#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/77/2227770.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227770_Fobs loop_ _publ_author_name 'Oudenhoven, Tracey A.' 'Walder, Brennan J.' 'Golen, James A.' 'Rheingold, Arnold L.' 'D'Acchioli, Jason S.' _publ_section_title ; Benzoyldicarbonyl(\h^5^-indenyl)ruthenium(II) ; _journal_coeditor_code LH5113 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1160 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 108.150 _cell_angle_gamma 90.000 _cell_length_a 11.5312 _cell_length_b 8.7313 _cell_length_c 15.1584 _exptl_crystal_F_000 752.00 _reflns_d_resolution_high 0.7554 _[local]_cod_data_source_file lh5113Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' golt01_0m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 200.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 31670.30 29609.10 296.48 o 4 0 0 98.04 98.83 14.92 o 6 0 0 9312.16 9717.60 194.43 o 8 0 0 8542.57 8643.39 250.45 o 10 0 0 5749.26 6010.57 222.33 o 12 0 0 100.69 198.48 36.29 o 1 1 0 5420.94 5450.47 58.04 o 2 1 0 15702.79 15084.66 113.57 o 3 1 0 5.34 3.76 4.83 o 4 1 0 17668.22 16710.48 165.16 o 5 1 0 1238.42 1363.68 35.79 o 6 1 0 7076.39 6557.39 100.36 o 7 1 0 1355.45 1355.90 43.93 o 8 1 0 1124.11 1041.74 46.50 o 9 1 0 3224.34 3404.02 107.87 o 10 1 0 44.46 24.46 16.56 o 11 1 0 171.70 213.78 27.60 o 12 1 0 671.93 589.67 44.37 o 13 1 0 280.92 297.98 57.19 o 14 1 0 1228.73 1131.92 146.88 o 0 2 0 6976.56 6807.17 91.28 o 1 2 0 0.71 6.60 4.42 o 2 2 0 24662.53 24301.12 197.02 o 3 2 0 8777.84 8451.38 90.03 o 4 2 0 58.42 78.10 9.43 o 5 2 0 8369.54 8094.85 100.44 o 6 2 0 4185.38 4237.83 73.35 o 7 2 0 8834.60 8883.48 130.47 o 8 2 0 900.23 903.91 37.55 o 9 2 0 850.40 808.92 46.79 o 10 2 0 306.19 294.38 34.00 o 11 2 0 53.94 67.05 16.80 o 12 2 0 744.90 774.69 59.39 o 13 2 0 1184.99 1556.98 103.28 o 14 2 0 3.97 41.09 56.56 o 1 3 0 8529.83 8131.99 89.70 o 2 3 0 1381.25 1348.22 32.93 o 3 3 0 11197.57 10956.15 120.75 o 4 3 0 906.82 808.17 27.93 o 5 3 0 55.31 33.37 9.33 o 6 3 0 23.28 13.51 8.95 o 7 3 0 2931.54 2847.12 68.79 o 8 3 0 372.58 350.08 24.27 o 9 3 0 3920.27 4117.97 111.19 o 10 3 0 1.04 -13.47 21.36 o 11 3 0 4122.14 4231.61 165.27 o 12 3 0 2.96 25.68 23.08 o 13 3 0 345.01 294.23 48.69 o 0 4 0 295.93 273.44 20.84 o 1 4 0 614.89 587.83 20.97 o 2 4 0 3148.91 3132.70 53.17 o 3 4 0 8191.87 7953.34 104.07 o 4 4 0 2580.25 2609.21 53.80 o 5 4 0 12959.92 12915.90 159.30 o 6 4 0 65.66 32.60 11.84 o 7 4 0 4808.76 4967.87 122.88 o 8 4 0 32.12 26.78 15.85 o 9 4 0 5.68 115.18 109.25 o 10 4 0 678.99 625.92 67.17 o 11 4 0 587.26 581.42 120.23 o 12 4 0 442.26 401.98 62.76 o 13 4 0 1086.36 1096.93 159.90 o 1 5 0 9428.06 9504.43 117.85 o 2 5 0 2034.00 2047.04 52.63 o 3 5 0 1380.81 1423.86 49.47 o 4 5 0 2673.75 2484.04 70.70 o 5 5 0 51.25 29.32 9.59 o 6 5 0 1387.75 1378.35 67.43 o 7 5 0 1845.99 1870.83 91.54 o 8 5 0 1169.30 1208.54 81.39 o 9 5 0 3299.69 3152.20 164.88 o 10 5 0 30.00 104.87 34.08 o 11 5 0 496.74 523.43 64.32 o 12 5 0 236.05 233.68 57.57 o 0 6 0 5086.77 5486.54 175.46 o 1 6 0 52.99 51.59 11.33 o 2 6 0 2396.73 2312.40 80.10 o 3 6 0 657.09 616.11 43.45 o 4 6 0 807.91 797.02 50.11 o 5 6 0 262.85 298.52 32.24 o 6 6 0 10.94 18.74 12.26 o 7 6 0 110.68 202.58 40.56 o 8 6 0 2276.97 2276.06 135.49 o 9 6 0 16.47 -20.80 24.15 o 10 6 0 3265.49 3334.81 185.99 o 11 6 0 244.53 212.82 54.87 o 12 6 0 1064.81 1166.91 160.31 o 1 7 0 623.74 632.07 36.03 o 2 7 0 2107.26 2053.41 74.72 o 3 7 0 3.56 -9.89 11.43 o 4 7 0 4673.22 5159.38 157.39 o 5 7 0 62.89 29.84 13.20 o 6 7 0 4281.62 4717.50 139.85 o 7 7 0 276.47 296.83 45.28 o 8 7 0 456.50 475.12 57.34 o 9 7 0 469.17 506.22 67.32 o 10 7 0 36.59 -3.68 69.37 o 11 7 0 42.97 -24.82 59.40 o 0 8 0 472.29 472.28 45.31 o 1 8 0 137.07 118.20 18.38 o 2 8 0 37.49 32.84 32.53 o 3 8 0 1337.94 1266.72 59.61 o 4 8 0 594.37 622.35 37.52 o 5 8 0 594.50 606.67 41.08 o 6 8 0 79.06 52.42 17.70 o 7 8 0 777.09 684.21 56.55 o 8 8 0 196.28 75.06 57.98 o 9 8 0 8.10 -11.73 64.69 o 10 8 0 1692.94 1892.78 176.99 o 1 9 0 1654.89 1660.42 74.22 o 2 9 0 394.21 337.03 42.46 o 3 9 0 990.23 941.55 68.53 o 4 9 0 899.56 784.22 58.32 o 5 9 0 6.86 38.80 15.86 o 6 9 0 403.91 471.76 39.04 o 7 9 0 948.82 1129.98 86.56 o 8 9 0 99.83 23.11 66.73 o 9 9 0 928.75 1013.93 112.70 o 0 10 0 642.77 456.26 57.98 o 1 10 0 69.42 62.95 27.80 o 2 10 0 35.85 26.93 31.30 o 3 10 0 1410.93 1434.53 73.34 o 4 10 0 0.25 14.67 22.55 o 5 10 0 1631.33 1756.40 125.08 o 6 10 0 137.78 107.91 32.79 o 7 10 0 418.52 385.37 60.52 o 1 11 0 1438.71 1418.74 82.01 o 2 11 0 319.00 281.25 39.30 o 3 11 0 317.36 277.05 55.26 o 4 11 0 624.31 579.82 66.72 o -13 0 1 303.91 318.15 48.46 o -11 0 1 195.43 202.58 36.62 o -9 0 1 5925.53 5953.14 206.61 o -7 0 1 3986.04 3642.99 96.29 o -5 0 1 17561.87 16487.84 216.64 o -3 0 1 2033.92 1851.99 39.97 o -1 0 1 9775.01 9613.13 162.09 o 1 0 1 34842.25 34130.54 382.35 o 3 0 1 20758.43 20251.64 276.80 o 5 0 1 7023.74 6204.78 143.39 o 7 0 1 57.17 35.84 13.15 o 9 0 1 4174.54 4225.88 175.98 o 11 0 1 4682.83 4772.91 210.39 o 13 0 1 2517.22 2990.93 275.86 o -14 1 1 153.09 139.92 46.50 o -13 1 1 833.15 839.20 56.48 o -12 1 1 36.51 46.24 21.67 o -11 1 1 2213.73 2217.90 90.19 o -10 1 1 100.76 79.30 14.11 o -9 1 1 1823.20 1866.80 66.38 o -8 1 1 275.46 222.51 29.13 o -7 1 1 135.66 110.65 12.87 o -6 1 1 770.17 603.86 24.17 o -5 1 1 3308.01 3157.61 54.19 o -4 1 1 585.68 540.16 19.56 o -3 1 1 12689.32 11726.04 104.95 o -2 1 1 1073.05 1065.51 22.71 o -1 1 1 14601.29 14515.67 114.20 o 0 1 1 178.16 193.05 8.85 o 1 1 1 1858.50 1828.68 35.32 o 2 1 1 2923.98 2726.80 39.98 o 3 1 1 65.64 77.82 9.20 o 4 1 1 7236.91 6958.07 86.46 o 5 1 1 5010.71 4817.62 80.73 o 6 1 1 554.96 519.62 26.09 o 7 1 1 11179.19 10609.44 159.88 o 8 1 1 341.89 319.31 25.85 o 9 1 1 6499.68 6632.99 163.77 o 10 1 1 295.10 286.60 26.00 o 11 1 1 966.96 914.56 80.69 o 12 1 1 339.35 321.54 54.64 o 13 1 1 118.30 149.14 39.11 o -14 2 1 579.95 629.20 115.96 o -13 2 1 55.77 86.15 25.07 o -12 2 1 1269.96 1235.62 81.04 o -11 2 1 26.02 45.32 20.91 o -10 2 1 1872.19 2033.73 83.48 o -9 2 1 8.75 1.41 19.06 o -8 2 1 86.02 62.01 14.74 o -7 2 1 4840.66 4938.54 89.70 o -6 2 1 2454.98 2456.40 51.76 o -5 2 1 2035.23 1894.22 46.26 o -4 2 1 6514.82 6152.53 78.02 o -3 2 1 3109.93 3014.19 49.84 o -2 2 1 12456.27 12078.54 123.37 o -1 2 1 382.49 367.69 19.38 o 0 2 1 6887.42 6843.25 76.92 o 1 2 1 5813.56 5742.85 70.18 o 2 2 1 408.40 446.95 17.64 o 3 2 1 18431.04 17955.32 167.14 o 4 2 1 2539.92 2512.85 48.70 o 5 2 1 5074.30 4912.34 76.91 o 6 2 1 4482.81 4427.44 77.55 o 7 2 1 326.85 334.89 22.77 o 8 2 1 2915.18 2851.26 87.27 o 9 2 1 684.12 656.32 62.49 o 10 2 1 309.22 305.04 44.57 o 11 2 1 2413.48 2382.77 119.22 o 12 2 1 3.90 -9.45 30.81 o 13 2 1 691.33 816.36 74.83 o -14 3 1 854.95 1020.03 140.78 o -13 3 1 5.53 3.27 26.08 o -12 3 1 228.42 145.34 29.71 o -11 3 1 10.72 -8.30 24.67 o -10 3 1 21.47 11.66 13.62 o -9 3 1 143.54 93.47 16.25 o -8 3 1 4875.21 4962.39 105.16 o -7 3 1 239.18 232.62 17.82 o -6 3 1 6663.65 6413.97 101.36 o -5 3 1 198.15 192.96 14.47 o -4 3 1 5713.08 5532.33 83.90 o -3 3 1 103.87 117.65 12.51 o -2 3 1 74.89 121.37 12.32 o -1 3 1 4181.03 4187.36 65.06 o 0 3 1 4137.75 3881.78 51.46 o 1 3 1 634.28 606.36 21.37 o 2 3 1 37027.74 35640.84 307.82 o 3 3 1 2174.83 2373.35 46.25 o 4 3 1 12149.80 12172.56 131.43 o 5 3 1 872.87 846.36 32.57 o 6 3 1 3552.51 3584.09 82.37 o 7 3 1 16.09 0.80 8.82 o 8 3 1 366.18 364.98 29.48 o 9 3 1 1241.62 1241.40 63.84 o 10 3 1 2955.94 2941.52 128.62 o 11 3 1 4.30 -23.82 23.82 o 12 3 1 3583.88 3783.80 210.49 o 13 3 1 88.71 77.58 66.52 o -13 4 1 24.86 -3.86 41.09 o -12 4 1 2048.48 2547.68 164.70 o -11 4 1 79.05 46.07 27.67 o -10 4 1 2671.15 2762.15 122.91 o -9 4 1 138.48 164.04 26.12 o -8 4 1 854.68 910.00 51.51 o -7 4 1 1879.66 1880.40 96.66 o -6 4 1 626.91 658.81 30.09 o -5 4 1 331.49 278.79 19.72 o -4 4 1 15374.16 15810.79 184.99 o -3 4 1 2.13 0.49 5.76 o -2 4 1 8913.54 8637.78 115.76 o -1 4 1 12.19 8.89 4.98 o 0 4 1 7547.31 7365.79 92.16 o 1 4 1 510.06 495.37 19.73 o 2 4 1 1735.58 1837.78 42.62 o 3 4 1 373.99 311.08 20.65 o 4 4 1 3439.25 3632.57 66.39 o 5 4 1 55.47 55.01 14.56 o 6 4 1 8830.62 9179.18 161.38 o 7 4 1 5.06 24.65 11.45 o 8 4 1 3225.25 3073.66 126.06 o 9 4 1 33.00 -12.67 46.18 o 10 4 1 1380.56 1399.64 109.32 o 11 4 1 619.21 636.37 119.01 o 12 4 1 2.43 23.55 46.79 o -13 5 1 1295.18 1398.42 162.75 o -12 5 1 22.97 48.90 36.11 o -11 5 1 2278.60 2520.89 188.59 o -10 5 1 1437.99 1555.32 111.47 o -9 5 1 5.66 15.20 21.69 o -8 5 1 3796.50 3728.75 168.72 o -7 5 1 101.62 86.04 14.16 o -6 5 1 2428.94 2512.76 70.98 o -5 5 1 2289.46 2382.32 66.16 o -4 5 1 954.85 924.68 41.00 o -3 5 1 1333.38 1202.75 41.18 o -2 5 1 1184.58 1231.68 40.62 o -1 5 1 4592.14 4358.06 74.44 o 0 5 1 3539.62 3640.82 66.02 o 1 5 1 146.18 237.82 19.86 o 2 5 1 3268.61 3340.04 64.74 o 3 5 1 23.07 23.52 8.74 o 4 5 1 3435.49 3519.56 80.72 o 5 5 1 3459.04 3640.44 106.95 o 6 5 1 661.49 615.21 50.15 o 7 5 1 72.75 75.62 37.42 o 8 5 1 484.91 459.76 48.52 o 9 5 1 2709.33 2882.13 160.49 o 10 5 1 397.98 354.34 83.41 o 11 5 1 198.51 251.20 97.04 o 12 5 1 530.03 542.26 83.63 o -12 6 1 81.49 68.76 48.82 o -11 6 1 665.78 672.30 74.95 o -10 6 1 510.01 395.71 111.48 o -9 6 1 2179.60 2246.85 138.35 o -8 6 1 91.11 71.86 39.67 o -7 6 1 3530.97 3678.21 120.11 o -6 6 1 245.60 185.78 41.39 o -5 6 1 2430.27 2522.77 99.59 o -4 6 1 18.82 6.70 10.72 o -3 6 1 790.51 803.13 44.27 o -2 6 1 1731.10 1661.18 55.63 o -1 6 1 2920.09 2908.44 84.91 o 0 6 1 1083.12 1111.24 49.60 o 1 6 1 3457.28 3495.20 118.75 o 2 6 1 0.26 8.15 7.81 o 3 6 1 2699.42 2603.85 97.48 o 4 6 1 25.33 15.40 10.37 o 5 6 1 1753.18 1666.07 71.61 o 6 6 1 216.24 219.93 43.52 o 7 6 1 171.87 104.94 22.42 o 8 6 1 1540.45 1372.04 83.68 o 9 6 1 164.55 125.97 57.98 o 10 6 1 490.35 524.84 114.94 o 11 6 1 625.38 605.65 80.94 o -11 7 1 1067.75 1302.66 257.96 o -10 7 1 12.14 1.56 32.35 o -9 7 1 1036.67 1066.13 103.35 o -8 7 1 64.78 86.62 25.96 o -7 7 1 3.75 -6.88 18.42 o -6 7 1 15.82 21.14 14.58 o -5 7 1 1547.95 1641.61 81.43 o -4 7 1 423.17 498.37 44.13 o -3 7 1 6810.10 7013.14 154.86 o -2 7 1 53.07 28.82 10.66 o -1 7 1 7777.19 8181.71 168.33 o 0 7 1 256.13 205.66 19.44 o 1 7 1 1752.76 1669.42 65.97 o 2 7 1 165.02 112.51 16.67 o 3 7 1 505.53 460.75 30.21 o 4 7 1 46.18 45.58 12.61 o 5 7 1 1645.15 1662.97 74.36 o 6 7 1 8.97 -10.63 14.68 o 7 7 1 3799.98 3932.60 152.72 o 8 7 1 371.60 431.89 56.90 o 9 7 1 772.79 594.01 73.16 o 10 7 1 1.54 14.58 43.54 o 11 7 1 128.71 304.75 81.37 o -10 8 1 841.85 876.81 155.83 o -9 8 1 800.50 893.36 85.65 o -8 8 1 92.41 90.16 29.92 o -7 8 1 1649.42 1704.89 96.65 o -6 8 1 155.49 115.16 20.14 o -5 8 1 2747.72 2907.18 120.75 o -4 8 1 257.23 222.83 24.49 o -3 8 1 265.85 226.83 22.51 o -2 8 1 1807.30 1794.88 72.32 o -1 8 1 230.58 192.57 26.52 o 0 8 1 2030.81 2202.13 82.73 o 1 8 1 4601.88 4844.02 132.79 o 2 8 1 53.98 25.03 13.51 o 3 8 1 3287.36 3407.05 109.96 o 4 8 1 34.95 26.13 13.27 o 5 8 1 592.14 597.41 49.10 o 6 8 1 778.54 775.29 51.20 o 7 8 1 285.73 303.39 41.45 o 8 8 1 996.68 1022.95 86.76 o 9 8 1 28.94 34.38 52.89 o 10 8 1 93.78 95.21 48.42 o -8 9 1 2531.20 2716.90 190.01 o -7 9 1 10.04 20.19 35.90 o -6 9 1 2461.40 2614.57 106.95 o -5 9 1 96.17 101.79 20.11 o -4 9 1 390.09 329.43 29.31 o -3 9 1 1464.12 1389.78 67.75 o -2 9 1 64.85 67.98 16.20 o -1 9 1 1574.06 1525.11 68.94 o 0 9 1 289.85 273.85 26.91 o 1 9 1 550.11 451.42 40.75 o 2 9 1 2737.66 2776.16 103.08 o 3 9 1 85.98 9.79 21.32 o 4 9 1 1547.53 1750.91 81.28 o 5 9 1 568.40 609.74 44.42 o 6 9 1 374.00 377.33 36.47 o 7 9 1 137.53 154.08 38.11 o 8 9 1 12.65 6.64 38.90 o -7 10 1 1.50 -51.27 61.03 o -6 10 1 64.66 63.15 38.09 o -5 10 1 103.40 126.12 29.66 o -4 10 1 1292.45 1420.22 74.55 o -3 10 1 30.35 24.73 19.13 o -2 10 1 1330.80 1364.39 70.45 o -1 10 1 207.18 192.82 28.27 o 0 10 1 1600.35 1595.88 78.62 o 1 10 1 27.81 34.02 19.01 o 2 10 1 1198.55 1096.69 60.85 o 3 10 1 50.50 3.05 20.36 o 4 10 1 74.69 71.83 24.90 o 5 10 1 0.38 5.40 24.37 o 6 10 1 1596.98 1520.09 100.12 o 7 10 1 113.38 198.96 70.39 o -3 11 1 964.18 1107.34 148.10 o -2 11 1 43.21 18.71 26.33 o -1 11 1 618.15 612.94 55.95 o 0 11 1 550.65 584.84 52.95 o 1 11 1 167.43 190.83 52.62 o 2 11 1 508.93 510.35 55.79 o 3 11 1 9.15 31.87 30.95 o 4 11 1 550.03 409.72 68.35 o -14 0 2 1837.84 2241.56 152.55 o -12 0 2 1046.53 987.12 81.27 o -10 0 2 63.26 32.56 16.66 o -8 0 2 135.48 226.14 53.50 o -6 0 2 3183.97 2868.54 75.02 o -4 0 2 742.74 625.60 27.44 o -2 0 2 34221.80 33583.16 468.58 o 0 0 2 1194.90 1274.24 37.54 o 2 0 2 1518.27 1582.57 54.14 o 4 0 2 14290.25 13661.64 229.28 o 6 0 2 6432.17 6339.83 159.76 o 8 0 2 7198.90 7453.73 241.40 o 10 0 2 11.59 35.59 22.38 o 12 0 2 527.40 791.78 120.84 o -14 1 2 11.89 -21.11 24.37 o -13 1 2 72.23 62.17 21.67 o -12 1 2 748.80 679.93 46.62 o -11 1 2 180.15 199.04 51.97 o -10 1 2 1392.62 1447.67 58.61 o -9 1 2 14.45 8.28 9.23 o -8 1 2 5376.72 5342.63 102.66 o -7 1 2 749.73 758.75 30.20 o -6 1 2 2849.70 2885.12 58.11 o -5 1 2 3723.85 3479.39 55.14 o -4 1 2 944.29 986.31 25.13 o -3 1 2 524.14 471.76 15.28 o -2 1 2 16372.10 16276.92 233.77 o -1 1 2 6171.05 6014.62 78.70 o 0 1 2 37505.87 37526.62 335.41 o 1 1 2 1766.08 1930.68 39.53 o 2 1 2 40025.19 40389.46 367.54 o 3 1 2 7.95 16.82 7.11 o 4 1 2 1990.84 1833.30 49.84 o 5 1 2 6090.98 6330.76 107.07 o 6 1 2 540.89 511.00 28.87 o 7 1 2 1680.21 1647.49 56.29 o 8 1 2 5275.28 5266.24 124.87 o 9 1 2 979.87 897.63 52.05 o 10 1 2 3030.83 3076.30 124.71 o 11 1 2 41.62 30.45 20.47 o 12 1 2 746.60 826.95 68.50 o 13 1 2 277.73 250.94 146.68 o -14 2 2 800.78 868.99 84.18 o -13 2 2 230.88 234.96 37.83 o -12 2 2 631.56 669.12 42.78 o -11 2 2 2259.48 2272.17 90.89 o -10 2 2 178.62 152.85 17.51 o -9 2 2 5751.24 5863.87 128.60 o -8 2 2 636.88 599.63 38.56 o -7 2 2 2606.69 2401.75 57.77 o -6 2 2 995.49 881.97 31.24 o -5 2 2 604.18 590.38 23.02 o -4 2 2 2194.79 1968.78 39.39 o -3 2 2 899.34 746.59 23.43 o -2 2 2 149.22 202.84 11.99 o -1 2 2 1760.41 1740.46 31.17 o 0 2 2 1707.78 1798.51 31.74 o 1 2 2 8739.58 8670.44 102.98 o 2 2 2 56.21 52.25 9.60 o 3 2 2 1081.09 955.86 30.23 o 4 2 2 1960.21 1828.66 45.73 o 5 2 2 187.54 183.63 15.03 o 6 2 2 7094.24 7031.35 112.33 o 7 2 2 851.89 794.34 49.57 o 8 2 2 912.21 961.65 48.91 o 9 2 2 1618.48 1694.38 77.04 o 10 2 2 51.17 70.39 35.96 o 11 2 2 1913.89 2050.75 113.14 o 12 2 2 461.66 484.11 52.23 o 13 2 2 406.45 425.40 154.21 o -14 3 2 29.72 67.91 41.30 o -13 3 2 2597.68 2843.19 138.97 o -12 3 2 74.74 36.63 20.43 o -11 3 2 1919.78 1855.10 81.53 o -10 3 2 0.33 -12.19 12.19 o -9 3 2 345.79 291.03 55.75 o -8 3 2 1304.05 1216.22 55.30 o -7 3 2 3653.58 3450.74 73.39 o -6 3 2 34.15 37.79 8.09 o -5 3 2 10591.75 10545.18 120.56 o -4 3 2 454.67 492.81 24.02 o -3 3 2 15766.02 15125.50 162.13 o -2 3 2 5386.25 5648.08 80.69 o -1 3 2 5324.05 5402.02 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