#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/77/2227755.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227755_Fobs loop_ _publ_author_name 'bin Shawkataly, Omar' 'Khan, Imthyaz Ahmed' 'Sirat, Siti Syaida' 'Yeap, Chin Sing' 'Fun, Hoong-Kun' _publ_section_title ; Undecacarbonyl-1\k^3^C,2\k^4^C,3\k^4^C-{tris[4-(methylsulfanyl)phenyl]arsine-1\kAs}-triangulo-triruthenium(0) ; _journal_coeditor_code LH5089 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1047 _journal_page_last m1048 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 118.221 _cell_angle_gamma 90.000 _cell_length_a 14.3855 _cell_length_b 15.1185 _cell_length_c 19.0966 _exptl_crystal_F_000 2056.00 _reflns_d_resolution_high 0.6151 _[local]_cod_data_source_file lh5089Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' iak15m in P2(1)/c (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 461.96 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 111610.05 126520.66 2114.46 o 3 0 0 31542.97 36416.63 629.93 o 4 0 0 5186.00 6095.67 203.48 o 5 0 0 15180.60 14598.14 413.98 o 6 0 0 82627.07 92548.96 2227.33 o 7 0 0 54479.59 54486.06 1369.88 o 8 0 0 125508.42 130444.18 3133.75 o 9 0 0 320.85 623.37 105.98 o 10 0 0 17952.54 18712.44 415.74 o 11 0 0 1582.62 1644.92 101.94 o 12 0 0 7892.60 7756.08 346.57 o 13 0 0 5816.05 6282.74 223.33 o 14 0 0 3180.85 3202.59 166.84 o 15 0 0 21772.18 22308.79 755.05 o 16 0 0 16570.29 17458.54 657.58 o 17 0 0 1056.26 976.96 171.02 o 1 1 0 117183.65 131779.31 3133.02 o 2 1 0 25686.20 29782.24 323.09 o 3 1 0 10818.70 11636.50 158.50 o 4 1 0 273.22 259.16 21.63 o 5 1 0 1858.71 1833.20 71.97 o 6 1 0 26916.70 26738.44 377.88 o 7 1 0 58661.50 61932.39 834.05 o 8 1 0 2642.14 2387.97 54.74 o 9 1 0 42585.11 44196.07 554.77 o 10 1 0 655.21 598.86 29.49 o 11 1 0 6537.62 6986.55 107.88 o 12 1 0 343.34 385.08 82.35 o 13 1 0 207.81 204.29 53.06 o 14 1 0 4139.93 4408.74 475.25 o 15 1 0 2038.38 2309.57 152.29 o 16 1 0 6236.26 6323.92 251.62 o 17 1 0 2309.64 2557.95 248.62 o 0 2 0 2932.33 3164.09 117.04 o 1 2 0 2068.53 2620.49 37.11 o 2 2 0 10806.77 11704.10 127.46 o 3 2 0 58334.11 67946.73 727.24 o 4 2 0 4156.05 4462.83 78.90 o 5 2 0 8470.13 9018.65 138.75 o 6 2 0 31979.29 34693.21 382.33 o 7 2 0 3548.29 3483.44 64.14 o 8 2 0 3809.00 4054.29 126.89 o 9 2 0 5913.87 5595.19 94.58 o 10 2 0 10332.30 10460.98 178.67 o 11 2 0 4391.40 4647.45 90.73 o 12 2 0 11.47 29.98 22.56 o 13 2 0 2541.73 2499.07 101.52 o 14 2 0 1368.09 1531.37 122.19 o 15 2 0 189.45 226.15 111.80 o 16 2 0 446.57 518.14 60.20 o 17 2 0 1371.99 1284.32 154.99 o 18 2 0 4044.57 4131.75 143.96 o 1 3 0 11613.05 13698.35 177.82 o 2 3 0 937.45 1167.75 48.95 o 3 3 0 15184.87 17012.90 200.59 o 4 3 0 5098.80 5518.54 81.40 o 5 3 0 2907.54 2472.75 47.77 o 6 3 0 12939.71 13484.12 168.46 o 7 3 0 3733.31 3851.67 62.11 o 8 3 0 2318.35 2451.97 65.91 o 9 3 0 3601.34 3446.46 56.82 o 10 3 0 658.58 653.05 21.12 o 11 3 0 79.62 73.43 15.08 o 12 3 0 7057.44 6935.45 117.78 o 13 3 0 2747.11 2800.19 71.67 o 14 3 0 2022.17 2078.34 61.88 o 15 3 0 4875.37 5003.61 132.36 o 16 3 0 180.89 109.53 49.61 o 17 3 0 159.51 203.76 52.17 o 18 3 0 10.73 57.24 50.84 o 19 3 0 292.05 267.60 68.01 o 20 3 0 294.16 260.47 72.11 o 0 4 0 3117.83 3787.63 96.24 o 1 4 0 3540.75 3830.80 113.66 o 2 4 0 62.31 99.73 27.29 o 3 4 0 9909.52 10640.07 121.37 o 4 4 0 1532.97 1403.92 31.43 o 5 4 0 1532.53 1641.76 41.85 o 6 4 0 658.97 831.89 25.85 o 7 4 0 5553.04 5245.98 65.66 o 8 4 0 7428.96 7507.44 100.07 o 9 4 0 3223.32 3223.57 52.32 o 10 4 0 37.04 66.12 15.94 o 11 4 0 2005.77 2100.21 47.82 o 12 4 0 206.89 202.22 27.61 o 13 4 0 16.27 24.17 25.41 o 14 4 0 120.37 55.46 27.72 o 15 4 0 932.83 962.27 65.40 o 16 4 0 107.65 83.96 46.75 o 17 4 0 169.10 239.81 66.26 o 18 4 0 78.88 59.92 55.81 o 19 4 0 505.34 608.89 104.51 o 20 4 0 328.96 488.55 84.97 o 1 5 0 7646.97 7958.22 101.64 o 2 5 0 6039.23 6552.95 129.48 o 3 5 0 56001.96 59604.89 1025.05 o 4 5 0 7678.25 7690.91 95.61 o 5 5 0 9693.06 10436.23 102.70 o 6 5 0 11455.30 12464.67 129.02 o 7 5 0 822.25 989.03 28.76 o 8 5 0 583.30 536.64 21.60 o 9 5 0 7361.97 7621.31 101.27 o 10 5 0 4984.79 5159.17 112.55 o 11 5 0 5401.24 5186.75 81.09 o 12 5 0 1401.39 1363.23 42.83 o 13 5 0 8672.21 8753.33 128.17 o 14 5 0 435.77 524.65 34.81 o 15 5 0 432.55 321.01 39.67 o 16 5 0 2100.67 2013.54 86.62 o 17 5 0 1398.44 1451.86 124.76 o 18 5 0 751.85 811.87 57.73 o 19 5 0 5.34 44.28 60.61 o 20 5 0 291.87 183.55 82.14 o 0 6 0 4029.00 3998.72 81.63 o 1 6 0 22162.56 22129.97 227.39 o 2 6 0 18343.45 18704.31 195.72 o 3 6 0 2039.22 2128.25 82.27 o 4 6 0 1267.91 1285.54 37.17 o 5 6 0 6365.94 6842.48 83.65 o 6 6 0 12302.22 12333.98 122.55 o 7 6 0 7260.57 7553.95 84.12 o 8 6 0 916.12 899.85 24.21 o 9 6 0 15017.39 15069.11 175.34 o 10 6 0 2873.61 2966.71 60.93 o 11 6 0 1669.72 1630.40 51.33 o 12 6 0 862.21 847.46 38.80 o 13 6 0 165.51 157.63 28.27 o 14 6 0 748.16 728.30 42.51 o 15 6 0 178.34 123.40 31.58 o 16 6 0 159.38 127.74 44.24 o 17 6 0 821.72 897.91 83.79 o 18 6 0 689.12 657.95 80.42 o 19 6 0 7.55 -43.58 43.58 o 1 7 0 79.59 41.35 13.20 o 2 7 0 5949.54 5926.11 72.36 o 3 7 0 74.24 67.01 9.52 o 4 7 0 11886.99 11901.00 137.81 o 5 7 0 1971.27 1895.19 49.08 o 6 7 0 3945.97 3679.75 59.91 o 7 7 0 6363.72 6671.85 88.31 o 8 7 0 51.89 48.60 24.79 o 9 7 0 611.78 553.75 26.40 o 10 7 0 2098.29 2005.34 46.59 o 11 7 0 981.31 1068.89 51.78 o 12 7 0 5036.25 5152.12 98.01 o 13 7 0 1620.47 1567.75 61.84 o 14 7 0 534.05 490.48 41.81 o 15 7 0 571.12 549.83 44.91 o 16 7 0 215.40 168.40 47.92 o 17 7 0 281.94 158.54 50.19 o 18 7 0 164.77 31.52 48.17 o 19 7 0 664.17 587.09 149.18 o 0 8 0 18221.67 20098.82 305.69 o 1 8 0 7500.87 7551.45 91.38 o 2 8 0 8035.52 8092.11 88.37 o 3 8 0 19130.18 19265.59 167.03 o 4 8 0 768.33 863.64 32.46 o 5 8 0 6143.69 5766.23 86.13 o 6 8 0 1861.28 1786.78 52.14 o 7 8 0 925.28 1047.98 39.13 o 8 8 0 3572.02 3855.90 74.62 o 9 8 0 504.05 482.21 31.78 o 10 8 0 4680.18 4605.35 102.21 o 11 8 0 5863.26 5993.41 123.21 o 12 8 0 30.08 9.76 22.77 o 13 8 0 1487.17 1412.31 52.82 o 14 8 0 19.40 -7.52 25.65 o 15 8 0 825.68 653.37 44.05 o 16 8 0 855.10 740.09 68.31 o 17 8 0 738.87 790.96 71.97 o 18 8 0 1287.30 1322.12 97.18 o 19 8 0 932.58 1110.66 83.94 o 1 9 0 6363.57 6897.16 88.58 o 2 9 0 17.57 29.08 12.18 o 3 9 0 3437.03 3301.20 43.14 o 4 9 0 8428.55 8031.40 91.43 o 5 9 0 4218.80 4300.64 68.27 o 6 9 0 497.64 496.59 30.37 o 7 9 0 1491.77 1517.82 60.09 o 8 9 0 6.46 -3.68 20.24 o 9 9 0 39.48 54.83 23.63 o 10 9 0 766.17 757.90 55.34 o 11 9 0 340.45 327.18 35.67 o 12 9 0 1797.01 1709.23 123.52 o 13 9 0 1027.36 1061.96 58.02 o 14 9 0 799.75 749.27 57.77 o 15 9 0 568.57 500.18 95.90 o 16 9 0 322.30 362.96 96.46 o 17 9 0 141.31 95.45 59.01 o 18 9 0 103.74 -0.31 56.76 o 19 9 0 12.72 -46.29 85.26 o 0 10 0 84.22 64.02 25.96 o 1 10 0 369.91 410.50 22.35 o 2 10 0 6789.88 6881.17 94.86 o 3 10 0 19208.83 19317.30 175.79 o 4 10 0 1047.43 1028.79 36.37 o 5 10 0 9252.98 9584.61 119.85 o 6 10 0 113.56 142.35 26.51 o 7 10 0 456.57 397.45 36.39 o 8 10 0 216.98 180.34 29.73 o 9 10 0 15.04 -27.75 27.75 o 10 10 0 7722.25 7719.74 150.05 o 11 10 0 3310.57 3153.19 94.79 o 12 10 0 1382.22 1440.86 130.23 o 13 10 0 1188.84 1129.64 62.97 o 14 10 0 122.00 118.59 43.50 o 15 10 0 114.17 107.37 56.39 o 16 10 0 58.38 51.45 58.95 o 17 10 0 466.27 432.66 77.26 o 18 10 0 1145.82 1283.26 99.72 o 1 11 0 6362.46 6640.16 81.64 o 2 11 0 1993.55 2129.04 45.03 o 3 11 0 10114.55 10063.46 106.50 o 4 11 0 49174.89 49820.05 427.42 o 5 11 0 2774.13 2864.55 61.51 o 6 11 0 4094.53 4087.92 81.52 o 7 11 0 212.83 287.55 34.34 o 8 11 0 5229.99 5446.33 109.74 o 9 11 0 1948.17 1829.84 75.36 o 10 11 0 406.10 493.41 65.68 o 11 11 0 8558.48 8720.44 167.92 o 12 11 0 9086.36 9443.17 180.46 o 13 11 0 55.79 63.20 41.39 o 14 11 0 494.04 467.37 57.12 o 15 11 0 1611.00 1760.84 107.72 o 16 11 0 2079.30 2016.97 119.73 o 17 11 0 1067.43 1206.00 125.22 o 18 11 0 8.33 35.64 68.44 o 0 12 0 5998.69 5895.59 117.41 o 1 12 0 4343.60 4352.54 65.42 o 2 12 0 13777.67 13811.21 139.36 o 3 12 0 50570.34 50730.02 411.31 o 4 12 0 1834.36 1794.96 46.31 o 5 12 0 32405.98 32556.08 322.26 o 6 12 0 70.64 68.85 25.99 o 7 12 0 4893.43 5001.60 95.83 o 8 12 0 2161.40 2303.23 97.67 o 9 12 0 156.89 166.47 40.49 o 10 12 0 10869.62 10452.02 192.23 o 11 12 0 12938.75 13021.19 225.75 o 12 12 0 3847.96 3703.20 123.33 o 13 12 0 7839.87 7885.31 183.71 o 14 12 0 1149.19 980.04 80.73 o 15 12 0 2645.49 2645.52 135.33 o 16 12 0 78.12 68.92 67.05 o 17 12 0 180.89 220.28 134.67 o 1 13 0 6210.13 6316.95 98.98 o 2 13 0 24936.52 24892.99 225.77 o 3 13 0 8.63 36.68 17.54 o 4 13 0 9323.08 9422.21 117.02 o 5 13 0 1960.11 1975.59 57.39 o 6 13 0 10915.44 10913.79 158.28 o 7 13 0 1682.68 1704.15 67.88 o 8 13 0 1074.74 789.84 58.34 o 9 13 0 3819.65 3503.53 108.81 o 10 13 0 6174.47 6173.98 146.02 o 11 13 0 1184.87 1227.21 105.29 o 12 13 0 2571.91 2769.56 114.37 o 13 13 0 5616.28 5834.24 162.45 o 14 13 0 5175.93 5642.31 243.41 o 15 13 0 41.90 46.15 67.53 o 16 13 0 76.53 -19.26 69.69 o 17 13 0 995.13 916.40 107.78 o 0 14 0 11789.93 11168.99 218.32 o 1 14 0 10588.17 10631.88 149.06 o 2 14 0 508.22 574.83 33.45 o 3 14 0 5834.89 5724.80 79.34 o 4 14 0 91.41 127.72 23.44 o 5 14 0 8513.93 8588.81 126.84 o 6 14 0 327.55 258.43 37.50 o 7 14 0 11094.90 11316.95 185.17 o 8 14 0 6526.84 6634.36 164.13 o 9 14 0 4162.11 4004.00 120.75 o 10 14 0 227.01 287.30 79.54 o 11 14 0 1010.47 973.27 77.68 o 12 14 0 988.08 991.10 79.99 o 13 14 0 2181.62 2262.36 168.90 o 14 14 0 78.97 64.93 70.26 o 15 14 0 1272.12 1334.10 113.85 o 16 14 0 584.41 601.10 95.98 o 1 15 0 32.34 51.80 27.11 o 2 15 0 551.56 565.50 35.57 o 3 15 0 176.98 148.36 30.19 o 4 15 0 152.35 68.60 24.91 o 5 15 0 54.41 34.70 28.19 o 6 15 0 547.72 467.02 55.21 o 7 15 0 364.98 343.26 47.71 o 8 15 0 2.66 -36.70 36.70 o 9 15 0 279.14 197.04 56.61 o 10 15 0 1.50 -36.60 46.59 o 11 15 0 15.86 -50.39 50.39 o 12 15 0 124.14 49.26 57.38 o 13 15 0 36.66 -20.34 68.71 o 14 15 0 29.22 63.60 75.10 o 15 15 0 171.49 166.32 85.65 o 16 15 0 13.33 96.54 84.95 o 0 16 0 408.35 259.82 50.98 o 1 16 0 1938.80 1861.15 63.04 o 2 16 0 522.47 461.08 37.83 o 3 16 0 36.68 25.96 28.64 o 4 16 0 296.17 268.30 38.63 o 5 16 0 9.21 11.54 31.92 o 6 16 0 670.16 649.80 49.81 o 7 16 0 1976.78 1946.56 82.15 o 8 16 0 964.43 1017.40 72.60 o 9 16 0 324.33 165.29 67.55 o 10 16 0 412.54 516.73 96.45 o 11 16 0 458.63 446.55 71.41 o 12 16 0 430.08 365.68 87.76 o 13 16 0 107.43 151.90 82.32 o 14 16 0 259.87 264.62 116.58 o 15 16 0 181.60 87.12 87.64 o 1 17 0 157.41 146.13 33.19 o 2 17 0 2430.62 2337.79 68.93 o 3 17 0 66.82 38.84 34.39 o 4 17 0 904.62 944.81 70.61 o 5 17 0 3457.02 3516.42 130.25 o 6 17 0 2602.67 2707.03 93.39 o 7 17 0 158.97 156.87 51.23 o 8 17 0 64.80 -44.84 44.84 o 9 17 0 23.07 -58.82 58.82 o 10 17 0 1827.56 1920.82 110.89 o 11 17 0 0.28 -45.70 72.84 o 12 17 0 38.19 -32.03 77.36 o 13 17 0 1466.16 1479.12 128.68 o 14 17 0 968.69 1078.43 155.20 o 0 18 0 2073.94 1774.02 93.11 o 1 18 0 44.73 84.47 33.68 o 2 18 0 13.54 -39.29 39.29 o 3 18 0 601.16 538.40 54.21 o 4 18 0 80.77 81.88 53.96 o 5 18 0 48.07 -60.51 61.18 o 6 18 0 257.42 100.64 121.10 o 7 18 0 307.50 333.56 110.02 o 8 18 0 753.32 695.33 158.50 o 9 18 0 19.01 -9.34 61.72 o 10 18 0 3.43 -78.39 78.39 o 11 18 0 208.09 433.99 200.02 o 12 18 0 396.80 403.76 166.41 o 13 18 0 381.40 219.25 93.65 o 14 18 0 92.16 115.33 105.86 o 1 19 0 1989.19 1980.60 70.67 o 2 19 0 160.87 128.32 45.79 o 3 19 0 243.51 309.38 106.39 o 4 19 0 4526.65 4226.38 181.34 o 5 19 0 323.71 332.12 90.75 o 6 19 0 281.15 250.59 65.89 o 7 19 0 2658.69 2658.57 193.02 o 8 19 0 65.15 -19.46 77.44 o 9 19 0 859.25 780.28 89.56 o 10 19 0 272.00 182.45 73.86 o 11 19 0 434.62 421.29 171.89 o 12 19 0 1194.11 1054.44 138.95 o 13 19 0 207.61 258.72 101.16 o 0 20 0 3812.91 3989.58 157.76 o 1 20 0 362.68 373.72 50.96 o 2 20 0 536.85 423.57 62.55 o 3 20 0 605.31 764.22 70.51 o 4 20 0 4.64 -30.99 69.99 o 5 20 0 180.84 156.23 79.30 o 6 20 0 732.92 688.22 98.52 o 7 20 0 186.80 114.25 108.03 o 8 20 0 1698.68 1805.90 141.32 o 9 20 0 8.47 18.99 85.13 o 10 20 0 10.86 -24.83 85.07 o 11 20 0 242.56 227.43 101.67 o 1 21 0 119.27 114.59 57.49 o 2 21 0 234.45 265.95 62.01 o 3 21 0 273.29 239.25 80.47 o 4 21 0 16.37 -63.58 72.17 o 5 21 0 430.75 340.14 92.66 o 6 21 0 336.27 350.41 91.97 o 7 21 0 24.15 -18.90 91.28 o 8 21 0 3.26 -81.74 81.74 o 9 21 0 11.05 -82.71 86.40 o 10 21 0 406.28 329.82 110.12 o 0 22 0 2942.95 2832.82 207.61 o 1 22 0 1060.35 1127.74 166.19 o 2 22 0 4.01 11.13 56.10 o 3 22 0 5.23 28.21 75.69 o 4 22 0 478.02 404.38 93.67 o 5 22 0 78.91 128.21 84.98 o 6 22 0 27.21 -73.88 73.88 o 7 22 0 728.87 649.40 110.85 o 8 22 0 1663.85 1971.09 201.46 o 9 22 0 58.70 98.40 136.32 o 1 23 0 2604.88 2871.81 121.21 o 2 23 0 885.00 712.16 101.45 o 3 23 0 549.88 597.39 178.61 o 4 23 0 591.08 645.11 115.48 o 5 23 0 8.39 -31.87 81.49 o 6 23 0 1227.47 981.75 128.11 o 7 23 0 1768.94 1976.21 149.81 o 0 24 0 1745.38 1971.09 180.95 o 1 24 0 131.00 132.58 76.30 o 2 24 0 3224.00 3686.74 172.62 o 3 24 0 910.53 924.66 110.67 o 4 24 0 5.24 -83.49 101.18 o -17 1 1 528.55 623.52 153.18 o -16 1 1 2519.99 2561.78 449.65 o -15 1 1 2366.21 2549.41 127.35 o -14 1 1 5571.91 5940.10 182.27 o -13 1 1 336.40 403.11 107.16 o -12 1 1 1317.28 1448.93 109.43 o -11 1 1 1450.73 1490.42 60.18 o -10 1 1 17985.40 18749.56 240.14 o -9 1 1 189.50 315.46 20.83 o -8 1 1 13188.74 13718.20 176.63 o -7 1 1 6307.00 5558.53 85.20 o -6 1 1 17002.18 18024.53 293.04 o -5 1 1 1411.30 1376.04 48.35 o -4 1 1 5754.26 6727.03 105.72 o -3 1 1 22548.55 24784.27 278.54 o -2 1 1 29709.63 33351.65 334.15 o 0 1 1 19796.92 22615.52 280.96 o 1 1 1 51330.05 59208.72 709.83 o 2 1 1 28748.07 33917.77 366.84 o 3 1 1 12724.91 14847.79 174.59 o 4 1 1 26188.78 31732.63 397.13 o 5 1 1 85775.29 93361.26 1576.92 o 6 1 1 6901.58 7704.26 187.80 o 7 1 1 20408.22 21171.29 311.64 o 8 1 1 556.71 625.25 31.04 o 9 1 1 5274.44 5536.74 102.74 o 10 1 1 8665.27 9457.44 146.87 o 11 1 1 786.90 809.29 40.81 o 12 1 1 3885.58 3813.61 88.71 o 13 1 1 17223.73 17278.47 370.45 o 14 1 1 978.34 1185.54 91.77 o 15 1 1 98.49 163.76 74.71 o 16 1 1 169.95 128.32 78.21 o 17 1 1 52.68 25.92 76.21 o 18 1 1 8.20 -42.18 117.50 o -18 2 1 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