#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:53:16 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181200 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/79/2227928.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227928_Fobs loop_ _publ_author_name 'Li, Gong-Chun' 'Ju, Zhi-Yu' 'Wang, Hong-Sheng' 'Niu, Yu-Jiao' 'Yang, Feng-Ling' _publ_section_title ; 6-Hydroxy-4-(pyridin-3-yl)-5-(2-thienylcarbonyl)-6-trifluoromethyl-3,4,5,6-tetrahydropyrimidin-2(1H)-one ; _journal_coeditor_code PV2334 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2852 _journal_volume 66 _journal_year 2010 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.223 _cell_angle_gamma 90.000 _cell_length_a 29.6940 _cell_length_b 5.9710 _cell_length_c 17.6910 _exptl_crystal_F_000 1520.00 _reflns_d_resolution_high 0.7601 _cod_data_source_file pv2334Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' _m100910e' _shelx_refln_list_code 4 _shelx_f_calc_maximum 354.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 7962.71 8229.80 241.99 o 6 0 0 12271.95 12416.67 181.17 o 8 0 0 8341.17 8449.78 141.97 o 10 0 0 22132.98 23099.20 438.28 o 12 0 0 8190.60 7837.57 413.07 o 14 0 0 10577.48 10367.82 284.29 o 16 0 0 638.35 479.77 29.83 o 18 0 0 13.68 24.88 6.62 o 20 0 0 1095.77 1174.51 75.06 o 22 0 0 7405.58 7444.33 456.38 o 24 0 0 18754.02 19773.50 258.30 o 26 0 0 286.71 255.67 129.17 o 28 0 0 5720.93 5465.73 519.68 o 30 0 0 0.71 11.09 15.71 o 32 0 0 1978.04 1917.18 153.16 o 34 0 0 150.78 135.69 85.76 o 36 0 0 1336.00 1285.16 145.03 o 38 0 0 411.09 325.96 42.75 o 1 1 0 40987.13 43444.79 854.71 o 3 1 0 19577.47 19876.60 569.83 o 5 1 0 25986.15 27482.36 634.16 o 7 1 0 15262.24 15544.68 150.65 o 9 1 0 24150.35 24890.86 346.52 o 11 1 0 4.69 11.09 2.34 o 13 1 0 14034.89 14929.64 249.28 o 15 1 0 594.40 477.40 23.95 o 17 1 0 6367.71 6442.04 139.56 o 19 1 0 380.35 387.25 24.39 o 21 1 0 42.95 58.50 12.07 o 23 1 0 10144.09 11356.19 354.90 o 25 1 0 4522.31 4564.53 189.33 o 27 1 0 6830.02 6865.17 255.69 o 29 1 0 1404.26 1388.36 54.62 o 31 1 0 18.33 38.46 22.25 o 33 1 0 1.17 11.60 20.75 o 35 1 0 1.23 16.36 22.29 o 37 1 0 67.74 59.81 50.26 o 0 2 0 1757.93 2215.42 114.03 o 2 2 0 13229.22 13441.74 98.95 o 4 2 0 10481.39 10653.44 152.09 o 6 2 0 12902.76 14072.01 270.08 o 8 2 0 77.28 44.06 5.96 o 10 2 0 204.64 184.12 9.19 o 12 2 0 87.85 110.17 10.41 o 14 2 0 3855.98 4106.68 83.10 o 16 2 0 50.34 55.18 11.88 o 18 2 0 2693.81 2771.32 101.34 o 20 2 0 870.07 872.31 50.89 o 22 2 0 31.05 26.17 8.67 o 24 2 0 984.85 957.85 42.23 o 26 2 0 157.26 132.38 24.01 o 28 2 0 245.11 232.28 20.80 o 30 2 0 264.37 212.49 29.14 o 32 2 0 2916.65 2816.74 186.24 o 34 2 0 2.30 10.49 12.98 o 36 2 0 14.58 33.03 25.47 o 1 3 0 22159.26 23617.19 384.68 o 3 3 0 1091.28 1430.32 36.99 o 5 3 0 1572.65 1862.94 48.68 o 7 3 0 5615.21 6127.26 135.51 o 9 3 0 302.97 140.90 39.25 o 11 3 0 522.05 637.10 49.44 o 13 3 0 289.34 279.35 15.97 o 15 3 0 753.50 847.88 49.88 o 17 3 0 1446.67 1350.24 60.12 o 19 3 0 1649.55 1601.96 77.92 o 21 3 0 6325.87 6282.28 263.25 o 23 3 0 404.50 352.27 18.14 o 25 3 0 1354.55 1372.54 102.85 o 27 3 0 114.17 134.93 55.61 o 29 3 0 147.84 202.16 95.56 o 31 3 0 420.06 424.74 97.82 o 33 3 0 289.96 203.78 111.98 o 35 3 0 236.20 237.69 41.79 o 0 4 0 1239.98 1108.45 137.88 o 2 4 0 11469.09 11336.20 324.31 o 4 4 0 188.84 222.08 31.94 o 6 4 0 415.12 502.64 38.76 o 8 4 0 2.60 9.92 8.97 o 10 4 0 1426.23 1474.72 74.91 o 12 4 0 2991.81 2720.89 148.35 o 14 4 0 231.44 194.20 20.53 o 16 4 0 419.19 394.97 19.72 o 18 4 0 97.09 102.90 17.22 o 20 4 0 2097.86 2268.21 141.93 o 22 4 0 51.34 59.20 34.75 o 24 4 0 647.44 669.80 91.34 o 26 4 0 43.18 68.36 47.38 o 28 4 0 608.30 593.88 62.14 o 30 4 0 731.39 712.63 89.58 o 32 4 0 72.35 54.24 38.37 o 1 5 0 304.09 264.08 37.02 o 3 5 0 111.26 126.61 42.69 o 5 5 0 205.61 145.56 54.27 o 7 5 0 1967.88 2167.49 117.16 o 9 5 0 89.47 135.48 51.07 o 11 5 0 67.88 64.74 26.38 o 13 5 0 1262.15 1188.52 73.71 o 15 5 0 154.61 278.85 77.75 o 17 5 0 0.90 14.46 24.67 o 19 5 0 2668.20 2857.30 225.15 o 21 5 0 314.38 417.11 169.88 o 23 5 0 1300.98 1524.33 146.27 o 25 5 0 74.26 69.77 59.59 o 27 5 0 10.67 13.90 25.03 o 29 5 0 343.77 358.82 71.70 o 0 6 0 838.29 702.08 65.98 o 2 6 0 900.38 835.46 65.78 o 4 6 0 158.68 153.99 27.87 o 6 6 0 1013.57 942.49 40.36 o 8 6 0 1896.22 1791.89 276.58 o 10 6 0 333.79 361.18 91.12 o 12 6 0 122.78 99.58 61.41 o 14 6 0 695.50 624.53 90.96 o 16 6 0 1167.40 1241.21 146.74 o 18 6 0 15.46 26.72 25.91 o 20 6 0 50.70 72.99 47.81 o 22 6 0 28.53 44.09 33.73 o 24 6 0 15.67 11.64 20.59 o 1 7 0 367.15 401.81 32.66 o 3 7 0 353.88 299.57 46.06 o 5 7 0 1.58 149.56 184.37 o 7 7 0 272.81 369.46 77.00 o 9 7 0 73.00 109.59 69.51 o 11 7 0 84.22 96.72 69.45 o 13 7 0 43.98 9.98 26.57 o 15 7 0 281.64 289.50 81.14 o 17 7 0 28.19 29.37 65.17 o -37 1 1 206.92 93.30 74.66 o -35 1 1 102.00 89.07 45.19 o -33 1 1 4.96 16.28 16.08 o -31 1 1 335.57 327.54 30.78 o -29 1 1 2651.90 2700.47 143.94 o -27 1 1 855.06 802.45 75.25 o -25 1 1 18835.18 19844.76 651.36 o -23 1 1 5018.58 4950.35 163.63 o -21 1 1 231.98 266.79 24.68 o -19 1 1 1396.32 1365.33 84.62 o -17 1 1 1311.72 1661.20 51.78 o -15 1 1 347.61 347.34 23.63 o -13 1 1 1474.23 1711.14 39.75 o -11 1 1 9150.03 9243.20 200.90 o -9 1 1 10.40 32.45 5.57 o -7 1 1 6193.64 6285.96 205.05 o -5 1 1 19983.23 20621.02 345.97 o -3 1 1 425.50 442.97 18.62 o -1 1 1 50406.45 53033.19 974.94 o 1 1 1 5913.98 5864.99 81.04 o 3 1 1 1878.49 2066.46 68.23 o 5 1 1 2090.87 1997.33 66.14 o 7 1 1 61436.48 64982.55 1713.39 o 9 1 1 8061.80 7869.70 181.92 o 11 1 1 10152.28 9473.97 177.03 o 13 1 1 950.05 1041.38 27.60 o 15 1 1 51.11 75.63 7.80 o 17 1 1 6035.31 5884.73 181.47 o 19 1 1 2747.58 2509.75 81.40 o 21 1 1 125.70 119.23 10.59 o 23 1 1 9181.54 9143.14 469.14 o 25 1 1 595.69 572.41 26.41 o 27 1 1 771.01 738.22 46.86 o 29 1 1 14.18 44.27 23.13 o 31 1 1 1517.78 1617.70 90.59 o 33 1 1 1220.04 1223.60 78.22 o 35 1 1 709.37 793.84 88.44 o 37 1 1 285.74 199.28 34.29 o -36 2 1 61.48 44.23 33.10 o -34 2 1 313.45 276.07 61.17 o -32 2 1 1594.08 1410.04 124.90 o -30 2 1 2068.07 2030.14 153.42 o -28 2 1 1465.19 1423.71 89.60 o -26 2 1 3901.16 3882.65 249.49 o -24 2 1 6350.89 6298.08 246.22 o -22 2 1 3025.85 3205.02 128.81 o -20 2 1 840.24 855.88 53.42 o -18 2 1 6915.65 6805.11 178.87 o -16 2 1 90.80 108.40 9.46 o -14 2 1 346.13 408.10 26.23 o -12 2 1 2570.98 2580.22 67.89 o -10 2 1 7894.87 7345.15 117.14 o -8 2 1 2569.66 2426.63 50.82 o -6 2 1 23857.96 25350.53 444.52 o -4 2 1 8005.69 7208.05 89.07 o -2 2 1 1874.24 1905.03 65.21 o 0 2 1 4504.28 4688.86 62.26 o 2 2 1 33744.50 37954.98 701.61 o 4 2 1 4414.65 4174.10 69.27 o 6 2 1 191.34 182.58 8.15 o 8 2 1 3468.50 1790.45 625.89 o 10 2 1 6611.63 6659.85 241.39 o 12 2 1 2020.39 1893.16 38.32 o 14 2 1 2408.90 2245.18 63.56 o 16 2 1 11021.07 11092.51 268.70 o 18 2 1 8005.58 8307.19 399.42 o 20 2 1 2476.16 2320.96 90.50 o 22 2 1 4297.17 4322.96 179.37 o 24 2 1 2114.66 2151.14 77.97 o 26 2 1 0.22 7.10 8.37 o 28 2 1 795.91 659.42 44.17 o 30 2 1 335.18 366.55 115.78 o 32 2 1 1354.25 1403.47 116.02 o 34 2 1 280.77 279.86 72.31 o 36 2 1 48.22 63.73 45.89 o -35 3 1 14.87 24.39 26.29 o -33 3 1 0.51 17.65 12.50 o -31 3 1 227.74 244.96 93.24 o -29 3 1 543.77 556.41 51.22 o -27 3 1 2769.26 2903.06 173.34 o -25 3 1 16.55 20.72 12.17 o -23 3 1 343.69 326.72 22.06 o -21 3 1 1066.33 965.34 30.70 o -19 3 1 522.82 458.88 42.16 o -17 3 1 280.80 300.34 20.19 o -15 3 1 75.89 93.63 10.50 o -13 3 1 918.71 908.35 53.89 o -11 3 1 97.19 67.08 17.82 o -9 3 1 359.80 293.30 25.28 o -7 3 1 5595.86 5645.64 164.35 o -5 3 1 15102.60 15514.72 277.75 o -3 3 1 1088.70 1137.42 33.72 o -1 3 1 335.91 410.01 32.09 o 1 3 1 58.39 42.10 8.81 o 3 3 1 7454.88 8139.13 188.21 o 5 3 1 4241.85 4377.42 132.16 o 7 3 1 5432.48 5803.37 125.28 o 9 3 1 11176.55 11664.60 457.64 o 11 3 1 573.58 413.36 62.59 o 13 3 1 2346.90 2216.63 249.43 o 15 3 1 70.23 60.66 19.02 o 17 3 1 176.21 165.21 18.43 o 19 3 1 43.98 39.56 13.06 o 21 3 1 1567.70 1523.35 69.56 o 23 3 1 20.11 23.71 9.54 o 25 3 1 976.55 1110.25 96.63 o 27 3 1 107.82 160.17 56.17 o 29 3 1 7.45 23.94 22.83 o 31 3 1 25.29 66.50 46.91 o 33 3 1 1263.17 1399.45 165.96 o 35 3 1 89.79 70.67 60.57 o -32 4 1 156.87 158.17 99.36 o -30 4 1 12.66 42.17 23.59 o -28 4 1 9.04 12.06 26.63 o -26 4 1 482.89 519.57 59.50 o -24 4 1 43.79 60.00 30.30 o -22 4 1 111.70 91.52 50.09 o -20 4 1 22.10 21.34 20.09 o -18 4 1 2340.29 2099.42 160.49 o -16 4 1 182.43 139.27 30.43 o -14 4 1 146.70 111.28 14.55 o -12 4 1 105.65 106.71 12.63 o -10 4 1 2166.10 2085.71 140.45 o -8 4 1 747.42 762.19 48.65 o -6 4 1 226.40 175.59 31.95 o -4 4 1 314.63 280.19 68.11 o -2 4 1 0.74 16.36 16.80 o 0 4 1 5700.00 5822.04 206.00 o 2 4 1 36.90 44.77 17.03 o 4 4 1 3408.06 4065.85 494.07 o 6 4 1 14563.60 15610.60 473.56 o 8 4 1 11.65 6.51 7.18 o 10 4 1 228.20 187.55 13.56 o 12 4 1 632.97 524.05 46.22 o 14 4 1 4500.71 4937.24 216.95 o 16 4 1 1532.57 1634.58 84.04 o 18 4 1 193.73 179.33 25.58 o 20 4 1 20.24 24.50 27.94 o 22 4 1 203.32 224.28 77.99 o 24 4 1 5.39 41.95 30.00 o 26 4 1 222.46 288.54 114.58 o 28 4 1 18.14 23.31 22.14 o 30 4 1 14.60 20.37 28.86 o 32 4 1 940.32 1115.42 132.75 o -29 5 1 1516.82 1634.55 230.58 o -27 5 1 6.25 26.85 38.17 o -25 5 1 0.09 10.97 17.71 o -23 5 1 1458.08 1370.11 130.09 o -21 5 1 159.31 80.34 58.76 o -19 5 1 177.08 237.00 94.37 o -17 5 1 714.94 805.08 89.95 o -15 5 1 902.70 814.01 87.93 o -13 5 1 784.66 905.64 70.14 o -11 5 1 828.38 776.51 75.56 o -9 5 1 764.16 750.07 73.98 o -7 5 1 2892.71 2949.61 148.73 o -5 5 1 2708.44 2747.95 141.48 o -3 5 1 86.24 118.10 42.74 o -1 5 1 0.40 14.93 14.60 o 1 5 1 584.84 499.78 28.55 o 3 5 1 161.48 158.19 40.37 o 5 5 1 172.51 179.22 22.26 o 7 5 1 117.16 61.33 23.95 o 9 5 1 2605.74 2512.78 100.77 o 11 5 1 1300.72 1327.55 121.23 o 13 5 1 1076.86 1120.26 124.72 o 15 5 1 555.05 582.01 45.28 o 17 5 1 2920.33 3023.16 238.91 o 19 5 1 2.21 47.27 30.79 o 21 5 1 117.57 195.12 65.35 o 23 5 1 291.55 342.01 54.76 o 25 5 1 91.11 99.60 58.86 o 27 5 1 11.52 11.91 22.59 o 29 5 1 18.12 42.21 31.06 o -24 6 1 50.52 41.79 41.75 o -22 6 1 10.73 25.69 29.51 o -20 6 1 625.94 535.68 75.72 o -18 6 1 444.87 451.01 60.91 o -16 6 1 54.00 22.30 45.26 o -14 6 1 368.53 415.81 88.00 o -12 6 1 61.32 57.51 25.19 o -10 6 1 121.01 130.96 57.43 o -8 6 1 832.27 945.55 109.48 o -6 6 1 7029.54 7026.69 357.08 o -4 6 1 157.82 88.49 46.40 o -2 6 1 56.90 111.39 36.58 o 0 6 1 986.15 1189.92 66.37 o 2 6 1 50.18 48.83 18.47 o 4 6 1 2.67 12.40 20.71 o 6 6 1 1636.47 1595.33 102.61 o 8 6 1 766.96 810.47 72.46 o 10 6 1 617.13 649.01 83.68 o 12 6 1 1900.17 2154.52 218.50 o 14 6 1 26.26 13.78 18.50 o 16 6 1 1014.98 1088.05 137.32 o 18 6 1 1872.33 1894.10 173.19 o 20 6 1 321.94 386.10 91.63 o 22 6 1 476.26 469.52 63.66 o 24 6 1 6.48 11.12 23.95 o -17 7 1 205.25 241.79 60.86 o -15 7 1 153.17 128.98 102.58 o -13 7 1 443.04 450.52 90.35 o -11 7 1 45.58 82.10 77.47 o -9 7 1 239.42 113.08 86.78 o -7 7 1 1823.46 1872.33 206.31 o -5 7 1 380.08 488.69 67.31 o -3 7 1 0.90 3.10 20.40 o -1 7 1 142.55 92.07 60.25 o 1 7 1 408.07 371.92 47.76 o 3 7 1 81.72 78.30 47.60 o 5 7 1 107.98 62.10 81.60 o 7 7 1 47.07 24.12 52.58 o 9 7 1 91.08 64.84 49.94 o 11 7 1 300.89 379.79 58.08 o 13 7 1 257.12 306.21 55.10 o 15 7 1 247.84 124.24 116.27 o 17 7 1 350.20 379.06 77.46 o -38 0 2 18.02 34.39 36.19 o -36 0 2 4643.61 5044.72 288.92 o -34 0 2 2368.67 2553.64 194.97 o -32 0 2 163.76 138.36 84.85 o -30 0 2 9459.80 9084.79 221.99 o -28 0 2 213.10 212.42 65.64 o -26 0 2 3120.23 2906.82 174.65 o -24 0 2 3736.24 3601.60 200.74 o -22 0 2 1826.61 1751.45 101.15 o -20 0 2 3658.96 3604.43 170.88 o -18 0 2 3324.71 3413.60 155.47 o -16 0 2 428.21 417.99 36.18 o -14 0 2 27507.80 29324.31 480.13 o -12 0 2 2574.99 2277.94 56.03 o -10 0 2 407.69 638.55 32.70 o -8 0 2 53268.95 58094.21 870.17 o -6 0 2 9889.10 9704.00 317.68 o -4 0 2 2498.12 2038.25 94.71 o -2 0 2 282.21 279.85 14.43 o 0 0 2 32882.54 36405.39 471.45 o 2 0 2 18783.74 19439.38 269.56 o 4 0 2 23579.89 25027.33 261.28 o 6 0 2 125901.85 140024.22 3523.30 o 8 0 2 9101.80 8239.21 151.83 o 10 0 2 58636.56 63077.89 1873.80 o 12 0 2 12127.46 11867.12 390.77 o 14 0 2 4838.63 5397.68 100.52 o 16 0 2 98.55 152.40 20.48 o 18 0 2 618.21 702.39 57.98 o 20 0 2 283.53 267.20 28.59 o 22 0 2 790.03 749.12 61.05 o 24 0 2 2011.24 2135.32 98.32 o 26 0 2 2425.62 2521.08 192.65 o 28 0 2 7411.57 7528.15 332.99 o 30 0 2 720.99 663.09 49.39 o 32 0 2 2703.66 2889.89 392.19 o 34 0 2 459.67 332.35 79.25 o 36 0 2 57.81 46.12 31.30 o 38 0 2 2070.17 2187.11 356.03 o -37 1 2 216.17 144.81 88.78 o -35 1 2 524.89 539.02 38.47 o -33 1 2 22.72 41.22 18.97 o -31 1 2 116.14 103.94 34.12 o -29 1 2 35.89 33.59 15.19 o -27 1 2 194.64 199.86 25.70 o -25 1 2 4199.32 3956.70 263.46 o -23 1 2 671.58 642.88 52.05 o -21 1 2 579.98 678.98 49.82 o -19 1 2 305.83 313.89 25.30 o -17 1 2 3468.94 3387.84 68.79 o -15 1 2 1.64 7.19 4.15 o -13 1 2 9803.38 9608.23 175.50 o -11 1 2 13744.16 13329.66 243.69 o -9 1 2 2842.28 3223.52 85.45 o -7 1 2 5222.99 5167.22 163.34 o -5 1 2 1058.91 1077.14 37.14 o -3 1 2 57716.29 61798.92 2275.28 o -1 1 2 9527.25 9199.32 81.26 o 1 1 2 9167.92 9101.83 105.33 o 3 1 2 28665.21 30047.84 1901.16 o 5 1 2 0.66 31.95 7.05 o 7 1 2 363.94 224.51 14.59 o 9 1 2 11390.03 11252.22 116.66 o 11 1 2 19.06 19.61 3.21 o 13 1 2 4594.65 4507.85 57.07 o 15 1 2 113.81 113.09 10.39 o 17 1 2 987.21 1049.61 50.03 o 19 1 2 1706.06 1650.54 46.97 o 21 1 2 2889.45 2695.25 146.07 o 23 1 2 371.80 373.75 33.52 o 25 1 2 78.23 99.86 12.72 o 27 1 2 5475.71 5577.55 195.68 o 29 1 2 307.23 303.71 18.22 o 31 1 2 111.86 141.82 37.20 o 33 1 2 165.15 137.23 41.02 o 35 1 2 432.31 392.03 77.16 o 37 1 2 11.38 26.77 48.88 o -36 2 2 1.86 15.79 24.97 o -34 2 2 103.49 68.76 64.23 o -32 2 2 220.14 242.45 38.99 o -30 2 2 0.34 9.80 8.34 o -28 2 2 115.42 110.86 39.42 o -26 2 2 4354.66 4303.25 177.95 o -24 2 2 2547.09 2310.20 111.32 o -22 2 2 611.72 500.15 61.01 o -20 2 2 635.67 576.05 49.55 o -18 2 2 7669.32 7813.00 262.68 o -16 2 2 9809.17 10640.12 574.02 o -14 2 2 890.39 921.66 53.40 o -12 2 2 1031.47 1129.95 30.24 o -10 2 2 9217.70 9848.77 196.26 o -8 2 2 2355.83 2386.20 56.84 o -6 2 2 7.46 15.43 5.32 o -4 2 2 560.08 609.23 27.76 o -2 2 2 5563.91 5760.15 115.11 o 0 2 2 4560.85 4632.58 73.16 o 2 2 2 6609.81 6919.06 100.84 o 4 2 2 5858.14 6185.96 138.29 o 6 2 2 2106.42 2141.51 34.97 o 8 2 2 1670.56 1605.25 61.93 o 10 2 2 4328.62 4075.92 105.28 o 12 2 2 11547.17 12399.77 342.58 o 14 2 2 885.57 960.06 56.18 o 16 2 2 713.55 800.65 45.59 o 18 2 2 132.74 135.10 9.40 o 20 2 2 49.75 49.31 12.12 o 22 2 2 19.71 17.29 5.78 o 24 2 2 3041.39 2914.01 95.50 o 26 2 2 1339.49 1354.81 57.11 o 28 2 2 947.19 867.98 68.96 o 30 2 2 254.32 290.13 96.70 o 32 2 2 1945.08 2073.70 145.91 o 34 2 2 2253.17 2160.57 184.65 o 36 2 2 881.67 926.24 103.99 o -35 3 2 814.89 678.36 91.54 o -33 3 2 3.85 64.49 54.36 o -31 3 2 22.42 38.62 37.52 o -29 3 2 688.70 670.79 91.53 o -27 3 2 15.38 20.30 13.71 o -25 3 2 2622.11 2501.91 136.75 o -23 3 2 3473.24 3212.74 244.30 o -21 3 2 6.16 29.68 12.49 o -19 3 2 1300.58 1137.30 87.86 o -17 3 2 1383.91 1179.60 71.99 o -15 3 2 4496.98 4297.98 171.75 o -13 3 2 5453.67 5424.26 129.37 o -11 3 2 517.91 459.56 31.89 o -9 3 2 7859.52 8393.92 198.12 o -7 3 2 503.84 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