Crystallography Open Database

Information card for entry 2227916

Preview

Coordinates	2227916.cif
Structure factors	2227916.hkl
Original IUCr paper	HTML

Structure parameters

Chemical name	Poly[[bis[μ~2~-<i>N</i>,<i>N</i>'-bis(2-pyridylmethyl)oxalamide- κ^4^<i>N</i>,<i>O</i>:<i>N</i>',<i>O</i>'][μ~2~-<i>N</i>,<i>N</i>'- bis(2-pyridylmethyl)oxalamide-κ^2^<i>N</i>:<i>N</i>']disilver(I)] bis(trifluoromethanesulfonate)]
Formula	C22 H21 Ag F3 N6 O6 S
Calculated formula	C22 H21 Ag F3 N6 O6 S
Title of publication	Poly[[bis[μ~2~-<i>N</i>,<i>N</i>'-bis(2-pyridylmethyl)oxalamide-κ^4^<i>N</i>,<i>O</i>:<i>N</i>',<i>O</i>'][μ~2~-<i>N</i>,<i>N</i>'-bis(2-pyridylmethyl)oxalamide-κ^2^<i>N</i>:<i>N</i>']disilver(I)] bis(trifluoromethanesulfonate)]
Authors of publication	Arman, Hadi D.; Miller, Tyler; Poplaukhin, Pavel; Tiekink, Edward R. T.
Journal of publication	Acta Crystallographica Section E
Year of publication	2010
Journal volume	66
Journal issue	9
Pages of publication	m1167 - m1168
a	8.7242 ± 0.0014 Å
b	11.1762 ± 0.0017 Å
c	14.21 ± 0.002 Å
α	95.977 ± 0.001°
β	105.948 ± 0.002°
γ	107.017 ± 0.003°
Cell volume	1247.9 ± 0.3 Å³
Cell temperature	98 ± 2 K
Ambient diffraction temperature	98 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.036
Residual factor for significantly intense reflections	0.034
Weighted residual factors for significantly intense reflections	0.077
Weighted residual factors for all reflections included in the refinement	0.079
Goodness-of-fit parameter for all reflections included in the refinement	1.05
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	Yes

Version history

Revision	Date	Message	Files
181200 (current)	2016-04-03	hkl/2/22/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/22/79.	2227916.cif 2227916.hkl
176435	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries from ranges 1, 2.	2227916.cif 2227916.hkl
120072	2014-07-11	Adding DOIs to range 2 structures.	2227916.cif 2227916.hkl
88064	2013-08-29	Adding _cod_database_fobs_code data item to all COD CIFs that have Fobs deposited and did not have this data item yet.	2227916.cif 2227916.hkl
26848	2011-09-28	cif/2/, hkl/2/, html/ Reorganising CIFs of the range 2* into the "prefix-directory" tree.	2227916.cif 2227916.hkl
5269	2010-12-22	hkl/ Adding Fobs data for the recent IUCr-published structres.	2227916.cif 2227916.hkl
4953	2010-12-18	../uploads/cif-deposit/cod/cif Adding structures of 2227916 via cif-deposit CGI script.	2227916.cif