#------------------------------------------------------------------------------ #$Date: 2010-12-22 21:36:50 +0200 (Wed, 22 Dec 2010) $ #$Revision: 5269 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2227816.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227816_Fobs loop_ _publ_author_name 'Jasinski, Jerry P.' 'Butcher, Ray J.' 'Chidan Kumar, C. S.' 'Yathirajan, H. S.' 'Mayekar, A. N.' _publ_section_title ; (2E)-1-(3-Bromophenyl)-3-(4,5-dimethoxy-2-nitrophenyl)prop-2-en-1-one ; _journal_coeditor_code LX2178 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2936 _journal_page_last o2937 _journal_volume 66 _journal_year 2010 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.8547 _cell_length_b 8.3205 _cell_length_c 27.1509 _exptl_crystal_F_000 792.00 _reflns_d_resolution_high 0.8016 _[local]_cod_data_source_file lx2178Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' hsy323a in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 239.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 30825.41 30718.77 113.82 o 4 0 0 16016.59 16146.78 85.29 o 6 0 0 8399.10 7762.26 33.93 o 8 0 0 13.58 16.62 7.20 o 1 1 0 1304.85 1228.85 7.02 o 2 1 0 1022.07 1068.91 19.75 o 3 1 0 3285.69 3079.84 18.23 o 4 1 0 2402.52 2420.62 31.57 o 5 1 0 11.99 11.86 1.92 o 6 1 0 1555.69 1407.60 16.57 o 7 1 0 354.10 406.20 13.02 o 8 1 0 2.03 17.13 5.54 o 0 2 0 3429.72 3986.33 88.90 o 1 2 0 7120.04 7704.20 28.19 o 2 2 0 3525.40 3837.32 40.05 o 3 2 0 151.84 159.72 6.96 o 4 2 0 3394.26 3203.43 28.91 o 5 2 0 1064.66 1045.57 23.60 o 6 2 0 1484.23 1471.54 21.76 o 7 2 0 248.82 253.53 7.34 o 8 2 0 15.65 32.21 3.52 o 1 3 0 2169.36 2354.41 21.60 o 2 3 0 5124.35 5707.11 41.54 o 3 3 0 959.59 1072.49 23.81 o 4 3 0 925.09 847.95 21.32 o 5 3 0 477.79 479.97 13.83 o 6 3 0 424.88 462.08 7.44 o 7 3 0 74.97 90.50 3.99 o 8 3 0 115.13 76.99 4.98 o 0 4 0 1781.17 1813.90 22.71 o 1 4 0 3377.18 3428.93 120.19 o 2 4 0 204.77 201.42 11.35 o 3 4 0 27.59 25.41 5.74 o 4 4 0 26.12 19.63 5.08 o 5 4 0 1351.38 1352.48 12.77 o 6 4 0 261.01 278.38 8.00 o 7 4 0 151.70 122.85 18.55 o 1 5 0 311.60 360.70 24.37 o 2 5 0 1701.57 1275.36 103.02 o 3 5 0 72.37 106.62 5.72 o 4 5 0 462.62 429.19 8.47 o 5 5 0 187.48 180.22 7.63 o 6 5 0 53.33 59.48 5.92 o 7 5 0 2.63 9.29 3.31 o 0 6 0 406.66 401.31 36.28 o 1 6 0 3297.78 3351.16 85.25 o 2 6 0 104.43 70.22 8.07 o 3 6 0 716.49 666.04 10.94 o 4 6 0 223.74 235.66 8.02 o 5 6 0 4306.22 4692.02 197.70 o 6 6 0 53.91 68.23 5.44 o 1 7 0 91.10 87.84 6.85 o 2 7 0 2353.96 2395.20 19.94 o 3 7 0 2027.46 2135.01 17.61 o 4 7 0 1207.18 1409.78 27.69 o 5 7 0 163.40 228.85 6.45 o 6 7 0 153.51 139.65 3.92 o 0 8 0 1469.73 1309.89 21.05 o 1 8 0 1394.85 1221.04 19.94 o 2 8 0 68.40 64.42 4.00 o 3 8 0 124.89 116.26 7.20 o 4 8 0 233.59 253.38 8.31 o 5 8 0 226.99 250.12 3.66 o 1 9 0 807.12 737.91 11.08 o 2 9 0 182.81 218.75 15.35 o 3 9 0 886.30 962.16 18.83 o 4 9 0 89.32 98.03 4.98 o 0 10 0 114.65 131.82 6.65 o 1 10 0 1.02 0.55 3.31 o 1 0 1 3329.32 3587.51 51.07 o 2 0 1 57443.91 53867.12 613.71 o 3 0 1 771.28 765.43 25.47 o 4 0 1 4735.25 4966.62 35.72 o 5 0 1 3699.97 3381.97 88.36 o 6 0 1 116.16 184.76 23.55 o 7 0 1 217.83 251.84 4.68 o 8 0 1 174.76 158.50 6.27 o -8 1 1 1500.56 1937.97 20.49 o -7 1 1 59.77 64.88 5.20 o -6 1 1 1308.44 1230.90 22.15 o -5 1 1 209.76 217.59 7.53 o -4 1 1 6362.76 6340.86 45.73 o -3 1 1 1044.85 1126.06 16.47 o -2 1 1 45471.21 44434.32 513.09 o -1 1 1 1007.60 1217.92 40.16 o 0 1 1 134.28 147.49 2.44 o 1 1 1 925.21 1096.40 19.74 o 2 1 1 47025.66 45201.52 427.67 o 3 1 1 1009.34 1131.39 30.58 o 4 1 1 6468.91 6162.01 57.90 o 5 1 1 213.97 218.75 5.75 o 6 1 1 1380.26 1282.71 30.51 o 7 1 1 51.68 57.20 6.49 o 8 1 1 1583.09 1940.18 20.49 o -8 2 1 150.73 184.15 15.73 o -7 2 1 179.07 189.66 7.38 o -6 2 1 306.70 299.05 5.15 o -5 2 1 823.47 786.11 16.17 o -4 2 1 1095.34 964.02 16.79 o -3 2 1 1271.87 1361.32 68.91 o -2 2 1 1533.29 1654.13 9.87 o -1 2 1 4010.94 4334.14 11.64 o 0 2 1 14959.02 15722.08 52.06 o 1 2 1 4093.73 4322.26 20.95 o 2 2 1 1562.34 1629.34 17.11 o 3 2 1 1187.80 1288.42 46.84 o 4 2 1 1117.37 1003.10 17.57 o 5 2 1 782.12 756.27 15.91 o 6 2 1 274.87 268.81 8.44 o 7 2 1 179.25 184.83 12.18 o 8 2 1 152.10 191.41 15.72 o -8 3 1 149.99 91.39 5.54 o -7 3 1 269.77 314.72 9.43 o -6 3 1 35.50 28.55 3.54 o -5 3 1 22.03 23.41 3.50 o -4 3 1 1169.31 1197.45 28.80 o -3 3 1 1763.81 1928.70 124.95 o -2 3 1 2482.31 2857.06 68.99 o -1 3 1 871.04 917.38 42.65 o 0 3 1 437.04 413.63 9.97 o 1 3 1 924.60 876.80 41.97 o 2 3 1 2422.40 2840.34 44.37 o 3 3 1 1960.87 1958.44 89.21 o 4 3 1 1258.26 1226.25 27.69 o 5 3 1 22.36 22.64 2.84 o 6 3 1 43.36 33.32 3.59 o 7 3 1 289.51 327.02 5.84 o 8 3 1 172.56 106.90 5.54 o -7 4 1 2.86 0.55 3.92 o -6 4 1 584.97 674.89 17.63 o -5 4 1 356.12 377.21 7.48 o -4 4 1 1041.28 1035.92 28.72 o -3 4 1 1039.06 1075.75 39.59 o -2 4 1 592.71 624.51 43.92 o -1 4 1 77.78 97.95 9.97 o 0 4 1 4817.98 5320.93 73.11 o 1 4 1 120.37 149.02 9.78 o 2 4 1 612.88 585.83 50.36 o 3 4 1 1042.12 1050.74 61.76 o 4 4 1 1056.64 1053.19 35.26 o 5 4 1 339.56 340.72 6.66 o 6 4 1 615.55 679.18 21.39 o 7 4 1 3.20 2.44 3.10 o -7 5 1 539.48 588.58 8.86 o -6 5 1 50.32 49.88 7.83 o -5 5 1 69.30 61.30 4.72 o -4 5 1 149.74 137.72 5.36 o -3 5 1 5194.05 4820.84 70.99 o -2 5 1 284.93 309.99 46.80 o -1 5 1 2855.96 2800.52 50.12 o 0 5 1 562.26 640.83 9.92 o 1 5 1 2905.34 2981.63 51.23 o 2 5 1 287.66 266.85 50.96 o 3 5 1 5173.31 5059.09 146.38 o 4 5 1 147.38 146.27 7.19 o 5 5 1 68.87 65.85 7.43 o 6 5 1 49.59 46.85 7.91 o -6 6 1 477.40 622.64 49.64 o -5 6 1 543.55 597.19 22.14 o -4 6 1 983.96 983.07 31.99 o -3 6 1 575.02 614.79 14.40 o -2 6 1 900.86 877.04 15.98 o -1 6 1 1485.45 1552.05 44.19 o 0 6 1 6355.34 6737.61 32.62 o 1 6 1 1473.89 1547.61 72.07 o 2 6 1 984.91 925.44 17.75 o 3 6 1 597.81 635.12 14.79 o 4 6 1 939.61 935.67 21.23 o 5 6 1 538.35 588.43 28.86 o 6 6 1 498.25 627.09 50.44 o -6 7 1 211.15 238.16 6.09 o -5 7 1 141.98 183.74 17.66 o -4 7 1 13.82 27.77 4.45 o -3 7 1 4241.91 4382.13 112.67 o -2 7 1 492.98 510.98 13.26 o -1 7 1 1908.11 1812.30 13.47 o 0 7 1 176.64 147.98 6.42 o 1 7 1 1892.01 1872.05 49.09 o 2 7 1 505.96 526.74 17.10 o 3 7 1 4134.55 4350.36 118.85 o 4 7 1 6.59 17.64 4.21 o 5 7 1 143.67 174.42 12.15 o 6 7 1 229.99 238.41 6.32 o -5 8 1 747.58 891.80 18.13 o -4 8 1 212.45 236.51 11.62 o -3 8 1 348.65 341.29 24.70 o -2 8 1 92.32 84.82 5.11 o -1 8 1 981.03 960.76 31.55 o 0 8 1 463.17 441.25 9.59 o 1 8 1 890.64 831.39 9.19 o 2 8 1 98.94 90.97 3.77 o 3 8 1 356.45 351.74 28.86 o 4 8 1 193.09 214.03 7.91 o 5 8 1 727.99 836.05 21.32 o -4 9 1 267.93 298.53 6.65 o -3 9 1 75.53 87.32 3.94 o -2 9 1 586.14 646.24 37.09 o -1 9 1 102.62 77.27 5.82 o 0 9 1 2.63 3.56 4.49 o 1 9 1 85.70 64.19 9.69 o 2 9 1 619.74 623.93 32.18 o 3 9 1 93.85 101.44 8.60 o 4 9 1 265.29 307.91 4.98 o -1 10 1 411.42 482.42 8.86 o 0 10 1 78.15 67.59 6.09 o 1 10 1 418.82 479.76 9.97 o 1 0 2 544.24 537.84 5.10 o 2 0 2 7749.67 7406.84 41.25 o 3 0 2 9.43 3.29 1.96 o 4 0 2 1588.42 1430.16 112.16 o 5 0 2 1.92 9.88 2.13 o 6 0 2 1294.92 1244.73 14.70 o 7 0 2 125.99 108.03 3.67 o 8 0 2 0.67 -1.38 4.71 o -8 1 2 353.16 466.35 11.08 o -7 1 2 599.86 666.30 9.97 o -6 1 2 812.69 756.16 11.67 o -5 1 2 298.61 278.87 8.75 o -4 1 2 4388.97 4346.41 90.66 o -3 1 2 7824.52 7736.78 208.24 o -2 1 2 2964.41 3061.55 52.02 o -1 1 2 6413.70 6866.69 31.30 o 0 1 2 10353.61 11244.80 381.06 o 1 1 2 6317.18 6444.87 32.61 o 2 1 2 3044.08 3087.99 76.29 o 3 1 2 7561.18 7544.01 243.99 o 4 1 2 4211.00 4258.82 77.26 o 5 1 2 307.80 288.94 7.13 o 6 1 2 849.43 803.94 22.06 o 7 1 2 600.38 675.16 14.95 o 8 1 2 348.78 441.98 11.08 o -8 2 2 69.36 94.62 13.21 o -7 2 2 132.63 140.28 12.96 o -6 2 2 1320.79 1322.92 11.72 o -5 2 2 420.92 387.90 7.83 o -4 2 2 1318.86 1207.41 18.36 o -3 2 2 567.69 628.71 9.81 o -2 2 2 408.99 404.98 8.15 o -1 2 2 233.14 299.14 10.57 o 0 2 2 24282.28 26205.24 78.37 o 1 2 2 378.53 487.54 10.74 o 2 2 2 504.12 494.94 10.47 o 3 2 2 538.35 613.20 9.83 o 4 2 2 1331.90 1210.19 25.48 o 5 2 2 461.04 424.80 11.28 o 6 2 2 1397.13 1401.33 17.41 o 7 2 2 160.48 152.92 10.82 o 8 2 2 71.28 87.87 8.83 o -8 3 2 202.89 217.96 33.23 o -7 3 2 157.38 190.20 6.60 o -6 3 2 40.53 37.52 3.59 o -5 3 2 157.07 154.17 3.97 o -4 3 2 1236.22 1097.14 18.80 o -3 3 2 1963.33 1868.41 24.65 o -2 3 2 3297.44 3498.49 101.13 o -1 3 2 1647.48 1885.05 87.02 o 0 3 2 19.98 22.75 3.92 o 1 3 2 1849.86 1834.83 118.43 o 2 3 2 3350.75 3585.49 75.79 o 3 3 2 1971.87 1939.47 23.07 o 4 3 2 1275.14 1153.99 20.10 o 5 3 2 141.60 128.05 6.69 o 6 3 2 32.55 30.86 3.65 o 7 3 2 143.83 168.61 7.67 o -7 4 2 179.04 147.70 22.93 o -6 4 2 117.29 140.63 8.01 o -5 4 2 1837.85 1892.17 27.87 o -4 4 2 286.68 291.80 9.19 o -3 4 2 300.36 308.47 10.83 o -2 4 2 645.89 628.03 34.08 o -1 4 2 5767.46 6092.40 234.84 o 0 4 2 2068.63 2502.15 87.06 o 1 4 2 5720.09 5918.24 190.29 o 2 4 2 653.52 591.55 38.24 o 3 4 2 284.49 275.06 10.89 o 4 4 2 282.86 276.98 9.25 o 5 4 2 1677.35 1698.54 39.89 o 6 4 2 106.16 115.67 6.18 o 7 4 2 156.64 109.34 31.65 o -7 5 2 58.74 62.28 3.71 o -6 5 2 225.04 225.59 25.66 o -5 5 2 10.40 7.88 4.03 o -4 5 2 1313.29 1286.00 23.26 o -3 5 2 411.75 407.46 22.15 o -2 5 2 4170.25 3893.11 45.42 o -1 5 2 465.18 445.88 11.73 o 0 5 2 141.33 105.48 4.62 o 1 5 2 446.38 464.05 12.46 o 2 5 2 4203.92 4105.79 47.08 o 3 5 2 405.04 424.67 19.48 o 4 5 2 1305.60 1270.04 14.26 o 5 5 2 12.45 11.72 4.14 o 6 5 2 233.93 224.11 30.52 o 7 5 2 60.88 61.32 4.15 o -6 6 2 61.78 60.92 6.92 o -5 6 2 1200.11 1317.52 67.23 o -4 6 2 99.45 105.69 5.63 o -3 6 2 890.09 830.58 45.97 o -2 6 2 234.37 228.10 6.13 o -1 6 2 2319.84 2341.88 36.58 o 0 6 2 188.13 242.30 7.51 o 1 6 2 2433.25 2542.08 64.32 o 2 6 2 233.16 230.74 9.77 o 3 6 2 836.00 823.32 18.60 o 4 6 2 87.98 97.63 6.43 o 5 6 2 1064.86 1181.99 61.72 o 6 6 2 59.88 59.18 3.92 o -6 7 2 47.63 55.72 7.75 o -5 7 2 445.87 501.55 33.09 o -4 7 2 273.37 308.56 11.87 o -3 7 2 1742.04 1839.28 33.83 o -2 7 2 1430.90 1354.64 29.82 o -1 7 2 4335.51 4276.65 79.86 o 0 7 2 54.15 60.34 5.21 o 1 7 2 4556.41 4469.28 100.69 o 2 7 2 1499.77 1378.44 29.93 o 3 7 2 1724.97 1828.46 68.57 o 4 7 2 336.00 383.61 17.67 o 5 7 2 432.83 488.64 23.90 o 6 7 2 48.07 45.17 3.31 o -5 8 2 528.17 629.74 8.31 o -4 8 2 237.44 272.35 14.27 o -3 8 2 57.10 57.23 9.23 o -2 8 2 245.96 239.66 7.01 o -1 8 2 657.85 646.74 18.63 o 0 8 2 639.14 602.73 10.76 o 1 8 2 698.25 639.78 10.76 o 2 8 2 265.15 251.27 7.61 o 3 8 2 62.32 62.75 8.13 o 4 8 2 251.88 291.10 12.98 o 5 8 2 587.07 645.84 15.51 o -4 9 2 77.65 86.96 4.98 o -3 9 2 490.53 577.76 18.12 o -2 9 2 69.94 68.16 9.83 o -1 9 2 209.42 177.19 9.97 o 0 9 2 1.42 5.54 4.31 o 1 9 2 172.24 173.54 11.91 o 2 9 2 56.22 40.72 5.16 o 3 9 2 488.13 530.73 19.55 o 4 9 2 73.07 81.43 6.92 o -1 10 2 7.57 2.77 3.13 o 0 10 2 563.99 579.76 13.02 o 1 10 2 7.84 3.60 3.13 o 2 10 2 49.10 57.60 3.88 o 1 0 3 6629.85 6520.81 138.47 o 2 0 3 4351.66 4786.72 24.10 o 3 0 3 2058.15 2178.04 42.06 o 4 0 3 2129.14 2128.11 27.42 o 5 0 3 1328.27 1138.37 36.76 o 6 0 3 69.22 72.07 6.94 o 7 0 3 60.36 62.45 3.59 o 8 0 3 27.59 27.34 5.09 o -8 1 3 168.82 272.50 8.86 o -7 1 3 9.71 19.43 3.23 o -6 1 3 69.21 73.98 3.72 o -5 1 3 32.18 31.24 2.11 o -4 1 3 3008.75 2796.56 104.41 o -3 1 3 699.04 665.58 6.81 o -2 1 3 3996.56 3764.90 80.42 o -1 1 3 2108.00 2297.63 23.27 o 0 1 3 2227.08 2552.61 128.22 o 1 1 3 2277.43 2254.70 76.78 o 2 1 3 3898.22 3527.62 47.37 o 3 1 3 744.72 727.59 13.89 o 4 1 3 3378.85 2979.28 203.82 o 5 1 3 41.97 42.16 2.09 o 6 1 3 42.84 43.45 3.31 o 7 1 3 11.72 17.91 3.61 o 8 1 3 220.18 288.62 6.45 o -7 2 3 83.02 104.20 4.36 o -6 2 3 872.69 861.69 13.46 o -5 2 3 2522.02 2513.39 62.44 o -4 2 3 893.73 850.85 32.53 o -3 2 3 1538.40 1785.27 66.15 o -2 2 3 340.25 383.69 11.55 o -1 2 3 7008.24 7600.98 112.08 o 0 2 3 4168.25 4582.31 48.85 o 1 2 3 6933.79 7506.47 186.28 o 2 2 3 285.06 319.31 5.84 o 3 2 3 1607.26 1830.30 41.75 o 4 2 3 926.72 832.62 50.68 o 5 2 3 2535.71 2491.28 40.46 o 6 2 3 864.25 895.29 18.39 o 7 2 3 75.72 81.17 5.95 o 8 2 3 97.65 115.56 4.71 o -8 3 3 134.00 158.40 8.58 o -7 3 3 325.08 387.38 6.03 o -6 3 3 29.18 32.63 3.24 o -5 3 3 260.46 249.47 7.61 o -4 3 3 1318.08 1154.86 40.16 o -3 3 3 4430.90 4206.39 37.39 o -2 3 3 2715.42 2966.61 87.06 o -1 3 3 2972.91 3027.62 20.88 o 0 3 3 86.49 87.76 3.46 o 1 3 3 2934.61 3051.20 42.37 o 2 3 3 2848.61 3033.07 127.96 o 3 3 3 4406.90 4233.29 76.21 o 4 3 3 1264.77 1100.92 38.77 o 5 3 3 281.34 268.21 14.54 o 6 3 3 33.96 29.77 3.60 o 7 3 3 316.10 347.41 13.44 o -7 4 3 114.89 90.66 11.45 o -6 4 3 689.37 695.59 20.54 o -5 4 3 49.37 59.18 3.44 o -4 4 3 1132.90 1141.88 24.14 o -3 4 3 246.21 255.28 8.28 o -2 4 3 396.69 329.45 21.03 o -1 4 3 1464.82 1536.97 26.59 o 0 4 3 3351.76 3136.23 87.94 o 1 4 3 1327.14 1568.74 21.05 o 2 4 3 355.37 281.42 27.92 o 3 4 3 268.84 238.39 10.26 o 4 4 3 1180.38 1170.08 30.22 o 5 4 3 72.79 75.86 4.70 o 6 4 3 692.20 676.51 33.88 o 7 4 3 111.71 70.69 18.85 o -6 5 3 98.85 85.67 8.40 o -5 5 3 356.55 377.57 16.54 o -4 5 3 24.53 21.57 4.45 o -3 5 3 3596.34 3640.96 73.07 o -2 5 3 88.79 93.20 6.55 o -1 5 3 1637.70 1665.32 24.92 o 0 5 3 48.76 63.73 7.58 o 1 5 3 1583.47 1718.46 37.39 o 2 5 3 85.41 106.39 8.41 o 3 5 3 3601.74 3853.57 72.15 o 4 5 3 30.77 26.85 4.69 o 5 5 3 377.48 393.08 7.66 o 6 5 3 89.55 94.78 5.18 o 7 5 3 498.03 518.31 7.24 o -6 6 3 565.07 678.12 33.77 o -5 6 3 139.51 165.40 7.36 o -4 6 3 397.76 397.18 13.33 o -3 6 3 151.18 120.19 9.97 o -2 6 3 1430.52 1448.12 32.57 o -1 6 3 526.88 556.31 14.17 o 0 6 3 2341.34 2351.51 17.79 o 1 6 3 464.30 453.27 9.34 o 2 6 3 1325.56 1295.69 15.71 o 3 6 3 169.01 146.14 6.56 o 4 6 3 466.95 489.52 10.68 o 5 6 3 125.14 144.28 9.35 o 6 6 3 552.30 675.08 48.05 o -6 7 3 14.43 14.49 4.43 o -5 7 3 200.99 228.67 15.68 o -4 7 3 109.32 123.75 6.34 o -3 7 3 1.85 8.47 4.13 o -2 7 3 28.06 34.47 6.08 o -1 7 3 2067.67 1997.98 18.68 o 0 7 3 83.74 74.92 4.78 o 1 7 3 1828.69 1794.20 42.35 o 2 7 3 17.03 24.14 3.69 o 3 7 3 26.53 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