#------------------------------------------------------------------------------ #$Date: 2010-12-22 21:36:50 +0200 (Wed, 22 Dec 2010) $ #$Revision: 5269 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2227754.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227754_Fobs loop_ _publ_author_name 'Sun, Tao' 'Li, Ke' 'Lai, Yulin' 'Chen, Ruihuan' 'Wu, Huilu' _publ_section_title ; Aqua[1,3-bis(benzimidazol-2-yl)-2-oxapropane]diethanolmanganese(II) dipicrate ethanol disolvate ; _journal_coeditor_code LH5083 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1058 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.504 _cell_angle_gamma 90.000 _cell_length_a 10.0519 _cell_length_b 24.8584 _cell_length_c 18.0291 _exptl_crystal_F_000 2060.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file lh5083Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I P2(1)/c R = 0.08' _shelx_refln_list_code 4 _shelx_f_calc_maximum 787.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 106.77 269.04 7.85 o 3 0 0 12372.99 9964.37 50.22 o 4 0 0 1515.70 1441.87 58.72 o 5 0 0 366.28 345.01 27.61 o 6 0 0 125.17 156.66 23.95 o 7 0 0 1088.30 1020.81 35.80 o 8 0 0 22.06 17.34 20.94 o 9 0 0 1677.87 2324.32 74.60 o 10 0 0 446.79 447.26 50.80 o 11 0 0 186.82 154.85 38.83 o 2 1 0 132.81 176.62 5.30 o 3 1 0 534.38 516.42 10.83 o 4 1 0 553.20 671.20 12.45 o 5 1 0 904.09 613.79 12.98 o 6 1 0 43.16 46.29 11.27 o 7 1 0 1292.11 1512.78 31.44 o 8 1 0 16.39 14.55 18.79 o 9 1 0 28.84 26.62 20.52 o 10 1 0 52.58 70.19 31.40 o 11 1 0 7.17 13.74 21.93 o 2 2 0 29684.88 27873.19 106.05 o 3 2 0 7040.32 6698.89 31.36 o 4 2 0 18.30 20.78 8.42 o 5 2 0 3970.20 3666.74 31.28 o 6 2 0 56.13 77.34 10.91 o 7 2 0 1251.46 1604.59 26.81 o 8 2 0 262.28 308.41 19.80 o 9 2 0 293.52 250.22 23.57 o 10 2 0 20.00 18.15 22.10 o 11 2 0 49.61 55.29 25.39 o 1 3 0 298.37 117.90 7.00 o 2 3 0 5966.66 4071.43 23.66 o 3 3 0 64.31 92.73 8.58 o 4 3 0 546.59 551.12 11.20 o 5 3 0 1562.40 1680.68 18.07 o 6 3 0 191.62 173.97 16.13 o 7 3 0 374.73 479.51 17.88 o 8 3 0 112.30 105.20 19.71 o 9 3 0 537.35 669.92 26.83 o 10 3 0 58.05 51.03 21.70 o 11 3 0 78.11 46.92 23.14 o 0 4 0 3235.76 2386.19 22.38 o 1 4 0 37.22 104.84 4.99 o 2 4 0 8.67 -3.09 5.25 o 3 4 0 1352.07 1317.97 15.65 o 4 4 0 430.18 472.19 10.41 o 5 4 0 9629.50 9044.15 48.83 o 6 4 0 284.93 297.08 13.25 o 7 4 0 2808.31 3306.91 33.90 o 8 4 0 490.22 486.72 24.14 o 9 4 0 533.55 596.40 30.79 o 10 4 0 6.15 15.11 17.96 o 11 4 0 45.74 43.69 25.97 o 1 5 0 1308.51 791.73 7.87 o 2 5 0 96.83 130.29 7.41 o 3 5 0 427.24 267.78 8.67 o 4 5 0 888.33 741.48 13.95 o 5 5 0 387.03 437.50 11.80 o 6 5 0 1370.55 1399.42 24.01 o 7 5 0 143.95 146.03 14.93 o 8 5 0 52.62 32.24 16.71 o 9 5 0 3.22 3.69 18.62 o 10 5 0 5.49 12.84 17.64 o 11 5 0 70.11 63.50 58.26 o 0 6 0 35069.39 29319.01 179.68 o 1 6 0 2532.34 1757.66 19.74 o 2 6 0 2476.41 2297.86 16.24 o 3 6 0 3655.81 2927.78 21.28 o 4 6 0 474.06 508.89 12.32 o 5 6 0 3658.38 3394.58 26.94 o 6 6 0 79.34 61.68 13.44 o 7 6 0 4451.83 4600.20 44.63 o 8 6 0 58.42 58.66 13.35 o 9 6 0 120.93 163.43 21.11 o 10 6 0 895.10 998.34 37.85 o 11 6 0 75.02 118.62 31.79 o 1 7 0 772.46 978.02 12.77 o 2 7 0 1115.41 1034.56 10.59 o 3 7 0 0.05 12.00 6.58 o 4 7 0 340.41 260.85 10.22 o 5 7 0 95.56 172.79 14.80 o 6 7 0 0.07 6.99 7.44 o 7 7 0 142.76 135.88 17.06 o 8 7 0 583.05 652.50 24.18 o 9 7 0 329.97 426.91 25.11 o 10 7 0 22.84 7.88 18.91 o 11 7 0 0.59 10.18 27.88 o 0 8 0 16447.10 14017.06 105.17 o 1 8 0 202.05 338.68 15.40 o 2 8 0 2716.69 2505.81 23.08 o 3 8 0 948.97 747.12 11.31 o 4 8 0 847.88 723.07 13.18 o 5 8 0 4159.84 4176.53 44.37 o 6 8 0 17.75 22.46 8.04 o 7 8 0 1520.28 1557.63 25.63 o 8 8 0 193.72 205.12 17.89 o 9 8 0 152.65 183.49 20.37 o 10 8 0 13.45 15.87 16.43 o 11 8 0 5.42 12.19 27.38 o 1 9 0 17.14 18.29 7.16 o 2 9 0 93.53 80.10 8.12 o 3 9 0 34.20 31.49 7.09 o 4 9 0 323.19 230.47 12.96 o 5 9 0 1277.79 1200.68 26.42 o 6 9 0 7.59 0.18 7.47 o 7 9 0 63.63 62.60 10.91 o 8 9 0 381.54 485.16 22.11 o 9 9 0 286.71 404.82 38.93 o 10 9 0 2.19 -11.03 15.90 o 11 9 0 3.03 29.76 36.16 o 0 10 0 5866.35 4404.48 44.55 o 1 10 0 18.06 3.04 7.03 o 2 10 0 612.70 749.34 27.99 o 3 10 0 3994.73 3581.58 26.50 o 4 10 0 871.60 1096.81 14.18 o 5 10 0 740.27 647.29 17.01 o 6 10 0 164.98 187.62 14.47 o 7 10 0 207.21 159.20 16.01 o 8 10 0 18.27 8.48 13.67 o 9 10 0 163.54 155.99 24.09 o 10 10 0 250.88 195.85 29.54 o 11 10 0 13.77 2.68 42.02 o 1 11 0 264.22 207.04 12.00 o 2 11 0 0.23 9.83 10.28 o 3 11 0 57.66 80.53 7.47 o 4 11 0 0.39 15.70 6.58 o 5 11 0 218.43 226.70 16.96 o 6 11 0 2.84 8.95 7.95 o 7 11 0 0.01 7.96 12.15 o 8 11 0 2.89 3.12 11.55 o 9 11 0 0.68 -1.30 8.54 o 10 11 0 27.52 24.69 27.16 o 0 12 0 26799.26 24875.89 333.00 o 1 12 0 18230.54 17908.74 98.13 o 2 12 0 11891.14 11548.68 71.00 o 3 12 0 1030.85 1531.09 19.27 o 4 12 0 384.58 569.48 11.48 o 5 12 0 1865.39 2036.63 43.18 o 6 12 0 89.58 86.09 16.13 o 7 12 0 425.99 422.45 17.42 o 8 12 0 6.06 4.81 10.93 o 9 12 0 177.73 130.94 26.68 o 10 12 0 46.85 106.62 70.31 o 1 13 0 485.39 552.09 16.02 o 2 13 0 625.09 687.41 14.76 o 3 13 0 98.04 132.90 15.00 o 4 13 0 265.06 315.08 26.54 o 5 13 0 258.31 216.65 27.01 o 6 13 0 71.92 114.51 32.74 o 7 13 0 169.80 90.65 29.70 o 8 13 0 105.83 74.35 18.72 o 9 13 0 371.39 347.01 46.10 o 10 13 0 6.13 66.44 108.94 o 0 14 0 14375.81 14836.51 199.33 o 1 14 0 684.78 575.39 18.86 o 2 14 0 2799.81 2605.93 30.41 o 3 14 0 664.72 628.12 24.43 o 4 14 0 178.62 182.48 14.04 o 5 14 0 2518.56 2888.95 80.33 o 6 14 0 16.94 14.68 44.04 o 7 14 0 661.05 911.64 76.49 o 8 14 0 19.78 8.46 7.75 o 9 14 0 152.28 48.40 74.17 o 10 14 0 423.71 699.21 146.02 o 1 15 0 78.14 72.09 14.52 o 2 15 0 955.01 1168.41 23.39 o 3 15 0 249.66 276.52 17.82 o 4 15 0 18.86 16.38 9.83 o 5 15 0 193.02 250.84 40.38 o 6 15 0 16.89 16.40 15.37 o 7 15 0 122.84 83.83 20.67 o 8 15 0 44.76 32.14 11.86 o 9 15 0 1.96 3.86 87.31 o 10 15 0 9.94 -8.50 64.90 o 0 16 0 819.30 914.33 36.72 o 1 16 0 154.98 109.57 16.62 o 2 16 0 192.25 135.18 16.66 o 3 16 0 722.01 765.64 19.11 o 4 16 0 206.27 204.06 14.67 o 5 16 0 508.97 625.22 42.66 o 6 16 0 195.03 238.83 22.46 o 7 16 0 1336.83 1704.57 62.79 o 8 16 0 0.17 0.48 7.63 o 9 16 0 11.04 24.72 102.76 o 1 17 0 39.10 47.80 17.09 o 2 17 0 173.28 121.36 21.50 o 3 17 0 60.99 49.50 14.45 o 4 17 0 71.23 61.59 13.67 o 5 17 0 465.80 547.69 50.47 o 6 17 0 32.52 46.61 29.42 o 7 17 0 12.90 14.97 15.80 o 8 17 0 447.92 357.34 62.55 o 9 17 0 192.17 -2.32 93.49 o 0 18 0 2283.77 2575.71 75.35 o 1 18 0 121.73 103.37 15.66 o 2 18 0 18.91 14.23 13.45 o 3 18 0 39.39 43.65 11.25 o 4 18 0 18.01 7.28 9.62 o 5 18 0 1289.12 1443.44 114.13 o 6 18 0 87.05 91.74 27.04 o 7 18 0 126.30 108.34 29.21 o 8 18 0 440.44 407.94 145.25 o 9 18 0 412.51 3.86 67.99 o 1 19 0 75.17 75.48 15.08 o 2 19 0 382.60 337.40 17.70 o 3 19 0 123.69 118.63 15.35 o 4 19 0 34.61 45.76 10.38 o 5 19 0 38.73 60.42 34.58 o 6 19 0 938.17 1111.51 229.47 o 7 19 0 0.35 17.57 26.47 o 8 19 0 1.84 6.18 101.98 o 9 19 0 112.61 -0.77 58.72 o 0 20 0 775.68 816.46 45.02 o 1 20 0 89.62 136.67 18.35 o 2 20 0 1806.07 2334.33 33.33 o 3 20 0 11.73 23.39 13.61 o 4 20 0 92.14 117.98 14.79 o 5 20 0 11.17 23.66 24.60 o 6 20 0 7.14 25.36 22.83 o 7 20 0 1051.29 1065.03 285.87 o 8 20 0 35.92 -4.64 104.30 o 1 21 0 357.96 463.58 29.00 o 2 21 0 1195.31 1365.38 30.69 o 3 21 0 925.64 1209.86 25.00 o 4 21 0 335.85 401.64 15.49 o 5 21 0 225.10 75.63 152.59 o 6 21 0 917.52 974.29 211.31 o 7 21 0 56.44 29.89 25.47 o 8 21 0 186.14 -3.86 108.17 o 0 22 0 4061.12 5287.79 85.96 o 1 22 0 30.37 36.33 17.75 o 2 22 0 1472.18 1743.62 32.01 o 3 22 0 34.97 7.62 15.06 o 4 22 0 172.48 160.76 17.87 o 5 22 0 147.71 71.73 83.06 o 6 22 0 158.40 92.39 65.67 o 7 22 0 21.36 0.41 28.49 o 1 23 0 260.55 240.46 21.29 o 2 23 0 70.26 62.14 19.74 o 3 23 0 33.57 37.53 14.85 o 4 23 0 0.76 1.02 12.97 o 5 23 0 45.85 4.84 28.12 o 6 23 0 100.20 -3.68 37.87 o 7 23 0 0.42 2.32 64.90 o 0 24 0 2912.46 3524.52 73.86 o 1 24 0 242.10 145.96 29.80 o 2 24 0 103.94 139.32 23.20 o 3 24 0 6.21 21.90 16.84 o 4 24 0 181.19 137.93 47.62 o 5 24 0 767.40 849.18 222.13 o 6 24 0 1.91 1.30 40.65 o 1 25 0 280.25 282.91 29.34 o 2 25 0 198.90 228.77 26.51 o 3 25 0 96.21 61.98 27.10 o 4 25 0 0.11 -7.13 16.04 o 5 25 0 97.99 1.83 40.79 o 6 25 0 42.04 10.06 32.59 o 0 26 0 63.57 51.78 29.56 o 1 26 0 9.51 22.25 21.73 o 2 26 0 35.42 19.83 22.31 o 3 26 0 115.59 57.70 28.33 o 4 26 0 85.34 3.25 51.24 o 5 26 0 118.08 30.13 34.74 o 1 27 0 9.28 -4.89 19.50 o 2 27 0 163.99 116.21 44.94 o 3 27 0 21.75 -0.50 20.18 o 4 27 0 3.35 15.34 37.91 o 0 28 0 263.57 177.01 82.66 o 1 28 0 1.37 14.58 24.05 o 2 28 0 52.76 22.08 23.28 o 3 28 0 32.46 -1.76 39.84 o 1 29 0 16.20 21.14 25.92 o 2 29 0 11.29 20.00 27.56 o -11 1 1 390.30 468.51 29.15 o -10 1 1 16.96 24.54 18.63 o -9 1 1 1227.25 1414.79 37.47 o -8 1 1 872.47 1158.71 28.91 o -7 1 1 264.60 300.08 20.74 o -6 1 1 50.12 69.86 13.15 o -5 1 1 929.64 986.89 21.48 o -4 1 1 11121.52 8394.83 47.71 o -3 1 1 35573.65 30843.85 125.38 o -2 1 1 3662.69 2500.36 81.51 o 2 1 1 3451.16 3189.03 14.32 o 3 1 1 124.26 170.36 6.48 o 4 1 1 2635.71 1574.53 13.46 o 5 1 1 5445.02 4809.29 42.57 o 6 1 1 3550.24 3837.76 35.73 o 7 1 1 33.49 36.31 13.05 o 8 1 1 996.90 958.92 30.41 o 9 1 1 172.20 170.74 20.90 o 10 1 1 241.28 374.70 59.03 o 11 1 1 16.67 13.51 40.63 o -11 2 1 9.23 7.38 20.28 o -10 2 1 63.43 39.20 20.20 o -9 2 1 12.84 42.55 19.07 o -8 2 1 9.45 24.11 19.02 o -7 2 1 882.02 852.81 34.39 o -6 2 1 1123.04 1229.38 21.96 o -5 2 1 77.87 55.26 10.21 o -4 2 1 1020.52 898.76 15.22 o -3 2 1 2489.46 2285.35 21.70 o -2 2 1 1389.92 642.74 12.76 o 2 2 1 493.84 368.76 5.92 o 3 2 1 12475.80 11061.36 42.56 o 4 2 1 2747.79 2236.88 23.91 o 5 2 1 322.12 279.13 11.33 o 6 2 1 791.21 852.02 17.45 o 7 2 1 445.66 451.63 21.26 o 8 2 1 0.16 4.16 13.67 o 9 2 1 198.92 264.33 23.80 o 10 2 1 7.73 5.45 33.54 o 11 2 1 145.56 186.14 52.45 o -11 3 1 254.99 273.09 31.62 o -10 3 1 267.54 340.63 26.84 o -9 3 1 382.30 522.46 29.18 o -8 3 1 53.64 39.19 23.13 o -7 3 1 589.29 601.09 18.30 o -6 3 1 608.23 614.64 20.86 o -5 3 1 530.04 439.36 13.95 o -4 3 1 5436.46 4398.77 33.27 o -3 3 1 2094.25 2383.25 38.30 o -2 3 1 262.03 185.23 13.34 o -1 3 1 11120.01 8436.13 32.76 o 1 3 1 683.84 893.16 7.92 o 2 3 1 10092.09 8051.84 35.56 o 3 3 1 2147.05 2841.30 17.91 o 4 3 1 589.09 457.28 11.41 o 5 3 1 978.56 1186.45 14.59 o 6 3 1 2773.77 2814.35 25.57 o 7 3 1 1968.36 1920.36 26.71 o 8 3 1 971.42 1108.57 25.22 o 9 3 1 0.33 6.80 14.78 o 10 3 1 2.09 7.10 34.53 o 11 3 1 45.53 12.97 49.85 o -11 4 1 3.70 3.48 21.78 o -10 4 1 2.24 -7.83 19.83 o -9 4 1 542.77 536.56 26.49 o -8 4 1 176.97 245.45 22.44 o -7 4 1 19.40 53.65 15.82 o -6 4 1 5.08 10.33 10.83 o -5 4 1 35.80 30.33 9.24 o -4 4 1 235.12 319.57 12.72 o -3 4 1 5499.89 4185.67 35.76 o -2 4 1 6245.16 5057.48 37.14 o -1 4 1 7268.77 6234.31 38.95 o 0 4 1 1386.51 1299.62 8.76 o 1 4 1 21.47 15.21 4.21 o 2 4 1 454.70 496.75 11.46 o 3 4 1 5497.79 4488.55 22.73 o 4 4 1 13.39 6.29 5.73 o 5 4 1 1586.36 1512.57 16.52 o 6 4 1 1144.24 1159.97 18.83 o 7 4 1 124.25 147.15 14.86 o 8 4 1 74.70 103.62 14.75 o 9 4 1 170.63 202.72 18.76 o 10 4 1 0.19 18.14 41.85 o 11 4 1 9.03 -8.08 50.25 o -11 5 1 369.22 360.64 34.99 o -10 5 1 2.67 3.59 15.84 o -9 5 1 558.19 736.51 32.96 o -8 5 1 336.20 384.81 22.53 o -7 5 1 1764.27 1825.42 33.15 o -6 5 1 1029.17 1107.80 19.68 o -5 5 1 4074.12 4471.91 41.05 o -4 5 1 547.50 351.10 13.50 o -3 5 1 2017.10 1318.29 17.44 o -2 5 1 30525.78 28380.39 155.61 o -1 5 1 27504.88 25092.15 128.74 o 0 5 1 3298.41 2749.36 17.17 o 1 5 1 6052.79 5851.17 29.73 o 2 5 1 3580.57 3106.85 29.61 o 3 5 1 378.03 350.54 16.36 o 4 5 1 3062.45 2481.43 18.53 o 5 5 1 1509.91 1660.25 19.15 o 6 5 1 99.15 107.25 11.89 o 7 5 1 276.41 306.35 15.67 o 8 5 1 1399.31 1407.57 28.18 o 9 5 1 3.27 2.86 10.46 o 10 5 1 514.42 587.54 137.14 o 11 5 1 19.20 23.05 42.45 o -11 6 1 17.74 8.53 22.62 o -10 6 1 0.66 4.44 16.05 o -9 6 1 819.65 954.02 33.46 o -8 6 1 11.24 25.75 14.25 o -7 6 1 113.45 120.20 14.77 o -6 6 1 17.83 24.23 10.37 o -5 6 1 31.38 29.95 10.70 o -4 6 1 170.16 239.82 13.63 o -3 6 1 1818.85 1628.94 17.05 o -2 6 1 3767.94 3679.86 33.60 o -1 6 1 5138.97 4904.83 24.95 o 0 6 1 16142.13 11849.07 52.05 o 1 6 1 271.17 222.47 15.99 o 2 6 1 498.76 481.90 9.41 o 3 6 1 803.00 945.62 16.12 o 4 6 1 454.40 383.80 11.92 o 5 6 1 16.91 22.33 6.09 o 6 6 1 2077.06 2472.28 22.46 o 7 6 1 43.91 33.53 20.27 o 8 6 1 144.07 181.46 17.16 o 9 6 1 188.93 153.70 24.89 o 10 6 1 27.37 49.06 31.35 o 11 6 1 14.66 25.99 54.90 o -11 7 1 110.23 125.86 29.87 o -10 7 1 95.07 77.61 21.20 o -9 7 1 115.60 110.37 23.06 o -8 7 1 1.68 5.87 15.49 o -7 7 1 1649.97 1931.09 29.01 o -6 7 1 574.23 601.06 17.83 o -5 7 1 27.53 54.08 16.02 o -4 7 1 1964.36 1521.64 19.95 o -3 7 1 723.63 979.53 11.07 o -2 7 1 2703.61 2504.01 17.27 o -1 7 1 4501.58 3733.13 22.54 o 0 7 1 6991.61 5437.31 29.40 o 1 7 1 15211.50 13321.10 58.30 o 2 7 1 1378.27 1022.67 12.06 o 3 7 1 83.74 123.42 8.89 o 4 7 1 1946.34 1612.77 20.30 o 5 7 1 3.11 18.71 7.14 o 6 7 1 1579.80 1774.11 35.24 o 7 7 1 2100.48 2173.57 38.09 o 8 7 1 612.03 679.10 41.03 o 9 7 1 13.57 21.07 14.72 o 10 7 1 112.73 130.05 34.55 o 11 7 1 96.64 85.72 48.93 o -11 8 1 0.00 0.15 23.41 o -10 8 1 50.53 42.02 18.01 o -9 8 1 136.88 177.87 17.45 o -8 8 1 376.10 495.93 27.36 o -7 8 1 3.82 -0.29 14.23 o -6 8 1 53.37 46.67 17.62 o -5 8 1 496.94 381.63 16.38 o -4 8 1 249.39 272.20 9.63 o -3 8 1 3779.86 3656.68 42.27 o -2 8 1 4498.68 4476.33 31.00 o -1 8 1 2412.52 2494.97 19.60 o 0 8 1 6509.03 5290.74 33.64 o 1 8 1 5.96 4.21 5.69 o 2 8 1 1008.92 711.82 11.61 o 3 8 1 622.61 500.10 12.58 o 4 8 1 3.11 6.90 8.01 o 5 8 1 293.92 277.43 14.61 o 6 8 1 2122.08 2238.12 47.20 o 7 8 1 186.20 192.87 11.65 o 8 8 1 42.83 21.79 19.45 o 9 8 1 28.52 52.62 38.92 o 10 8 1 1.30 -3.23 28.87 o 11 8 1 17.79 80.61 79.58 o -11 9 1 162.75 121.22 72.82 o -10 9 1 53.45 67.89 19.53 o -9 9 1 630.91 786.25 42.70 o -8 9 1 342.33 433.91 24.66 o -7 9 1 200.93 191.71 16.18 o -6 9 1 1720.19 1739.86 31.96 o -5 9 1 370.05 386.24 25.22 o -4 9 1 2116.70 2141.37 35.77 o -3 9 1 1.64 48.26 18.05 o -2 9 1 655.63 434.86 11.47 o -1 9 1 7531.90 6111.59 33.30 o 0 9 1 25026.44 23829.08 121.95 o 1 9 1 16657.17 16196.08 81.22 o 2 9 1 5617.99 5894.34 32.46 o 3 9 1 2549.98 1759.35 19.24 o 4 9 1 610.87 560.65 16.69 o 5 9 1 2656.07 2874.40 40.46 o 6 9 1 2633.91 2749.36 43.69 o 7 9 1 131.41 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