#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:52:42 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181199 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/78/2227810.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227810_Fobs loop_ _publ_author_name 'Mangwala Kimpende, Peter' 'Van Meervelt, Luc' _publ_section_title ; Redetermination of {5-[(7-chloroquinolinium-4-yl)amino]-2-hydroxybenzyl}diethylammonium dichloride dihydrate ; _journal_coeditor_code LX2163 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2353 _journal_page_last o2354 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.784 _cell_angle_gamma 90.000 _cell_length_a 7.7622 _cell_length_b 26.8709 _cell_length_c 10.7085 _exptl_crystal_F_000 976.00 _reflns_d_resolution_high 0.8400 _cod_data_source_file lx2163Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' pm24 in P2(1)/c - new numbering' _shelx_refln_list_code 4 _shelx_f_calc_maximum 252.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1023.28 930.94 72.23 o 2 0 0 63558.98 62922.49 4484.07 o 3 0 0 4298.05 4501.19 271.81 o 4 0 0 883.99 793.73 51.55 o 5 0 0 2334.96 2183.18 154.57 o 6 0 0 1173.44 1120.11 57.32 o 7 0 0 1597.99 1531.32 104.64 o 8 0 0 3198.73 3379.24 242.44 o 9 0 0 59.59 64.07 7.55 o 1 1 0 14.92 0.98 2.28 o 2 1 0 68.07 67.03 6.72 o 3 1 0 232.17 208.35 14.64 o 4 1 0 380.28 363.73 23.22 o 5 1 0 264.57 240.19 26.81 o 6 1 0 636.54 635.01 23.19 o 7 1 0 37.13 35.91 3.83 o 8 1 0 40.51 61.42 5.16 o 9 1 0 119.62 143.50 11.40 o 0 2 0 1637.57 1403.10 109.57 o 1 2 0 2029.28 1877.78 86.51 o 2 2 0 3496.60 3074.10 145.49 o 3 2 0 750.26 807.16 34.71 o 4 2 0 4699.74 4725.38 195.77 o 5 2 0 371.57 336.69 35.10 o 6 2 0 32.01 32.45 4.45 o 7 2 0 67.59 55.61 5.33 o 8 2 0 49.29 58.66 5.28 o 9 2 0 108.96 121.13 8.29 o 1 3 0 4323.06 4799.75 249.63 o 2 3 0 3920.42 3862.05 207.18 o 3 3 0 7767.27 8272.79 343.03 o 4 3 0 369.88 389.96 20.77 o 5 3 0 1218.30 1113.49 54.69 o 6 3 0 139.08 157.23 15.32 o 7 3 0 33.35 25.67 3.68 o 8 3 0 189.85 214.78 12.14 o 9 3 0 288.60 327.70 18.61 o 0 4 0 2223.63 2007.04 141.10 o 1 4 0 1944.46 1802.22 87.78 o 2 4 0 1734.81 1810.91 87.49 o 3 4 0 31.92 31.34 4.97 o 4 4 0 2875.39 2968.86 133.52 o 5 4 0 552.77 494.52 47.76 o 6 4 0 548.81 535.21 28.87 o 7 4 0 109.55 90.51 7.76 o 8 4 0 754.40 797.12 43.79 o 9 4 0 35.27 33.86 4.62 o 1 5 0 1818.88 2185.23 108.73 o 2 5 0 2950.36 3223.32 156.04 o 3 5 0 896.17 871.49 41.29 o 4 5 0 1.01 6.06 5.69 o 5 5 0 381.69 305.06 23.33 o 6 5 0 201.88 196.72 14.73 o 7 5 0 23.59 23.60 6.42 o 8 5 0 65.15 72.09 6.05 o 9 5 0 862.03 813.76 42.97 o 0 6 0 14561.77 8203.52 768.14 o 1 6 0 175.60 204.75 17.72 o 2 6 0 55.16 55.02 8.86 o 3 6 0 1776.56 1746.92 74.12 o 4 6 0 934.15 966.01 46.26 o 5 6 0 59.71 90.13 14.22 o 6 6 0 53.06 46.23 4.40 o 7 6 0 90.14 99.86 10.17 o 8 6 0 530.84 559.43 28.09 o 9 6 0 257.50 264.40 19.92 o 1 7 0 7173.29 7097.62 395.17 o 2 7 0 18803.33 19664.91 932.87 o 3 7 0 5031.31 5439.92 249.25 o 4 7 0 3468.30 3883.39 172.94 o 5 7 0 2514.40 2450.31 114.92 o 6 7 0 57.89 53.07 4.85 o 7 7 0 8.05 5.97 3.22 o 8 7 0 523.65 533.28 29.88 o 9 7 0 6.76 7.02 4.12 o 0 8 0 14688.84 14559.30 1185.84 o 1 8 0 747.90 670.25 36.79 o 2 8 0 2511.49 2478.12 108.07 o 3 8 0 0.58 30.77 4.23 o 4 8 0 171.41 132.51 13.54 o 5 8 0 476.27 506.87 29.15 o 6 8 0 1213.13 1137.10 47.46 o 7 8 0 461.21 438.58 19.37 o 8 8 0 1531.86 1540.01 82.93 o 1 9 0 67.14 79.23 10.68 o 2 9 0 674.30 615.85 26.99 o 3 9 0 916.90 1079.71 49.52 o 4 9 0 133.44 124.03 10.51 o 5 9 0 882.68 939.23 67.48 o 6 9 0 28.62 29.27 3.77 o 7 9 0 142.67 161.96 12.71 o 8 9 0 340.62 341.47 23.02 o 0 10 0 7336.42 7538.33 392.88 o 1 10 0 74.39 39.74 6.16 o 2 10 0 2540.89 2349.19 92.86 o 3 10 0 18.22 41.81 8.13 o 4 10 0 1267.80 1084.88 65.00 o 5 10 0 264.86 246.12 14.19 o 6 10 0 791.86 799.93 39.63 o 7 10 0 166.15 186.34 12.38 o 8 10 0 501.02 540.48 27.44 o 1 11 0 237.25 178.40 12.63 o 2 11 0 1068.41 877.66 35.13 o 3 11 0 2397.46 2062.58 100.10 o 4 11 0 600.01 633.72 39.05 o 5 11 0 3529.19 3573.74 125.91 o 6 11 0 268.37 250.46 12.63 o 7 11 0 175.40 187.61 10.73 o 8 11 0 1.88 7.41 4.32 o 0 12 0 3805.06 3311.87 221.04 o 1 12 0 5.78 8.25 3.20 o 2 12 0 311.34 271.27 17.03 o 3 12 0 45.91 41.29 4.80 o 4 12 0 649.36 624.38 40.01 o 5 12 0 143.86 135.66 7.67 o 6 12 0 277.18 235.96 23.09 o 7 12 0 631.03 635.18 29.81 o 8 12 0 330.25 377.92 19.95 o 1 13 0 4498.51 4191.68 167.63 o 2 13 0 573.52 605.69 26.21 o 3 13 0 3766.26 3915.92 171.18 o 4 13 0 159.79 172.37 18.12 o 5 13 0 984.23 943.42 44.62 o 6 13 0 863.56 881.32 44.39 o 7 13 0 74.68 90.30 10.79 o 8 13 0 0.26 3.47 4.29 o 0 14 0 714.99 758.37 46.24 o 1 14 0 68.00 67.13 6.73 o 2 14 0 2.35 9.14 3.04 o 3 14 0 1516.44 1510.33 77.06 o 4 14 0 61.93 64.21 6.73 o 5 14 0 144.35 152.41 11.30 o 6 14 0 23.98 22.88 4.36 o 7 14 0 30.68 28.72 6.72 o 8 14 0 70.47 90.94 7.24 o 1 15 0 38.62 31.04 6.46 o 2 15 0 436.30 466.74 45.05 o 3 15 0 42.35 68.92 9.56 o 4 15 0 988.82 909.09 37.88 o 5 15 0 819.77 736.54 38.51 o 6 15 0 117.33 117.96 9.35 o 7 15 0 763.14 763.77 41.71 o 8 15 0 3.31 10.31 3.48 o 0 16 0 3098.37 2162.00 166.24 o 1 16 0 653.96 637.48 44.39 o 2 16 0 323.72 256.05 24.63 o 3 16 0 1476.15 1527.98 62.07 o 4 16 0 890.30 828.70 34.99 o 5 16 0 593.89 528.14 21.10 o 6 16 0 0.22 0.95 3.76 o 7 16 0 102.48 108.53 9.38 o 1 17 0 830.29 884.85 77.10 o 2 17 0 484.58 451.67 24.54 o 3 17 0 4089.29 3531.73 128.88 o 4 17 0 284.34 278.13 17.43 o 5 17 0 2106.35 1959.19 76.61 o 6 17 0 14.42 27.30 5.57 o 7 17 0 557.30 536.13 29.39 o 0 18 0 8410.65 8340.95 593.84 o 1 18 0 1090.30 1108.26 60.88 o 2 18 0 4656.93 4421.13 157.65 o 3 18 0 69.68 54.65 5.61 o 4 18 0 63.67 63.57 7.23 o 5 18 0 121.70 128.12 7.59 o 6 18 0 978.12 951.07 43.20 o 7 18 0 757.52 749.67 41.03 o 1 19 0 804.46 800.10 28.65 o 2 19 0 536.18 492.58 29.96 o 3 19 0 1312.08 1107.23 40.14 o 4 19 0 14.32 11.52 3.44 o 5 19 0 2828.47 2818.75 122.52 o 6 19 0 374.00 373.07 18.20 o 7 19 0 3.26 5.86 3.34 o 0 20 0 738.65 743.21 34.84 o 1 20 0 943.33 933.13 32.08 o 2 20 0 1175.50 1102.59 37.46 o 3 20 0 1310.93 1273.19 50.76 o 4 20 0 72.48 78.54 5.24 o 5 20 0 123.52 140.26 7.53 o 6 20 0 263.11 273.95 16.18 o 7 20 0 0.26 4.43 3.22 o 1 21 0 2780.97 2656.73 95.19 o 2 21 0 516.84 516.13 21.54 o 3 21 0 7.18 8.11 2.83 o 4 21 0 0.07 1.45 2.94 o 5 21 0 42.97 53.99 4.32 o 6 21 0 0.56 2.60 3.30 o 0 22 0 25221.46 21356.82 1002.06 o 1 22 0 0.39 6.26 2.31 o 2 22 0 4862.41 4899.33 168.71 o 3 22 0 369.51 401.68 16.95 o 4 22 0 176.04 216.43 10.79 o 5 22 0 574.57 584.14 25.25 o 6 22 0 15.89 24.10 3.75 o 1 23 0 2415.15 2424.02 88.79 o 2 23 0 1330.37 1272.47 46.95 o 3 23 0 236.80 242.17 11.44 o 4 23 0 7.13 13.67 3.35 o 5 23 0 32.08 34.40 4.38 o 6 23 0 281.03 269.63 15.28 o 0 24 0 61.13 66.20 6.27 o 1 24 0 73.21 84.74 6.74 o 2 24 0 242.93 241.25 9.69 o 3 24 0 59.40 75.70 5.27 o 4 24 0 619.92 626.48 26.74 o 5 24 0 184.80 195.34 11.74 o 6 24 0 51.74 62.12 5.57 o 1 25 0 413.19 391.83 15.65 o 2 25 0 594.89 548.80 19.92 o 3 25 0 1549.61 1576.38 68.57 o 4 25 0 159.67 170.05 10.69 o 5 25 0 1295.02 1347.28 69.66 o 0 26 0 2069.25 2178.08 113.93 o 1 26 0 1366.66 1336.73 49.52 o 2 26 0 43.32 54.94 3.97 o 3 26 0 284.46 281.35 12.74 o 4 26 0 165.61 173.45 11.59 o 5 26 0 168.66 188.27 12.01 o 1 27 0 2.64 4.38 2.42 o 2 27 0 0.23 3.90 2.54 o 3 27 0 18.72 27.70 4.26 o 4 27 0 0.14 0.09 3.00 o 0 28 0 5708.97 5748.00 338.75 o 1 28 0 9.12 13.40 3.54 o 2 28 0 1014.09 1067.72 50.99 o 3 28 0 182.80 193.53 12.86 o 4 28 0 371.08 414.72 28.87 o 1 29 0 505.31 532.22 25.96 o 2 29 0 1219.11 1242.82 64.40 o 3 29 0 1025.73 1078.22 62.25 o 0 30 0 1610.59 1649.20 136.86 o 1 30 0 170.16 185.13 12.45 o 2 30 0 220.10 211.85 12.14 o 3 30 0 546.57 518.17 35.26 o 1 31 0 289.42 315.96 19.19 o 2 31 0 348.31 352.46 18.78 o -9 1 1 20.82 22.59 4.18 o -8 1 1 514.61 523.95 21.58 o -7 1 1 1247.26 1280.48 55.37 o -6 1 1 1228.71 1281.60 45.36 o -5 1 1 8.52 12.59 5.76 o -4 1 1 1287.38 1462.23 62.32 o -3 1 1 301.40 357.90 17.57 o -2 1 1 1928.98 2212.55 104.19 o -1 1 1 8159.81 8427.44 375.31 o 0 1 1 3433.70 3211.32 157.16 o 1 1 1 520.42 481.60 25.96 o 2 1 1 7506.80 8198.99 393.64 o 3 1 1 1295.01 1415.46 70.61 o 4 1 1 678.83 590.75 45.06 o 5 1 1 27.97 26.23 7.78 o 6 1 1 638.11 627.77 38.86 o 7 1 1 187.07 200.23 9.75 o 8 1 1 27.93 30.62 3.88 o 9 1 1 48.55 69.62 12.00 o -9 2 1 21.22 31.46 5.51 o -8 2 1 53.62 56.10 7.15 o -7 2 1 69.74 76.17 5.56 o -6 2 1 1843.03 1894.69 68.06 o -5 2 1 561.33 563.63 40.91 o -4 2 1 7736.88 7756.27 331.08 o -3 2 1 3710.15 4583.74 206.87 o -2 2 1 13669.95 15116.48 707.97 o -1 2 1 3482.33 3708.17 170.82 o 0 2 1 831.09 793.40 38.52 o 1 2 1 547.77 521.79 30.20 o 2 2 1 29715.72 28969.58 1372.95 o 3 2 1 1499.04 1609.53 69.67 o 4 2 1 7357.05 7891.72 336.58 o 5 2 1 2.29 9.51 6.09 o 6 2 1 592.13 542.68 37.49 o 7 2 1 1040.03 956.34 38.51 o 8 2 1 22.22 30.74 3.90 o 9 2 1 48.29 49.40 6.03 o -9 3 1 399.70 461.32 24.71 o -8 3 1 191.44 188.13 9.59 o -7 3 1 520.20 525.04 22.51 o -6 3 1 213.33 236.41 22.92 o -5 3 1 55.79 72.49 7.90 o -4 3 1 12005.86 12356.72 562.04 o -3 3 1 7522.30 8599.44 368.54 o -2 3 1 27991.80 31308.40 1492.18 o -1 3 1 791.93 726.34 37.20 o 0 3 1 4083.95 4099.19 218.20 o 1 3 1 3279.95 2547.45 132.93 o 2 3 1 14403.96 17215.62 864.80 o 3 3 1 87.15 105.32 11.07 o 4 3 1 4152.76 3834.30 165.06 o 5 3 1 3.26 5.66 4.32 o 6 3 1 3344.07 2925.26 102.07 o 7 3 1 535.76 460.59 19.40 o 8 3 1 2220.27 1995.10 110.72 o 9 3 1 152.62 168.16 12.11 o -9 4 1 46.50 49.52 5.72 o -8 4 1 188.59 223.98 12.28 o -7 4 1 1532.61 1578.11 68.43 o -6 4 1 289.67 271.65 23.10 o -5 4 1 8023.81 8806.38 457.59 o -4 4 1 4120.46 3731.00 160.35 o -3 4 1 2806.44 3056.69 124.23 o -2 4 1 197.58 267.88 19.42 o -1 4 1 107.19 77.11 8.67 o 0 4 1 325.15 305.15 25.54 o 1 4 1 1004.22 1051.91 49.32 o 2 4 1 4908.53 4633.55 332.92 o 3 4 1 6896.35 7149.23 315.71 o 4 4 1 5735.99 6105.14 321.92 o 5 4 1 1165.06 1228.36 67.18 o 6 4 1 112.07 122.75 8.23 o 7 4 1 413.06 402.86 17.25 o 8 4 1 425.24 461.13 25.79 o 9 4 1 213.30 230.25 21.05 o -9 5 1 371.95 417.21 20.50 o -8 5 1 219.80 188.86 15.57 o -7 5 1 209.55 185.56 15.19 o -6 5 1 862.70 804.70 42.92 o -5 5 1 1415.49 1454.33 74.89 o -4 5 1 435.61 465.31 24.35 o -3 5 1 247.36 296.43 16.54 o -2 5 1 4392.13 4610.71 243.11 o -1 5 1 600.68 625.73 34.18 o 0 5 1 9248.26 8447.02 444.89 o 1 5 1 26.63 18.73 4.32 o 2 5 1 106.19 98.33 11.19 o 3 5 1 47.08 54.92 4.81 o 4 5 1 2528.55 2644.72 116.67 o 5 5 1 1.67 11.29 8.77 o 6 5 1 1652.62 1578.09 56.56 o 7 5 1 646.71 660.56 35.82 o 8 5 1 8.20 12.59 4.27 o 9 5 1 401.64 410.65 30.48 o -9 6 1 616.96 667.57 32.76 o -8 6 1 81.13 70.52 7.70 o -7 6 1 1255.78 1265.96 60.57 o -6 6 1 613.08 669.52 30.81 o -5 6 1 746.28 725.72 51.83 o -4 6 1 0.26 7.74 4.40 o -3 6 1 394.26 311.30 22.07 o -2 6 1 8097.68 8249.62 413.19 o -1 6 1 3117.79 3273.69 146.84 o 0 6 1 11.14 8.91 3.23 o 1 6 1 7560.35 8337.77 502.79 o 2 6 1 1724.95 1770.34 91.78 o 3 6 1 1266.99 1193.53 57.66 o 4 6 1 187.76 179.56 12.43 o 5 6 1 23.55 11.04 7.26 o 6 6 1 461.43 443.25 23.45 o 7 6 1 123.74 128.93 10.69 o 8 6 1 383.97 395.41 22.68 o 9 6 1 330.71 378.96 28.42 o -9 7 1 343.78 330.63 18.71 o -8 7 1 88.50 90.11 9.04 o -7 7 1 181.79 170.08 13.71 o -6 7 1 18.89 19.00 3.39 o -5 7 1 922.77 934.95 49.52 o -4 7 1 1943.32 2224.75 105.61 o -3 7 1 22.19 25.37 3.80 o -2 7 1 13769.19 14569.26 626.46 o -1 7 1 252.26 243.82 29.43 o 0 7 1 681.66 748.29 41.99 o 1 7 1 5189.00 4923.29 247.79 o 2 7 1 1818.80 1762.01 89.00 o 3 7 1 865.52 909.77 40.78 o 4 7 1 3274.78 3464.80 160.24 o 5 7 1 58.58 42.49 9.48 o 6 7 1 1223.23 1164.67 52.08 o 7 7 1 331.75 344.58 18.10 o 8 7 1 644.65 560.60 41.91 o -8 8 1 23.98 32.42 4.61 o -7 8 1 647.75 689.06 29.36 o -6 8 1 2975.36 2851.96 116.45 o -5 8 1 1969.62 1957.97 71.62 o -4 8 1 454.41 376.52 21.74 o -3 8 1 776.35 714.75 30.87 o -2 8 1 2616.22 2980.11 125.83 o -1 8 1 15.73 13.95 5.87 o 0 8 1 1034.11 1029.79 57.48 o 1 8 1 1593.47 1537.28 80.82 o 2 8 1 3.62 10.72 3.71 o 3 8 1 32.52 16.03 3.89 o 4 8 1 60.83 39.04 6.25 o 5 8 1 329.74 306.52 15.97 o 6 8 1 643.20 672.58 31.08 o 7 8 1 393.36 393.80 21.33 o 8 8 1 153.50 174.17 12.87 o -8 9 1 425.94 413.48 22.56 o -7 9 1 913.57 938.74 38.94 o -6 9 1 3902.32 3625.57 146.59 o -5 9 1 749.28 813.29 38.85 o -4 9 1 14.03 15.47 6.46 o -3 9 1 1888.57 2044.20 85.30 o -2 9 1 339.27 296.54 16.69 o -1 9 1 2796.01 2839.14 122.73 o 0 9 1 1289.07 1361.73 70.17 o 1 9 1 13979.47 14049.56 765.94 o 2 9 1 1330.12 1174.22 53.71 o 3 9 1 710.49 717.80 33.43 o 4 9 1 65.79 85.96 8.59 o 5 9 1 1202.31 1267.84 46.09 o 6 9 1 518.34 539.75 25.13 o 7 9 1 389.75 435.89 22.74 o 8 9 1 13.89 14.04 4.62 o -8 10 1 8.67 19.54 4.86 o -7 10 1 138.03 145.28 13.02 o -6 10 1 182.20 191.62 12.71 o -5 10 1 25.49 26.55 6.56 o -4 10 1 6964.21 7261.96 309.17 o -3 10 1 1077.81 1188.24 51.06 o -2 10 1 34.31 56.81 4.97 o -1 10 1 5432.11 5531.20 214.85 o 0 10 1 740.03 787.95 35.24 o 1 10 1 1141.10 1012.32 39.14 o 2 10 1 271.29 236.93 15.19 o 3 10 1 22.00 18.84 6.63 o 4 10 1 4669.28 4529.55 236.52 o 5 10 1 765.00 834.73 38.34 o 6 10 1 16.07 15.42 3.71 o 7 10 1 541.43 528.66 29.82 o 8 10 1 2.60 4.11 3.87 o -8 11 1 41.63 45.16 5.53 o -7 11 1 276.53 284.25 18.92 o -6 11 1 168.14 182.73 10.50 o -5 11 1 36.65 42.09 5.47 o -4 11 1 865.89 916.97 46.00 o -3 11 1 481.86 516.42 26.49 o -2 11 1 4473.23 4671.87 194.93 o -1 11 1 4263.42 3954.32 155.22 o 0 11 1 7089.62 4803.71 318.14 o 1 11 1 170.02 127.09 10.14 o 2 11 1 686.42 628.15 27.17 o 3 11 1 1138.94 1117.53 50.02 o 4 11 1 621.02 621.28 59.89 o 5 11 1 89.24 84.87 10.72 o 6 11 1 1342.43 1430.51 68.02 o 7 11 1 0.10 9.82 4.77 o 8 11 1 390.63 383.93 22.83 o -8 12 1 405.89 424.76 23.93 o -7 12 1 412.27 471.44 20.60 o -6 12 1 40.77 33.97 4.21 o -5 12 1 249.25 235.70 17.88 o -4 12 1 471.42 489.73 28.80 o -3 12 1 3022.84 2927.86 119.92 o -2 12 1 14.24 29.55 4.56 o -1 12 1 8174.97 8166.84 371.11 o 0 12 1 461.69 416.70 24.70 o 1 12 1 287.04 254.60 18.54 o 2 12 1 96.06 134.82 8.12 o 3 12 1 3263.50 3148.94 130.34 o 4 12 1 220.52 199.06 16.78 o 5 12 1 979.29 969.09 43.66 o 6 12 1 4.21 5.69 4.42 o 7 12 1 198.26 218.78 14.40 o 8 12 1 142.55 143.06 10.19 o -8 13 1 1.35 5.31 3.30 o -7 13 1 314.90 328.88 17.73 o -6 13 1 13.31 10.95 3.81 o -5 13 1 356.79 353.36 14.07 o -4 13 1 1284.52 1184.40 66.20 o -3 13 1 2.71 21.58 4.34 o -2 13 1 1052.42 1029.12 44.19 o -1 13 1 1123.13 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