#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/79/2227917.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227917_Fobs loop_ _publ_author_name 'Wang, Xiao-Jun' 'Zheng, Chun' 'Mai, Shao-Wei' 'Xu, Xuan' 'Luo, Yi-Fan' _publ_section_title ; Bis(2,2'-bipyridine)(2-hydroxy-2,2-diphenylacetato)copper(II) nitrate dihydrate ; _journal_coeditor_code PV2323 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1245 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 108.220 _cell_angle_gamma 90.000 _cell_length_a 10.6119 _cell_length_b 25.7584 _cell_length_c 12.3219 _exptl_crystal_F_000 1452.00 _reflns_d_resolution_high 0.8347 _[local]_cod_data_source_file pv2323Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 315.75 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 7414.71 9489.97 348.06 o 2 0 0 5391.48 6820.59 259.98 o 3 0 0 667.77 763.85 28.85 o 4 0 0 976.66 925.24 69.59 o 5 0 0 2802.13 3283.09 96.13 o 6 0 0 2786.38 3110.98 160.30 o 7 0 0 759.30 751.05 80.86 o 8 0 0 1134.74 978.64 100.01 o 9 0 0 53.26 42.24 54.05 o 10 0 0 525.84 410.32 85.46 o 11 0 0 551.65 811.23 117.30 o 12 0 0 1525.92 1529.89 162.05 o 1 1 0 523.91 611.02 25.02 o 2 1 0 20515.21 24485.05 499.86 o 3 1 0 13206.50 15139.09 315.40 o 4 1 0 2033.09 1982.79 67.34 o 5 1 0 64.91 74.61 14.14 o 6 1 0 14.08 39.21 27.30 o 7 1 0 1569.57 1626.65 80.70 o 8 1 0 868.22 864.81 65.69 o 9 1 0 330.80 422.53 55.45 o 10 1 0 155.47 74.94 43.32 o 11 1 0 43.40 50.19 114.18 o 12 1 0 151.42 31.95 102.69 o 0 2 0 163.34 308.11 21.17 o 1 2 0 96.04 64.91 11.82 o 2 2 0 6398.74 7499.12 159.71 o 3 2 0 3516.32 4552.40 122.95 o 4 2 0 10.52 5.60 10.62 o 5 2 0 595.52 587.58 29.18 o 6 2 0 652.03 657.55 33.66 o 7 2 0 50.97 100.94 31.71 o 8 2 0 0.66 -25.22 27.82 o 9 2 0 0.09 -10.30 34.54 o 10 2 0 1.76 -27.25 39.72 o 11 2 0 10.65 15.34 48.19 o 12 2 0 208.87 25.85 76.05 o 1 3 0 1854.81 1848.85 37.10 o 2 3 0 3741.06 4062.83 127.86 o 3 3 0 1525.34 1713.35 47.73 o 4 3 0 10928.18 11539.33 247.87 o 5 3 0 777.62 785.79 39.64 o 6 3 0 63.21 105.45 20.01 o 7 3 0 679.31 804.21 59.87 o 8 3 0 1181.75 1234.49 77.24 o 9 3 0 588.64 804.08 69.51 o 10 3 0 178.72 128.21 54.82 o 11 3 0 93.94 86.30 51.53 o 12 3 0 11.33 -10.70 53.69 o 0 4 0 4011.89 5367.44 240.99 o 1 4 0 169.54 160.10 12.95 o 2 4 0 370.89 365.46 21.64 o 3 4 0 7903.74 7948.70 224.79 o 4 4 0 2292.69 2475.39 78.89 o 5 4 0 2607.28 3093.48 82.63 o 6 4 0 7772.17 8555.98 196.14 o 7 4 0 2191.31 2375.38 101.08 o 8 4 0 1352.87 1486.43 111.94 o 9 4 0 93.17 86.34 41.98 o 10 4 0 485.00 628.05 122.77 o 11 4 0 150.44 103.01 53.73 o 1 5 0 6872.51 6504.87 120.33 o 2 5 0 450.72 704.14 35.24 o 3 5 0 5062.95 5202.12 113.49 o 4 5 0 1224.70 1515.83 49.13 o 5 5 0 2976.60 3223.22 86.66 o 6 5 0 520.68 642.42 58.96 o 7 5 0 3864.72 4046.37 146.03 o 8 5 0 3993.33 3928.00 150.13 o 9 5 0 30.73 -21.64 34.61 o 10 5 0 16.27 -4.68 42.51 o 11 5 0 11.70 -8.03 47.75 o 0 6 0 5234.44 5816.46 127.87 o 1 6 0 9219.89 9599.98 195.93 o 2 6 0 1891.91 1687.91 40.23 o 3 6 0 6072.95 5872.33 128.34 o 4 6 0 526.17 531.57 29.42 o 5 6 0 943.40 1090.93 59.61 o 6 6 0 1908.94 2011.79 94.42 o 7 6 0 20.42 25.78 21.37 o 8 6 0 11.00 -45.71 30.47 o 9 6 0 23.02 15.46 35.62 o 10 6 0 108.98 42.61 44.76 o 11 6 0 56.69 41.75 52.11 o 1 7 0 3.20 14.05 15.94 o 2 7 0 571.21 462.31 20.13 o 3 7 0 6273.61 6443.10 124.47 o 4 7 0 790.01 985.91 50.96 o 5 7 0 79.09 70.88 29.32 o 6 7 0 5.70 49.15 19.88 o 7 7 0 384.40 414.08 34.89 o 8 7 0 8.54 -17.09 33.36 o 9 7 0 258.52 281.97 51.76 o 10 7 0 404.40 459.87 120.96 o 11 7 0 4.83 -10.23 48.77 o 0 8 0 4087.00 4021.66 95.68 o 1 8 0 6978.81 7332.67 139.32 o 2 8 0 2356.74 2602.31 58.70 o 3 8 0 954.66 968.25 31.43 o 4 8 0 2403.97 2403.81 76.08 o 5 8 0 161.41 178.95 23.62 o 6 8 0 329.49 320.01 34.94 o 7 8 0 779.45 790.65 46.01 o 8 8 0 22.35 -2.95 30.76 o 9 8 0 217.75 242.32 52.42 o 10 8 0 69.96 140.40 53.75 o 11 8 0 166.53 80.39 57.19 o 1 9 0 202.54 74.86 13.04 o 2 9 0 2300.19 2347.30 56.08 o 3 9 0 2026.24 1893.86 52.35 o 4 9 0 1831.54 1639.66 52.67 o 5 9 0 531.88 547.93 35.91 o 6 9 0 500.04 557.30 38.60 o 7 9 0 204.40 204.02 36.12 o 8 9 0 946.50 1015.70 77.78 o 9 9 0 232.00 150.59 134.97 o 10 9 0 1.87 -32.04 42.84 o 11 9 0 0.78 -66.76 44.51 o 0 10 0 3854.20 3757.87 93.97 o 1 10 0 475.44 473.74 24.10 o 2 10 0 1067.35 1117.48 36.31 o 3 10 0 548.52 592.50 27.09 o 4 10 0 1260.63 1405.72 42.58 o 5 10 0 172.23 126.07 23.88 o 6 10 0 16.20 36.16 22.87 o 7 10 0 316.97 292.16 34.36 o 8 10 0 447.68 327.44 52.87 o 9 10 0 41.67 64.54 43.09 o 10 10 0 0.23 31.61 66.36 o 11 10 0 2.97 -15.67 50.44 o 1 11 0 3438.40 3354.36 75.49 o 2 11 0 66.53 124.22 18.82 o 3 11 0 7373.35 7367.97 145.89 o 4 11 0 652.43 697.08 31.35 o 5 11 0 1521.67 1688.97 110.46 o 6 11 0 3.01 6.18 18.98 o 7 11 0 753.75 598.58 38.54 o 8 11 0 111.77 144.77 45.91 o 9 11 0 256.15 309.83 59.48 o 10 11 0 221.81 118.95 53.31 o 11 11 0 7.50 -4.29 50.38 o 0 12 0 2403.68 2225.23 66.99 o 1 12 0 15391.79 14836.06 274.97 o 2 12 0 681.89 713.59 31.22 o 3 12 0 49.08 50.57 15.69 o 4 12 0 5202.20 5046.36 108.90 o 5 12 0 2537.46 2491.44 81.84 o 6 12 0 1288.53 1278.32 50.88 o 7 12 0 1864.06 1830.48 64.28 o 8 12 0 263.21 221.13 43.66 o 9 12 0 145.92 114.75 35.89 o 10 12 0 366.32 337.58 66.67 o 11 12 0 502.98 404.14 55.18 o 1 13 0 39.55 67.83 16.37 o 2 13 0 8889.56 8818.53 173.48 o 3 13 0 5452.04 5810.36 122.67 o 4 13 0 3324.26 3148.36 79.41 o 5 13 0 2387.32 2510.20 84.09 o 6 13 0 68.34 52.74 29.61 o 7 13 0 1756.08 1747.26 63.75 o 8 13 0 468.30 424.86 38.02 o 9 13 0 708.13 759.65 64.00 o 10 13 0 198.96 196.79 45.79 o 0 14 0 1334.93 1248.63 74.88 o 1 14 0 599.92 666.72 38.16 o 2 14 0 1456.82 1584.01 50.35 o 3 14 0 86.76 61.68 18.57 o 4 14 0 78.02 115.19 21.52 o 5 14 0 1313.29 1331.17 61.06 o 6 14 0 8.89 4.39 25.41 o 7 14 0 0.59 -12.30 22.22 o 8 14 0 105.88 54.35 27.36 o 9 14 0 57.39 33.80 42.87 o 10 14 0 35.09 -15.96 34.98 o 1 15 0 166.73 208.53 23.82 o 2 15 0 5.05 -6.74 21.35 o 3 15 0 5141.62 5281.40 117.26 o 4 15 0 409.68 409.38 53.76 o 5 15 0 620.63 605.69 46.09 o 6 15 0 113.77 72.71 49.81 o 7 15 0 324.15 374.49 36.95 o 8 15 0 3.81 -26.01 24.59 o 9 15 0 343.13 388.20 51.01 o 10 15 0 62.10 -25.59 37.09 o 0 16 0 1698.35 1530.26 60.41 o 1 16 0 2151.32 1982.75 68.73 o 2 16 0 1387.39 1457.03 66.68 o 3 16 0 2.59 14.97 19.24 o 4 16 0 407.91 458.45 33.06 o 5 16 0 597.72 654.15 48.65 o 6 16 0 1316.75 1436.81 69.04 o 7 16 0 1469.74 1419.54 60.45 o 8 16 0 9.88 0.39 26.42 o 9 16 0 311.28 274.77 49.22 o 10 16 0 109.58 166.58 45.14 o 1 17 0 376.88 369.87 30.26 o 2 17 0 1338.88 1369.67 51.27 o 3 17 0 7556.02 7661.41 188.84 o 4 17 0 4795.95 4795.30 113.03 o 5 17 0 45.34 40.83 28.91 o 6 17 0 628.55 627.35 51.50 o 7 17 0 676.58 617.07 45.03 o 8 17 0 169.85 174.75 33.52 o 9 17 0 1048.90 802.79 66.66 o 10 17 0 237.62 102.36 52.44 o 0 18 0 691.38 670.70 56.35 o 1 18 0 614.25 639.77 38.14 o 2 18 0 34.48 22.04 21.86 o 3 18 0 589.69 588.55 38.06 o 4 18 0 1042.68 1142.68 50.53 o 5 18 0 521.60 524.56 48.57 o 6 18 0 58.72 80.23 34.11 o 7 18 0 247.66 247.44 35.31 o 8 18 0 46.48 41.16 29.04 o 9 18 0 189.42 114.91 41.86 o 1 19 0 214.19 261.75 41.06 o 2 19 0 686.54 677.28 41.09 o 3 19 0 182.66 146.62 27.34 o 4 19 0 3.15 -10.23 28.13 o 5 19 0 484.15 445.08 46.53 o 6 19 0 8.08 0.19 32.50 o 7 19 0 667.03 591.22 56.92 o 8 19 0 9.74 -23.62 57.36 o 9 19 0 8.39 -22.87 61.60 o 0 20 0 981.79 1082.31 72.39 o 1 20 0 96.37 74.76 23.49 o 2 20 0 208.12 221.42 30.45 o 3 20 0 410.69 385.70 35.88 o 4 20 0 360.17 370.72 45.13 o 5 20 0 1474.72 1547.33 76.24 o 6 20 0 372.94 416.05 50.10 o 7 20 0 3.64 -34.42 41.43 o 8 20 0 6.62 -34.79 34.22 o 9 20 0 12.60 3.21 46.41 o 1 21 0 292.12 349.75 36.23 o 2 21 0 573.87 623.00 41.81 o 3 21 0 1169.54 1163.08 76.19 o 4 21 0 5.01 -21.23 30.48 o 5 21 0 177.16 176.65 52.57 o 6 21 0 51.04 31.36 36.62 o 7 21 0 39.78 41.46 38.38 o 8 21 0 193.56 200.83 44.10 o 0 22 0 3.08 -27.25 40.92 o 1 22 0 370.25 433.01 38.23 o 2 22 0 62.74 89.27 26.36 o 3 22 0 169.91 201.65 31.57 o 4 22 0 65.58 50.44 33.89 o 5 22 0 3.99 -22.73 33.60 o 6 22 0 121.01 97.05 41.30 o 7 22 0 3.20 82.05 51.00 o 8 22 0 38.60 58.28 40.99 o 1 23 0 7.05 33.66 25.26 o 2 23 0 6.50 4.00 27.57 o 3 23 0 46.88 80.32 28.08 o 4 23 0 21.19 31.49 35.11 o 5 23 0 0.73 3.51 35.80 o 6 23 0 0.05 45.48 89.45 o 7 23 0 0.12 -77.80 58.54 o 8 23 0 9.44 -8.33 76.81 o 0 24 0 2658.32 2875.30 173.76 o 1 24 0 908.65 880.50 59.89 o 2 24 0 13.12 4.79 25.65 o 3 24 0 126.20 143.75 31.73 o 4 24 0 21.39 4.16 36.55 o 5 24 0 211.86 24.84 63.13 o 6 24 0 146.33 135.46 72.33 o 7 24 0 218.03 199.80 79.55 o 1 25 0 96.08 -15.34 37.37 o 2 25 0 1855.46 2027.76 76.85 o 3 25 0 1355.95 1584.50 81.33 o 4 25 0 251.23 221.90 79.55 o 5 25 0 164.26 188.09 79.55 o 6 25 0 0.51 24.73 66.20 o 7 25 0 159.40 194.87 84.91 o 0 26 0 306.60 322.13 76.05 o 1 26 0 71.92 47.24 34.89 o 2 26 0 0.39 51.22 30.28 o 3 26 0 0.38 44.23 52.96 o 4 26 0 56.39 29.76 66.09 o 5 26 0 358.55 281.21 88.96 o 6 26 0 97.39 180.98 83.05 o 1 27 0 1.70 19.97 39.59 o 2 27 0 2.21 -4.71 37.41 o 3 27 0 4.60 55.58 64.78 o 4 27 0 7.99 58.21 71.67 o 5 27 0 3.62 -35.01 59.30 o 0 28 0 569.18 851.49 111.50 o 1 28 0 184.93 186.38 50.71 o 2 28 0 125.66 154.72 68.39 o 3 28 0 15.25 16.41 67.62 o 4 28 0 235.27 271.58 90.27 o 5 28 0 259.44 290.94 93.33 o 1 29 0 40.28 32.58 45.85 o 2 29 0 1100.62 1252.78 93.81 o 3 29 0 674.66 831.69 121.02 o 4 29 0 295.49 475.97 107.01 o 0 30 0 89.99 5.36 64.01 o 1 30 0 130.49 99.12 77.09 o 2 30 0 46.77 122.90 52.26 o -12 1 1 294.99 205.50 105.15 o -11 1 1 183.24 94.02 48.41 o -10 1 1 144.45 129.99 50.50 o -9 1 1 190.21 255.35 47.85 o -8 1 1 2698.86 2857.88 116.86 o -7 1 1 967.72 1001.08 62.71 o -6 1 1 2607.52 2523.69 69.34 o -5 1 1 2.15 17.58 11.10 o -4 1 1 687.26 615.49 27.28 o -3 1 1 2580.25 2988.77 58.78 o -2 1 1 8286.45 8594.71 174.72 o -1 1 1 20697.42 18063.50 432.19 o 0 1 1 19090.31 19998.16 369.49 o 1 1 1 7491.07 8868.36 158.62 o 2 1 1 26461.88 32041.01 557.36 o 3 1 1 13137.12 14527.20 259.37 o 4 1 1 4874.39 5539.44 179.16 o 5 1 1 1912.34 1911.97 57.25 o 6 1 1 950.60 937.32 58.60 o 7 1 1 54.24 45.80 30.54 o 8 1 1 35.01 61.25 61.88 o 9 1 1 77.62 150.93 67.13 o 10 1 1 415.03 393.21 61.31 o 11 1 1 296.37 400.03 90.98 o -12 2 1 67.88 -6.75 51.11 o -11 2 1 214.15 197.74 55.63 o -10 2 1 431.63 452.59 60.26 o -9 2 1 648.76 571.93 60.58 o -8 2 1 1050.58 1094.22 70.97 o -7 2 1 43.58 24.70 29.16 o -6 2 1 3273.38 3423.52 88.90 o -5 2 1 12275.49 13189.58 282.60 o -4 2 1 10709.95 11413.37 278.11 o -3 2 1 4080.63 4773.68 145.31 o -2 2 1 15496.91 15445.80 455.96 o -1 2 1 11463.77 10877.87 353.36 o 0 2 1 27072.46 26153.98 456.21 o 1 2 1 17487.20 18413.06 497.73 o 2 2 1 8241.71 9520.42 171.55 o 3 2 1 31.41 26.82 11.58 o 4 2 1 1867.81 2229.73 94.68 o 5 2 1 2.09 14.51 14.59 o 6 2 1 2697.14 2954.85 99.99 o 7 2 1 4244.80 4460.41 156.79 o 8 2 1 5442.88 5597.22 192.73 o 9 2 1 4.00 -3.28 34.27 o 10 2 1 56.27 4.00 42.40 o 11 2 1 158.47 117.38 52.25 o -12 3 1 438.35 462.65 115.22 o -11 3 1 67.04 1.61 46.02 o -10 3 1 29.82 23.00 60.13 o -9 3 1 292.33 270.42 47.96 o -8 3 1 2130.76 2087.63 98.13 o -7 3 1 3952.63 4249.58 147.37 o -6 3 1 892.06 888.25 37.92 o -5 3 1 24.34 44.15 13.40 o -4 3 1 704.66 785.37 30.48 o -3 3 1 7.10 82.11 13.51 o -2 3 1 2756.59 2739.80 61.21 o -1 3 1 5308.91 5335.62 98.30 o 0 3 1 8093.23 6960.62 137.73 o 1 3 1 1523.08 1706.06 58.13 o 2 3 1 7250.22 9125.35 189.62 o 3 3 1 2254.26 2539.78 53.95 o 4 3 1 3024.00 3060.57 79.81 o 5 3 1 2129.89 2389.96 92.96 o 6 3 1 16.60 34.91 21.92 o 7 3 1 241.62 315.59 56.24 o 8 3 1 120.01 161.45 41.49 o 9 3 1 56.51 50.26 38.30 o 10 3 1 602.35 576.02 70.95 o 11 3 1 469.77 439.75 71.93 o -12 4 1 0.95 -66.83 46.49 o -11 4 1 12.65 -16.79 46.01 o -10 4 1 21.17 -1.82 38.56 o -9 4 1 828.15 742.76 67.21 o -8 4 1 159.26 184.20 41.28 o -7 4 1 156.02 207.81 36.33 o -6 4 1 122.95 196.49 49.74 o -5 4 1 1129.88 1357.02 46.01 o -4 4 1 9.07 16.37 17.18 o -3 4 1 559.16 451.04 37.57 o -2 4 1 1924.24 2232.77 46.95 o -1 4 1 3852.12 3923.70 74.57 o 0 4 1 4626.83 4979.48 96.33 o 1 4 1 9521.93 9632.51 174.19 o 2 4 1 3590.31 3763.16 111.25 o 3 4 1 893.19 909.46 49.48 o 4 4 1 246.10 219.41 20.46 o 5 4 1 1607.88 1715.61 56.29 o 6 4 1 815.38 948.60 43.87 o 7 4 1 115.96 182.86 39.69 o 8 4 1 270.42 318.02 50.65 o 9 4 1 60.99 15.20 36.73 o 10 4 1 47.50 65.62 47.65 o 11 4 1 48.09 -24.88 46.29 o -12 5 1 239.45 157.64 63.76 o -11 5 1 183.44 158.96 78.34 o -10 5 1 105.56 50.44 57.06 o -9 5 1 380.66 411.31 54.78 o -8 5 1 1855.48 1964.06 97.16 o -7 5 1 383.95 392.14 43.76 o -6 5 1 575.99 623.20 34.45 o -5 5 1 41.57 45.95 15.31 o -4 5 1 9.83 30.00 14.73 o -3 5 1 330.67 205.12 14.40 o -2 5 1 3271.07 3362.26 67.46 o -1 5 1 8156.23 8161.76 161.69 o 0 5 1 3192.85 2492.73 46.60 o 1 5 1 18063.42 18603.38 329.76 o 2 5 1 2399.23 2407.20 147.52 o 3 5 1 5230.81 5944.68 115.45 o 4 5 1 3437.09 4008.23 146.05 o 5 5 1 76.00 168.83 44.53 o 6 5 1 209.65 244.22 32.73 o 7 5 1 737.93 912.87 67.15 o 8 5 1 277.31 272.81 48.73 o 9 5 1 778.66 683.13 74.13 o 10 5 1 423.23 337.66 61.41 o 11 5 1 33.48 43.11 48.83 o -12 6 1 120.68 174.53 80.91 o -11 6 1 118.37 135.36 55.43 o -10 6 1 272.91 224.54 55.38 o -9 6 1 883.20 1012.48 77.78 o -8 6 1 42.84 1.58 32.60 o -7 6 1 49.33 24.46 19.64 o -6 6 1 31.56 36.68 17.60 o -5 6 1 7904.47 8145.70 186.22 o -4 6 1 6197.18 5823.55 289.69 o -3 6 1 3178.54 3087.83 65.56 o -2 6 1 3336.51 3380.31 69.37 o -1 6 1 5761.17 5962.86 112.81 o 0 6 1 5979.73 6335.09 107.52 o 1 6 1 5028.61 4019.35 79.68 o 2 6 1 2368.62 2308.23 51.30 o 3 6 1 1009.16 1282.83 43.73 o 4 6 1 991.07 852.06 27.22 o 5 6 1 1188.53 1219.21 48.49 o 6 6 1 1186.32 1250.79 52.82 o 7 6 1 4525.57 4844.19 169.36 o 8 6 1 2099.47 2200.74 135.51 o 9 6 1 4.85 19.73 37.04 o 10 6 1 0.73 -59.98 39.99 o 11 6 1 1.11 -2.85 47.57 o -12 7 1 309.71 224.33 68.39 o -11 7 1 178.38 187.90 72.38 o -10 7 1 0.27 7.58 40.77 o -9 7 1 202.23 209.68 80.64 o -8 7 1 266.78 363.38 69.81 o -7 7 1 1391.34 1369.72 93.74 o -6 7 1 4219.63 4667.87 120.38 o -5 7 1 1772.03 1708.71 89.29 o -4 7 1 142.82 195.20 14.89 o -3 7 1 3093.47 3172.37 67.97 o -2 7 1 270.78 179.88 15.11 o -1 7 1 1669.75 1483.85 37.31 o 0 7 1 23153.81 23615.50 377.33 o 1 7 1 854.65 776.42 25.54 o 2 7 1 2.35 12.44 9.12 o 3 7 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