 9.01 7.66 0.27 o -3 3 0 90.63 91.12 2.24 o -1 3 0 182.68 200.51 3.52 o 0 3 0 496.22 533.92 10.45 o 1 3 0 175.11 181.03 3.07 o 2 3 0 175.52 168.25 2.96 o 3 3 0 1.15 1.03 0.07 o 4 3 0 184.43 170.07 2.86 o -5 4 0 81.11 82.79 1.55 o -4 4 0 29.71 27.09 0.57 o -3 4 0 574.06 580.50 10.16 o -2 4 0 795.47 784.89 13.85 o -1 4 0 52.65 61.95 1.12 o 0 4 0 265.75 264.26 6.81 o 1 4 0 34.19 32.88 0.49 o 2 4 0 212.01 199.28 3.41 o 3 4 0 1.00 0.88 0.11 o 4 4 0 49.51 45.50 1.17 o -5 5 0 8.09 8.76 0.25 o -4 5 0 6.21 6.93 0.20 o -3 5 0 58.80 56.58 1.06 o -2 5 0 31.04 29.51 0.58 o -1 5 0 95.65 114.47 2.05 o 0 5 0 32.42 35.47 0.99 o 1 5 0 2.20 2.41 0.14 o 2 5 0 27.03 29.82 0.80 o 3 5 0 135.73 132.67 3.10 o -4 6 0 46.86 49.91 1.46 o -3 6 0 3.25 2.88 0.19 o -2 6 0 110.99 113.83 3.05 o -1 6 0 37.03 43.80 1.25 o 0 6 0 21.93 20.18 0.42 o 1 6 0 5.05 4.99 0.22 o 2 6 0 91.87 93.84 2.25 o -2 7 0 100.05 99.40 2.72 o -1 7 0 89.50 84.79 2.32 o 0 7 0 9.92 9.08 0.35 o 0 -7 1 84.43 83.08 2.01 o 1 -7 1 20.12 18.23 0.61 o 2 -7 1 61.97 63.60 1.81 o -2 -6 1 151.44 148.47 3.47 o -1 -6 1 191.84 195.43 4.49 o 0 -6 1 60.58 61.14 1.68 o 1 -6 1 4.34 5.05 0.24 o 2 -6 1 93.41 92.29 2.51 o 3 -6 1 192.84 197.34 5.20 o 4 -6 1 120.83 114.37 3.10 o -3 -5 1 7.76 7.68 0.30 o -2 -5 1 41.82 42.92 1.09 o -1 -5 1 83.91 89.70 2.97 o 0 -5 1 36.26 45.86 1.26 o 1 -5 1 89.73 86.56 2.32 o 2 -5 1 68.20 65.02 1.19 o 3 -5 1 5.79 6.98 0.19 o 4 -5 1 12.90 13.76 0.33 o 5 -5 1 87.84 87.05 1.62 o -4 -4 1 57.69 54.79 1.38 o -3 -4 1 65.00 60.06 1.46 o -2 -4 1 1.75 2.88 0.14 o 0 -4 1 20.31 30.43 0.56 o 1 -4 1 4.28 3.64 0.10 o 3 -4 1 15.76 14.75 0.32 o 4 -4 1 342.02 339.74 5.99 o 5 -4 1 53.14 50.55 0.98 o -4 -3 1 34.93 35.08 0.66 o -3 -3 1 253.15 249.41 4.12 o -2 -3 1 43.28 48.73 0.71 o -1 -3 1 6.38 6.66 0.12 o 0 -3 1 568.95 601.44 10.57 o 1 -3 1 286.37 301.91 5.30 o 2 -3 1 0.35 0.74 0.06 o 3 -3 1 64.18 64.60 1.18 o 4 -3 1 238.93 233.51 4.13 o 5 -3 1 0.04 0.10 0.05 o -5 -2 1 5.36 5.26 0.18 o -4 -2 1 360.53 370.07 6.09 o -3 -2 1 20.77 18.87 0.30 o -2 -2 1 4.73 5.99 0.11 o -1 -2 1 9.97 8.21 0.13 o 2 -2 1 36.20 33.47 0.62 o 3 -2 1 622.28 644.24 11.30 o 4 -2 1 85.21 79.39 1.45 o 5 -2 1 69.78 72.17 1.34 o -5 -1 1 25.44 23.90 0.53 o -4 -1 1 170.77 170.61 2.85 o -3 -1 1 0.67 1.34 0.07 o -2 -1 1 0.03 0.14 0.02 o -1 -1 1 531.41 511.34 7.07 o 0 -1 1 59.32 91.73 1.67 o 1 -1 1 611.97 611.60 12.93 o 2 -1 1 157.84 89.04 2.30 o 3 -1 1 232.19 257.99 4.52 o 4 -1 1 17.14 18.25 0.38 o 5 -1 1 123.83 125.50 3.13 o -5 0 1 162.38 162.99 4.01 o -4 0 1 1.69 1.30 0.11 o -3 0 1 46.65 53.60 0.92 o -1 0 1 1014.25 951.70 16.64 o 0 0 1 31.79 34.86 0.64 o 1 0 1 934.84 878.01 19.70 o 2 0 1 162.10 144.78 15.26 o 3 0 1 93.31 93.81 1.33 o 4 0 1 353.99 357.75 8.60 o 5 0 1 23.16 21.24 0.66 o -5 1 1 168.70 170.49 4.19 o -4 1 1 8.55 5.73 0.22 o -1 1 1 443.47 477.35 11.48 o 0 1 1 434.10 500.34 8.21 o 1 1 1 21.28 26.76 0.46 o 2 1 1 107.09 106.73 2.43 o 3 1 1 28.00 26.45 0.50 o 4 1 1 133.05 134.90 2.28 o 5 1 1 2.42 1.90 0.11 o -5 2 1 12.06 10.54 0.38 o -4 2 1 45.17 40.67 1.07 o -3 2 1 74.07 68.76 1.71 o -2 2 1 1237.03 1355.60 32.46 o -1 2 1 79.67 99.42 2.40 o 1 2 1 297.05 326.56 4.50 o 2 2 1 0.02 0.24 0.05 o 3 2 1 130.20 129.57 2.17 o 4 2 1 20.07 20.83 0.43 o 5 2 1 2.44 2.78 0.14 o -5 3 1 20.36 16.52 0.53 o -4 3 1 42.79 42.46 1.12 o -3 3 1 166.45 162.08 3.93 o -2 3 1 29.30 34.00 0.88 o -1 3 1 533.76 657.45 15.80 o 0 3 1 145.22 141.26 2.49 o 1 3 1 13.79 16.98 0.26 o 2 3 1 45.24 46.95 0.82 o 3 3 1 189.02 182.97 3.04 o 4 3 1 5.91 5.96 0.18 o -5 4 1 0.21 0.18 0.05 o -4 4 1 31.84 33.10 0.90 o -3 4 1 318.99 308.75 7.42 o -2 4 1 48.42 47.29 1.20 o -1 4 1 256.66 282.51 9.83 o 0 4 1 128.98 166.83 10.82 o 1 4 1 106.05 117.50 1.66 o 2 4 1 50.90 51.29 0.91 o 3 4 1 0.10 0.09 0.10 o 4 4 1 20.11 20.45 0.61 o -4 5 1 26.43 25.81 0.86 o -3 5 1 0.37 0.98 0.12 o -2 5 1 209.90 209.42 3.71 o -1 5 1 26.49 24.73 0.50 o 0 5 1 15.45 20.90 0.34 o 1 5 1 51.07 58.26 1.41 o 2 5 1 89.69 84.02 2.00 o 3 5 1 8.47 8.03 0.32 o -4 6 1 4.54 4.74 0.17 o -3 6 1 314.11 310.94 8.09 o -2 6 1 356.19 354.50 9.20 o -1 6 1 4.71 5.76 0.26 o 0 6 1 32.00 32.62 0.86 o 1 6 1 52.70 53.88 1.34 o -1 7 1 7.91 8.06 0.32 o 0 -7 2 0.00 0.03 0.06 o 1 -7 2 166.79 155.95 4.13 o 2 -7 2 80.38 78.33 2.17 o -2 -6 2 146.92 153.10 3.57 o -1 -6 2 56.97 61.23 1.52 o 0 -6 2 43.51 42.23 1.20 o 1 -6 2 11.40 13.34 0.46 o 2 -6 2 15.71 13.16 0.48 o 3 -6 2 5.28 6.72 0.30 o 4 -6 2 21.40 21.73 0.74 o -3 -5 2 45.85 48.61 1.23 o -2 -5 2 63.48 67.28 1.63 o -1 -5 2 0.28 0.36 0.06 o 0 -5 2 210.36 216.48 5.63 o 1 -5 2 9.60 12.39 0.42 o 2 -5 2 28.78 21.86 0.67 o 3 -5 2 55.96 58.24 1.09 o 4 -5 2 74.68 73.30 1.37 o 5 -5 2 26.00 26.41 0.57 o -4 -4 2 147.85 136.28 3.18 o -3 -4 2 40.83 40.60 1.02 o -2 -4 2 127.63 127.29 2.20 o -1 -4 2 680.33 681.79 13.58 o 0 -4 2 247.28 262.12 6.76 o 1 -4 2 15.87 20.31 0.51 o 3 -4 2 457.44 476.91 8.34 o 4 -4 2 259.07 262.88 4.65 o 5 -4 2 57.29 58.10 1.12 o -4 -3 2 153.08 147.11 3.41 o -3 -3 2 25.70 26.50 0.49 o -2 -3 2 53.87 54.60 0.79 o -1 -3 2 687.80 669.18 13.30 o 0 -3 2 56.30 66.17 1.76 o 1 -3 2 34.59 40.29 0.73 o 2 -3 2 62.17 59.56 1.08 o 3 -3 2 237.69 248.14 4.37 o 4 -3 2 5.88 6.19 0.17 o 5 -3 2 50.23 49.38 0.96 o -5 -2 2 244.20 230.67 3.85 o -4 -2 2 106.90 102.67 1.75 o -3 -2 2 0.75 1.24 0.07 o -2 -2 2 20.15 25.67 0.38 o -1 -2 2 24.17 42.32 0.60 o 0 -2 2 19.51 18.93 0.53 o 1 -2 2 367.97 438.70 7.73 o 2 -2 2 38.72 34.60 0.64 o 3 -2 2 12.51 16.17 0.33 o 4 -2 2 639.99 644.33 11.26 o 5 -2 2 37.08 35.31 0.99 o -5 -1 2 56.79 57.31 1.04 o -4 -1 2 18.85 19.90 0.40 o -3 -1 2 93.21 93.42 1.32 o -2 -1 2 231.22 263.65 3.63 o -1 -1 2 43.96 63.45 0.89 o 0 -1 2 1044.46 0.00 0.16 o 1 -1 2 69.73 73.89 3.13 o 2 -1 2 98.50 118.74 2.88 o 3 -1 2 257.15 288.24 5.06 o 4 -1 2 323.58 340.96 5.98 o 5 -1 2 2.89 4.01 0.22 o -5 0 2 51.37 47.21 1.26 o -4 0 2 517.24 550.79 13.18 o -3 0 2 268.44 274.43 4.50 o -2 0 2 197.39 223.43 3.31 o -1 0 2 101.57 111.40 1.36 o 0 0 2 1625.30 1599.17 38.17 o 2 0 2 279.95 295.38 18.01 o 4 0 2 43.32 43.34 1.15 o 5 0 2 1.78 1.52 0.14 o -5 1 2 11.62 10.36 0.38 o -4 1 2 75.24 77.00 1.93 o -3 1 2 253.53 255.10 6.14 o -2 1 2 52.78 72.73 1.79 o -1 1 2 352.78 0.00 0.16 o 0 1 2 0.14 0.29 0.02 o 1 1 2 37.83 56.23 0.79 o 2 1 2 122.55 114.53 1.91 o 3 1 2 87.24 93.60 1.59 o 4 1 2 44.14 40.18 0.75 o 5 1 2 18.52 18.87 0.61 o -5 2 2 11.18 12.09 0.42 o -4 2 2 21.01 18.92 0.56 o -2 2 2 33.46 50.85 1.28 o -1 2 2 8.04 5.69 0.21 o 0 2 2 50.24 59.21 1.00 o 1 2 2 488.98 550.04 8.95 o 2 2 2 674.19 698.29 11.50 o 3 2 2 51.27 49.33 0.87 o 4 2 2 224.41 217.82 3.64 o 5 2 2 51.14 47.88 0.90 o -5 3 2 69.69 68.62 1.79 o -4 3 2 5.72 7.50 0.29 o -3 3 2 96.44 96.67 2.40 o -2 3 2 695.37 751.29 18.07 o -1 3 2 76.13 71.20 1.78 o 0 3 2 19.52 21.15 0.39 o 1 3 2 268.76 281.93 3.89 o 2 3 2 223.20 218.17 3.79 o 3 3 2 11.38 10.78 0.25 o 4 3 2 21.28 19.63 0.42 o -5 4 2 11.36 12.11 0.43 o -4 4 2 12.30 11.64 0.40 o -3 4 2 194.84 188.24 4.57 o -2 4 2 764.63 795.59 18.97 o -1 4 2 73.92 62.61 1.58 o 0 4 2 97.42 99.41 1.41 o 1 4 2 203.12 200.14 3.32 o 2 4 2 0.05 0.09 0.07 o 3 4 2 4.69 5.34 0.30 o -4 5 2 0.66 1.09 0.11 o -3 5 2 63.37 64.53 1.65 o -2 5 2 3.64 3.76 0.30 o -1 5 2 51.72 63.04 1.84 o 0 5 2 42.33 45.45 0.68 o 1 5 2 8.59 8.47 0.21 o 2 5 2 77.40 74.55 1.79 o -3 6 2 40.76 41.26 0.82 o -2 6 2 99.62 102.22 1.87 o -1 6 2 159.13 170.94 2.95 o 0 6 2 7.18 8.16 0.29 o 1 6 2 67.91 64.97 1.58 o 0 -7 3 136.94 139.03 3.71 o 1 -7 3 22.62 20.33 0.67 o 2 -7 3 27.15 25.09 0.80 o -2 -6 3 0.31 0.40 0.10 o -1 -6 3 426.14 429.09 7.29 o 0 -6 3 329.40 318.25 8.25 o 1 -6 3 25.97 25.51 0.78 o 2 -6 3 68.37 65.20 1.82 o 3 -6 3 67.60 68.83 1.93 o 4 -6 3 43.25 41.77 1.25 o -3 -5 3 14.71 16.49 0.51 o -2 -5 3 0.23 0.38 0.08 o -1 -5 3 175.79 182.35 3.14 o 0 -5 3 1.12 1.97 0.14 o 1 -5 3 68.53 62.02 1.70 o 2 -5 3 35.47 36.03 1.06 o 3 -5 3 14.59 13.48 0.48 o 4 -5 3 63.45 63.41 1.78 o -4 -4 3 54.63 46.42 1.17 o -3 -4 3 4.56 5.20 0.21 o -2 -4 3 151.14 153.68 2.65 o -1 -4 3 8.57 10.86 0.37 o 0 -4 3 458.75 441.26 11.45 o 1 -4 3 2.82 1.47 0.11 o 2 -4 3 17.97 18.71 0.38 o 3 -4 3 13.68 15.42 0.34 o 4 -4 3 210.57 208.34 3.70 o 5 -4 3 81.25 83.09 1.55 o -4 -3 3 14.14 13.59 0.42 o -3 -3 3 112.60 108.65 1.89 o -2 -3 3 479.52 472.42 7.96 o -1 -3 3 16.12 14.49 0.29 o 0 -3 3 462.39 504.06 13.07 o 2 -3 3 84.79 108.26 1.93 o 3 -3 3 111.24 112.79 2.03 o 4 -3 3 125.09 121.00 2.18 o 5 -3 3 0.38 0.51 0.10 o -5 -2 3 0.61 0.78 0.08 o -4 -2 3 173.82 171.15 2.86 o -3 -2 3 531.21 524.86 7.28 o -2 -2 3 28.37 23.04 0.35 o -1 -2 3 885.95 911.84 13.07 o 0 -2 3 47.18 47.09 0.84 o 1 -2 3 250.07 242.41 4.24 o 2 -2 3 282.17 318.55 5.57 o 3 -2 3 244.62 259.82 4.57 o 4 -2 3 68.73 71.72 1.32 o 5 -2 3 12.60 11.95 0.43 o -5 -1 3 3.48 4.07 0.15 o -4 -1 3 34.38 32.88 0.60 o -3 -1 3 156.02 164.24 2.29 o -2 -1 3 121.29 136.05 1.90 o -1 -1 3 634.41 660.79 9.14 o 0 -1 3 38.10 47.69 1.17 o 2 -1 3 454.43 459.82 8.11 o 3 -1 3 170.77 198.04 3.49 o 4 -1 3 39.97 36.61 0.99 o 5 -1 3 46.30 44.74 1.23 o -5 0 3 105.80 108.26 2.72 o -4 0 3 79.92 84.16 2.11 o -3 0 3 12.39 12.06 0.37 o -2 0 3 215.30 231.19 4.61 o -1 0 3 321.09 396.05 7.24 o 0 0 3 75.76 81.32 1.13 o 1 0 3 26.57 29.79 0.55 o 2 0 3 773.44 840.36 14.80 o 4 0 3 242.07 235.45 5.73 o 5 0 3 81.61 79.99 2.08 o -5 1 3 99.12 100.25 2.53 o -4 1 3 61.03 66.49 1.70 o -3 1 3 145.70 140.92 3.44 o -2 1 3 578.01 655.93 15.78 o -1 1 3 3.30 2.94 0.09 o 0 1 3 3.87 8.13 0.38 o 1 1 3 180.68 186.87 2.59 o 2 1 3 112.13 118.87 1.99 o 3 1 3 105.30 107.51 1.82 o 4 1 3 33.53 34.38 0.65 o 5 1 3 8.78 8.36 0.35 o -5 2 3 0.69 1.87 0.14 o -4 2 3 104.39 101.60 2.54 o -2 2 3 35.82 43.53 1.12 o -1 2 3 22.52 23.43 0.64 o 0 2 3 12.57 10.44 0.21 o 1 2 3 1072.89 1129.79 24.11 o 2 2 3 3.62 4.77 0.16 o 3 2 3 171.22 176.58 2.95 o 4 2 3 9.27 9.51 0.25 o -5 3 3 0.16 0.50 0.10 o -4 3 3 75.20 71.80 1.84 o -3 3 3 161.43 170.17 4.16 o -2 3 3 26.54 27.51 0.75 o -1 3 3 70.41 85.46 2.14 o 0 3 3 152.81 152.42 2.52 o 1 3 3 68.02 63.70 0.98 o 2 3 3 150.52 145.31 3.21 o 3 3 3 46.18 45.00 0.82 o 4 3 3 6.81 5.65 0.26 o -5 4 3 1.24 2.43 0.18 o -4 4 3 8.65 10.35 0.37 o -3 4 3 3.79 4.62 0.21 o -2 4 3 0.18 0.42 0.08 o -1 4 3 25.48 24.77 0.70 o 0 4 3 89.57 85.06 1.45 o 1 4 3 150.07 154.80 2.59 o 2 4 3 247.14 237.06 3.94 o 3 4 3 1.12 1.06 0.09 o -4 5 3 59.04 61.95 1.62 o -3 5 3 24.19 22.96 0.67 o -2 5 3 68.55 72.83 1.84 o -1 5 3 36.98 32.43 0.51 o 0 5 3 0.41 0.20 0.05 o 1 5 3 114.65 118.95 2.03 o 2 5 3 22.58 22.60 0.56 o -3 6 3 58.82 56.40 1.09 o -2 6 3 193.92 192.72 3.45 o -1 6 3 97.15 95.83 1.65 o 0 6 3 40.96 42.60 1.07 o 1 -7 4 58.02 54.34 1.57 o -2 -6 4 54.58 54.29 1.38 o -1 -6 4 115.24 119.24 2.10 o 0 -6 4 24.09 23.88 0.75 o 1 -6 4 70.13 64.59 1.81 o 2 -6 4 0.05 0.03 0.06 o 3 -6 4 85.23 82.45 2.27 o -3 -5 4 19.69 19.93 0.58 o -2 -5 4 66.45 70.59 1.28 o -1 -5 4 4.42 3.73 0.13 o 0 -5 4 100.88 105.90 2.83 o 1 -5 4 42.26 40.24 1.15 o 2 -5 4 4.27 4.62 0.22 o 3 -5 4 173.01 162.40 4.29 o 4 -5 4 35.00 33.95 1.02 o -3 -4 4 150.02 144.45 3.33 o -2 -4 4 14.81 14.14 0.31 o -1 -4 4 803.96 821.88 24.17 o 0 -4 4 527.12 544.74 14.22 o 1 -4 4 8.71 8.25 0.30 o 2 -4 4 96.97 95.01 2.53 o 3 -4 4 126.13 124.79 2.86 o 4 -4 4 26.20 28.42 0.59 o 5 -4 4 9.26 9.89 0.27 o -4 -3 4 41.08 39.88 1.01 o -3 -3 4 114.65 112.76 1.96 o -2 -3 4 29.84 29.98 0.56 o -1 -3 4 402.35 419.53 10.78 o 0 -3 4 41.66 37.29 1.04 o 1 -3 4 0.05 0.45 0.06 o 2 -3 4 191.75 203.06 3.58 o 3 -3 4 32.13 30.80 0.60 o 4 -3 4 15.64 14.56 0.33 o 5 -3 4 8.68 9.96 0.38 o -4 -2 4 169.36 160.11 2.25 o -3 -2 4 64.82 62.08 0.90 o -2 -2 4 260.42 265.50 3.67 o -1 -2 4 62.35 77.35 1.09 o 1 -2 4 22.68 20.60 0.59 o 2 -2 4 0.63 0.27 0.03 o 3 -2 4 78.65 84.43 1.53 o 4 -2 4 115.08 112.96 2.04 o 5 -2 4 119.82 115.96 2.93 o -5 -1 4 2.51 2.43 0.16 o -4 -1 4 8.19 8.14 0.20 o -3 -1 4 181.24 188.26 2.62 o -2 -1 4 464.47 476.74 8.37 o -1 -1 4 70.44 90.74 1.27 o 0 -1 4 147.78 187.26 3.29 o 1 -1 4 509.19 513.58 9.11 o 2 -1 4 36.95 47.31 0.87 o 3 -1 4 149.18 154.46 2.74 o 4 -1 4 85.08 85.96 2.17 o 5 -1 4 49.51 47.32 1.30 o -5 0 4 24.36 26.99 0.78 o -4 0 4 163.09 159.04 3.89 o -3 0 4 1414.51 1457.67 25.64 o -2 0 4 95.31 103.52 1.86 o -1 0 4 225.59 263.44 4.63 o 0 0 4 13.81 10.58 0.78 o 1 0 4 682.08 391.30 10.20 o 2 0 4 197.27 221.47 5.36 o 3 0 4 7.09 6.99 0.27 o 4 0 4 48.40 49.43 1.31 o 5 0 4 3.29 3.05 0.19 o -5 1 4 31.48 32.24 0.93 o -4 1 4 56.48 56.79 1.47 o -3 1 4 196.92 221.42 5.36 o -2 1 4 42.91 46.61 0.79 o -1 1 4 7.60 6.31 0.17 o 0 1 4 32.79 33.50 0.49 o 1 1 4 0.18 0.69 0.08 o 3 1 4 14.54 15.87 0.34 o 4 1 4 1.94 1.78 0.14 o -5 2 4 4.95 4.64 0.24 o -4 2 4 71.43 80.60 2.05 o -3 2 4 140.02 137.29 3.37 o -2 2 4 197.23 0.00 0.02 o -1 2 4 91.40 108.17 3.78 o 0 2 4 0.41 0.73 0.04 o 1 2 4 182.50 188.03 3.11 o 2 2 4 436.55 433.41 7.11 o 3 2 4 25.30 27.61 0.54 o 4 2 4 45.31 41.55 0.78 o -5 3 4 143.81 144.23 3.61 o -4 3 4 91.78 92.64 2.35 o -3 3 4 167.76 166.39 4.08 o -2 3 4 230.12 253.45 6.12 o -1 3 4 144.03 139.69 3.05 o 0 3 4 9.27 9.80 0.21 o 1 3 4 220.73 226.07 3.75 o 2 3 4 49.48 49.24 0.89 o 3 3 4 0.53 0.25 0.06 o -4 4 4 8.00 7.79 0.32 o -3 4 4 94.98 96.94 2.43 o -2 4 4 38.30 34.51 0.94 o -1 4 4 218.22 209.86 3.48 o 0 4 4 0.08 0.48 0.08 o 1 4 4 125.27 121.87 2.06 o 2 4 4 0.04 0.00 0.05 o 3 4 4 10.87 12.17 0.31 o -3 5 4 12.92 14.54 0.48 o -2 5 4 7.69 7.37 0.29 o -1 5 4 35.71 36.64 1.02 o 0 5 4 115.50 117.32 1.99 o 1 5 4 0.22 0.20 0.06 o 2 5 4 41.43 38.44 0.75 o -2 6 4 1.53 2.13 0.18 o -1 6 4 102.05 97.55 2.49 o -1 -6 5 101.10 103.83 2.21 o 0 -6 5 255.78 245.41 6.43 o 1 -6 5 96.95 96.13 2.62 o 2 -6 5 86.49 84.88 2.33 o 3 -6 5 101.64 96.56 2.64 o -2 -5 5 25.58 27.11 0.55 o -1 -5 5 15.00 16.60 0.78 o 0 -5 5 0.59 0.40 0.08 o 1 -5 5 15.98 14.71 0.51 o 2 -5 5 144.52 141.88 3.76 o 3 -5 5 0.01 0.00 0.06 o 4 -5 5 65.56 61.63 1.74 o -3 -4 5 8.21 6.57 0.19 o -2 -4 5 48.75 49.34 0.91 o -1 -4 5 14.80 16.59 0.35 o 0 -4 5 73.11 80.31 2.17 o 1 -4 5 418.33 416.38 10.73 o 2 -4 5 39.12 38.08 1.09 o 3 -4 5 209.85 209.81 5.49 o 4 -4 5 77.10 75.42 1.41 o -3 -3 5 163.47 156.53 3.87 o -2 -3 5 200.83 189.33 3.23 o -1 -3 5 9.57 8.59 0.32 o 1 -3 5 411.42 411.87 7.22 o 2 -3 5 8.94 9.13 0.22 o 3 -3 5 66.62 63.20 1.17 o 4 -3 5 15.18 14.93 0.39 o 5 -3 5 12.28 12.14 0.45 o -4 -2 5 9.51 8.64 0.35 o -3 -2 5 476.35 472.86 8.27 o -2 -2 5 181.30 168.01 2.34 o -1 -2 5 105.34 120.38 3.43 o 0 -2 5 370.12 342.97 17.38 o 1 -2 5 74.66 70.99 1.29 o 2 -2 5 65.91 75.33 1.37 o 3 -2 5 2.16 1.60 0.08 o 4 -2 5 0.94 1.25 0.13 o 5 -2 5 1.41 1.36 0.14 o -5 -1 5 0.02 0.05 0.06 o -4 -1 5 26.83 28.49 0.59 o -3 -1 5 30.82 31.11 0.61 o -2 -1 5 75.65 90.83 1.64 o -1 -1 5 132.10 143.02 3.86 o 0 -1 5 162.18 158.42 2.81 o 1 -1 5 71.84 77.04 1.39 o 2 -1 5 396.76 405.34 7.12 o 3 -1 5 34.57 36.89 1.26 o 4 -1 5 1.32 2.03 0.14 o 5 -1 5 49.41 44.82 1.25 o -5 0 5 0.37 0.22 0.08 o -4 0 5 205.90 212.27 5.17 o -3 0 5 1.37 1.62 0.09 o -2 0 5 385.13 450.07 10.76 o -1 0 5 32.85 33.44 1.24 o 0 0 5 101.68 108.42 1.95 o 1 0 5 384.87 378.71 6.64 o 2 0 5 28.35 34.38 0.66 o 3 0 5 8.44 10.60 0.37 o 4 0 5 2.01 1.97 0.14 o -5 1 5 93.80 103.32 2.62 o -4 1 5 94.17 98.99 2.49 o -3 1 5 84.52 92.77 2.32 o -2 1 5 155.40 158.10 3.94 o -1 1 5 104.08 109.80 1.98 o 0 1 5 2.40 1.27 0.07 o 1 1 5 190.59 184.37 3.14 o 2 1 5 0.22 0.49 0.24 o 3 1 5 5.38 6.22 0.27 o 4 1 5 39.12 37.66 1.07 o -5 2 5 145.12 163.16 4.06 o -4 2 5 45.50 40.81 1.12 o -3 2 5 461.40 483.85 11.61 o -2 2 5 38.45 36.78 0.99 o -1 2 5 2.76 0.02 0.02 o 0 2 5 48.34 49.57 1.15 o 1 2 5 39.55 39.58 0.71 o 2 2 5 7.06 8.57 0.22 o 3 2 5 3.40 3.58 0.14 o 4 2 5 69.81 66.76 1.21 o -4 3 5 111.96 111.43 2.81 o -3 3 5 56.19 54.92 1.44 o -2 3 5 0.98 1.74 0.13 o -1 3 5 72.40 70.12 1.81 o 0 3 5 197.73 207.99 3.43 o 1 3 5 0.17 0.35 0.05 o 2 3 5 19.21 19.65 0.41 o 3 3 5 34.59 34.41 0.89 o -4 4 5 70.09 81.77 2.11 o -3 4 5 32.54 29.66 0.85 o -2 4 5 24.90 26.26 0.75 o -1 4 5 15.59 13.37 0.46 o 0 4 5 11.59 10.52 0.38 o 1 4 5 22.30 21.37 0.44 o 2 4 5 60.15 56.56 1.02 o -3 5 5 4.38 4.21 0.22 o -2 5 5 31.28 30.16 0.86 o -1 5 5 55.67 52.90 1.44 o 0 5 5 5.99 6.41 0.30 o 1 5 5 39.23 41.37 1.18 o -1 -6 6 0.14 0.51 0.19 o 0 -6 6 6.96 6.06 0.30 o 1 -6 6 40.94 37.82 1.14 o 2 -6 6 38.17 35.63 1.09 o -2 -5 6 12.17 11.92 0.29 o -1 -5 6 17.22 17.84 0.41 o 0 -5 6 18.35 16.94 0.58 o 1 -5 6 81.81 77.96 2.14 o 2 -5 6 6.02 6.25 0.29 o 3 -5 6 101.07 92.22 2.51 o -3 -4 6 70.97 73.63 2.03 o -2 -4 6 0.34 0.31 0.08 o -1 -4 6 28.29 30.97 0.60 o 0 -4 6 424.95 417.43 10.78 o 1 -4 6 227.78 233.05 6.08 o 2 -4 6 124.94 126.32 3.36 o 3 -4 6 82.00 79.89 2.17 o 4 -4 6 2.40 2.56 0.18 o -3 -3 6 6.83 6.44 0.29 o -2 -3 6 32.42 34.69 1.01 o -1 -3 6 22.81 22.93 0.70 o 0 -3 6 165.45 158.30 4.16 o 1 -3 6 10.22 9.62 0.22 o 2 -3 6 141.03 140.65 2.52 o 3 -3 6 3.85 3.81 0.14 o 4 -3 6 1.46 1.84 0.14 o -4 -2 6 12.19 10.36 0.40 o -3 -2 6 1.69 0.67 0.10 o -2 -2 6 1.54 2.59 0.10 o -1 -2 6 36.36 32.61 0.48 o 0 -2 6 27.84 33.93 0.65 o 1 -2 6 757.46 746.77 13.19 o 2 -2 6 20.51 22.40 0.46 o 3 -2 6 96.77 93.06 1.70 o 4 -2 6 57.87 58.69 1.55 o -4 -1 6 5.17 5.18 0.17 o -3 -1 6 143.34 154.33 2.76 o -2 -1 6 77.34 73.31 1.77 o -1 -1 6 87.78 77.85 1.43 o 0 -1 6 107.56 114.80 2.83 o 1 -1 6 390.28 419.28 7.34 o 2 -1 6 1.85 2.70 0.11 o 3 -1 6 9.53 9.13 0.34 o 4 -1 6 67.38 63.46 1.68 o -4 0 6 25.22 25.09 0.74 o -3 0 6 366.51 382.18 6.74 o -2 0 6 429.76 439.91 7.72 o -1 0 6 12.27 12.57 0.30 o 0 0 6 431.78 439.69 7.71 o 1 0 6 19.64 21.37 0.44 o 2 0 6 2.06 2.42 0.10 o 3 0 6 20.26 17.65 0.56 o 4 0 6 7.79 6.64 0.30 o -4 1 6 29.19 34.88 0.98 o -3 1 6 3.67 3.79 0.19 o -2 1 6 1.24 0.53 0.06 o -1 1 6 65.65 63.61 1.20 o 0 1 6 105.16 109.86 1.99 o 1 1 6 71.75 73.40 1.36 o 2 1 6 55.85 58.42 1.55 o 3 1 6 34.52 35.77 1.02 o 4 1 6 0.74 0.96 0.13 o -4 2 6 42.14 45.82 1.25 o -3 2 6 12.65 12.23 0.42 o -2 2 6 184.31 195.63 4.78 o -1 2 6 224.46 228.59 5.58 o 0 2 6 41.69 43.26 1.17 o 1 2 6 207.32 216.25 3.59 o 2 2 6 48.67 47.02 0.86 o 3 2 6 79.73 73.17 1.30 o -4 3 6 46.16 42.63 1.18 o -3 3 6 2.22 3.57 0.19 o -2 3 6 121.48 115.84 2.89 o -1 3 6 175.22 172.90 4.27 o 0 3 6 4.48 4.08 0.22 o 1 3 6 25.05 25.57 0.78 o 2 3 6 16.32 16.86 0.38 o -3 4 6 43.88 45.50 1.25 o -2 4 6 58.91 53.22 1.42 o -1 4 6 1.01 0.59 0.11 o 0 4 6 0.87 1.54 0.16 o 1 4 6 3.41 3.89 0.22 o -1 5 6 82.80 73.53 1.95 o -1 -5 7 10.71 12.17 0.48 o 0 -5 7 0.15 0.34 0.10 o 1 -5 7 62.10 61.90 1.76 o 2 -5 7 61.32 58.13 1.65 o 3 -5 7 1.12 1.46 0.16 o -2 -4 7 4.97 6.19 0.29 o -1 -4 7 0.05 0.19 0.06 o 0 -4 7 3.25 3.87 0.22 o 1 -4 7 255.06 257.11 6.72 o 2 -4 7 113.21 116.02 3.12 o 3 -4 7 8.87 8.33 0.35 o -3 -3 7 180.11 168.50 4.46 o -2 -3 7 60.25 53.36 1.52 o -1 -3 7 34.05 28.31 0.86 o 0 -3 7 21.18 21.67 0.69 o 1 -3 7 109.20 106.73 2.86 o 2 -3 7 4.25 6.09 0.27 o 3 -3 7 3.26 3.62 0.14 o 4 -3 7 31.07 30.43 0.88 o -3 -2 7 31.62 29.58 0.91 o -2 -2 7 66.74 57.27 1.62 o -1 -2 7 42.43 38.97 0.75 o 0 -2 7 220.45 216.26 3.83 o 1 -2 7 47.14 46.44 0.89 o 2 -2 7 41.62 46.81 0.98 o 3 -2 7 28.82 31.42 0.90 o 4 -2 7 0.14 0.29 0.08 o -4 -1 7 75.17 83.80 1.57 o -3 -1 7 10.53 10.58 0.27 o -2 -1 7 23.35 29.14 0.82 o -1 -1 7 118.16 120.99 2.19 o 0 -1 7 140.36 139.16 2.50 o 1 -1 7 47.45 48.54 0.93 o 2 -1 7 95.61 97.53 1.78 o 3 -1 7 92.60 90.18 2.30 o 4 -1 7 1.60 1.41 0.16 o -4 0 7 2.44 2.51 0.16 o -3 0 7 0.29 0.20 0.14 o -2 0 7 13.13 13.33 0.32 o -1 0 7 339.09 358.12 6.32 o 0 0 7 0.15 0.38 0.06 o 1 0 7 279.54 280.09 4.96 o 2 0 7 58.25 58.96 1.57 o 3 0 7 5.14 10.84 0.42 o -4 1 7 4.09 5.31 0.26 o -3 1 7 0.04 0.00 0.05 o -2 1 7 48.29 45.98 0.90 o -1 1 7 97.37 95.39 1.77 o 0 1 7 33.13 34.28 0.69 o 1 1 7 24.83 24.45 0.74 o 2 1 7 3.79 9.96 0.38 o 3 1 7 6.58 6.80 0.32 o -4 2 7 0.02 0.10 0.08 o -3 2 7 46.87 43.72 1.20 o -2 2 7 239.99 239.57 5.84 o -1 2 7 1.78 1.46 0.16 o 0 2 7 154.93 159.18 3.95 o 1 2 7 0.72 0.85 0.13 o 2 2 7 0.11 0.10 0.06 o -3 3 7 38.44 36.67 1.04 o -2 3 7 15.48 14.28 0.50 o -1 3 7 101.28 96.13 2.48 o 0 3 7 72.11 71.71 1.90 o 1 3 7 4.37 4.78 0.26 o 2 3 7 2.51 2.54 0.21 o -2 4 7 58.26 52.63 1.42 o -1 4 7 98.71 97.25 2.53 o 0 4 7 4.51 5.28 0.29 o 0 -5 8 85.53 86.20 2.40 o 1 -5 8 13.20 12.41 0.50 o -2 -4 8 0.33 0.19 0.08 o -1 -4 8 23.55 24.15 0.78 o 0 -4 8 85.49 84.87 2.35 o 1 -4 8 39.06 38.22 1.15 o 2 -4 8 2.07 2.08 0.18 o -2 -3 8 19.14 18.26 0.64 o -1 -3 8 81.40 80.53 2.22 o 0 -3 8 13.59 12.25 0.46 o 1 -3 8 14.65 17.30 0.59 o 2 -3 8 13.11 14.14 0.50 o -3 -2 8 43.92 48.01 1.41 o -2 -2 8 2.25 3.02 0.19 o -1 -2 8 9.64 7.77 0.34 o 0 -2 8 16.36 17.10 0.39 o 1 -2 8 125.58 125.68 2.28 o 2 -2 8 117.40 116.23 2.12 o 3 -2 8 0.76 1.02 0.13 o -3 -1 8 65.49 64.85 1.84 o -2 -1 8 95.27 94.59 1.74 o -1 -1 8 20.26 17.09 0.40 o 0 -1 8 50.70 56.57 1.08 o 1 -1 8 47.88 48.39 0.94 o 2 -1 8 40.03 40.35 1.12 o 3 -1 8 4.40 4.72 0.26 o -3 0 8 22.07 20.10 0.46 o -2 0 8 178.02 172.13 3.10 o -1 0 8 36.64 39.03 0.79 o 0 0 8 45.14 45.89 0.90 o 1 0 8 33.98 33.86 0.69 o 2 0 8 0.18 0.22 0.08 o 3 0 8 28.01 30.50 0.93 o -3 1 8 1.70 2.35 0.18 o -2 1 8 1.79 2.17 0.18 o -1 1 8 87.29 89.71 1.68 o 0 1 8 18.79 17.60 0.50 o 1 1 8 1.67 1.78 0.16 o 2 1 8 39.86 38.92 1.14 o -3 2 8 2.30 1.81 0.16 o -2 2 8 59.51 57.73 1.54 o -1 2 8 207.22 214.91 5.31 o 0 2 8 4.12 4.64 0.26 o 1 2 8 51.29 50.17 1.41 o -2 3 8 49.70 51.48 1.41 o -1 3 8 30.73 31.18 0.96 o 0 3 8 0.76 0.53 0.11 o 0 -4 9 74.73 76.04 2.14 o 1 -4 9 45.46 42.51 1.28 o -1 -3 9 7.12 6.48 0.32 o 0 -3 9 32.27 33.63 1.04 o 1 -3 9 1.67 1.74 0.16 o 2 -3 9 4.97 4.16 0.24 o -2 -2 9 7.46 5.82 0.30 o -1 -2 9 11.09 12.51 0.48 o 0 -2 9 0.98 1.18 0.14 o 1 -2 9 2.62 3.53 0.21 o 2 -2 9 0.40 0.87 0.26 o -2 -1 9 47.28 44.97 1.34 o -1 -1 9 170.91 171.15 3.09 o 0 -1 9 15.88 16.59 0.39 o 1 -1 9 0.13 0.16 0.06 o 2 -1 9 38.71 37.60 1.09 o -2 0 9 39.76 39.70 0.81 o -1 0 9 32.98 34.13 0.72 o 0 0 9 8.06 8.39 0.25 o 1 0 9 2.88 2.51 0.19 o 2 0 9 102.45 100.36 2.61 o -2 1 9 31.59 34.22 0.73 o -1 1 9 0.04 0.14 0.06 o 0 1 9 1.91 3.50 0.42 o 1 1 9 10.54 10.35 0.43 o