#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/77/2227758.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227758_Fobs loop_ _publ_author_name 'Hu, Xiaoqin' _publ_section_title ; catena-Poly[[[dipyridinecopper(II)]-\m-2,3,5,6-tetramethylbenzene-1,4-dicarboxylato] monohydrate] ; _journal_coeditor_code LH5099 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1301 _journal_volume 66 _journal_year 2010 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 108.481 _cell_angle_gamma 90.000 _cell_length_a 13.3280 _cell_length_b 17.1434 _cell_length_c 10.7390 _exptl_crystal_F_000 956.00 _reflns_d_resolution_high 0.7704 _[local]_cod_data_source_file lh5099Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' test in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 366.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 340.64 380.78 9.01 o 4 0 0 280.05 232.27 6.16 o 6 0 0 16262.62 17357.39 181.71 o 8 0 0 9428.07 9004.31 98.32 o 10 0 0 4042.37 3950.11 60.08 o 12 0 0 1322.33 1591.35 47.91 o 14 0 0 622.25 619.20 31.75 o 16 0 0 1003.72 1027.11 44.34 o 3 1 0 1814.80 1836.17 18.50 o 5 1 0 68.81 215.56 4.13 o 7 1 0 8458.79 8559.22 65.75 o 9 1 0 3288.42 3300.10 35.93 o 11 1 0 3167.91 3133.56 51.92 o 13 1 0 487.27 526.63 27.77 o 15 1 0 658.88 661.51 23.68 o 0 2 0 365.69 423.61 10.74 o 2 2 0 9347.55 9500.26 121.13 o 4 2 0 497.02 741.64 8.46 o 6 2 0 738.43 581.10 9.25 o 8 2 0 2865.35 2595.57 25.41 o 10 2 0 1212.71 1211.76 20.94 o 12 2 0 2053.37 1942.00 45.89 o 14 2 0 569.68 568.61 48.90 o 16 2 0 331.06 352.21 31.87 o 1 3 0 11747.49 11987.97 170.82 o 3 3 0 4506.70 4703.58 51.31 o 5 3 0 18238.41 18816.31 173.41 o 7 3 0 1883.60 1784.62 18.52 o 9 3 0 3755.65 3832.18 47.31 o 11 3 0 780.05 810.09 17.44 o 13 3 0 1393.53 1395.26 32.28 o 15 3 0 707.59 744.57 25.29 o 0 4 0 11604.50 12579.20 233.80 o 2 4 0 58540.17 56225.91 778.47 o 4 4 0 25197.95 25304.75 262.31 o 6 4 0 15306.28 15909.39 131.05 o 8 4 0 3886.01 4042.08 37.55 o 10 4 0 2071.60 2021.26 37.11 o 12 4 0 789.47 817.26 31.40 o 14 4 0 1509.42 1493.94 36.20 o 16 4 0 159.68 177.92 15.14 o 1 5 0 393.14 465.64 15.38 o 3 5 0 26264.93 26234.84 236.74 o 5 5 0 18324.39 18653.30 543.35 o 7 5 0 4478.24 4411.18 40.40 o 9 5 0 1311.98 1212.22 20.50 o 11 5 0 1474.85 1485.03 31.43 o 13 5 0 1625.47 1559.74 35.39 o 15 5 0 236.71 268.04 24.71 o 0 6 0 2690.59 3609.54 74.59 o 2 6 0 21.98 71.37 4.05 o 4 6 0 42857.14 44224.84 457.11 o 6 6 0 1877.55 1566.24 19.15 o 8 6 0 642.20 740.61 12.79 o 10 6 0 4513.85 4407.98 68.51 o 12 6 0 411.41 387.41 16.29 o 14 6 0 258.39 225.87 17.03 o 1 7 0 1090.14 894.53 18.25 o 3 7 0 16304.76 15837.57 145.67 o 5 7 0 3187.47 2981.42 42.03 o 7 7 0 6806.53 6676.16 59.36 o 9 7 0 2886.54 2858.06 39.16 o 11 7 0 517.66 578.21 19.39 o 13 7 0 505.62 502.87 31.52 o 15 7 0 273.57 278.21 16.51 o 0 8 0 5427.89 5336.56 108.99 o 2 8 0 8571.65 9213.76 87.38 o 4 8 0 4631.53 4580.44 46.82 o 6 8 0 2551.93 2476.77 98.70 o 8 8 0 9626.33 9521.14 93.03 o 10 8 0 305.03 336.17 14.65 o 12 8 0 1134.75 1125.76 29.06 o 14 8 0 299.16 348.00 17.55 o 1 9 0 7519.03 7399.36 104.66 o 3 9 0 2908.63 3035.56 33.22 o 5 9 0 5143.69 5300.02 54.23 o 7 9 0 1352.73 1326.08 18.91 o 9 9 0 3038.54 3206.16 48.34 o 11 9 0 2233.09 2250.68 43.71 o 13 9 0 151.97 167.01 13.26 o 15 9 0 439.01 431.51 20.26 o 0 10 0 13428.47 12871.42 248.70 o 2 10 0 6141.42 5750.94 84.87 o 4 10 0 800.69 726.59 12.83 o 6 10 0 5973.93 5845.59 60.11 o 8 10 0 618.74 579.54 14.57 o 10 10 0 1926.62 1915.43 39.05 o 12 10 0 1266.74 1225.50 31.19 o 14 10 0 332.36 343.91 17.79 o 1 11 0 8811.44 8661.42 123.36 o 3 11 0 2260.00 2150.19 30.82 o 5 11 0 3098.31 3104.20 35.91 o 7 11 0 1870.71 1777.99 63.18 o 9 11 0 526.93 515.18 14.77 o 11 11 0 1216.24 1135.93 29.61 o 13 11 0 711.62 718.60 25.26 o 0 12 0 10203.06 10097.79 202.17 o 2 12 0 1717.59 1831.10 36.12 o 4 12 0 1273.59 1377.27 23.65 o 6 12 0 3504.61 3424.07 49.09 o 8 12 0 146.45 207.44 11.80 o 10 12 0 705.46 713.59 23.22 o 12 12 0 741.62 752.21 25.06 o 1 13 0 2276.30 2202.66 42.37 o 3 13 0 3842.16 3769.14 63.27 o 5 13 0 1704.67 1806.25 29.51 o 7 13 0 618.84 663.91 16.91 o 9 13 0 611.81 632.46 34.58 o 11 13 0 632.53 592.12 43.76 o 13 13 0 1399.91 1391.77 48.49 o 0 14 0 1442.52 1274.77 43.18 o 2 14 0 5013.69 4834.95 95.19 o 4 14 0 3822.30 3631.80 63.10 o 6 14 0 449.43 534.92 15.46 o 8 14 0 1925.69 1790.17 46.59 o 10 14 0 451.93 448.11 23.44 o 12 14 0 1149.21 1229.62 45.72 o 1 15 0 5134.66 5181.08 84.25 o 3 15 0 535.74 551.09 24.71 o 5 15 0 1563.12 1510.23 35.67 o 7 15 0 1960.52 1917.43 32.91 o 9 15 0 916.58 968.39 27.84 o 11 15 0 450.38 455.90 21.23 o 0 16 0 2624.71 2582.32 72.05 o 2 16 0 805.65 822.98 37.81 o 4 16 0 535.12 585.28 22.30 o 6 16 0 458.51 504.07 21.26 o 8 16 0 1311.64 1312.97 32.86 o 10 16 0 1125.60 1154.95 32.12 o 1 17 0 946.84 914.39 33.08 o 3 17 0 1076.77 1148.74 32.41 o 5 17 0 127.52 148.29 33.66 o 7 17 0 1323.08 1429.66 65.00 o 9 17 0 1102.86 1030.00 45.95 o 0 18 0 1021.72 1002.86 42.95 o 2 18 0 1678.68 1635.43 50.92 o 4 18 0 903.40 879.93 29.09 o 6 18 0 908.94 931.83 30.46 o 8 18 0 1415.05 1503.60 57.27 o 1 19 0 784.46 769.20 28.29 o 3 19 0 1223.06 1185.18 34.74 o 5 19 0 833.72 861.50 30.28 o 7 19 0 971.74 1037.04 47.11 o 0 20 0 124.83 124.81 21.24 o 2 20 0 423.95 464.17 40.12 o 4 20 0 468.36 412.22 22.57 o 6 20 0 1048.42 982.30 33.92 o 1 21 0 56.02 31.87 13.06 o 3 21 0 752.81 786.38 43.07 o 5 21 0 1543.60 1611.55 63.96 o -15 1 1 51.25 48.86 12.58 o -13 1 1 0.09 0.46 6.19 o -11 1 1 240.21 228.53 8.12 o -9 1 1 698.97 783.60 15.09 o -7 1 1 292.83 403.95 6.15 o -5 1 1 914.14 1048.24 12.01 o -3 1 1 7734.89 8327.45 78.48 o -1 1 1 2703.89 3026.06 41.43 o 1 1 1 3677.85 4116.44 55.68 o 3 1 1 11217.35 10843.63 369.51 o 5 1 1 384.53 566.79 6.84 o 7 1 1 38.22 58.06 2.83 o 9 1 1 229.60 201.85 6.73 o 11 1 1 532.76 496.93 57.96 o 13 1 1 126.81 110.86 11.26 o 15 1 1 37.58 49.34 10.67 o -16 2 1 2.54 -7.54 7.54 o -14 2 1 24.28 15.69 7.67 o -12 2 1 245.01 221.19 9.68 o -10 2 1 238.16 179.70 8.10 o -8 2 1 6367.12 6491.98 56.24 o -6 2 1 23.38 54.33 2.32 o -4 2 1 10838.88 11963.91 98.04 o -2 2 1 2126.59 1980.27 22.86 o 0 2 1 11.31 5.78 1.71 o 2 2 1 4322.88 4610.34 50.46 o 4 2 1 751.32 462.97 32.91 o 6 2 1 371.91 365.20 5.82 o 8 2 1 1419.54 1535.93 15.73 o 10 2 1 136.84 161.67 9.92 o 12 2 1 8.89 10.08 6.92 o 14 2 1 37.12 29.76 9.02 o -15 3 1 12.45 26.64 9.05 o -13 3 1 100.23 96.16 9.67 o -11 3 1 26.67 14.12 6.01 o -9 3 1 3214.57 3468.59 43.82 o -7 3 1 1949.78 1941.68 23.98 o -5 3 1 2622.55 3154.49 28.49 o -3 3 1 4433.15 5029.04 42.70 o -1 3 1 2191.37 2324.59 27.17 o 1 3 1 9062.70 9748.11 102.98 o 3 3 1 7119.78 7706.19 83.05 o 5 3 1 232.47 297.70 12.10 o 7 3 1 2093.33 2047.48 19.13 o 9 3 1 210.58 210.78 7.27 o 11 3 1 174.06 159.35 10.69 o 13 3 1 209.67 210.60 13.79 o 15 3 1 0.33 6.69 9.13 o -16 4 1 103.53 97.49 12.08 o -14 4 1 132.15 114.41 11.24 o -12 4 1 22.23 12.43 9.64 o -10 4 1 55.21 56.87 5.60 o -8 4 1 1561.46 1620.73 20.28 o -6 4 1 874.47 863.39 10.66 o -4 4 1 11766.63 12852.70 105.77 o -2 4 1 2.02 -1.41 1.41 o 0 4 1 152.62 163.62 5.68 o 2 4 1 12713.86 13042.46 137.50 o 4 4 1 6610.93 7279.35 78.91 o 6 4 1 9.39 3.57 1.95 o 8 4 1 598.04 631.29 11.26 o 10 4 1 17.83 9.99 5.35 o 12 4 1 69.78 59.93 8.86 o 14 4 1 0.03 0.42 7.96 o -15 5 1 173.98 166.04 17.55 o -13 5 1 11.81 4.51 7.09 o -11 5 1 649.88 628.72 26.61 o -9 5 1 236.85 234.83 8.67 o -7 5 1 86.44 94.69 3.78 o -5 5 1 1267.37 1334.20 14.67 o -3 5 1 2014.60 2302.35 35.02 o -1 5 1 2787.16 3001.49 35.72 o 1 5 1 381.06 408.39 11.54 o 3 5 1 0.65 13.47 2.07 o 5 5 1 3186.36 3449.31 40.69 o 7 5 1 39.22 44.19 3.54 o 9 5 1 2.71 7.71 5.53 o 11 5 1 297.25 293.58 13.65 o 13 5 1 35.00 23.96 8.34 o 15 5 1 116.13 111.14 19.28 o -16 6 1 19.42 25.95 9.63 o -14 6 1 10.12 16.15 8.11 o -12 6 1 195.15 178.66 12.58 o -10 6 1 1833.40 1876.92 42.32 o -8 6 1 266.73 320.64 8.37 o -6 6 1 72.53 57.44 3.30 o -4 6 1 6703.77 6957.56 66.44 o -2 6 1 3306.32 3441.01 34.62 o 0 6 1 221.21 184.18 6.05 o 2 6 1 2737.83 3344.34 39.88 o 4 6 1 1117.16 1122.64 14.70 o 6 6 1 1820.50 1827.19 37.84 o 8 6 1 30.13 20.60 4.38 o 10 6 1 1923.75 1783.69 35.19 o 12 6 1 3.59 -2.24 6.31 o 14 6 1 26.96 24.52 8.61 o -15 7 1 71.98 75.95 10.88 o -13 7 1 46.76 69.26 9.33 o -11 7 1 30.13 25.69 6.93 o -9 7 1 237.91 216.52 7.82 o -7 7 1 675.16 760.59 11.29 o -5 7 1 108.69 125.00 4.82 o -3 7 1 5922.24 6733.35 76.34 o -1 7 1 552.65 519.65 20.27 o 1 7 1 5.51 -3.12 3.12 o 3 7 1 10287.87 11489.10 107.54 o 5 7 1 1620.46 1527.24 21.01 o 7 7 1 1276.53 1370.94 22.13 o 9 7 1 3157.70 3196.39 53.10 o 11 7 1 37.11 37.73 6.27 o 13 7 1 120.25 105.63 10.94 o 15 7 1 72.51 93.46 11.93 o -14 8 1 0.24 5.77 7.87 o -12 8 1 13.27 28.15 8.28 o -10 8 1 41.35 49.03 7.46 o -8 8 1 3584.57 3548.07 39.51 o -6 8 1 25.94 17.65 3.34 o -4 8 1 1405.95 1480.76 18.71 o -2 8 1 592.42 587.73 9.73 o 0 8 1 2934.47 2902.67 45.92 o 2 8 1 476.22 616.74 12.45 o 4 8 1 4275.85 4102.50 42.77 o 6 8 1 63.72 55.62 4.29 o 8 8 1 86.13 101.09 6.91 o 10 8 1 4.64 3.96 5.91 o 12 8 1 6.82 9.34 6.89 o 14 8 1 39.18 65.04 10.56 o -15 9 1 23.35 26.44 14.78 o -13 9 1 212.08 202.59 13.57 o -11 9 1 17.58 15.71 7.07 o -9 9 1 1049.24 1085.23 17.79 o -7 9 1 7.62 15.09 4.34 o -5 9 1 1831.71 2047.73 24.80 o -3 9 1 1507.31 1837.16 22.23 o -1 9 1 1246.13 1388.64 22.16 o 1 9 1 85.48 94.24 7.13 o 3 9 1 30.35 38.03 4.32 o 5 9 1 2724.31 2892.23 32.84 o 7 9 1 203.31 192.75 10.72 o 9 9 1 506.92 531.52 14.26 o 11 9 1 30.16 27.91 8.07 o 13 9 1 15.79 13.51 7.69 o -14 10 1 292.81 315.98 33.19 o -12 10 1 40.45 55.46 9.66 o -10 10 1 46.67 57.88 8.69 o -8 10 1 727.11 724.76 14.06 o -6 10 1 587.40 573.16 14.72 o -4 10 1 902.03 883.80 17.01 o -2 10 1 13.11 7.53 4.01 o 0 10 1 1980.40 1812.11 33.67 o 2 10 1 2017.88 1911.49 42.83 o 4 10 1 1403.00 1602.25 25.37 o 6 10 1 1174.88 1222.88 21.66 o 8 10 1 0.16 3.25 3.20 o 10 10 1 334.00 293.41 15.09 o 12 10 1 13.11 13.43 11.95 o 14 10 1 138.61 97.68 18.24 o -13 11 1 3.40 -6.50 7.91 o -11 11 1 106.79 94.19 24.53 o -9 11 1 237.50 233.90 10.42 o -7 11 1 233.89 260.79 11.92 o -5 11 1 97.36 102.68 5.78 o -3 11 1 3.13 7.58 4.48 o -1 11 1 11.45 5.54 8.08 o 1 11 1 2409.83 2484.02 43.96 o 3 11 1 201.93 206.94 8.76 o 5 11 1 2869.27 2652.78 40.50 o 7 11 1 116.79 124.72 7.91 o 9 11 1 244.01 255.23 22.05 o 11 11 1 73.33 57.84 9.22 o 13 11 1 43.36 24.02 13.97 o -14 12 1 175.72 176.76 15.24 o -12 12 1 46.76 51.03 9.87 o -10 12 1 214.84 205.32 13.10 o -8 12 1 28.91 33.37 8.30 o -6 12 1 20.19 16.09 7.55 o -4 12 1 511.43 458.63 18.83 o -2 12 1 1301.19 1301.70 49.59 o 0 12 1 346.94 373.13 15.17 o 2 12 1 77.36 102.34 9.47 o 4 12 1 113.13 99.44 8.15 o 6 12 1 1364.50 1207.37 23.30 o 8 12 1 35.03 22.32 5.99 o 10 12 1 272.47 244.45 19.63 o 12 12 1 0.68 -2.02 8.49 o -13 13 1 62.70 75.46 12.08 o -11 13 1 24.13 15.24 8.23 o -9 13 1 23.67 17.55 6.46 o -7 13 1 17.16 27.42 5.09 o -5 13 1 10.21 3.48 3.44 o -3 13 1 22.66 18.33 7.39 o -1 13 1 1641.33 1738.07 52.71 o 1 13 1 417.64 355.81 15.61 o 3 13 1 9.95 10.99 11.03 o 5 13 1 351.61 344.08 13.66 o 7 13 1 202.32 201.65 10.22 o 9 13 1 92.63 103.93 10.48 o 11 13 1 25.77 26.19 9.46 o -12 14 1 97.40 96.20 11.88 o -10 14 1 167.30 174.88 19.57 o -8 14 1 753.89 708.71 22.34 o -6 14 1 95.56 94.72 9.12 o -4 14 1 327.25 315.28 23.90 o -2 14 1 1467.96 1441.23 34.87 o 0 14 1 37.42 44.02 8.68 o 2 14 1 537.08 551.64 20.35 o 4 14 1 366.47 300.98 15.50 o 6 14 1 137.09 151.45 9.38 o 8 14 1 188.11 198.29 13.06 o 10 14 1 222.58 216.77 14.57 o 12 14 1 147.94 146.21 14.26 o -11 15 1 356.40 342.29 18.26 o -9 15 1 11.02 20.64 7.13 o -7 15 1 246.95 232.91 11.79 o -5 15 1 13.69 5.32 14.09 o -3 15 1 14.04 13.76 7.71 o -1 15 1 798.72 793.27 57.09 o 1 15 1 1466.77 1353.60 36.89 o 3 15 1 34.62 51.31 9.91 o 5 15 1 1373.01 1214.17 47.40 o 7 15 1 34.66 19.19 6.59 o 9 15 1 41.31 46.48 10.14 o 11 15 1 288.07 321.94 18.37 o -10 16 1 103.27 79.90 16.86 o -8 16 1 23.64 11.78 14.20 o -6 16 1 1.39 -3.59 8.86 o -4 16 1 64.34 54.44 10.74 o -2 16 1 118.74 113.62 11.92 o 0 16 1 397.98 380.46 18.61 o 2 16 1 0.24 10.03 8.38 o 4 16 1 58.64 89.28 11.70 o 6 16 1 256.22 232.30 15.67 o 8 16 1 58.38 52.53 10.41 o 10 16 1 148.89 131.06 13.38 o -9 17 1 221.35 233.19 21.01 o -7 17 1 0.57 -10.56 10.56 o -5 17 1 57.94 36.89 10.78 o -3 17 1 7.74 2.88 9.51 o -1 17 1 67.41 92.32 12.93 o 1 17 1 22.12 18.86 9.34 o 3 17 1 55.36 56.73 10.85 o 5 17 1 51.20 43.01 11.10 o 7 17 1 27.13 -9.19 9.19 o 9 17 1 888.67 911.28 28.71 o -8 18 1 48.35 45.14 18.36 o -6 18 1 26.36 20.67 11.15 o -4 18 1 71.03 78.22 12.67 o -2 18 1 11.95 12.44 10.16 o 0 18 1 12.35 3.85 13.22 o 2 18 1 51.44 52.34 19.69 o 4 18 1 18.64 17.51 10.81 o 6 18 1 6.19 6.82 12.58 o 8 18 1 145.46 169.15 22.40 o -7 19 1 80.15 87.86 20.67 o -5 19 1 17.60 18.16 11.29 o -3 19 1 4.95 -1.19 10.57 o -1 19 1 25.29 25.64 21.24 o 1 19 1 8.84 2.46 10.85 o 3 19 1 9.21 -0.07 15.01 o 5 19 1 2.06 4.83 10.45 o 7 19 1 18.79 35.15 12.47 o -6 20 1 23.13 14.31 12.93 o -4 20 1 18.24 -5.05 12.24 o -2 20 1 1.63 0.20 11.02 o 0 20 1 0.65 -9.12 9.12 o 2 20 1 72.02 57.37 12.91 o 4 20 1 38.37 20.60 12.16 o 6 20 1 190.25 210.02 25.98 o -5 21 1 54.92 82.32 22.40 o -3 21 1 57.79 52.79 13.72 o -1 21 1 54.09 43.97 13.71 o 1 21 1 3.38 1.69 12.53 o 3 21 1 11.68 17.32 18.70 o -16 0 2 215.39 193.16 19.86 o -14 0 2 600.70 677.97 31.06 o -12 0 2 880.62 922.17 31.92 o -10 0 2 6925.86 6922.36 140.40 o -8 0 2 2147.86 1932.18 47.11 o -6 0 2 1076.34 1010.60 27.59 o -4 0 2 2106.17 1951.00 42.72 o -2 0 2 90.36 44.43 3.38 o 0 0 2 133999.63 115432.47 2120.03 o 2 0 2 4280.60 4256.21 57.11 o 4 0 2 38.74 68.96 7.74 o 6 0 2 20068.35 21118.88 286.97 o 8 0 2 3082.70 2901.89 54.50 o 10 0 2 1155.41 1052.16 35.68 o 12 0 2 48.57 95.48 14.78 o 14 0 2 1153.79 1136.79 44.34 o -17 1 2 529.47 578.31 23.76 o -15 1 2 663.07 674.95 23.27 o -13 1 2 713.44 717.43 17.31 o -11 1 2 4702.21 4306.98 54.18 o -9 1 2 6781.45 6378.89 73.59 o -7 1 2 3944.31 4077.50 47.46 o -5 1 2 727.87 1027.91 14.36 o -3 1 2 7163.22 7237.01 68.03 o -1 1 2 68568.45 63782.04 1264.78 o 1 1 2 2161.01 2162.67 25.36 o 3 1 2 3084.61 2895.49 29.04 o 5 1 2 7411.29 7377.42 62.29 o 7 1 2 4896.48 4765.97 47.84 o 9 1 2 1005.75 1086.40 16.69 o 11 1 2 562.92 565.26 18.65 o 13 1 2 463.36 472.25 19.23 o 15 1 2 784.99 855.54 27.92 o -16 2 2 819.41 904.31 28.08 o -14 2 2 608.20 589.39 20.57 o -12 2 2 3619.23 3307.99 44.84 o -10 2 2 5962.36 5715.32 67.85 o -8 2 2 7841.41 7593.87 73.09 o -6 2 2 2202.46 1855.11 23.94 o -4 2 2 4625.51 4414.93 42.89 o -2 2 2 27149.82 27474.01 252.29 o 0 2 2 6690.16 6547.67 71.74 o 2 2 2 10670.57 10907.78 98.69 o 4 2 2 8325.76 8439.18 78.66 o 6 2 2 2201.18 2045.85 23.27 o 8 2 2 3155.21 3035.25 30.10 o 10 2 2 319.85 343.25 14.37 o 12 2 2 1120.88 1131.50 40.81 o 14 2 2 628.58 683.10 33.71 o -15 3 2 827.99 832.42 25.42 o -13 3 2 1498.70 1461.68 32.41 o -11 3 2 845.57 857.85 17.67 o -9 3 2 6370.77 6383.62 73.97 o -7 3 2 4690.74 4563.49 40.44 o -5 3 2 15930.61 16043.69 131.20 o -3 3 2 12308.37 12870.69 105.26 o -1 3 2 972.34 882.04 11.33 o 1 3 2 51475.51 49983.70 601.30 o 3 3 2 9670.23 9800.40 89.82 o 5 3 2 7124.34 6782.41 64.84 o 7 3 2 4007.99 3798.97 57.63 o 9 3 2 2121.61 2095.29 26.32 o 11 3 2 1538.11 1568.55 33.21 o 13 3 2 1061.06 1124.68 53.80 o 15 3 2 369.12 389.08 34.58 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