#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:52:42 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181199 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/78/2227869.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227869_Fobs loop_ _publ_author_name 'Schmitt, Laurette' 'Labat, Ga\"el' 'Stoeckli-Evans, Helen' _publ_section_title ; Aquachlorido(2,2':6',2''-terpyridyl)copper(II) chloride monohydrate ; _journal_coeditor_code OM2357 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1169 _journal_volume 66 _journal_year 2010 _space_group_IT_number 12 _symmetry_space_group_name_Hall '-C 2y' _symmetry_space_group_name_H-M 'C 1 2/m 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.532 _cell_angle_gamma 90.000 _cell_length_a 9.7155 _cell_length_b 13.6929 _cell_length_c 12.6599 _exptl_crystal_F_000 820.00 _reflns_d_resolution_high 0.7280 _cod_data_source_file om2357Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' LS70TG-3B IPDS2 -100DEGC C2/M' _shelx_refln_list_code 4 _shelx_f_calc_maximum 238.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x, -y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4133.48 4085.98 40.84 o 4 0 0 8194.75 7612.35 145.39 o 6 0 0 3542.14 3527.90 24.97 o 8 0 0 2843.00 2905.83 71.18 o 10 0 0 446.87 463.96 17.82 o 12 0 0 256.23 243.40 19.38 o 1 1 0 26730.00 29121.39 275.73 o 3 1 0 751.73 629.89 11.33 o 5 1 0 2715.36 2439.84 16.08 o 7 1 0 277.40 310.87 9.23 o 9 1 0 3844.31 3845.75 54.05 o 11 1 0 398.76 426.80 12.68 o 0 2 0 5117.76 5704.47 55.29 o 2 2 0 5497.11 5625.23 34.11 o 4 2 0 2186.11 1885.69 26.44 o 6 2 0 630.60 670.33 11.33 o 8 2 0 1135.72 1104.98 19.37 o 10 2 0 26.52 39.80 11.41 o 12 2 0 399.71 384.11 25.15 o 1 3 0 17242.73 17052.47 213.82 o 3 3 0 11392.58 10701.00 56.38 o 5 3 0 98.14 115.67 9.28 o 7 3 0 269.85 260.24 9.66 o 9 3 0 809.29 846.55 12.52 o 11 3 0 221.73 224.60 13.33 o 0 4 0 13743.40 13892.14 140.30 o 2 4 0 3714.70 3638.05 20.67 o 4 4 0 824.40 730.22 12.02 o 6 4 0 201.14 246.68 11.41 o 8 4 0 2341.22 2392.42 49.59 o 10 4 0 54.50 45.72 10.82 o 12 4 0 194.92 201.67 16.05 o 1 5 0 503.58 350.80 10.17 o 3 5 0 1545.14 1352.42 20.88 o 5 5 0 371.39 317.17 9.34 o 7 5 0 433.18 419.76 10.61 o 9 5 0 1850.35 1901.55 30.40 o 11 5 0 347.60 354.84 14.26 o 2 6 0 2672.25 2623.57 17.74 o 4 6 0 3413.12 3108.48 39.70 o 6 6 0 369.32 371.06 10.54 o 8 6 0 284.85 294.71 13.34 o 10 6 0 419.77 403.93 12.59 o 12 6 0 5.30 14.46 24.53 o 1 7 0 3799.75 3725.78 21.12 o 3 7 0 284.20 205.19 10.16 o 5 7 0 801.69 746.87 10.71 o 7 7 0 3.21 13.55 9.98 o 9 7 0 2966.63 3064.28 54.05 o 11 7 0 25.08 22.41 13.78 o 0 8 0 8777.30 8388.67 39.12 o 2 8 0 207.84 236.14 10.74 o 4 8 0 1031.85 959.42 12.25 o 6 8 0 144.25 126.59 10.84 o 8 8 0 1264.11 1287.25 19.95 o 10 8 0 71.32 64.85 12.44 o 1 9 0 5443.46 5255.44 62.46 o 3 9 0 9000.22 8888.10 51.47 o 5 9 0 299.58 315.66 10.89 o 7 9 0 127.83 155.94 11.50 o 9 9 0 377.59 412.36 17.93 o 11 9 0 322.53 303.13 18.99 o 0 10 0 9020.09 9157.03 218.03 o 2 10 0 1200.88 1150.95 18.17 o 4 10 0 2022.61 2003.42 26.54 o 6 10 0 1.19 3.57 12.29 o 8 10 0 1133.64 1151.36 43.95 o 10 10 0 15.73 33.82 15.35 o 1 11 0 2898.66 2880.98 16.78 o 3 11 0 125.52 121.46 11.72 o 5 11 0 7.72 21.80 10.02 o 7 11 0 433.76 421.11 15.13 o 9 11 0 1304.57 1255.02 42.29 o 0 12 0 20547.94 20714.62 122.09 o 2 12 0 59.33 80.03 12.30 o 4 12 0 129.64 148.05 10.29 o 6 12 0 361.71 330.80 12.47 o 8 12 0 451.49 429.99 22.58 o 1 13 0 2518.55 2468.38 29.13 o 3 13 0 1941.02 1870.70 17.30 o 5 13 0 964.11 993.37 18.06 o 7 13 0 36.69 37.29 12.81 o 9 13 0 959.10 898.94 78.33 o 0 14 0 3985.24 3951.88 30.20 o 2 14 0 52.87 58.46 13.85 o 4 14 0 1065.90 1011.26 15.00 o 6 14 0 137.79 128.16 11.80 o 8 14 0 514.77 506.97 31.05 o 1 15 0 1658.03 1726.93 15.82 o 3 15 0 662.46 672.57 16.88 o 5 15 0 3.91 4.39 11.91 o 7 15 0 10.29 37.32 15.62 o 0 16 0 1116.11 1037.16 19.90 o 2 16 0 530.74 558.03 14.42 o 4 16 0 322.79 287.85 13.46 o 6 16 0 0.98 9.07 14.22 o 1 17 0 4.16 19.40 12.78 o 3 17 0 36.74 32.60 13.61 o 5 17 0 23.14 29.70 14.89 o 0 18 0 2145.52 2009.99 43.36 o 2 18 0 57.51 52.39 14.11 o -12 0 1 304.57 311.50 19.13 o -10 0 1 1630.35 1686.15 47.81 o -8 0 1 545.59 551.60 16.59 o -6 0 1 15842.32 15301.67 302.91 o -4 0 1 1484.66 1513.92 24.69 o -2 0 1 12669.82 12888.32 98.33 o 0 0 1 5202.89 5348.97 51.54 o 2 0 1 4807.84 4499.09 62.08 o 4 0 1 4771.40 4685.60 60.13 o 6 0 1 17.54 25.39 15.30 o 8 0 1 4642.35 4431.30 197.25 o 10 0 1 325.96 333.89 15.05 o 12 0 1 442.18 402.12 20.54 o -11 1 1 35.89 42.78 11.08 o -9 1 1 472.03 502.74 12.17 o -7 1 1 2023.74 2048.72 21.22 o -5 1 1 1614.77 1475.41 22.16 o -3 1 1 3990.63 3880.90 51.67 o -1 1 1 16196.33 17665.45 87.18 o 1 1 1 447.28 411.42 13.89 o 3 1 1 12862.38 11886.39 61.41 o 5 1 1 3477.04 3342.32 20.16 o 7 1 1 495.99 478.92 11.71 o 9 1 1 369.28 356.46 12.84 o 11 1 1 133.98 145.43 14.00 o -12 2 1 30.94 46.83 13.02 o -10 2 1 1096.81 1148.12 14.35 o -8 2 1 174.93 227.62 9.12 o -6 2 1 2104.76 1935.31 18.45 o -4 2 1 476.58 523.28 12.30 o -2 2 1 4913.21 5380.20 30.42 o 0 2 1 3711.83 3713.03 47.66 o 2 2 1 2922.90 2647.21 20.39 o 4 2 1 9.09 15.91 9.24 o 6 2 1 578.04 532.44 11.09 o 8 2 1 406.62 393.92 15.85 o 10 2 1 14.08 13.86 12.29 o 12 2 1 158.39 124.87 14.35 o -11 3 1 59.97 61.42 12.38 o -9 3 1 4396.02 4561.27 57.96 o -7 3 1 1388.51 1333.05 14.27 o -5 3 1 4639.67 4140.66 82.74 o -3 3 1 2842.16 2764.58 21.61 o -1 3 1 4651.20 4518.37 33.84 o 1 3 1 1588.18 1544.92 16.76 o 3 3 1 1285.24 1113.10 13.48 o 5 3 1 2.06 0.62 9.88 o 7 3 1 554.87 546.28 12.05 o 9 3 1 559.80 572.05 12.15 o 11 3 1 1343.19 1243.89 52.62 o -12 4 1 502.88 455.83 17.29 o -10 4 1 1020.20 1099.17 15.16 o -8 4 1 208.39 213.39 12.45 o -6 4 1 3876.35 3855.02 45.59 o -4 4 1 1997.33 1835.38 18.52 o -2 4 1 147.68 194.24 9.23 o 0 4 1 14738.19 14033.37 121.15 o 2 4 1 10365.36 9609.58 77.46 o 4 4 1 471.80 447.96 10.78 o 6 4 1 3245.99 3156.99 58.00 o 8 4 1 1027.18 1024.00 15.27 o 10 4 1 383.79 409.78 12.23 o 12 4 1 141.92 112.91 15.12 o -11 5 1 165.44 174.82 15.36 o -9 5 1 2374.32 2388.05 38.68 o -7 5 1 66.50 51.17 10.27 o -5 5 1 320.24 266.11 10.65 o -3 5 1 497.23 449.80 12.06 o -1 5 1 29666.23 29801.47 186.79 o 1 5 1 353.65 363.42 11.14 o 3 5 1 20516.33 19771.96 187.40 o 5 5 1 1679.92 1596.49 14.34 o 7 5 1 77.95 81.54 10.66 o 9 5 1 47.51 51.35 10.88 o 11 5 1 778.61 718.74 32.21 o -12 6 1 13.14 18.06 14.84 o -10 6 1 3800.31 3987.67 90.21 o -8 6 1 1737.83 1867.49 24.29 o -6 6 1 5809.92 5664.15 54.73 o -4 6 1 4311.93 4773.16 55.84 o -2 6 1 15938.81 16277.10 105.15 o 0 6 1 4423.84 4498.22 23.13 o 2 6 1 6107.15 6125.92 63.41 o 4 6 1 7587.25 7937.48 57.07 o 6 6 1 686.58 758.60 11.75 o 8 6 1 1498.39 1512.06 28.23 o 10 6 1 1056.98 1076.32 14.19 o -11 7 1 201.25 188.24 16.03 o -9 7 1 1041.66 1105.13 13.40 o -7 7 1 1967.57 2012.32 14.36 o -5 7 1 1448.93 1403.06 15.11 o -3 7 1 172.61 249.36 10.65 o -1 7 1 14965.53 15001.97 58.14 o 1 7 1 158.67 170.09 9.17 o 3 7 1 11366.08 11195.80 87.80 o 5 7 1 117.30 96.66 9.28 o 7 7 1 531.95 513.99 19.09 o 9 7 1 490.77 485.42 14.33 o 11 7 1 366.57 335.22 15.03 o -10 8 1 591.07 666.19 19.48 o -8 8 1 181.23 198.86 11.76 o -6 8 1 1805.03 1796.43 22.19 o -4 8 1 3.79 11.90 9.24 o -2 8 1 113.75 101.98 9.81 o 0 8 1 6414.95 5945.21 29.42 o 2 8 1 5896.44 5660.38 27.20 o 4 8 1 417.94 400.30 10.86 o 6 8 1 723.49 707.46 10.98 o 8 8 1 417.26 422.64 11.70 o 10 8 1 1.85 21.02 15.40 o -11 9 1 71.73 77.25 14.74 o -9 9 1 2539.99 2692.45 28.92 o -7 9 1 347.14 367.86 13.05 o -5 9 1 2067.99 2080.14 29.04 o -3 9 1 704.93 747.70 13.77 o -1 9 1 5259.15 5256.79 69.77 o 1 9 1 399.22 405.29 10.16 o 3 9 1 3063.00 3050.91 33.86 o 5 9 1 1.36 -4.69 9.84 o 7 9 1 397.38 415.72 12.22 o 9 9 1 89.56 102.86 13.83 o -10 10 1 438.84 425.96 16.07 o -8 10 1 125.08 135.72 12.33 o -6 10 1 1737.02 1775.20 16.47 o -4 10 1 693.84 701.50 11.88 o -2 10 1 52.13 55.80 9.82 o 0 10 1 2603.69 2607.66 24.07 o 2 10 1 2561.76 2544.47 37.81 o 4 10 1 24.46 28.06 9.44 o 6 10 1 1088.23 1109.64 13.50 o 8 10 1 553.86 575.45 13.58 o 10 10 1 189.10 200.00 15.03 o -9 11 1 98.19 114.84 13.46 o -7 11 1 417.83 457.25 13.30 o -5 11 1 8.13 11.69 10.57 o -3 11 1 1396.93 1480.76 21.68 o -1 11 1 712.15 766.31 16.95 o 1 11 1 32.71 40.82 9.85 o 3 11 1 702.60 721.73 14.82 o 5 11 1 1956.34 1953.46 40.03 o 7 11 1 7.24 12.25 11.83 o 9 11 1 40.78 28.88 16.21 o -8 12 1 71.93 87.10 13.22 o -6 12 1 1772.31 1815.86 32.35 o -4 12 1 449.84 496.59 11.13 o -2 12 1 300.05 323.31 10.40 o 0 12 1 187.64 204.97 11.14 o 2 12 1 303.73 339.09 11.11 o 4 12 1 118.89 134.26 10.63 o 6 12 1 43.57 55.63 11.09 o 8 12 1 612.48 632.85 21.45 o -9 13 1 493.23 444.55 25.77 o -7 13 1 681.21 668.08 20.57 o -5 13 1 1293.83 1280.66 21.26 o -3 13 1 12.76 15.15 11.08 o -1 13 1 3398.16 3442.01 35.81 o 1 13 1 72.91 66.33 11.86 o 3 13 1 2931.01 2945.62 51.53 o 5 13 1 160.38 150.02 11.64 o 7 13 1 530.61 550.11 16.80 o -8 14 1 61.83 51.64 15.92 o -6 14 1 678.74 671.77 16.94 o -4 14 1 61.50 69.45 12.54 o -2 14 1 107.29 118.80 12.92 o 0 14 1 2533.96 2518.41 16.42 o 2 14 1 2543.82 2582.25 22.23 o 4 14 1 210.07 214.89 13.32 o 6 14 1 441.39 406.15 14.54 o 8 14 1 196.35 191.14 17.51 o -7 15 1 454.73 403.57 23.65 o -5 15 1 514.03 537.22 13.25 o -3 15 1 212.64 214.42 12.29 o -1 15 1 1464.26 1482.03 15.64 o 1 15 1 58.46 66.84 12.04 o 3 15 1 919.80 946.00 17.00 o 5 15 1 0.32 3.28 12.50 o 7 15 1 171.76 187.16 19.11 o -6 16 1 1031.73 930.62 34.43 o -4 16 1 14.18 16.98 14.21 o -2 16 1 162.72 170.51 12.57 o 0 16 1 606.90 597.37 13.46 o 2 16 1 731.29 750.01 17.09 o 4 16 1 173.72 171.10 13.16 o 6 16 1 98.36 84.02 15.21 o -5 17 1 18.47 31.49 14.92 o -3 17 1 25.32 23.38 13.08 o -1 17 1 1164.87 1082.60 20.45 o 1 17 1 13.43 24.94 15.05 o 3 17 1 1125.30 1027.98 20.41 o 5 17 1 133.84 117.91 16.19 o -2 18 1 328.11 324.90 14.24 o 0 18 1 379.95 368.79 15.44 o 2 18 1 450.83 424.14 16.73 o -12 0 2 237.51 236.00 19.36 o -10 0 2 899.84 941.22 26.17 o -8 0 2 2149.35 2191.09 26.25 o -6 0 2 8763.00 9388.04 197.92 o -4 0 2 1592.55 1641.28 38.16 o -2 0 2 8112.23 7365.73 50.31 o 0 0 2 15017.14 15009.38 131.87 o 4 0 2 332.38 528.26 16.14 o 6 0 2 2871.03 2651.40 26.23 o 8 0 2 1831.94 1892.38 24.04 o 10 0 2 1119.76 1153.99 18.97 o 12 0 2 68.06 74.77 21.46 o -13 1 2 0.25 -2.31 18.04 o -11 1 2 178.24 202.80 10.92 o -9 1 2 418.63 423.10 9.71 o -7 1 2 10953.86 11033.10 94.12 o -5 1 2 2.22 3.38 9.28 o -3 1 2 4618.02 4395.90 21.45 o -1 1 2 110.25 117.62 8.99 o 1 1 2 28179.49 29322.86 208.66 o 3 1 2 12254.68 12702.43 75.26 o 5 1 2 3134.97 2902.53 29.07 o 7 1 2 261.69 294.14 12.31 o 9 1 2 404.35 432.60 16.19 o 11 1 2 670.48 614.34 13.08 o -12 2 2 10.57 8.22 13.11 o -10 2 2 879.14 894.80 13.63 o -8 2 2 66.70 65.90 10.06 o -6 2 2 5115.07 4847.49 49.12 o -4 2 2 5934.03 6023.72 57.11 o -2 2 2 5384.01 4798.88 37.13 o 0 2 2 67.05 42.09 8.46 o 2 2 2 2198.21 1932.37 14.20 o 4 2 2 5664.32 5728.75 32.29 o 6 2 2 270.16 257.88 10.03 o 8 2 2 91.64 102.27 12.66 o 10 2 2 197.21 207.37 10.57 o 12 2 2 8.29 9.99 13.73 o -11 3 2 1297.46 1341.51 33.40 o -9 3 2 127.84 135.18 9.45 o -7 3 2 3298.77 3231.02 20.26 o -5 3 2 400.81 399.12 11.97 o -3 3 2 2196.94 2217.05 18.88 o -1 3 2 12436.40 12349.84 93.71 o 1 3 2 5179.59 4915.50 56.64 o 3 3 2 15619.15 14804.73 361.61 o 5 3 2 8530.97 8151.35 104.93 o 7 3 2 31.00 30.82 10.37 o 9 3 2 659.66 700.57 13.14 o 11 3 2 45.07 42.81 12.10 o -12 4 2 204.06 186.65 13.80 o -10 4 2 486.43 534.31 13.51 o -8 4 2 202.49 188.33 10.18 o -6 4 2 9426.74 9610.34 78.26 o -4 4 2 97.90 55.75 10.85 o -2 4 2 1793.09 1559.81 16.14 o 0 4 2 77.70 60.55 8.30 o 2 4 2 6679.92 6265.00 45.80 o 4 4 2 4700.69 4379.14 126.57 o 6 4 2 111.34 117.94 9.99 o 8 4 2 219.52 251.72 12.93 o 10 4 2 507.15 507.53 12.90 o -11 5 2 105.02 87.41 13.84 o -9 5 2 406.46 396.40 11.13 o -7 5 2 4497.33 4447.42 77.73 o -5 5 2 234.13 259.27 10.82 o -3 5 2 345.80 179.54 9.07 o -1 5 2 1267.38 1234.98 13.15 o 1 5 2 1285.79 1021.01 12.58 o 3 5 2 519.31 445.56 10.40 o 5 5 2 2583.64 2533.80 19.00 o 7 5 2 4.98 12.11 9.80 o 9 5 2 371.27 401.45 11.44 o 11 5 2 324.93 313.87 19.73 o -12 6 2 41.08 41.00 13.12 o -10 6 2 72.67 105.02 13.07 o -8 6 2 1451.52 1443.90 13.15 o -6 6 2 945.58 912.85 15.28 o -4 6 2 221.73 208.05 10.40 o -2 6 2 2833.97 2639.75 27.81 o 0 6 2 807.89 767.05 12.64 o 2 6 2 32661.58 32464.38 407.37 o 4 6 2 1496.11 1446.10 13.28 o 6 6 2 1390.83 1288.94 12.82 o 8 6 2 394.86 411.11 11.50 o 10 6 2 146.07 155.30 13.86 o -11 7 2 7.05 3.76 13.40 o -9 7 2 178.60 175.90 11.03 o -7 7 2 7602.29 7743.44 45.79 o -5 7 2 247.78 245.00 11.53 o -3 7 2 1360.37 1159.37 11.03 o -1 7 2 6.54 1.56 8.35 o 1 7 2 4739.00 4553.39 41.45 o 3 7 2 2401.76 2455.84 15.80 o 5 7 2 1437.69 1316.42 26.98 o 7 7 2 75.85 93.43 10.25 o 9 7 2 54.54 69.26 12.69 o 11 7 2 610.55 498.21 31.97 o -10 8 2 42.51 54.99 12.81 o -8 8 2 159.75 166.10 11.41 o -6 8 2 3892.34 3971.90 31.78 o -4 8 2 1439.39 1344.75 12.24 o -2 8 2 1751.15 1603.18 12.20 o 0 8 2 817.49 748.74 11.47 o 2 8 2 4762.85 4465.58 34.51 o 4 8 2 1119.83 1128.17 11.28 o 6 8 2 150.04 137.89 11.24 o 8 8 2 14.40 26.29 13.29 o 10 8 2 309.43 304.06 15.40 o -11 9 2 727.58 660.44 27.99 o -9 9 2 373.96 372.95 13.69 o -7 9 2 1469.75 1491.86 15.45 o -5 9 2 125.34 127.97 10.35 o -3 9 2 352.46 335.34 10.38 o -1 9 2 8195.23 7846.28 51.47 o 1 9 2 3315.99 3192.96 37.15 o 3 9 2 4980.78 4969.11 62.98 o 5 9 2 7122.87 7212.37 33.86 o 7 9 2 65.35 66.49 11.50 o 9 9 2 393.72 435.12 16.67 o -10 10 2 983.76 970.86 32.27 o -8 10 2 108.77 117.49 12.83 o -6 10 2 3630.02 3757.94 20.84 o -4 10 2 532.45 528.88 12.56 o -2 10 2 2848.26 2766.94 39.36 o 0 10 2 9.55 2.31 8.55 o 2 10 2 5626.78 5714.32 71.19 o 4 10 2 1906.05 1888.51 27.14 o 6 10 2 727.49 741.26 15.89 o 8 10 2 60.10 75.01 13.27 o 10 10 2 295.74 273.96 18.04 o -9 11 2 278.22 298.52 13.81 o -7 11 2 2817.67 2895.64 40.47 o -5 11 2 339.96 309.51 11.70 o -3 11 2 16.11 21.51 10.70 o -1 11 2 411.09 351.27 11.31 o 1 11 2 3553.66 3578.22 28.82 o 3 11 2 1702.61 1721.86 20.59 o 5 11 2 20.04 27.90 10.37 o 7 11 2 106.29 114.45 13.42 o 9 11 2 339.44 371.79 27.32 o -10 12 2 388.22 343.09 28.83 o -8 12 2 579.71 560.48 31.42 o -6 12 2 1134.20 1073.61 15.52 o -4 12 2 4.35 26.16 10.23 o -2 12 2 35.29 61.65 10.30 o 0 12 2 606.30 595.77 11.17 o 2 12 2 14147.14 14404.67 142.95 o 4 12 2 2.86 13.97 11.72 o 6 12 2 47.27 51.70 12.03 o 8 12 2 405.39 398.96 28.14 o -9 13 2 75.64 55.83 15.00 o -7 13 2 2418.19 2458.06 62.66 o -5 13 2 11.58 23.25 12.68 o -3 13 2 1552.05 1567.36 21.91 o -1 13 2 1311.90 1236.90 13.10 o 1 13 2 2660.94 2659.07 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