#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/78/2227841.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227841_Fobs loop_ _publ_author_name 'Trzybi\'nski, Damian' 'Krzymi\'nski, Karol' 'B\/la\.zejowski, Jerzy' _publ_section_title ; 9-(4-Fluorophenoxycarbonyl)-10-methylacridinium trifluoromethanesulfonate ; _journal_coeditor_code NG5037 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2769 _journal_page_last o2770 _journal_volume 66 _journal_year 2010 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.893 _cell_angle_gamma 90.000 _cell_length_a 20.8537 _cell_length_b 7.8092 _cell_length_c 25.6896 _exptl_crystal_F_000 1968.00 _reflns_d_resolution_high 0.8394 _[local]_cod_data_source_file ng5037Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' DT130410 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 488.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 36704.14 36510.71 395.07 o 6 0 0 313.71 285.67 26.17 o 8 0 0 2732.43 2626.31 59.28 o 10 0 0 1237.59 1256.17 36.78 o 12 0 0 191.48 206.39 34.73 o 14 0 0 202.83 176.65 43.42 o 16 0 0 2553.38 2388.63 119.99 o 18 0 0 7.50 11.39 55.18 o 20 0 0 23.10 46.05 68.94 o 22 0 0 24.70 88.67 75.89 o 24 0 0 21.65 56.87 81.62 o 3 1 0 38974.35 39230.56 316.52 o 5 1 0 844.33 1025.73 24.05 o 7 1 0 4376.66 4266.26 32.78 o 9 1 0 447.52 376.74 21.72 o 11 1 0 27.16 26.00 23.15 o 13 1 0 687.56 712.65 28.65 o 15 1 0 863.10 877.94 36.54 o 17 1 0 348.75 319.79 44.94 o 19 1 0 440.14 436.11 50.20 o 21 1 0 0.00 -23.82 50.84 o 23 1 0 0.08 25.06 56.52 o 0 2 0 29971.66 31771.00 531.19 o 2 2 0 1903.41 1947.32 46.05 o 4 2 0 58889.79 61139.20 347.59 o 6 2 0 8729.28 9252.68 66.36 o 8 2 0 335.53 402.02 25.32 o 10 2 0 14.60 70.71 25.84 o 12 2 0 2753.26 2566.66 31.60 o 14 2 0 22.18 30.17 27.98 o 16 2 0 580.29 550.57 36.29 o 18 2 0 208.02 238.12 41.08 o 20 2 0 571.82 574.91 52.13 o 22 2 0 41.68 66.52 52.63 o 1 3 0 4037.41 4218.74 57.67 o 3 3 0 2487.31 2195.72 24.99 o 5 3 0 15080.83 15576.50 74.31 o 7 3 0 1360.18 1392.52 28.52 o 9 3 0 2.10 -11.69 25.72 o 11 3 0 991.13 991.01 34.67 o 13 3 0 528.25 490.71 29.28 o 15 3 0 0.70 3.06 31.64 o 17 3 0 0.41 -13.69 36.11 o 19 3 0 22.44 84.59 42.20 o 21 3 0 143.09 131.30 51.21 o 23 3 0 2.17 -44.95 84.70 o 0 4 0 128.18 87.15 26.40 o 2 4 0 3878.97 4196.33 49.38 o 4 4 0 285.54 344.21 23.41 o 6 4 0 1414.61 1662.80 26.81 o 8 4 0 804.98 940.93 24.17 o 10 4 0 1110.35 1101.55 32.85 o 12 4 0 626.33 570.88 29.75 o 14 4 0 491.87 478.24 33.72 o 16 4 0 16.44 -18.46 35.46 o 18 4 0 173.62 158.40 39.45 o 20 4 0 276.11 289.24 68.19 o 22 4 0 463.76 563.26 76.49 o 1 5 0 378.26 385.72 21.63 o 3 5 0 3638.89 3826.95 50.95 o 5 5 0 988.83 994.37 34.43 o 7 5 0 1562.90 1539.28 34.74 o 9 5 0 444.83 543.36 25.63 o 11 5 0 336.85 349.30 26.29 o 13 5 0 560.06 599.17 29.24 o 15 5 0 0.37 -3.90 55.96 o 17 5 0 279.78 232.60 59.46 o 19 5 0 36.54 87.97 59.85 o 0 6 0 26.10 60.52 31.72 o 2 6 0 83.75 135.68 26.60 o 4 6 0 1265.48 1283.84 44.10 o 6 6 0 148.37 189.98 34.34 o 8 6 0 111.87 132.06 35.73 o 10 6 0 468.69 461.20 32.44 o 12 6 0 27.14 23.36 30.51 o 14 6 0 27.00 54.33 61.38 o 16 6 0 1.31 -31.33 62.95 o 18 6 0 11.77 -7.58 67.06 o 1 7 0 742.37 815.36 39.31 o 3 7 0 86.03 108.65 34.67 o 5 7 0 156.83 115.23 41.04 o 7 7 0 12.16 35.58 38.78 o 9 7 0 0.04 44.82 51.31 o 11 7 0 76.87 62.70 69.32 o 13 7 0 455.73 485.54 68.28 o 15 7 0 0.02 1.19 65.25 o 0 8 0 159.00 190.33 60.43 o 2 8 0 37.45 49.39 43.06 o 4 8 0 170.79 131.09 38.82 o 6 8 0 10.79 40.39 40.49 o 8 8 0 1.77 40.41 48.58 o 10 8 0 41.56 20.50 61.35 o 12 8 0 0.25 1.09 69.09 o 1 9 0 141.72 88.46 50.82 o 3 9 0 22.22 -6.92 48.40 o 5 9 0 22.69 13.08 48.98 o -23 1 1 143.92 127.52 54.35 o -21 1 1 41.65 30.14 49.00 o -19 1 1 2.70 44.51 44.79 o -17 1 1 1417.44 1460.86 55.66 o -15 1 1 245.77 272.49 30.50 o -13 1 1 3.35 -1.29 24.06 o -11 1 1 4159.03 4284.73 49.20 o -9 1 1 7192.01 7505.29 37.12 o -7 1 1 5271.42 4833.49 27.21 o -5 1 1 6447.47 6047.92 67.85 o -3 1 1 6251.35 6351.01 37.26 o 3 1 1 12561.06 12184.55 61.39 o 5 1 1 31178.99 29520.91 125.99 o 7 1 1 1759.67 1470.14 26.40 o 9 1 1 7618.31 7391.93 53.67 o 11 1 1 1984.42 1960.82 31.77 o 13 1 1 553.64 634.76 28.78 o 15 1 1 78.03 88.50 34.26 o 17 1 1 422.72 431.48 48.12 o 19 1 1 1345.80 1497.26 71.49 o 21 1 1 422.98 372.06 56.67 o 23 1 1 46.27 26.21 56.05 o -22 2 1 92.47 77.06 50.48 o -20 2 1 465.55 557.00 60.57 o -18 2 1 102.05 73.56 39.02 o -16 2 1 89.34 57.07 32.13 o -14 2 1 225.28 234.12 26.66 o -12 2 1 2686.65 2763.60 41.34 o -10 2 1 250.35 168.68 24.44 o -8 2 1 2686.70 2216.99 42.28 o -6 2 1 4771.84 4829.24 36.46 o -4 2 1 50225.61 49366.96 275.31 o -2 2 1 7739.35 7305.35 36.40 o 0 2 1 3475.75 3423.24 44.03 o 2 2 1 100542.86 93848.47 1046.16 o 4 2 1 9869.35 9507.74 74.81 o 6 2 1 1125.60 922.27 24.87 o 8 2 1 2953.87 3140.54 42.69 o 10 2 1 4554.41 4263.02 63.06 o 12 2 1 2140.98 2478.83 45.71 o 14 2 1 372.98 471.42 31.11 o 16 2 1 913.29 1002.50 39.22 o 18 2 1 70.81 74.83 47.52 o 20 2 1 1163.12 1166.35 59.14 o 22 2 1 12.01 40.13 52.87 o -23 3 1 3.11 54.19 83.04 o -21 3 1 226.55 216.09 68.64 o -19 3 1 3.38 24.62 39.33 o -17 3 1 248.65 302.30 41.01 o -15 3 1 94.74 100.71 29.96 o -13 3 1 29.08 28.91 26.55 o -11 3 1 3.33 5.13 24.25 o -9 3 1 1404.88 1658.01 33.52 o -7 3 1 0.80 20.04 19.54 o -5 3 1 412.65 496.81 20.81 o -3 3 1 597.50 577.60 21.60 o -1 3 1 146.91 158.77 23.35 o 1 3 1 7704.81 7537.38 66.68 o 3 3 1 96.39 72.01 17.32 o 5 3 1 5349.11 5388.76 45.04 o 7 3 1 1744.22 1748.84 28.80 o 9 3 1 2249.78 2006.73 46.40 o 11 3 1 467.23 438.81 26.66 o 13 3 1 80.74 92.09 28.53 o 15 3 1 440.34 411.12 33.30 o 17 3 1 11.91 25.61 38.65 o 19 3 1 146.84 142.24 44.85 o 21 3 1 573.12 553.19 61.68 o -22 4 1 314.69 317.24 76.03 o -20 4 1 81.24 52.82 60.14 o -18 4 1 3.67 18.10 48.84 o -16 4 1 4.11 29.45 35.22 o -14 4 1 406.56 404.79 31.42 o -12 4 1 4.83 6.94 27.97 o -10 4 1 98.66 93.80 21.75 o -8 4 1 74.19 36.11 20.26 o -6 4 1 672.58 692.58 24.00 o -4 4 1 4757.84 4938.30 55.02 o -2 4 1 181.88 219.71 21.46 o 0 4 1 2046.03 2002.43 30.37 o 2 4 1 87.87 55.29 23.89 o 4 4 1 77.43 98.08 20.94 o 6 4 1 390.59 383.36 20.66 o 8 4 1 15.73 6.21 19.01 o 10 4 1 554.46 567.33 28.77 o 12 4 1 5.07 -12.75 29.27 o 14 4 1 438.27 461.24 35.49 o 16 4 1 593.42 621.14 39.20 o 18 4 1 79.45 50.56 40.82 o 20 4 1 525.81 567.04 71.08 o -19 5 1 26.41 73.64 62.49 o -17 5 1 38.24 23.22 58.69 o -15 5 1 105.73 68.19 38.53 o -13 5 1 33.50 28.22 25.09 o -11 5 1 118.95 110.23 24.96 o -9 5 1 1364.88 1271.49 29.42 o -7 5 1 0.03 -13.76 22.61 o -5 5 1 56.35 68.25 24.87 o -3 5 1 1462.68 1499.76 34.23 o -1 5 1 225.20 226.91 20.77 o 1 5 1 19.54 16.80 21.01 o 3 5 1 3048.12 3418.95 41.45 o 5 5 1 183.62 151.11 29.29 o 7 5 1 1359.28 1341.46 28.51 o 9 5 1 0.19 33.29 22.64 o 11 5 1 202.19 179.82 25.09 o 13 5 1 45.49 5.09 25.98 o 15 5 1 153.97 163.55 44.65 o 17 5 1 3.04 -19.33 51.20 o 19 5 1 0.66 7.31 57.91 o -18 6 1 7.28 -8.80 72.98 o -16 6 1 33.83 46.66 62.01 o -14 6 1 274.32 269.40 47.66 o -12 6 1 18.68 -5.60 34.85 o -10 6 1 65.53 61.59 30.12 o -8 6 1 942.03 878.21 41.15 o -6 6 1 25.96 -11.05 34.53 o -4 6 1 2012.56 2220.10 46.62 o -2 6 1 23.74 17.01 26.67 o 0 6 1 1196.82 1245.41 32.74 o 2 6 1 628.70 665.32 30.32 o 4 6 1 3129.13 3285.44 61.99 o 6 6 1 939.68 1001.18 39.72 o 8 6 1 126.60 62.60 36.04 o 10 6 1 90.11 93.54 26.22 o 12 6 1 25.15 41.41 30.16 o 14 6 1 35.88 105.23 61.10 o 16 6 1 288.56 297.09 66.80 o 18 6 1 4.26 32.91 75.28 o -15 7 1 64.64 57.20 67.05 o -13 7 1 231.07 218.09 67.76 o -11 7 1 75.22 0.99 59.89 o -9 7 1 14.88 78.73 52.43 o -7 7 1 24.81 16.71 38.81 o -5 7 1 543.36 510.23 38.52 o -3 7 1 243.40 288.58 35.50 o -1 7 1 592.73 663.15 42.83 o 1 7 1 11.26 7.08 37.08 o 3 7 1 31.60 26.92 34.40 o 5 7 1 56.45 84.16 43.67 o 7 7 1 271.58 276.75 48.59 o 9 7 1 82.25 51.87 50.59 o 11 7 1 19.46 38.07 57.63 o 13 7 1 29.19 0.93 62.06 o 15 7 1 514.83 416.92 82.93 o -12 8 1 19.72 20.99 66.42 o -10 8 1 1.61 -16.80 62.40 o -8 8 1 5.03 2.34 49.20 o -6 8 1 47.81 25.82 40.28 o -4 8 1 34.07 -10.65 38.66 o -2 8 1 188.52 126.19 44.15 o 0 8 1 39.63 14.67 42.79 o 2 8 1 78.70 63.45 37.85 o 4 8 1 101.55 64.70 39.44 o 6 8 1 127.16 68.41 42.70 o 8 8 1 54.99 10.13 47.89 o 10 8 1 39.74 33.47 59.32 o 12 8 1 156.27 55.61 78.02 o -5 9 1 0.27 -23.56 57.34 o -3 9 1 1.02 8.18 74.72 o -1 9 1 0.32 6.07 75.53 o 1 9 1 3.11 -5.61 48.32 o 3 9 1 44.46 59.93 49.01 o 5 9 1 12.82 47.66 45.81 o -24 0 2 39.05 -21.72 77.68 o -22 0 2 19.36 -14.58 76.45 o -20 0 2 261.54 236.49 93.53 o -18 0 2 3857.69 4272.68 127.88 o -16 0 2 452.07 453.37 54.97 o -14 0 2 12.48 23.19 33.34 o -12 0 2 12445.03 13548.70 131.46 o -10 0 2 367.84 483.97 27.61 o -8 0 2 1474.85 1699.78 32.25 o -6 0 2 3961.69 3713.28 34.07 o -4 0 2 66601.95 68119.16 830.71 o 4 0 2 5996.70 5894.41 62.28 o 6 0 2 7213.48 6828.95 46.68 o 8 0 2 7519.95 7372.98 86.27 o 10 0 2 4574.08 4822.20 48.49 o 12 0 2 1641.30 1480.66 44.04 o 14 0 2 3118.32 3083.02 99.37 o 16 0 2 286.90 316.59 53.05 o 18 0 2 30.21 36.02 68.96 o 20 0 2 159.03 191.81 76.00 o 22 0 2 110.74 89.02 116.30 o 24 0 2 213.09 218.67 86.31 o -23 1 2 0.03 -8.57 51.91 o -21 1 2 115.25 173.17 49.21 o -19 1 2 181.71 170.31 44.30 o -17 1 2 1057.59 1122.99 40.54 o -15 1 2 226.35 235.82 28.12 o -13 1 2 93.34 95.08 22.89 o -11 1 2 4.73 10.11 20.64 o -9 1 2 3070.27 3125.64 28.36 o -7 1 2 4493.20 4672.43 30.77 o -5 1 2 30517.18 30278.85 186.45 o -3 1 2 28141.07 27257.36 211.45 o -1 1 2 15721.51 15496.35 227.86 o 1 1 2 154.75 95.24 33.13 o 3 1 2 47349.71 46638.07 188.75 o 5 1 2 314.78 301.57 21.92 o 7 1 2 4690.01 5305.43 33.53 o 9 1 2 2343.27 2482.67 32.85 o 11 1 2 2718.15 2743.68 35.21 o 13 1 2 357.31 369.18 29.36 o 15 1 2 625.89 614.63 37.83 o 17 1 2 120.56 148.82 48.27 o 19 1 2 1411.38 1509.50 64.28 o 21 1 2 66.17 102.55 63.80 o 23 1 2 2.50 49.02 59.52 o -24 2 2 46.50 131.56 78.59 o -22 2 2 6.24 14.08 47.55 o -20 2 2 240.85 240.68 42.11 o -18 2 2 96.94 69.33 36.54 o -16 2 2 212.74 254.53 32.75 o -14 2 2 480.05 451.02 26.40 o -12 2 2 870.16 865.99 24.28 o -10 2 2 6200.19 6666.22 81.17 o -8 2 2 838.91 1055.52 36.76 o -6 2 2 138.25 143.38 25.48 o -4 2 2 21269.00 20985.79 176.99 o -2 2 2 238894.98 224108.33 1630.44 o 0 2 2 7074.71 6898.59 75.01 o 2 2 2 24.57 -1.38 17.54 o 4 2 2 1670.50 1750.71 25.12 o 6 2 2 4558.54 4663.45 41.65 o 8 2 2 2199.93 2152.33 31.58 o 10 2 2 147.54 121.58 25.87 o 12 2 2 571.55 571.96 27.59 o 14 2 2 148.14 196.73 32.64 o 16 2 2 65.79 58.56 39.67 o 18 2 2 783.11 853.51 57.85 o 20 2 2 701.89 827.06 58.93 o 22 2 2 0.03 -32.59 54.84 o -23 3 2 27.01 58.12 89.90 o -21 3 2 18.84 62.21 112.04 o -19 3 2 462.38 443.48 46.17 o -17 3 2 31.82 24.93 32.84 o -15 3 2 423.62 427.65 30.37 o -13 3 2 835.38 779.05 31.07 o -11 3 2 95.76 88.54 22.66 o -9 3 2 59.42 36.36 27.53 o -7 3 2 23450.57 24651.94 112.87 o -5 3 2 12113.13 13249.60 60.85 o -3 3 2 3335.66 3918.36 28.24 o -1 3 2 8057.10 8570.42 67.98 o 1 3 2 2130.11 2121.12 28.89 o 3 3 2 6676.47 6320.95 41.87 o 5 3 2 373.32 291.54 19.63 o 7 3 2 53.80 78.59 21.02 o 9 3 2 3848.83 4027.89 46.52 o 11 3 2 1454.81 1542.27 30.89 o 13 3 2 230.98 227.66 29.79 o 15 3 2 146.63 115.87 32.69 o 17 3 2 77.59 124.06 36.57 o 19 3 2 4.20 37.28 50.33 o 21 3 2 78.85 64.83 54.83 o -22 4 2 498.79 453.81 76.97 o -20 4 2 8.73 5.14 66.04 o -18 4 2 12.23 11.19 27.03 o -16 4 2 18.64 8.76 26.63 o -14 4 2 95.19 95.95 18.95 o -12 4 2 562.76 474.18 20.55 o -10 4 2 689.66 702.81 24.11 o -8 4 2 3496.18 3634.04 36.07 o -6 4 2 31830.07 33006.70 208.24 o -4 4 2 260.28 261.88 22.48 o -2 4 2 1716.60 1969.55 29.40 o 0 4 2 183.85 238.88 20.99 o 2 4 2 6901.96 6785.25 50.91 o 4 4 2 956.24 876.74 26.86 o 6 4 2 3308.23 3051.81 64.73 o 8 4 2 0.32 0.72 20.76 o 10 4 2 444.96 407.00 26.73 o 12 4 2 216.91 203.30 29.67 o 14 4 2 44.29 62.51 31.42 o 16 4 2 34.58 27.59 33.25 o 18 4 2 213.78 196.05 48.68 o 20 4 2 550.27 573.78 72.53 o -19 5 2 2.33 14.63 60.80 o -17 5 2 1.81 13.31 63.63 o -15 5 2 1.26 28.28 49.81 o -13 5 2 189.85 155.03 22.16 o -11 5 2 780.02 722.19 26.99 o -9 5 2 963.20 893.15 28.06 o -7 5 2 6155.76 6694.05 78.02 o -5 5 2 808.71 676.70 29.78 o -3 5 2 94.55 101.20 26.65 o -1 5 2 1005.67 1022.44 24.50 o 1 5 2 635.19 620.66 24.27 o 3 5 2 2618.94 3071.71 36.97 o 5 5 2 2133.35 2185.40 50.95 o 7 5 2 230.13 304.29 26.66 o 9 5 2 1172.77 1068.26 28.14 o 11 5 2 53.32 47.96 23.61 o 13 5 2 443.87 440.98 36.94 o 15 5 2 189.30 176.18 36.55 o 17 5 2 6.18 30.20 44.86 o 19 5 2 0.05 13.50 72.10 o -18 6 2 25.14 56.46 63.09 o -16 6 2 82.28 137.52 64.69 o -14 6 2 135.62 123.71 40.52 o -12 6 2 19.99 15.03 36.42 o -10 6 2 376.72 328.94 32.22 o -8 6 2 487.14 497.38 33.80 o -6 6 2 1977.23 2042.89 47.29 o -4 6 2 38.73 47.75 32.69 o -2 6 2 79.78 83.47 24.39 o 0 6 2 1.53 -21.96 25.02 o 2 6 2 3.89 21.99 26.25 o 4 6 2 2879.57 3123.54 43.05 o 6 6 2 363.46 376.81 35.37 o 8 6 2 70.19 85.59 36.04 o 10 6 2 0.23 -5.44 31.71 o 12 6 2 172.94 165.67 31.49 o 14 6 2 78.94 81.92 60.40 o 16 6 2 18.20 37.79 59.53 o 18 6 2 0.19 -12.47 69.54 o -15 7 2 76.20 23.92 67.34 o -13 7 2 6.82 -13.14 64.90 o -11 7 2 0.11 -48.32 60.17 o -9 7 2 70.60 35.33 54.74 o -7 7 2 30.20 15.79 39.58 o -5 7 2 98.17 87.91 36.07 o -3 7 2 3.50 35.51 33.53 o -1 7 2 25.20 18.14 31.94 o 1 7 2 27.32 31.35 33.34 o 3 7 2 128.24 115.05 34.44 o 5 7 2 124.59 103.86 36.41 o 7 7 2 4.56 41.29 40.74 o 9 7 2 23.37 45.45 50.38 o 11 7 2 1.10 48.02 64.28 o 13 7 2 32.09 70.00 60.71 o 15 7 2 149.02 124.49 77.25 o -12 8 2 0.57 -17.88 87.11 o -10 8 2 183.92 180.91 64.01 o -8 8 2 50.53 92.33 57.78 o -6 8 2 102.74 91.75 41.71 o -4 8 2 2.49 21.29 45.84 o -2 8 2 210.52 223.72 46.22 o 0 8 2 68.61 66.17 41.98 o 2 8 2 0.51 13.98 37.09 o 4 8 2 296.30 320.19 42.08 o 6 8 2 354.16 335.57 44.77 o 8 8 2 52.23 21.71 49.70 o 10 8 2 1.30 -2.04 51.61 o 12 8 2 67.96 120.72 91.29 o -5 9 2 64.86 69.76 52.44 o -3 9 2 8.02 20.17 50.67 o -1 9 2 362.21 408.53 52.28 o 1 9 2 9.58 26.71 49.00 o 3 9 2 3.00 -19.17 57.91 o 5 9 2 49.15 54.92 47.53 o -23 1 3 0.24 -8.17 49.57 o -21 1 3 221.24 218.04 47.76 o -19 1 3 225.50 179.44 42.09 o -17 1 3 1.21 33.11 33.24 o -15 1 3 362.67 370.88 26.83 o -13 1 3 12.28 -3.90 21.76 o -11 1 3 20307.11 22213.82 123.91 o -9 1 3 11.47 -6.80 17.09 o -7 1 3 21113.14 21054.89 133.52 o -5 1 3 20970.78 19621.38 99.59 o -3 1 3 25345.35 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