#------------------------------------------------------------------------------ #$Date: 2010-12-22 21:36:50 +0200 (Wed, 22 Dec 2010) $ #$Revision: 5269 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2227871.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227871_Fobs loop_ _publ_author_name 'Karpoormath, Rajshekhar' 'Govender, Thavendran' 'Govender, Patrick' 'Kruger, Hendrik G.' 'Maguire, Glenn E. M.' _publ_section_title ; tert-Butyl N-[(11-exo-benzyloxycarbonyl-8-oxopentacyclo[5.4.0.0^2,6^.0^3,10^.0^5,9^]undecane-11-endo-yloxy)carbonylmethyl]carbamate ; _journal_coeditor_code OM2360 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2607 _journal_page_last o2608 _journal_volume 66 _journal_year 2010 _space_group_IT_number 9 _symmetry_space_group_name_Hall 'C -2yc' _symmetry_space_group_name_H-M 'C 1 c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.679 _cell_angle_gamma 90.000 _cell_length_a 9.7260 _cell_length_b 27.5398 _cell_length_c 9.3500 _exptl_crystal_F_000 992.00 _reflns_d_resolution_high 0.8307 _[local]_cod_data_source_file om2360Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' gk07bocp in Cc' _shelx_refln_list_code 4 _shelx_f_calc_maximum 285.31 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 1 -11 15.02 11.13 2.70 o 4 2 -11 51.28 48.98 3.82 o 3 3 -11 58.20 73.27 6.17 o 3 5 -11 11.08 5.40 2.31 o 0 0 -10 100.10 94.82 4.82 o 2 0 -10 43.73 35.18 2.80 o 4 0 -10 31.95 31.08 2.80 o 6 0 -10 15.89 24.90 3.27 o -1 1 -10 6.45 11.75 2.04 o 1 1 -10 17.67 14.41 2.01 o 3 1 -10 20.20 20.97 1.91 o 5 1 -10 114.15 115.22 3.76 o 7 1 -10 193.79 187.66 5.18 o 0 2 -10 1.72 5.40 2.04 o 2 2 -10 11.69 18.71 2.20 o 4 2 -10 34.06 39.71 2.59 o 6 2 -10 69.68 65.84 2.89 o -1 3 -10 33.40 47.95 5.01 o 1 3 -10 18.92 24.17 2.48 o 3 3 -10 2.07 1.66 1.62 o 5 3 -10 27.57 37.29 2.59 o 7 3 -10 20.55 14.81 2.04 o 0 4 -10 7.20 8.69 1.95 o 2 4 -10 35.09 34.64 2.58 o 4 4 -10 0.85 1.91 1.62 o 6 4 -10 39.18 57.56 2.74 o -1 5 -10 56.73 59.43 3.82 o 1 5 -10 16.33 14.29 2.09 o 3 5 -10 162.44 175.35 4.37 o 5 5 -10 427.11 437.17 9.02 o 7 5 -10 197.34 196.52 4.11 o 0 6 -10 25.04 33.63 2.80 o 2 6 -10 5.69 1.89 1.70 o 4 6 -10 14.81 18.66 2.09 o 6 6 -10 25.67 43.47 2.67 o -1 7 -10 37.88 57.84 5.40 o 1 7 -10 19.74 21.32 2.66 o 3 7 -10 40.96 47.69 2.97 o 5 7 -10 5.84 0.39 1.78 o 7 7 -10 59.45 53.99 3.27 o 0 8 -10 29.86 24.54 2.50 o 2 8 -10 56.45 56.49 3.39 o 4 8 -10 76.32 52.11 4.47 o 6 8 -10 19.14 24.23 2.96 o 1 9 -10 74.41 76.72 4.26 o 3 9 -10 36.54 45.69 3.05 o 5 9 -10 85.21 78.67 6.94 o 7 9 -10 8.90 16.24 4.24 o 0 10 -10 52.03 43.02 3.86 o 2 10 -10 184.79 192.43 4.69 o 4 10 -10 54.86 44.37 3.51 o 6 10 -10 2.98 0.33 1.85 o 1 11 -10 18.94 22.53 2.96 o 3 11 -10 7.28 10.17 2.41 o 5 11 -10 67.20 70.96 6.17 o 2 12 -10 1.16 3.58 1.76 o 4 12 -10 27.38 28.54 4.63 o 6 12 -10 82.97 105.84 3.85 o 1 13 -10 35.34 39.33 3.86 o 3 13 -10 24.26 26.89 2.57 o 5 13 -10 33.82 55.53 5.40 o 2 14 -10 44.88 49.36 3.86 o 4 14 -10 24.35 28.54 4.63 o -3 1 -9 73.10 55.63 3.25 o -1 1 -9 27.58 38.68 3.05 o 1 1 -9 50.75 65.80 3.83 o 3 1 -9 123.07 104.44 3.39 o 5 1 -9 4.33 13.31 1.71 o 7 1 -9 13.67 11.48 1.81 o 9 1 -9 48.33 52.06 3.55 o -2 2 -9 65.45 72.01 3.90 o 0 2 -9 534.11 566.71 11.78 o 2 2 -9 298.08 293.80 5.96 o 4 2 -9 217.85 206.24 4.78 o 6 2 -9 71.66 80.91 3.80 o 8 2 -9 74.63 69.90 2.96 o -3 3 -9 18.49 17.91 2.04 o -1 3 -9 18.03 16.27 2.20 o 1 3 -9 22.04 20.45 2.09 o 3 3 -9 252.16 226.85 5.40 o 5 3 -9 51.99 69.70 4.09 o 7 3 -9 9.74 13.95 2.09 o 9 3 -9 8.74 7.46 1.78 o -2 4 -9 16.53 22.34 2.50 o 0 4 -9 162.23 151.88 6.79 o 2 4 -9 48.98 66.57 3.51 o 4 4 -9 57.21 57.79 3.02 o 6 4 -9 230.95 217.94 9.59 o 8 4 -9 146.53 156.01 4.11 o -3 5 -9 8.78 8.57 2.70 o -1 5 -9 3.01 5.92 1.76 o 1 5 -9 149.76 168.59 5.45 o 3 5 -9 127.09 91.66 4.22 o 5 5 -9 681.49 681.12 12.44 o 7 5 -9 78.18 63.79 3.94 o 9 5 -9 10.37 7.71 2.31 o -2 6 -9 37.76 32.64 6.94 o 0 6 -9 13.52 14.11 2.60 o 2 6 -9 74.68 59.47 4.23 o 4 6 -9 26.85 21.92 2.21 o 6 6 -9 45.03 41.13 2.86 o 8 6 -9 57.35 72.40 3.05 o -3 7 -9 38.43 28.16 3.27 o -1 7 -9 59.62 64.57 4.78 o 1 7 -9 166.98 163.95 5.34 o 3 7 -9 158.00 122.74 5.87 o 5 7 -9 211.74 195.30 5.79 o 7 7 -9 69.11 58.03 3.51 o 9 7 -9 20.48 23.14 3.09 o -2 8 -9 44.27 50.79 3.25 o 0 8 -9 152.20 159.21 4.51 o 2 8 -9 16.09 18.64 2.34 o 4 8 -9 43.37 45.05 3.73 o 6 8 -9 46.91 49.80 2.97 o 8 8 -9 18.97 21.83 2.96 o -1 9 -9 10.70 13.23 1.91 o 1 9 -9 28.08 23.75 2.31 o 3 9 -9 106.53 123.35 4.59 o 5 9 -9 57.26 53.42 4.26 o 7 9 -9 15.09 9.16 4.63 o -2 10 -9 21.50 27.93 2.96 o 0 10 -9 55.95 49.38 4.36 o 2 10 -9 144.34 138.01 4.31 o 4 10 -9 67.60 77.81 7.84 o 6 10 -9 56.14 49.33 3.85 o 8 10 -9 95.60 99.30 4.26 o -1 11 -9 1.41 2.57 1.78 o 1 11 -9 182.05 202.38 5.48 o 3 11 -9 24.43 30.93 3.27 o 5 11 -9 253.30 258.91 11.57 o 7 11 -9 23.61 25.44 2.57 o -2 12 -9 2.32 0.77 2.31 o 0 12 -9 5.70 6.68 1.78 o 2 12 -9 311.43 337.48 8.48 o 4 12 -9 156.04 163.15 6.17 o 6 12 -9 27.13 29.18 3.14 o 8 12 -9 41.31 34.57 5.01 o -1 13 -9 11.91 10.06 2.37 o 1 13 -9 71.82 98.45 8.48 o 3 13 -9 33.53 35.20 3.27 o 5 13 -9 70.81 83.96 13.88 o 7 13 -9 40.33 46.14 3.14 o 0 14 -9 55.46 56.19 3.51 o 2 14 -9 88.18 110.91 11.57 o 4 14 -9 33.65 57.74 3.51 o 6 14 -9 10.91 13.45 2.07 o -1 15 -9 12.15 12.34 2.31 o 1 15 -9 12.79 1.87 1.85 o 3 15 -9 18.49 14.86 2.41 o 5 15 -9 67.45 73.65 3.86 o 0 16 -9 69.75 75.95 7.71 o 2 16 -9 225.52 233.34 15.81 o 4 16 -9 18.07 22.37 3.86 o 1 17 -9 2.93 2.09 1.85 o 3 17 -9 51.42 53.22 4.63 o 5 17 -9 53.78 43.19 3.86 o 2 18 -9 59.38 58.62 4.63 o 4 18 -9 20.02 19.28 3.09 o -4 0 -8 96.39 108.75 7.71 o -2 0 -8 273.37 325.03 10.62 o 0 0 -8 91.80 83.19 5.10 o 2 0 -8 307.53 325.89 9.00 o 4 0 -8 1505.29 1479.99 17.69 o 6 0 -8 454.57 483.66 23.47 o 8 0 -8 64.83 48.38 3.59 o 10 0 -8 26.09 34.71 4.63 o -5 1 -8 9.41 7.71 2.18 o -3 1 -8 418.30 441.46 15.04 o -1 1 -8 15.97 14.22 2.46 o 1 1 -8 635.95 607.93 8.23 o 3 1 -8 40.77 42.39 2.44 o 5 1 -8 1038.60 972.06 12.06 o 7 1 -8 86.48 96.29 5.23 o 9 1 -8 41.11 42.84 2.48 o -4 2 -8 53.60 41.58 3.12 o -2 2 -8 33.18 24.52 2.87 o 0 2 -8 86.09 77.18 3.58 o 2 2 -8 191.75 179.88 4.23 o 4 2 -8 140.77 123.62 3.40 o 6 2 -8 480.38 468.87 7.67 o 8 2 -8 103.61 97.03 7.08 o 10 2 -8 0.53 -1.76 1.85 o -5 3 -8 3.44 -1.85 1.85 o -3 3 -8 109.50 111.66 10.40 o -1 3 -8 333.14 334.07 5.77 o 1 3 -8 34.53 42.77 2.70 o 3 3 -8 184.40 187.37 4.24 o 5 3 -8 19.57 14.82 1.95 o 7 3 -8 24.14 27.68 2.56 o 9 3 -8 34.82 35.92 2.48 o -4 4 -8 1.84 3.32 2.04 o -2 4 -8 389.93 399.96 7.58 o 0 4 -8 59.79 65.56 2.73 o 2 4 -8 427.92 462.13 6.49 o 4 4 -8 191.70 193.03 4.96 o 6 4 -8 417.13 418.92 8.26 o 8 4 -8 3.12 5.73 1.91 o -5 5 -8 2.55 3.09 3.09 o -3 5 -8 77.40 79.97 5.94 o -1 5 -8 141.28 140.31 4.17 o 1 5 -8 545.17 512.33 6.93 o 3 5 -8 188.01 192.22 3.97 o 5 5 -8 706.35 676.31 13.02 o 7 5 -8 15.13 18.75 2.34 o 9 5 -8 67.91 80.22 3.33 o -4 6 -8 41.04 52.60 3.17 o -2 6 -8 65.14 85.71 3.29 o 0 6 -8 222.62 218.47 5.38 o 2 6 -8 30.07 29.47 2.34 o 4 6 -8 519.51 535.90 7.84 o 6 6 -8 391.50 366.23 9.20 o 8 6 -8 126.78 128.93 6.38 o -3 7 -8 86.83 96.98 4.56 o -1 7 -8 197.82 178.98 4.76 o 1 7 -8 219.59 240.05 6.41 o 3 7 -8 19.10 14.71 2.07 o 5 7 -8 35.61 34.15 2.48 o 7 7 -8 456.05 464.15 13.98 o 9 7 -8 93.03 84.28 4.01 o -4 8 -8 109.35 131.37 4.82 o -2 8 -8 29.15 33.45 3.52 o 0 8 -8 21.91 14.92 2.35 o 2 8 -8 135.46 140.26 5.03 o 4 8 -8 1970.79 1817.95 20.34 o 6 8 -8 886.69 905.84 20.18 o 8 8 -8 23.88 35.34 2.66 o -3 9 -8 86.45 81.73 6.73 o -1 9 -8 749.44 772.51 13.15 o 1 9 -8 245.55 265.86 8.96 o 3 9 -8 273.11 258.32 16.97 o 5 9 -8 41.13 33.21 2.96 o 7 9 -8 116.48 131.11 10.03 o 9 9 -8 42.60 55.91 3.70 o -4 10 -8 20.78 20.33 2.04 o -2 10 -8 105.57 110.10 6.14 o 0 10 -8 139.25 151.26 7.66 o 2 10 -8 269.22 296.46 8.44 o 4 10 -8 255.64 300.33 8.44 o 6 10 -8 294.43 287.93 13.21 o 8 10 -8 98.68 123.71 5.37 o -3 11 -8 9.90 8.02 1.90 o -1 11 -8 65.85 50.92 3.35 o 1 11 -8 106.94 110.75 5.20 o 3 11 -8 501.96 520.34 22.75 o 5 11 -8 90.26 79.56 5.78 o 7 11 -8 35.86 41.20 2.96 o 9 11 -8 133.09 138.05 7.71 o -2 12 -8 76.66 74.25 4.96 o 0 12 -8 58.25 71.40 3.51 o 2 12 -8 219.49 216.50 5.60 o 4 12 -8 13.59 12.00 5.40 o 6 12 -8 154.20 163.32 13.50 o 8 12 -8 29.44 38.43 4.24 o -3 13 -8 16.78 19.36 2.23 o -1 13 -8 88.33 101.64 3.52 o 1 13 -8 19.91 19.95 2.35 o 3 13 -8 362.48 343.72 21.60 o 5 13 -8 26.69 27.92 2.96 o 7 13 -8 91.90 96.37 5.78 o -2 14 -8 19.42 19.87 1.81 o 0 14 -8 177.42 189.78 5.15 o 2 14 -8 274.26 292.81 12.24 o 4 14 -8 604.30 596.41 12.51 o 6 14 -8 184.25 204.18 20.05 o 8 14 -8 31.70 26.22 5.40 o -3 15 -8 20.84 21.22 2.18 o -1 15 -8 26.57 13.38 2.04 o 1 15 -8 146.65 163.74 4.86 o 3 15 -8 517.37 512.00 8.84 o 5 15 -8 198.64 189.73 9.26 o 7 15 -8 0.52 0.44 1.85 o -2 16 -8 24.83 20.15 2.04 o 0 16 -8 62.71 52.15 2.89 o 2 16 -8 288.20 299.38 8.94 o 4 16 -8 65.75 65.04 4.06 o 6 16 -8 56.16 70.96 5.40 o -1 17 -8 20.54 36.45 2.35 o 1 17 -8 8.80 10.19 1.90 o 3 17 -8 63.98 95.04 9.64 o 5 17 -8 117.44 155.79 8.48 o 7 17 -8 64.37 74.04 5.40 o -2 18 -8 19.00 17.00 2.18 o 0 18 -8 38.83 40.22 2.60 o 2 18 -8 5.16 7.54 2.41 o 4 18 -8 33.32 41.90 7.71 o 6 18 -8 80.39 80.98 6.17 o -1 19 -8 3.87 6.02 1.59 o 1 19 -8 222.82 216.04 6.48 o 3 19 -8 194.97 194.96 5.92 o 5 19 -8 35.46 31.62 4.63 o 0 20 -8 27.57 30.70 3.47 o 2 20 -8 2.88 1.87 1.85 o 4 20 -8 274.53 259.11 7.03 o 6 20 -8 150.65 147.31 6.94 o 1 21 -8 20.92 22.67 2.41 o 3 21 -8 90.94 89.28 4.36 o 5 21 -8 87.84 94.09 6.17 o 2 22 -8 25.61 23.91 3.86 o 4 22 -8 40.42 44.73 4.63 o -5 1 -7 38.93 34.67 3.82 o -3 1 -7 116.56 116.91 5.52 o -1 1 -7 202.94 200.55 6.17 o 1 1 -7 572.78 601.83 16.36 o 3 1 -7 521.54 438.96 13.09 o 5 1 -7 409.48 409.63 13.09 o 7 1 -7 923.72 872.03 16.04 o 9 1 -7 25.12 34.75 2.30 o -6 2 -7 33.82 42.77 3.86 o -4 2 -7 151.43 147.70 5.22 o -2 2 -7 1230.35 1184.07 16.54 o 0 2 -7 147.95 139.99 7.64 o 2 2 -7 58.96 65.42 5.71 o 4 2 -7 1095.71 1054.96 24.26 o 6 2 -7 850.81 788.66 12.54 o 8 2 -7 263.46 257.01 5.39 o 10 2 -7 65.65 66.56 3.17 o -5 3 -7 144.16 132.22 4.15 o -3 3 -7 416.48 425.79 9.15 o -1 3 -7 370.97 358.76 7.67 o 1 3 -7 122.31 119.72 7.09 o 3 3 -7 42.83 60.84 5.45 o 5 3 -7 1311.01 1286.11 39.33 o 7 3 -7 1198.62 1063.00 33.68 o 9 3 -7 43.65 52.50 3.26 o -6 4 -7 63.89 75.63 5.78 o -4 4 -7 151.99 184.91 6.95 o -2 4 -7 1005.77 977.82 20.07 o 0 4 -7 280.65 259.91 14.65 o 2 4 -7 316.92 288.86 11.18 o 4 4 -7 1032.78 1018.73 23.17 o 6 4 -7 1786.65 1800.59 24.08 o 8 4 -7 456.72 483.61 9.02 o 10 4 -7 23.46 27.77 3.27 o -5 5 -7 10.96 8.13 2.04 o -3 5 -7 192.04 191.45 6.20 o -1 5 -7 49.80 37.62 3.27 o 1 5 -7 581.47 588.47 23.14 o 3 5 -7 278.37 271.48 14.65 o 5 5 -7 802.09 738.35 17.33 o 7 5 -7 201.62 176.96 5.38 o 9 5 -7 51.78 59.19 4.34 o -6 6 -7 24.40 22.37 3.09 o -4 6 -7 157.17 155.94 5.31 o -2 6 -7 430.25 380.28 8.03 o 0 6 -7 1552.08 1486.21 44.73 o 2 6 -7 177.31 167.36 11.57 o 4 6 -7 745.33 739.64 26.22 o 6 6 -7 649.52 616.50 8.41 o 8 6 -7 601.14 657.12 22.82 o 10 6 -7 102.29 116.46 6.94 o -5 7 -7 166.63 170.14 7.02 o -3 7 -7 58.45 51.96 3.26 o -1 7 -7 163.66 180.41 4.46 o 1 7 -7 39.20 48.30 6.56 o 3 7 -7 2.44 -0.77 3.09 o 5 7 -7 1034.66 1031.14 21.49 o 7 7 -7 253.83 224.74 5.06 o 9 7 -7 421.96 434.20 10.46 o -4 8 -7 5.02 10.34 2.35 o -2 8 -7 174.59 193.87 4.39 o 0 8 -7 232.55 252.60 6.44 o 2 8 -7 161.94 158.71 6.84 o 4 8 -7 494.33 524.08 14.27 o 6 8 -7 281.36 323.66 9.13 o 8 8 -7 84.28 99.51 4.41 o 10 8 -7 2.95 2.31 3.09 o -5 9 -7 7.79 13.44 2.70 o -3 9 -7 109.54 140.89 3.70 o -1 9 -7 236.82 212.51 4.38 o 1 9 -7 743.25 691.41 11.47 o 3 9 -7 617.47 606.98 9.66 o 5 9 -7 396.18 382.75 10.19 o 7 9 -7 166.85 135.96 4.87 o 9 9 -7 9.98 3.92 2.04 o -4 10 -7 127.58 137.97 4.08 o -2 10 -7 141.81 134.69 4.34 o 0 10 -7 667.69 641.29 8.28 o 2 10 -7 10.48 19.43 3.23 o 4 10 -7 496.89 466.98 11.13 o 6 10 -7 1034.10 1027.88 53.22 o 8 10 -7 557.14 554.00 9.76 o 10 10 -7 135.43 159.65 7.71 o -5 11 -7 0.71 5.78 2.18 o -3 11 -7 213.55 194.58 7.17 o -1 11 -7 34.78 40.39 2.74 o 1 11 -7 110.07 117.74 3.58 o 3 11 -7 210.23 204.29 6.99 o 5 11 -7 1392.24 1336.15 16.83 o 7 11 -7 85.94 74.88 5.78 o 9 11 -7 250.04 264.54 12.34 o -4 12 -7 82.52 91.08 4.79 o -2 12 -7 118.04 114.87 4.23 o 0 12 -7 418.21 444.22 14.54 o 2 12 -7 295.58 259.98 6.55 o 4 12 -7 268.38 243.14 5.45 o 6 12 -7 170.41 190.99 6.80 o 8 12 -7 19.76 17.68 2.41 o -5 13 -7 134.55 142.76 4.14 o -3 13 -7 65.91 61.95 2.97 o -1 13 -7 371.09 373.65 17.19 o 1 13 -7 301.70 295.26 7.68 o 3 13 -7 965.82 903.96 12.19 o 5 13 -7 151.99 158.78 4.86 o 7 13 -7 184.87 198.75 8.42 o 9 13 -7 332.75 339.35 13.88 o -4 14 -7 26.30 23.61 2.01 o -2 14 -7 193.92 189.35 4.69 o 0 14 -7 74.28 77.22 6.02 o 2 14 -7 172.90 162.01 4.86 o 4 14 -7 284.80 284.00 8.13 o 6 14 -7 23.62 25.14 2.50 o 8 14 -7 117.77 112.37 4.61 o -3 15 -7 66.68 77.73 5.34 o -1 15 -7 391.66 400.87 17.49 o 1 15 -7 109.69 108.59 5.67 o 3 15 -7 177.13 181.29 6.94 o 5 15 -7 52.10 48.03 4.05 o 7 15 -7 77.95 73.50 4.42 o -4 16 -7 7.49 9.95 1.62 o -2 16 -7 0.92 6.56 1.90 o 0 16 -7 299.31 286.18 6.76 o 2 16 -7 53.01 49.94 4.63 o 4 16 -7 109.35 115.77 4.54 o 6 16 -7 21.72 29.14 2.80 o 8 16 -7 42.45 50.13 4.63 o -3 17 -7 59.26 67.53 3.35 o 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13.83 21.60 4.63 o 2 6 9 38.61 31.83 3.51 o -7 7 9 69.11 65.56 6.17 o -5 7 9 208.28 168.91 9.26 o -3 7 9 156.87 121.09 9.26 o -1 7 9 165.35 174.30 10.03 o 1 7 9 60.28 62.47 6.17 o 3 7 9 37.81 35.90 3.27 o -8 8 9 18.53 24.68 3.86 o -6 8 9 47.57 50.90 5.40 o -2 8 9 14.90 25.45 5.40 o 0 8 9 153.20 158.11 9.26 o 2 8 9 44.05 63.58 4.06 o -7 9 9 14.51 12.34 3.86 o -5 9 9 56.91 43.96 5.40 o -3 9 9 107.59 131.11 9.26 o -1 9 9 28.21 24.68 5.40 o 1 9 9 10.26 12.34 3.86 o -8 10 9 95.38 102.58 6.17 o -6 10 9 56.31 44.73 4.63 o -4 10 9 65.22 72.50 6.17 o -2 10 9 145.62 141.91 9.26 o 0 10 9 55.60 50.13 6.17 o 2 10 9 20.94 31.10 3.51 o -7 11 9 23.82 24.68 3.86 o -5 11 9 253.37 236.00 10.03 o -3 11 9 24.08 21.60 5.40 o -1 11 9 181.25 202.07 10.03 o 1 11 9 1.40 0.00 2.73 o -6 12 9 25.25 26.22 3.86 o -4 12 9 158.37 168.91 8.48 o -2 12 9 310.50 293.85 13.11 o 0 12 9 5.97 8.62 6.56 o 2 12 9 2.39 1.54 3.09 o -7 13 9 40.53 53.22 3.86 o -5 13 9 68.96 86.38 6.17 o -3 13 9 34.63 21.60 3.86 o -1 13 9 71.20 82.97 5.16 o 1 13 9 11.79 7.03 2.70 o -6 14 9 11.59 12.34 3.09 o -4 14 9 34.30 50.90 4.63 o -2 14 9 88.36 102.24 6.94 o 0 14 9 55.83 53.01 4.06 o -5 15 9 68.54 71.73 6.94 o -3 15 9 18.61 18.51 4.63 o -1 15 9 12.84 3.09 3.09 o 1 15 9 12.18 12.34 3.09 o -6 16 9 31.61 40.88 5.40 o -4 16 9 18.22 16.97 4.63 o -2 16 9 225.88 229.83 10.80 o 0 16 9 69.22 73.27 6.17 o -5 17 9 53.10 50.13 5.40 o -3 17 9 51.34 43.96 5.40 o -1 17 9 2.94 0.00 3.09 o -4 18 9 20.68 18.51 3.86 o -2 18 9 58.99 47.82 4.63 o -3 19 9 9.73 13.11 3.09 o -1 19 9 31.81 54.76 4.63 o 0 0 10 100.75 108.75 7.71 o -1 1 10 18.00 21.54 3.86 o 1 1 10 6.41 8.48 2.73 o -2 2 10 11.31 18.51 4.63 o 0 2 10 1.75 3.39 6.17 o -7 3 10 19.70 17.74 3.86 o -3 3 10 2.17 4.63 3.86 o -1 3 10 18.97 32.39 5.40 o 1 3 10 33.60 51.67 3.82 o -6 4 10 38.42 57.07 5.40 o -2 4 10 34.92 23.91 4.63 o 0 4 10 7.14 8.48 3.86 o -7 5 10 198.81 198.98 8.48 o -5 5 10 425.22 447.33 14.65 o -3 5 10 162.35 172.76 10.03 o -1 5 10 17.21 15.43 4.63 o 1 5 10 56.79 70.26 3.82 o -6 6 10 26.57 45.50 4.63 o -2 6 10 5.38 0.77 3.86 o 0 6 10 24.98 31.62 4.63 o -7 7 10 59.79 47.82 4.63 o -5 7 10 5.90 6.94 3.09 o -3 7 10 39.75 41.65 6.17 o -1 7 10 20.49 23.91 4.63 o 1 7 10 38.02 60.93 5.40 o -6 8 10 19.26 19.28 3.86 o -4 8 10 77.15 48.59 4.63 o -2 8 10 56.64 63.24 6.17 o 0 8 10 29.48 23.91 3.86 o -5 9 10 83.29 80.21 6.17 o -1 9 10 74.31 74.04 6.17 o -6 10 10 3.02 1.54 2.31 o -4 10 10 57.32 40.88 4.63 o -2 10 10 183.92 198.98 10.03 o 0 10 10 51.63 47.82 4.63 o -5 11 10 67.57 85.61 5.40 o -3 11 10 7.02 10.80 3.09 o -1 11 10 19.47 25.45 4.63 o -4 12 10 26.68 33.94 3.86 o -2 12 10 1.04 5.40 2.31 o