#------------------------------------------------------------------------------ #$Date: 2010-12-22 21:36:50 +0200 (Wed, 22 Dec 2010) $ #$Revision: 5269 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2227819.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227819_Fobs loop_ _publ_author_name 'Hu, Hui-Ling' 'Cheng, Pei-Chi' 'Wu, Chia-Jun' 'Chen, Jhy-Der' _publ_section_title ; 6,6'-Dimethyl-2,2'-[oxalylbis(azanediyl)]dipyridinium dichloride acetonitrile solvate ; _journal_coeditor_code NC2195 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2386 _journal_volume 66 _journal_year 2010 _space_group_IT_number 13 _symmetry_space_group_name_Hall '-P 2yc' _symmetry_space_group_name_H-M 'P 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.834 _cell_angle_gamma 90.000 _cell_length_a 10.6740 _cell_length_b 8.7637 _cell_length_c 10.3700 _exptl_crystal_F_000 400.00 _reflns_d_resolution_high 0.8408 _[local]_cod_data_source_file nc2195Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 254.45 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2372.84 2165.62 36.51 o 2 0 0 2614.23 2395.33 24.40 o 3 0 0 386.68 356.33 8.67 o 4 0 0 2436.93 2320.12 34.58 o 5 0 0 985.42 1027.18 23.28 o 6 0 0 580.56 532.00 17.35 o 7 0 0 75.44 79.77 2.47 o 8 0 0 724.52 755.72 16.42 o 9 0 0 111.81 108.16 3.09 o 10 0 0 10.93 10.62 1.74 o 11 0 0 8.13 13.52 2.77 o 0 1 0 1079.15 1248.49 12.31 o 1 1 0 542.10 536.06 13.78 o 2 1 0 451.77 434.53 8.70 o 3 1 0 569.92 610.32 16.26 o 4 1 0 999.61 978.31 16.44 o 5 1 0 55.93 52.33 1.31 o 6 1 0 198.33 190.44 3.92 o 7 1 0 0.16 -0.95 1.02 o 8 1 0 64.04 65.68 2.36 o 9 1 0 7.10 6.73 1.22 o 10 1 0 0.37 0.97 1.09 o 11 1 0 4.54 6.11 1.77 o 0 2 0 365.69 360.65 14.63 o 1 2 0 169.86 148.80 3.65 o 2 2 0 85.53 112.63 3.15 o 3 2 0 21.66 21.47 1.24 o 4 2 0 60.77 66.12 1.95 o 5 2 0 1.32 -1.02 1.24 o 6 2 0 1.57 2.19 1.44 o 7 2 0 118.49 116.51 6.41 o 8 2 0 1.78 -1.58 2.48 o 9 2 0 7.75 5.10 1.65 o 10 2 0 5.24 5.90 1.75 o 11 2 0 47.40 43.49 3.49 o 0 3 0 2489.23 2405.84 43.55 o 1 3 0 1823.98 1907.77 28.25 o 2 3 0 1333.36 1372.43 40.53 o 3 3 0 42.76 55.35 2.48 o 4 3 0 768.37 761.64 19.73 o 5 3 0 21.81 25.80 1.65 o 6 3 0 264.35 266.56 6.68 o 7 3 0 9.14 11.27 1.65 o 8 3 0 0.99 1.60 1.65 o 9 3 0 11.14 14.21 1.85 o 10 3 0 93.24 89.21 2.68 o 11 3 0 0.85 4.21 3.35 o 0 4 0 954.60 982.77 30.46 o 1 4 0 92.24 113.62 3.19 o 2 4 0 13.92 4.19 1.12 o 3 4 0 500.15 587.90 17.13 o 4 4 0 304.63 281.91 7.84 o 5 4 0 760.77 872.92 36.96 o 6 4 0 423.46 456.42 15.03 o 7 4 0 70.58 70.13 2.68 o 8 4 0 56.32 59.00 2.62 o 9 4 0 0.62 1.60 1.65 o 10 4 0 22.45 20.25 2.78 o 11 4 0 47.88 50.11 3.60 o 0 5 0 1430.05 1453.92 34.30 o 1 5 0 54.80 58.60 1.86 o 2 5 0 1037.83 990.29 36.87 o 3 5 0 186.17 202.01 5.14 o 4 5 0 298.58 305.54 7.73 o 5 5 0 9.81 11.82 1.65 o 6 5 0 76.37 79.29 2.68 o 7 5 0 155.44 161.90 4.02 o 8 5 0 131.00 132.80 3.35 o 9 5 0 25.33 26.57 4.08 o 10 5 0 2.67 2.04 2.57 o 0 6 0 133.39 142.87 4.08 o 1 6 0 15.39 17.27 1.65 o 2 6 0 22.04 23.03 1.85 o 3 6 0 13.04 15.63 1.85 o 4 6 0 18.86 18.04 4.37 o 5 6 0 7.25 8.51 1.65 o 6 6 0 1.11 1.17 2.33 o 7 6 0 14.49 12.41 1.74 o 8 6 0 110.79 107.79 2.89 o 9 6 0 38.42 31.51 3.64 o 0 7 0 779.67 787.53 20.16 o 1 7 0 129.93 131.71 3.71 o 2 7 0 7.28 10.62 1.74 o 3 7 0 134.73 140.24 3.30 o 4 7 0 63.92 64.72 2.47 o 5 7 0 3.35 1.46 1.65 o 6 7 0 34.94 37.00 3.21 o 7 7 0 1.20 -1.31 1.44 o 8 7 0 6.30 7.58 2.47 o 0 8 0 496.32 507.77 13.42 o 1 8 0 1.47 4.23 1.65 o 2 8 0 544.42 569.79 9.80 o 3 8 0 161.92 171.93 3.81 o 4 8 0 41.89 47.36 2.27 o 5 8 0 49.54 48.61 2.16 o 6 8 0 36.70 32.28 3.09 o 7 8 0 52.68 47.97 3.30 o 0 9 0 302.91 298.36 8.46 o 1 9 0 4.74 5.57 2.62 o 2 9 0 350.54 373.68 6.19 o 3 9 0 17.28 17.26 2.47 o 4 9 0 222.13 227.86 12.98 o 5 9 0 43.11 43.48 3.71 o 6 9 0 77.34 79.69 4.34 o 0 10 0 315.15 333.05 9.04 o 1 10 0 39.49 47.31 3.35 o 2 10 0 45.59 50.52 3.19 o 3 10 0 4.24 9.33 2.47 o -12 1 1 14.14 18.39 3.16 o -11 1 1 16.01 17.52 1.92 o -10 1 1 4.07 4.74 1.17 o -9 1 1 1.47 2.91 1.17 o -8 1 1 37.91 34.31 1.62 o -7 1 1 35.76 37.61 1.46 o -6 1 1 915.82 895.23 26.05 o -5 1 1 122.84 112.81 2.65 o -4 1 1 18.36 20.64 0.87 o -3 1 1 1143.57 1160.45 15.66 o -2 1 1 107.50 90.30 1.65 o -1 1 1 498.70 415.01 9.74 o 0 1 1 3257.68 3173.84 27.00 o 1 1 1 11.77 14.62 0.74 o 2 1 1 953.98 1015.82 13.72 o 3 1 1 3960.38 4202.51 34.80 o 4 1 1 57.74 60.20 1.43 o 5 1 1 260.39 291.14 5.94 o 6 1 1 90.41 97.82 2.23 o 7 1 1 89.53 82.41 1.86 o 8 1 1 51.59 60.66 1.82 o 9 1 1 70.94 70.64 2.61 o 10 1 1 16.32 16.70 1.23 o 11 1 1 23.82 23.62 2.07 o -12 2 1 21.12 18.07 3.40 o -11 2 1 10.98 8.58 2.57 o -10 2 1 81.63 81.19 3.50 o -9 2 1 0.08 0.31 2.77 o -8 2 1 176.33 182.17 4.81 o -7 2 1 54.56 42.27 2.06 o -6 2 1 659.28 659.60 18.45 o -5 2 1 0.07 0.34 1.12 o -4 2 1 1024.97 1083.72 23.71 o -3 2 1 865.30 963.11 21.02 o -2 2 1 3028.45 3160.37 32.56 o -1 2 1 2710.86 2896.91 57.14 o 0 2 1 455.28 535.92 13.75 o 1 2 1 3171.76 3307.06 61.71 o 2 2 1 7.54 9.53 1.03 o 3 2 1 2325.57 2405.71 34.75 o 4 2 1 220.94 223.77 5.65 o 5 2 1 567.33 558.08 17.14 o 6 2 1 23.37 25.65 1.85 o 7 2 1 460.99 452.71 13.09 o 8 2 1 41.37 38.92 2.27 o 9 2 1 113.67 117.06 3.09 o 10 2 1 1.87 4.19 3.79 o 11 2 1 0.23 0.73 2.47 o -11 3 1 2.43 -1.31 2.06 o -10 3 1 60.22 60.78 2.47 o -9 3 1 0.13 -0.33 4.37 o -8 3 1 21.01 20.50 1.95 o -7 3 1 25.58 23.03 1.95 o -6 3 1 4.70 2.19 1.44 o -5 3 1 1053.33 1065.36 30.44 o -4 3 1 1496.50 1552.08 50.91 o -3 3 1 113.12 111.59 6.12 o -2 3 1 1515.73 1521.83 50.13 o -1 3 1 2401.07 2442.08 82.54 o 0 3 1 56.38 61.84 1.95 o 1 3 1 3297.71 3424.34 38.55 o 2 3 1 2317.66 2449.47 34.37 o 3 3 1 4.54 0.73 2.77 o 4 3 1 25.86 22.65 1.54 o 5 3 1 128.39 120.84 3.50 o 6 3 1 1.59 1.89 3.35 o 7 3 1 271.46 269.74 6.08 o 8 3 1 0.52 0.04 1.54 o 9 3 1 92.61 100.70 3.79 o 10 3 1 32.17 25.41 2.86 o 11 3 1 11.15 12.69 3.39 o -11 4 1 19.36 22.97 2.89 o -10 4 1 3.40 1.91 3.35 o -9 4 1 9.43 6.88 1.65 o -8 4 1 10.24 10.28 4.23 o -7 4 1 0.73 0.00 1.65 o -6 4 1 3.51 7.53 1.74 o -5 4 1 895.86 920.29 19.53 o -4 4 1 189.35 177.04 9.33 o -3 4 1 4.95 4.97 1.46 o -2 4 1 0.05 1.60 1.03 o -1 4 1 53.56 57.26 2.03 o 0 4 1 0.01 0.29 1.46 o 1 4 1 234.39 228.72 5.86 o 2 4 1 2029.78 2251.20 51.75 o 3 4 1 7.14 15.02 1.44 o 4 4 1 40.57 37.64 1.85 o 5 4 1 104.62 107.16 3.09 o 6 4 1 72.40 76.72 2.57 o 7 4 1 1.85 0.44 1.65 o 8 4 1 38.02 39.01 2.16 o 9 4 1 2.45 4.95 1.54 o 10 4 1 24.78 25.74 2.86 o -10 5 1 6.56 5.74 2.36 o -9 5 1 5.20 3.98 1.54 o -8 5 1 6.84 8.33 1.65 o -7 5 1 66.30 68.72 4.37 o -6 5 1 6.33 7.11 4.66 o -5 5 1 41.22 44.35 2.06 o -4 5 1 6.51 4.95 1.44 o -3 5 1 353.70 380.97 9.63 o -2 5 1 126.60 115.84 3.07 o -1 5 1 114.32 108.04 4.08 o 0 5 1 373.43 427.07 31.38 o 1 5 1 33.84 28.32 2.77 o 2 5 1 47.13 60.61 3.35 o 3 5 1 32.54 30.12 1.74 o 4 5 1 223.06 240.56 6.08 o 5 5 1 13.29 16.05 1.85 o 6 5 1 3.80 4.30 1.74 o 7 5 1 52.81 51.43 2.36 o 8 5 1 49.36 46.25 2.27 o 9 5 1 34.89 36.32 4.08 o 10 5 1 26.29 22.51 2.89 o -10 6 1 4.26 5.97 3.06 o -9 6 1 0.69 1.29 2.62 o -8 6 1 120.07 130.07 2.98 o -7 6 1 4.55 5.93 2.62 o -6 6 1 20.52 18.27 2.48 o -5 6 1 244.89 250.63 5.76 o -4 6 1 364.81 353.47 12.40 o -3 6 1 674.00 637.81 20.59 o -2 6 1 79.92 85.29 2.36 o -1 6 1 183.83 179.67 7.58 o 0 6 1 918.29 891.40 17.76 o 1 6 1 631.83 642.92 15.06 o 2 6 1 318.50 313.71 7.32 o 3 6 1 84.79 86.02 2.57 o 4 6 1 4.25 7.18 1.65 o 5 6 1 449.55 469.29 14.01 o 6 6 1 1.81 3.38 1.54 o 7 6 1 16.16 17.70 2.48 o 8 6 1 20.84 17.60 2.57 o 9 6 1 15.05 13.41 2.78 o -9 7 1 0.11 1.46 4.37 o -8 7 1 37.92 44.46 3.19 o -7 7 1 16.02 15.48 3.35 o -6 7 1 145.59 151.64 6.71 o -5 7 1 274.45 273.60 7.51 o -4 7 1 1037.32 1056.88 14.45 o -3 7 1 13.87 14.09 1.74 o -2 7 1 169.86 166.69 4.81 o -1 7 1 373.82 351.22 13.13 o 0 7 1 6.66 5.42 1.54 o 1 7 1 1608.09 1622.26 35.28 o 2 7 1 427.11 431.82 10.73 o 3 7 1 295.47 278.64 8.88 o 4 7 1 7.10 5.48 1.75 o 5 7 1 177.23 186.05 4.58 o 6 7 1 1.30 1.15 2.48 o 7 7 1 126.36 132.69 4.33 o 8 7 1 21.77 19.66 4.37 o -7 8 1 0.44 0.44 2.91 o -6 8 1 0.07 0.87 2.27 o -5 8 1 4.02 4.82 2.04 o -4 8 1 10.42 15.45 2.33 o -3 8 1 119.72 116.85 3.35 o -2 8 1 0.04 -0.25 1.54 o -1 8 1 1.55 4.37 1.44 o 0 8 1 153.74 150.30 3.50 o 1 8 1 24.20 25.01 1.95 o 2 8 1 7.21 7.46 1.65 o 3 8 1 0.03 0.58 1.44 o 4 8 1 5.05 4.90 1.54 o 5 8 1 2.90 1.86 1.33 o 6 8 1 1.31 4.23 3.21 o 7 8 1 20.45 20.43 2.78 o -6 9 1 3.31 5.07 2.66 o -5 9 1 0.21 -0.20 2.36 o -4 9 1 1.56 2.53 2.48 o -3 9 1 22.02 18.62 2.57 o -2 9 1 0.16 0.25 1.60 o -1 9 1 8.03 10.49 1.65 o 0 9 1 12.89 8.72 1.65 o 1 9 1 0.45 0.15 1.89 o 2 9 1 0.16 -1.31 1.44 o 3 9 1 5.79 7.42 3.06 o 4 9 1 1.31 3.16 5.25 o 5 9 1 2.01 1.02 2.27 o -3 10 1 4.88 4.81 2.57 o -2 10 1 6.16 6.46 2.96 o -1 10 1 23.86 24.09 2.68 o 0 10 1 12.45 13.92 2.73 o 1 10 1 57.53 59.90 3.50 o 2 10 1 1.97 1.22 2.24 o -12 0 2 9.58 8.45 3.50 o -11 0 2 160.26 157.44 6.71 o -10 0 2 17.13 20.40 2.62 o -9 0 2 113.99 107.58 4.08 o -8 0 2 194.20 195.97 7.29 o -7 0 2 467.55 460.36 20.43 o -6 0 2 304.78 285.68 10.50 o -5 0 2 1579.75 1381.51 37.59 o -4 0 2 1191.71 1079.86 32.87 o -3 0 2 64743.25 65217.64 272.40 o -2 0 2 1726.30 1613.83 30.52 o -1 0 2 1409.21 1332.27 25.47 o 0 0 2 20.13 15.16 1.17 o 1 0 2 5528.85 5108.91 54.37 o 2 0 2 1985.43 1893.60 38.11 o 3 0 2 1242.35 1284.65 35.80 o 4 0 2 449.63 463.46 14.60 o 5 0 2 2559.26 2573.22 46.80 o 6 0 2 588.66 553.96 21.61 o 7 0 2 61.91 61.80 3.21 o 8 0 2 32.55 38.47 2.91 o 9 0 2 20.74 20.40 2.62 o 10 0 2 13.83 12.53 3.50 o 11 0 2 0.06 4.08 3.50 o -12 1 2 5.57 3.50 2.24 o -11 1 2 15.51 16.10 2.33 o -10 1 2 0.13 1.90 1.54 o -9 1 2 35.29 35.85 4.52 o -8 1 2 7.16 9.08 1.65 o -7 1 2 165.67 156.05 4.12 o -6 1 2 73.13 73.82 2.16 o -5 1 2 43.89 52.39 1.89 o -4 1 2 371.15 362.43 9.19 o -3 1 2 503.78 494.96 16.96 o -2 1 2 255.49 240.15 15.48 o -1 1 2 470.70 429.78 11.16 o 0 1 2 1219.94 1249.98 18.45 o 1 1 2 2550.48 2651.55 28.92 o 2 1 2 144.02 151.67 4.96 o 3 1 2 372.62 376.84 10.22 o 4 1 2 11.72 8.25 1.24 o 5 1 2 193.22 177.44 4.61 o 6 1 2 4.51 6.70 2.04 o 7 1 2 0.18 -0.58 1.44 o 8 1 2 21.56 20.57 1.85 o 9 1 2 14.68 12.59 1.74 o 10 1 2 5.90 3.68 2.16 o 11 1 2 1.22 1.17 3.79 o -12 2 2 2.39 6.70 3.21 o -11 2 2 0.17 -0.29 2.91 o -10 2 2 19.50 19.82 2.62 o -9 2 2 0.51 -2.04 2.33 o -8 2 2 5.46 4.66 2.33 o -7 2 2 28.28 27.69 2.62 o -6 2 2 13.48 12.53 2.04 o -5 2 2 2.45 4.95 1.46 o -4 2 2 61.88 56.27 2.62 o -3 2 2 133.18 130.09 4.96 o -2 2 2 79.47 74.94 2.62 o -1 2 2 135.60 161.62 5.54 o 0 2 2 177.72 180.35 6.71 o 1 2 2 76.49 80.48 2.62 o 2 2 2 228.51 263.22 9.05 o 3 2 2 1.61 2.33 1.46 o 4 2 2 299.63 299.39 10.80 o 5 2 2 0.14 2.62 1.75 o 6 2 2 17.32 18.07 2.33 o 7 2 2 20.01 18.65 2.62 o 8 2 2 181.09 167.37 6.12 o 9 2 2 74.64 66.17 3.50 o 10 2 2 13.70 12.82 3.21 o -11 3 2 1.09 1.75 3.21 o -10 3 2 7.19 1.75 2.04 o -9 3 2 68.75 65.00 3.50 o -8 3 2 3.17 3.79 2.04 o -7 3 2 127.05 109.63 4.37 o -6 3 2 100.67 109.04 4.37 o -5 3 2 565.30 518.76 22.20 o -4 3 2 567.10 554.56 23.08 o -3 3 2 1317.43 1238.04 33.44 o -2 3 2 1164.47 1180.01 33.44 o -1 3 2 1024.92 1029.92 30.20 o 0 3 2 4.93 3.21 1.17 o 1 3 2 1865.39 1800.80 39.74 o 2 3 2 169.40 215.26 8.46 o 3 3 2 398.60 444.62 20.73 o 4 3 2 2.62 2.62 1.75 o 5 3 2 3.79 5.83 2.04 o 6 3 2 69.79 70.25 3.50 o 7 3 2 390.01 399.70 14.30 o 8 3 2 2.38 6.70 2.04 o 9 3 2 61.91 59.75 3.21 o 10 3 2 3.19 1.75 3.21 o -11 4 2 10.55 8.45 3.21 o -10 4 2 16.59 17.49 2.33 o -9 4 2 98.70 85.41 3.79 o -8 4 2 160.08 165.03 5.54 o -7 4 2 70.51 66.17 3.50 o -6 4 2 120.53 117.50 3.79 o -5 4 2 10.88 5.54 2.04 o -4 4 2 41.44 34.69 2.33 o -3 4 2 631.55 556.09 23.96 o -2 4 2 13.77 17.49 1.75 o -1 4 2 2.65 -1.17 1.46 o 0 4 2 971.48 1013.18 29.86 o 1 4 2 630.88 518.45 22.21 o 2 4 2 1841.59 2005.55 40.52 o 3 4 2 869.32 940.04 28.07 o 4 4 2 204.18 195.11 7.58 o 5 4 2 135.70 128.29 4.67 o 6 4 2 2.92 1.46 2.04 o 7 4 2 58.33 54.80 3.21 o 8 4 2 190.69 181.07 7.58 o 9 4 2 1.14 7.87 3.21 o 10 4 2 77.03 74.04 5.83 o -10 5 2 34.45 36.43 4.08 o -9 5 2 13.34 13.41 2.33 o -8 5 2 0.49 -1.17 2.04 o -7 5 2 159.22 159.49 5.83 o -6 5 2 99.40 94.75 3.50 o -5 5 2 309.64 306.02 10.21 o -4 5 2 0.46 0.58 1.75 o -3 5 2 1014.29 937.78 25.74 o -2 5 2 102.40 99.71 3.50 o -1 5 2 1177.62 1077.94 28.98 o 0 5 2 203.65 213.21 8.17 o 1 5 2 226.84 215.85 7.88 o 2 5 2 130.53 128.88 4.96 o 3 5 2 229.95 235.37 8.46 o 4 5 2 371.11 364.43 16.34 o 5 5 2 312.91 301.62 12.83 o 6 5 2 134.79 134.69 5.25 o 7 5 2 6.74 5.25 2.33 o 8 5 2 389.68 407.80 9.04 o 9 5 2 56.57 40.22 4.37 o -10 6 2 3.00 6.99 3.21 o -9 6 2 4.17 4.95 3.21 o -8 6 2 0.22 0.87 2.04 o -7 6 2 15.13 11.95 2.33 o -6 6 2 2.07 4.37 2.04 o -5 6 2 39.60 43.43 2.91 o -4 6 2 45.94 43.72 2.91 o -3 6 2 105.83 109.62 3.79 o -2 6 2 6.20 11.07 2.33 o -1 6 2 8.15 5.54 2.04 o 0 6 2 31.71 32.06 2.62 o 1 6 2 1.25 1.46 2.04 o 2 6 2 63.27 62.09 3.21 o 3 6 2 7.28 9.91 2.33 o 4 6 2 23.48 19.82 2.62 o 5 6 2 239.44 239.13 10.21 o 6 6 2 87.82 81.04 3.50 o 7 6 2 26.04 26.23 2.62 o 8 6 2 1.88 2.91 2.91 o -9 7 2 7.94 6.12 3.50 o -8 7 2 0.79 0.58 2.91 o -7 7 2 29.51 31.48 2.62 o -6 7 2 55.19 60.34 3.21 o -5 7 2 1.09 2.62 2.04 o -4 7 2 73.32 75.21 3.50 o -3 7 2 569.36 544.69 15.18 o -2 7 2 127.77 123.91 3.79 o -1 7 2 9.30 13.70 2.33 o 0 7 2 171.77 169.12 5.25 o 1 7 2 79.92 74.92 3.21 o 2 7 2 6.17 1.75 2.33 o 3 7 2 71.95 74.04 3.50 o 4 7 2 0.71 1.75 2.04 o 5 7 2 12.64 12.82 2.33 o 6 7 2 8.80 8.16 2.04 o 7 7 2 4.93 4.37 3.50 o -8 8 2 5.53 5.25 2.91 o -7 8 2 19.84 16.61 3.79 o -6 8 2 81.91 78.12 4.66 o -5 8 2 257.87 264.21 7.87 o -4 8 2 8.29 8.74 2.04 o -3 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