#------------------------------------------------------------------------------ #$Date: 2010-12-22 21:36:50 +0200 (Wed, 22 Dec 2010) $ #$Revision: 5269 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2227768.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227768_Fobs loop_ _publ_author_name 'Derakhshandeh, Maryam' 'Derikvand, Zohreh' 'Nemati, Andya' 'Stoeckli-Evans, Helen' _publ_section_title ; 2,9-Dimethyl-1,10-phenanthrolin-1-ium (6-carboxy-4-hydroxypyridine-2-carboxylato-\k^3^O^2^,N,O^6^)(4-hydroxypyridine-2,6-dicarboxylato-\k^3^O^2^,N,O^6^)nickelate(II) 2.35-hydrate: a proton-transfer compound ; _journal_coeditor_code LH5110 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1084 _journal_page_last m1085 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.330 _cell_angle_gamma 90.000 _cell_length_a 11.1663 _cell_length_b 9.7296 _cell_length_c 25.6985 _exptl_crystal_F_000 1390.00 _reflns_d_resolution_high 0.8077 _[local]_cod_data_source_file lh5110Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' NI-CHEL IPDS1 -50DEGC' _shelx_refln_list_code 4 _shelx_f_calc_maximum 269.20 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5689.61 5345.43 153.32 o 3 0 0 12111.03 11304.64 304.98 o 4 0 0 312.43 353.43 51.85 o 5 0 0 1790.32 1637.67 67.81 o 6 0 0 15832.95 16180.58 442.51 o 7 0 0 8769.84 8697.88 154.81 o 8 0 0 1450.40 1408.53 81.63 o 9 0 0 87.28 73.71 71.89 o 10 0 0 1829.87 1889.61 94.16 o 11 0 0 156.28 158.17 95.72 o 12 0 0 797.69 880.03 118.67 o 13 0 0 669.97 761.64 154.61 o 1 1 0 14945.48 14102.48 194.14 o 2 1 0 8239.01 7735.87 165.18 o 3 1 0 32.63 19.68 49.51 o 4 1 0 3869.21 3855.44 77.07 o 5 1 0 0.87 2.42 41.03 o 6 1 0 2234.57 2389.46 60.31 o 7 1 0 462.65 556.80 44.81 o 8 1 0 205.85 250.63 47.16 o 9 1 0 114.75 114.78 52.33 o 10 1 0 0.35 9.76 51.04 o 11 1 0 11.89 11.13 76.28 o 12 1 0 3.61 -4.42 74.94 o 13 1 0 297.93 323.89 138.42 o 0 2 0 931.70 579.31 71.32 o 1 2 0 25698.68 24614.40 258.28 o 2 2 0 2268.36 1936.76 66.80 o 3 2 0 1043.09 882.48 45.32 o 4 2 0 1162.65 1292.70 51.71 o 5 2 0 50.08 55.55 42.27 o 6 2 0 7.89 34.74 44.88 o 7 2 0 4831.93 4810.34 113.88 o 8 2 0 1683.33 1592.32 56.43 o 9 2 0 439.75 408.76 49.53 o 10 2 0 2215.11 2359.11 71.76 o 11 2 0 1161.81 1153.34 94.43 o 12 2 0 391.72 301.41 92.16 o 13 2 0 455.92 443.93 126.46 o 1 3 0 2276.61 2204.70 56.61 o 2 3 0 972.51 948.52 47.73 o 3 3 0 157.57 92.97 40.33 o 4 3 0 5683.30 5706.67 89.43 o 5 3 0 1799.35 1715.06 55.76 o 6 3 0 2022.97 2018.80 64.56 o 7 3 0 0.72 5.20 42.17 o 8 3 0 3591.37 3705.60 79.10 o 9 3 0 16.39 25.07 53.61 o 10 3 0 0.26 29.23 59.43 o 11 3 0 815.94 800.46 75.07 o 12 3 0 1418.30 1422.60 95.09 o 13 3 0 6.16 -12.83 124.00 o 0 4 0 2961.74 2851.36 80.18 o 1 4 0 292.66 279.51 36.19 o 2 4 0 56.88 51.22 33.64 o 3 4 0 7673.54 7659.88 80.26 o 4 4 0 1850.10 1851.97 57.36 o 5 4 0 1.00 -3.21 39.69 o 6 4 0 846.26 871.22 45.72 o 7 4 0 1280.39 1251.59 53.12 o 8 4 0 53.67 55.14 49.55 o 9 4 0 490.94 499.92 70.28 o 10 4 0 500.29 478.20 62.80 o 11 4 0 1.69 -6.18 71.79 o 12 4 0 20.18 23.21 78.41 o 1 5 0 2757.92 2685.18 48.85 o 2 5 0 327.56 292.96 42.12 o 3 5 0 1.73 5.19 36.36 o 4 5 0 17.98 -1.95 39.62 o 5 5 0 1786.45 1785.28 54.98 o 6 5 0 2282.32 2409.25 62.88 o 7 5 0 34.31 16.53 44.74 o 8 5 0 100.00 72.71 45.85 o 9 5 0 779.45 787.09 75.62 o 10 5 0 0.66 36.48 70.36 o 11 5 0 109.11 70.96 64.07 o 12 5 0 289.20 286.81 92.96 o 0 6 0 402.94 464.02 56.56 o 1 6 0 3565.52 3781.49 58.63 o 2 6 0 1017.95 1035.15 42.63 o 3 6 0 43.18 66.00 34.08 o 4 6 0 62.38 71.72 34.28 o 5 6 0 829.70 769.18 49.89 o 6 6 0 325.87 349.23 48.05 o 7 6 0 148.58 137.43 42.69 o 8 6 0 84.81 57.39 65.64 o 9 6 0 257.66 192.88 71.79 o 10 6 0 0.79 24.72 72.03 o 11 6 0 4.26 24.17 90.38 o 1 7 0 1080.41 978.77 45.10 o 2 7 0 2356.32 2478.87 55.43 o 3 7 0 213.67 209.74 38.45 o 4 7 0 2077.38 2119.07 51.79 o 5 7 0 1402.32 1461.34 53.64 o 6 7 0 40.80 25.05 41.81 o 7 7 0 246.61 191.40 63.94 o 8 7 0 1177.08 1158.59 59.07 o 9 7 0 1085.89 1034.38 66.47 o 10 7 0 36.98 50.27 87.62 o 11 7 0 226.41 211.41 94.27 o 0 8 0 134.25 149.40 54.34 o 1 8 0 704.59 779.93 49.29 o 2 8 0 122.36 128.62 41.73 o 3 8 0 1643.23 1664.77 50.42 o 4 8 0 35.22 29.27 46.79 o 5 8 0 74.08 64.68 53.59 o 6 8 0 94.01 86.30 49.73 o 7 8 0 4.13 -10.16 50.01 o 8 8 0 89.03 34.54 61.17 o 9 8 0 1.68 15.76 74.51 o 10 8 0 112.29 62.17 94.73 o 1 9 0 708.59 827.50 51.92 o 2 9 0 1234.37 1272.06 47.52 o 3 9 0 285.31 271.57 55.42 o 4 9 0 15.73 14.71 54.45 o 5 9 0 755.80 799.59 58.41 o 6 9 0 1173.18 1151.12 67.56 o 7 9 0 19.50 17.32 71.16 o 8 9 0 1098.69 946.58 86.22 o 9 9 0 542.07 427.77 69.32 o 0 10 0 414.79 413.94 87.88 o 1 10 0 174.33 137.17 61.83 o 2 10 0 2.08 6.29 46.64 o 3 10 0 3.57 25.57 55.49 o 4 10 0 117.69 109.30 56.63 o 5 10 0 13.14 -11.50 65.54 o 6 10 0 1.64 -40.35 70.53 o 7 10 0 6.77 64.45 79.46 o 1 11 0 502.59 453.32 56.64 o 2 11 0 411.70 369.08 64.79 o 3 11 0 116.57 72.38 70.61 o 4 11 0 60.06 22.27 59.51 o 5 11 0 64.14 44.60 61.17 o -13 1 1 8.30 13.69 99.95 o -12 1 1 279.25 315.52 72.60 o -11 1 1 243.78 269.69 68.15 o -10 1 1 249.74 222.17 53.02 o -9 1 1 1142.23 1175.32 57.72 o -8 1 1 3816.03 3702.74 69.81 o -7 1 1 1961.26 2006.74 55.73 o -6 1 1 333.02 295.92 42.99 o -5 1 1 1573.97 1397.08 44.60 o -4 1 1 6268.91 5299.01 132.82 o -3 1 1 15821.67 15092.75 349.50 o -2 1 1 6026.34 5019.95 202.53 o -1 1 1 31227.93 30833.61 262.46 o 0 1 1 21232.42 19522.44 258.22 o 1 1 1 5795.85 5060.43 125.91 o 2 1 1 14548.16 12944.30 200.40 o 3 1 1 5599.86 4927.84 122.40 o 4 1 1 1796.41 1794.14 69.04 o 5 1 1 1852.90 1723.91 63.38 o 6 1 1 3935.11 3716.63 83.24 o 7 1 1 724.39 718.82 52.53 o 8 1 1 3522.18 3565.56 69.02 o 9 1 1 3616.07 3640.77 70.85 o 10 1 1 437.61 442.56 57.09 o 11 1 1 277.14 296.68 74.81 o 12 1 1 1867.11 2007.87 125.88 o 13 1 1 769.11 704.50 129.53 o -13 2 1 17.65 33.57 111.57 o -12 2 1 154.67 112.16 89.29 o -11 2 1 445.12 391.92 73.92 o -10 2 1 340.15 314.79 51.54 o -9 2 1 405.62 394.16 46.79 o -8 2 1 691.22 694.49 48.49 o -7 2 1 235.72 186.83 44.53 o -6 2 1 3354.15 3321.05 67.99 o -5 2 1 277.04 290.07 40.53 o -4 2 1 2926.91 2769.81 63.25 o -3 2 1 2967.16 2858.07 65.65 o -2 2 1 4965.09 4779.66 86.02 o -1 2 1 71.36 75.75 42.65 o 0 2 1 3109.94 2886.33 75.45 o 1 2 1 6830.24 6554.84 100.12 o 2 2 1 228.91 210.31 50.18 o 3 2 1 314.67 334.89 48.04 o 4 2 1 669.05 577.96 42.69 o 5 2 1 550.41 612.24 47.97 o 6 2 1 271.50 310.51 56.28 o 7 2 1 470.04 514.22 59.84 o 8 2 1 109.99 84.43 57.98 o 9 2 1 13.56 18.40 53.39 o 10 2 1 85.27 78.45 69.26 o 11 2 1 14.43 16.41 70.72 o 12 2 1 15.96 13.79 89.01 o 13 2 1 13.34 -3.47 112.88 o -13 3 1 8.43 11.78 113.05 o -12 3 1 67.96 12.83 90.22 o -11 3 1 459.53 382.00 73.01 o -10 3 1 310.41 303.75 57.32 o -9 3 1 307.95 303.36 48.77 o -8 3 1 1364.58 1320.17 60.42 o -7 3 1 2614.83 2613.42 67.78 o -6 3 1 114.47 146.58 48.03 o -5 3 1 3081.08 2945.52 67.69 o -4 3 1 6983.83 6423.19 94.81 o -3 3 1 3.16 7.37 33.45 o -2 3 1 783.45 703.39 45.95 o -1 3 1 3346.71 3123.73 62.39 o 0 3 1 307.36 306.73 40.89 o 1 3 1 2857.69 2742.86 60.96 o 2 3 1 3831.64 3498.70 66.62 o 3 3 1 2426.83 2171.22 54.54 o 4 3 1 10595.14 10514.58 322.10 o 5 3 1 3571.41 3401.12 70.08 o 6 3 1 8109.24 8051.14 131.83 o 7 3 1 1171.56 1196.24 65.96 o 8 3 1 5.16 -36.93 64.67 o 9 3 1 2671.63 2679.95 130.14 o 10 3 1 443.00 447.75 71.74 o 11 3 1 983.93 887.72 75.86 o 12 3 1 2069.99 2054.82 113.69 o 13 3 1 231.56 159.43 114.50 o -12 4 1 85.92 65.78 69.96 o -11 4 1 115.93 79.02 72.42 o -10 4 1 350.55 320.70 71.41 o -9 4 1 1168.91 1195.58 63.66 o -8 4 1 1546.03 1601.98 61.27 o -7 4 1 1874.95 1909.69 61.98 o -6 4 1 981.62 926.07 51.78 o -5 4 1 241.37 265.43 43.54 o -4 4 1 3863.44 3763.92 92.95 o -3 4 1 464.44 356.97 34.09 o -2 4 1 131.03 111.78 30.91 o -1 4 1 1286.96 1262.76 42.48 o 0 4 1 555.75 577.70 34.09 o 1 4 1 863.28 751.31 40.53 o 2 4 1 24.79 30.88 30.67 o 3 4 1 577.98 540.01 37.94 o 4 4 1 7565.99 7769.74 95.26 o 5 4 1 4033.39 4005.90 66.90 o 6 4 1 51.41 44.26 39.05 o 7 4 1 1320.97 1324.53 62.69 o 8 4 1 4.84 27.21 53.34 o 9 4 1 64.01 47.83 66.88 o 10 4 1 762.18 735.81 90.64 o 11 4 1 1102.51 1265.40 78.35 o 12 4 1 496.20 493.93 92.84 o -12 5 1 143.57 75.42 79.87 o -11 5 1 73.09 55.34 63.80 o -10 5 1 17.22 -0.24 54.88 o -9 5 1 833.07 769.15 68.11 o -8 5 1 52.94 66.89 44.68 o -7 5 1 901.47 893.17 50.36 o -6 5 1 1253.15 1247.77 49.57 o -5 5 1 42.51 29.89 41.35 o -4 5 1 446.92 442.08 42.47 o -3 5 1 3.04 6.70 33.56 o -2 5 1 492.36 506.92 43.53 o -1 5 1 423.31 385.30 35.74 o 0 5 1 373.34 326.82 30.70 o 1 5 1 224.33 176.02 39.71 o 2 5 1 65.93 73.82 40.31 o 3 5 1 1222.84 1270.74 52.06 o 4 5 1 451.06 528.78 47.40 o 5 5 1 1056.23 1072.15 54.85 o 6 5 1 164.27 180.81 48.61 o 7 5 1 232.55 231.91 46.42 o 8 5 1 507.75 404.97 51.00 o 9 5 1 51.05 61.82 69.81 o 10 5 1 143.68 164.02 87.40 o 11 5 1 0.24 17.60 63.24 o 12 5 1 31.06 -14.67 80.08 o -11 6 1 3.61 4.61 78.28 o -10 6 1 659.66 652.23 76.93 o -9 6 1 1712.54 1766.34 68.99 o -8 6 1 563.33 455.61 54.85 o -7 6 1 189.38 156.30 42.85 o -6 6 1 5347.23 5269.43 79.29 o -5 6 1 291.16 289.39 42.20 o -4 6 1 4.62 9.83 33.68 o -3 6 1 2424.63 2403.14 49.62 o -2 6 1 2094.87 2134.20 67.62 o -1 6 1 714.59 728.86 38.35 o 0 6 1 4151.08 4292.03 117.47 o 1 6 1 6272.38 6251.72 151.08 o 2 6 1 31.95 15.67 40.04 o 3 6 1 2483.84 2445.66 50.24 o 4 6 1 4587.42 4632.24 60.62 o 5 6 1 1015.04 1053.88 51.64 o 6 6 1 1256.63 1261.55 46.65 o 7 6 1 15.82 10.49 48.60 o 8 6 1 896.56 923.60 73.97 o 9 6 1 112.67 78.06 77.57 o 10 6 1 6.35 15.39 89.03 o 11 6 1 428.98 509.05 112.70 o -11 7 1 29.04 0.13 80.86 o -10 7 1 2.98 -31.03 78.28 o -9 7 1 0.11 12.46 68.50 o -8 7 1 118.25 60.01 57.18 o -7 7 1 129.92 116.55 49.66 o -6 7 1 150.10 106.27 42.51 o -5 7 1 1205.80 1195.26 51.12 o -4 7 1 648.60 616.07 44.78 o -3 7 1 32.54 9.87 40.61 o -2 7 1 388.55 438.37 46.74 o -1 7 1 240.90 200.85 41.77 o 0 7 1 3.46 -5.29 39.89 o 1 7 1 2979.53 3211.23 108.33 o 2 7 1 12.68 -1.53 40.27 o 3 7 1 25.97 21.89 45.47 o 4 7 1 317.71 330.48 42.52 o 5 7 1 39.13 41.21 38.11 o 6 7 1 4.69 -3.84 47.02 o 7 7 1 1.95 -10.98 53.70 o 8 7 1 136.44 123.83 59.34 o 9 7 1 128.50 57.23 73.06 o 10 7 1 30.99 93.47 109.94 o 11 7 1 219.09 215.35 114.91 o -10 8 1 590.49 510.63 82.57 o -9 8 1 454.77 418.85 74.41 o -8 8 1 28.38 28.41 63.37 o -7 8 1 919.29 894.37 54.28 o -6 8 1 599.37 571.89 56.92 o -5 8 1 905.02 951.54 57.17 o -4 8 1 222.89 218.66 43.42 o -3 8 1 1253.07 1418.28 53.15 o -2 8 1 308.66 298.31 39.34 o -1 8 1 698.76 709.97 41.17 o 0 8 1 1048.94 1048.04 50.35 o 1 8 1 1723.39 1798.52 49.35 o 2 8 1 1065.47 1080.45 46.29 o 3 8 1 30.28 23.71 38.16 o 4 8 1 750.57 757.43 45.95 o 5 8 1 791.88 818.26 56.87 o 6 8 1 34.73 40.11 54.03 o 7 8 1 1460.08 1540.80 62.50 o 8 8 1 660.27 739.65 55.10 o 9 8 1 8.58 28.09 85.40 o 10 8 1 208.75 146.76 114.60 o -9 9 1 0.10 -6.37 74.71 o -8 9 1 28.38 27.90 72.82 o -7 9 1 148.70 83.03 70.46 o -6 9 1 3.03 -20.96 62.34 o -5 9 1 64.11 71.66 54.90 o -4 9 1 752.78 757.35 57.42 o -3 9 1 3436.17 3649.07 102.16 o -2 9 1 21.50 0.95 53.21 o -1 9 1 208.55 206.55 53.71 o 0 9 1 483.06 540.57 54.94 o 1 9 1 15.83 14.06 44.76 o 2 9 1 204.01 182.10 54.38 o 3 9 1 0.28 14.73 60.53 o 4 9 1 160.64 108.76 54.80 o 5 9 1 26.41 33.76 50.20 o 6 9 1 16.26 25.24 55.79 o 7 9 1 20.59 16.67 72.22 o 8 9 1 10.95 34.63 82.30 o 9 9 1 51.71 -85.18 100.09 o -7 10 1 283.55 186.31 72.62 o -6 10 1 1071.43 1158.81 105.63 o -5 10 1 440.56 439.64 72.29 o -4 10 1 953.07 884.67 66.30 o -3 10 1 2052.47 2231.14 69.93 o -2 10 1 479.46 524.79 52.50 o -1 10 1 14.13 -19.27 55.07 o 0 10 1 892.58 934.10 58.57 o 1 10 1 295.52 254.71 56.43 o 2 10 1 7.90 35.51 50.41 o 3 10 1 583.10 624.77 58.62 o 4 10 1 798.54 781.86 60.28 o 5 10 1 1324.03 1364.26 71.53 o 6 10 1 15.02 33.99 69.67 o 7 10 1 203.50 128.16 84.87 o -5 11 1 72.94 57.49 71.91 o -4 11 1 182.48 122.98 71.23 o -3 11 1 82.28 31.89 78.51 o -2 11 1 0.98 27.23 69.16 o -1 11 1 105.82 64.12 63.87 o 0 11 1 263.33 232.83 63.49 o 1 11 1 47.40 14.98 59.33 o 2 11 1 180.62 163.84 64.17 o 3 11 1 134.52 130.18 70.26 o 4 11 1 1.55 63.34 78.41 o 5 11 1 8.74 50.64 71.51 o 0 12 1 96.16 98.17 115.26 o -13 0 2 1162.82 1208.39 132.96 o -12 0 2 1479.53 1566.04 103.58 o -11 0 2 745.37 686.54 92.58 o -10 0 2 1295.82 1325.24 86.36 o -9 0 2 2771.47 2697.38 92.41 o -8 0 2 956.96 937.93 74.44 o -7 0 2 938.59 995.03 75.66 o -6 0 2 27.54 60.83 65.92 o -5 0 2 8612.37 7753.69 163.33 o -4 0 2 1507.09 1450.21 78.56 o -3 0 2 1193.45 1280.19 70.63 o -2 0 2 49.61 39.63 56.05 o -1 0 2 9216.57 8333.18 206.56 o 1 0 2 103.45 169.47 101.21 o 2 0 2 126.05 89.15 95.28 o 3 0 2 25.29 35.45 78.45 o 4 0 2 3553.23 3501.73 128.88 o 5 0 2 10746.99 9707.32 335.38 o 6 0 2 4.35 10.63 63.92 o 7 0 2 6408.77 6879.44 122.96 o 8 0 2 3006.90 2984.77 114.20 o 9 0 2 5066.19 5165.47 204.62 o 10 0 2 2046.27 1961.83 106.10 o 11 0 2 728.84 862.21 115.51 o 12 0 2 490.65 496.65 123.49 o 13 0 2 363.63 284.76 182.09 o -13 1 2 91.07 42.18 103.65 o -12 1 2 0.73 -8.82 69.81 o -11 1 2 692.61 655.66 74.71 o -10 1 2 161.53 125.83 52.71 o -9 1 2 224.36 228.32 49.53 o -8 1 2 8.00 1.70 45.35 o -7 1 2 106.27 93.14 36.93 o -6 1 2 2870.51 3062.24 67.21 o -5 1 2 175.01 135.93 33.64 o -4 1 2 399.85 361.52 36.00 o -3 1 2 2201.87 2104.96 57.45 o -2 1 2 86.10 97.34 53.60 o -1 1 2 592.66 694.66 59.99 o 0 1 2 4106.13 3510.77 95.43 o 1 1 2 117.62 126.21 57.24 o 2 1 2 3110.99 2914.27 114.18 o 3 1 2 0.79 -8.99 60.73 o 4 1 2 1374.91 1283.44 73.77 o 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o -1 3 28 95.08 87.40 54.59 o 0 3 28 440.17 366.14 64.28 o 1 3 28 26.21 22.21 69.55 o 2 3 28 37.64 2.23 64.02 o 3 3 28 429.34 378.12 71.96 o 4 3 28 142.13 117.39 61.83 o -5 4 28 303.00 176.99 66.76 o -4 4 28 121.09 126.58 70.64 o -3 4 28 79.60 -24.79 70.68 o -2 4 28 66.25 78.45 59.39 o -1 4 28 45.43 82.45 63.96 o 0 4 28 10.20 10.18 78.46 o 1 4 28 50.26 63.61 78.53 o 2 4 28 257.65 260.41 71.97 o 3 4 28 10.74 -20.58 80.32 o -4 5 28 25.00 -23.29 114.32 o -3 5 28 505.09 415.01 67.40 o -2 5 28 49.67 24.01 71.33 o -1 5 28 5.69 28.37 70.70 o 0 5 28 150.14 64.70 72.08 o 1 5 28 256.81 174.03 66.16 o 2 5 28 275.49 216.58 114.17 o -6 1 29 52.35 31.57 60.61 o -5 1 29 18.11 87.70 59.29 o -4 1 29 296.53 209.50 64.65 o -3 1 29 885.34 922.57 66.07 o -2 1 29 2174.44 2258.08 70.26 o -1 1 29 215.35 135.05 58.59 o 0 1 29 117.37 75.89 69.45 o 1 1 29 522.64 544.78 65.30 o 2 1 29 4.38 11.96 69.26 o 3 1 29 750.55 653.01 63.18 o 4 1 29 711.95 689.52 82.96 o -6 2 29 66.58 37.87 114.63 o -5 2 29 620.84 542.69 57.97 o -4 2 29 2.41 18.78 63.85 o -3 2 29 0.30 16.41 51.66 o -2 2 29 192.24 143.58 63.76 o -1 2 29 227.16 155.97 59.13 o 0 2 29 240.58 248.44 69.79 o 1 2 29 0.80 -9.59 69.87 o 2 2 29 209.92 117.39 71.09 o 3 2 29 13.61 4.86 60.42 o 4 2 29 23.27 37.00 93.83 o -5 3 29 171.74 103.48 57.28 o -4 3 29 57.26 26.84 56.23 o -3 3 29 156.67 130.79 52.83 o -2 3 29 351.39 380.49 59.76 o -1 3 29 59.02 39.36 64.32 o 0 3 29 443.55 414.65 57.15 o 1 3 29 580.24 533.49 58.27 o 2 3 29 238.15 206.40 65.83 o 3 3 29 61.11 3.92 66.51 o -4 4 29 59.44 -19.29 115.34 o -3 4 29 65.35 62.52 79.87 o -2 4 29 68.87 25.59 71.47 o -1 4 29 666.89 603.68 81.81 o 0 4 29 147.08 62.66 60.66 o 1 4 29 9.44 27.83 56.55 o 2 4 29 832.73 719.32 98.52 o -5 0 30 257.13 240.93 71.95 o -4 0 30 1226.55 1189.57 97.15 o -3 0 30 111.33 115.38 90.79 o -2 0 30 3.95 -90.81 90.81 o -1 0 30 285.47 167.76 90.60 o 0 0 30 50.25 43.47 111.00 o 1 0 30 173.52 80.43 91.65 o 2 0 30 304.31 181.96 113.75 o 3 0 30 903.81 850.01 118.87 o -5 1 30 112.04 54.99 65.57 o -4 1 30 295.61 189.64 65.65 o -3 1 30 295.00 287.65 64.94 o -2 1 30 224.96 136.28 56.28 o -1 1 30 0.11 -10.31 59.09 o 0 1 30 15.76 -11.66 69.98 o 1 1 30 31.74 76.35 78.20 o 2 1 30 144.72 149.66 70.94 o 3 1 30 129.77 68.16 80.82 o -4 2 30 96.38 39.14 50.71 o -3 2 30 122.69 105.36 59.94 o -2 2 30 99.11 72.24 64.26 o -1 2 30 142.22 84.51 59.96 o 0 2 30 28.47 34.34 59.47 o 1 2 30 6.67 23.04 59.87 o 2 2 30 250.85 226.62 61.66 o -3 3 30 0.98 8.95 65.43 o -2 3 30 477.54 413.49 58.03 o -1 3 30 233.22 114.18 65.71 o 0 3 30 22.98 -29.78 65.39 o 1 3 30 3.01 1.15 71.86 o -3 1 31 23.70 -31.14 56.75 o -2 1 31 166.39 90.76 65.28 o -1 1 31 5.57 8.68 64.94 o 0 1 31 49.36 84.40 56.31 o 1 1 31 7.93 45.62 60.52 o -2 2 31 43.95 50.90 60.54 o -1 2 31 23.94 -59.32 65.86 o 0 2 31 0.64 -5.58 56.55 o