#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/79/2227953.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227953_Fobs loop_ _publ_author_name 'DeBurgomaster, Paul' 'Zubieta, Jon' _publ_section_title ; catena-Poly[[bis(\m-5-bromopyridine-3-carboxylato-\k^2^O:O')dicopper(II)]-bis(\m-5-bromopyridine-3-carboxylato)-\k^3^O,O':N;\k^3^N:O,O'] ; _journal_coeditor_code RN2072 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1459 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 115.432 _cell_angle_gamma 90.000 _cell_length_a 11.1390 _cell_length_b 11.5866 _cell_length_c 12.6325 _exptl_crystal_F_000 892.00 _reflns_d_resolution_high 0.7553 _[local]_cod_data_source_file rn2072Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21n in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 309.44 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8601.21 8499.74 77.30 o 4 0 0 8875.50 9012.86 101.35 o 6 0 0 5102.83 5137.95 69.75 o 8 0 0 16577.84 16487.66 192.79 o 10 0 0 118.53 119.26 21.67 o 12 0 0 3214.49 3471.97 93.96 o 1 1 0 752.89 1010.26 14.25 o 2 1 0 12266.62 12549.56 91.24 o 3 1 0 8673.44 9151.82 70.22 o 4 1 0 23911.69 24462.40 195.57 o 5 1 0 2882.27 2834.24 28.26 o 6 1 0 3223.68 3283.03 33.34 o 7 1 0 14178.45 14291.34 116.58 o 8 1 0 6510.92 6615.07 128.23 o 9 1 0 179.19 169.56 12.22 o 10 1 0 3368.98 3259.98 61.11 o 11 1 0 17.15 22.26 15.37 o 12 1 0 569.61 479.62 28.36 o 13 1 0 269.77 277.64 26.90 o 0 2 0 2098.86 2464.70 29.18 o 1 2 0 74.97 88.87 4.28 o 2 2 0 1347.85 1228.86 19.52 o 3 2 0 21.14 23.81 3.67 o 4 2 0 2.28 1.68 4.24 o 5 2 0 11857.16 11925.71 94.23 o 6 2 0 20113.14 20348.70 153.69 o 7 2 0 2201.63 2271.36 28.28 o 8 2 0 761.95 736.42 17.60 o 9 2 0 3163.31 3076.74 42.07 o 10 2 0 40.31 34.21 12.28 o 11 2 0 251.95 231.52 20.39 o 12 2 0 230.08 241.36 23.16 o 13 2 0 481.58 488.77 31.74 o 1 3 0 35897.00 35265.67 248.83 o 2 3 0 197.25 279.16 11.06 o 3 3 0 8822.35 9055.70 73.22 o 4 3 0 4486.96 4428.40 43.74 o 5 3 0 2.66 1.66 5.17 o 6 3 0 85.18 77.94 11.64 o 7 3 0 2441.88 2425.94 32.94 o 8 3 0 7.23 20.29 7.50 o 9 3 0 3387.26 3344.85 44.11 o 10 3 0 106.43 86.79 14.00 o 11 3 0 25.24 14.73 17.36 o 12 3 0 3121.52 3308.65 65.71 o 13 3 0 1341.63 1367.24 46.68 o 0 4 0 284.20 220.80 22.37 o 1 4 0 19558.26 20312.56 147.46 o 2 4 0 7.61 29.01 7.65 o 3 4 0 3965.21 4015.23 37.15 o 4 4 0 2035.53 2033.36 26.25 o 5 4 0 584.99 625.06 13.99 o 6 4 0 2284.55 2341.86 29.82 o 7 4 0 2003.39 1958.65 29.23 o 8 4 0 11084.51 11242.84 98.43 o 9 4 0 3849.77 3919.13 49.08 o 10 4 0 1116.82 1072.37 26.98 o 11 4 0 29.05 21.52 15.64 o 12 4 0 194.49 214.12 23.22 o 1 5 0 15085.68 16003.66 131.22 o 2 5 0 8645.14 9558.18 76.09 o 3 5 0 47.88 37.78 5.44 o 4 5 0 132.66 107.28 10.92 o 5 5 0 3693.95 3772.29 39.34 o 6 5 0 5467.60 5502.83 58.60 o 7 5 0 559.74 583.60 16.64 o 8 5 0 3603.52 3649.26 47.69 o 9 5 0 673.02 617.09 21.98 o 10 5 0 3258.72 3224.94 52.07 o 11 5 0 45.74 32.86 35.69 o 12 5 0 162.52 206.50 26.86 o 0 6 0 605.01 616.13 17.36 o 1 6 0 8107.10 8788.87 71.45 o 2 6 0 12491.15 13039.33 101.79 o 3 6 0 5514.17 5451.40 49.99 o 4 6 0 27.66 57.67 7.00 o 5 6 0 842.01 865.56 17.63 o 6 6 0 4057.84 3978.54 43.72 o 7 6 0 712.48 681.73 18.25 o 8 6 0 1999.38 1951.51 31.48 o 9 6 0 143.15 163.96 17.80 o 10 6 0 1341.53 1385.50 39.03 o 11 6 0 1913.93 2080.27 73.68 o 12 6 0 51.67 55.19 30.54 o 1 7 0 165.35 208.72 10.16 o 2 7 0 49.84 72.36 7.25 o 3 7 0 1049.67 1046.28 20.19 o 4 7 0 20596.01 21434.54 183.87 o 5 7 0 1042.12 1092.45 20.62 o 6 7 0 679.46 652.21 17.41 o 7 7 0 2967.93 3098.33 39.95 o 8 7 0 3839.49 3736.07 52.30 o 9 7 0 104.64 128.56 19.62 o 10 7 0 16.55 11.49 18.73 o 11 7 0 440.83 538.55 45.11 o 0 8 0 14185.70 14438.18 286.68 o 1 8 0 972.09 939.11 17.66 o 2 8 0 1329.80 1271.77 20.97 o 3 8 0 1410.18 1472.71 26.38 o 4 8 0 7356.13 7542.65 76.78 o 5 8 0 3622.35 3619.41 47.00 o 6 8 0 2504.88 2448.45 38.74 o 7 8 0 199.65 201.70 16.33 o 8 8 0 1619.74 1537.06 43.84 o 9 8 0 4004.09 4017.72 76.74 o 10 8 0 1213.68 1271.54 46.16 o 11 8 0 1129.11 1075.11 57.66 o 1 9 0 364.52 357.10 13.64 o 2 9 0 23985.54 24017.06 200.27 o 3 9 0 5648.56 5735.40 83.03 o 4 9 0 895.66 848.76 22.51 o 5 9 0 3225.45 2988.41 65.72 o 6 9 0 467.46 505.14 21.19 o 7 9 0 94.01 104.28 15.09 o 8 9 0 2008.31 1932.89 50.52 o 9 9 0 205.31 194.83 23.95 o 10 9 0 6607.55 6705.00 112.26 o 0 10 0 6509.06 6214.27 139.18 o 1 10 0 7541.18 7727.26 92.53 o 2 10 0 2430.10 2470.94 41.30 o 3 10 0 5093.08 5231.04 77.54 o 4 10 0 157.88 157.79 14.55 o 5 10 0 12319.74 12305.38 132.21 o 6 10 0 1984.84 1972.63 41.08 o 7 10 0 2199.48 2163.89 44.49 o 8 10 0 443.07 465.38 29.69 o 9 10 0 140.26 134.25 23.62 o 10 10 0 170.36 172.32 27.22 o 1 11 0 414.41 423.58 22.06 o 2 11 0 771.78 832.47 29.62 o 3 11 0 2005.73 2031.88 45.26 o 4 11 0 2650.75 2607.44 106.52 o 5 11 0 1214.12 1199.53 44.70 o 6 11 0 2.68 16.00 14.72 o 7 11 0 1217.07 1187.86 58.82 o 8 11 0 121.76 118.13 27.06 o 9 11 0 871.72 934.53 50.28 o 0 12 0 1065.58 1036.54 60.55 o 1 12 0 2412.45 2396.41 63.42 o 2 12 0 8.28 14.09 13.86 o 3 12 0 4252.42 4119.05 71.30 o 4 12 0 403.10 424.94 30.26 o 5 12 0 94.86 68.51 17.15 o 6 12 0 267.76 238.02 36.65 o 7 12 0 295.97 353.38 32.49 o 8 12 0 66.91 34.34 25.12 o 1 13 0 1525.04 1487.06 52.29 o 2 13 0 3.91 5.80 18.05 o 3 13 0 85.82 57.08 22.49 o 4 13 0 4565.01 4667.45 81.85 o 5 13 0 685.77 668.15 32.37 o 6 13 0 552.93 665.20 32.91 o 7 13 0 948.07 1057.79 51.72 o 0 14 0 48.12 123.08 35.49 o 1 14 0 346.17 365.93 40.74 o 2 14 0 510.98 553.99 40.27 o 3 14 0 2595.95 2605.78 74.27 o 4 14 0 128.02 139.17 27.18 o 5 14 0 3.53 13.80 21.68 o 1 15 0 523.65 463.22 57.22 o 2 15 0 31.12 10.82 22.14 o -13 0 1 41.90 56.50 27.07 o -11 0 1 956.03 890.76 44.67 o -9 0 1 38.13 47.88 16.02 o -7 0 1 4784.00 4956.07 74.26 o -5 0 1 2677.20 2498.72 46.67 o -3 0 1 377.97 561.28 13.76 o -1 0 1 5239.61 5290.35 159.46 o 1 0 1 46885.18 45191.02 468.16 o 3 0 1 3857.63 3750.28 40.34 o 5 0 1 49544.66 49144.26 588.75 o 7 0 1 4471.62 4266.87 65.75 o 9 0 1 350.61 341.65 48.86 o 11 0 1 811.57 850.10 104.02 o -13 1 1 557.97 549.17 38.16 o -12 1 1 306.81 349.49 24.59 o -11 1 1 154.92 138.68 18.54 o -10 1 1 36.52 33.23 11.38 o -9 1 1 610.54 631.20 18.90 o -8 1 1 3677.93 3695.47 47.17 o -7 1 1 21.73 29.27 6.81 o -6 1 1 2942.32 2876.03 30.30 o -5 1 1 1710.39 1736.78 26.73 o -4 1 1 371.66 286.43 8.91 o -3 1 1 20548.12 21626.02 155.49 o -2 1 1 64384.54 60545.14 575.58 o -1 1 1 39.56 44.57 2.60 o 0 1 1 11507.50 11862.99 103.79 o 1 1 1 4285.95 4437.87 34.21 o 2 1 1 971.54 1037.83 13.12 o 3 1 1 19679.26 19757.21 156.30 o 4 1 1 1699.90 1865.97 25.55 o 5 1 1 1504.58 1254.89 17.28 o 6 1 1 13176.80 13631.23 101.23 o 7 1 1 1916.52 1831.27 27.58 o 8 1 1 3041.43 2912.38 44.97 o 9 1 1 3006.93 3037.08 72.66 o 10 1 1 3861.82 3795.07 63.75 o 11 1 1 1368.40 1333.32 39.64 o 12 1 1 527.52 529.39 29.76 o -13 2 1 206.50 278.76 26.15 o -12 2 1 17.21 4.87 17.66 o -11 2 1 219.81 193.20 17.35 o -10 2 1 3366.79 3415.91 46.48 o -9 2 1 10387.04 10407.52 95.42 o -8 2 1 538.80 546.72 15.26 o -7 2 1 40.32 63.74 11.14 o -6 2 1 69.79 59.30 6.67 o -5 2 1 815.45 766.27 14.43 o -4 2 1 3502.08 3429.90 32.53 o -3 2 1 5191.60 5823.30 47.26 o -2 2 1 190.06 199.63 5.49 o -1 2 1 42926.36 40087.33 344.21 o 0 2 1 4996.77 5210.35 43.99 o 1 2 1 422.94 427.34 6.92 o 2 2 1 11466.61 12143.85 89.65 o 3 2 1 4909.64 4890.11 41.34 o 4 2 1 1519.95 1738.09 20.82 o 5 2 1 314.04 330.43 10.27 o 6 2 1 7142.53 7116.31 78.76 o 7 2 1 14349.92 14442.11 109.01 o 8 2 1 2913.46 2915.47 35.44 o 9 2 1 187.51 199.14 18.39 o 10 2 1 30.67 15.61 14.22 o 11 2 1 3833.31 3914.55 98.90 o 12 2 1 485.91 612.35 51.78 o -13 3 1 1136.62 1110.55 48.64 o -12 3 1 72.43 62.41 19.05 o -11 3 1 5321.42 5527.12 82.51 o -10 3 1 2785.69 2795.83 38.78 o -9 3 1 1342.38 1312.34 24.36 o -8 3 1 4046.17 4020.93 42.98 o -7 3 1 22890.22 23627.40 202.37 o -6 3 1 1205.16 1217.21 24.63 o -5 3 1 6433.59 6551.33 57.31 o -4 3 1 249.28 386.00 11.22 o -3 3 1 1759.38 1750.32 19.64 o -2 3 1 4026.70 4526.46 38.38 o -1 3 1 22472.80 22956.35 163.99 o 0 3 1 3120.01 3078.98 28.98 o 1 3 1 63265.05 61377.88 455.31 o 2 3 1 14.44 12.78 3.58 o 3 3 1 1445.41 1611.39 18.76 o 4 3 1 18885.83 18960.76 141.08 o 5 3 1 22.43 29.00 5.70 o 6 3 1 4250.73 4329.70 44.00 o 7 3 1 1223.95 1219.36 24.56 o 8 3 1 5.94 13.04 8.84 o 9 3 1 5859.24 5921.47 64.89 o 10 3 1 2215.16 2304.37 48.71 o 11 3 1 0.60 19.28 15.50 o 12 3 1 1331.15 1320.31 48.86 o -13 4 1 170.16 225.96 29.13 o -12 4 1 765.30 808.12 40.55 o -11 4 1 1717.82 1731.96 37.72 o -10 4 1 49.65 67.48 12.12 o -9 4 1 1200.77 1176.15 23.88 o -8 4 1 289.90 289.08 13.46 o -7 4 1 9421.12 9538.61 83.63 o -6 4 1 1222.34 1157.27 20.06 o -5 4 1 4258.27 4211.78 41.49 o -4 4 1 3268.58 3433.51 34.43 o -3 4 1 49827.10 47471.86 358.61 o -2 4 1 22.94 40.48 4.45 o -1 4 1 343.03 370.58 13.04 o 0 4 1 844.83 822.96 11.55 o 1 4 1 30.73 56.45 4.79 o 2 4 1 8309.47 8496.48 67.03 o 3 4 1 11473.57 12284.77 94.67 o 4 4 1 2742.68 2772.19 29.70 o 5 4 1 8422.32 8585.53 72.62 o 6 4 1 1190.51 1115.31 19.96 o 7 4 1 6236.09 6129.88 59.73 o 8 4 1 1651.63 1628.10 31.33 o 9 4 1 159.16 171.21 13.07 o 10 4 1 553.62 551.55 26.13 o 11 4 1 940.50 931.24 34.87 o 12 4 1 902.50 993.91 67.75 o -12 5 1 292.10 307.86 38.21 o -11 5 1 2664.77 2668.36 56.08 o -10 5 1 481.37 511.74 19.77 o -9 5 1 16.60 17.77 9.76 o -8 5 1 1877.91 1889.82 30.35 o -7 5 1 1764.19 1699.01 54.29 o -6 5 1 1567.71 1534.46 26.25 o -5 5 1 23674.75 23466.87 176.19 o -4 5 1 78.99 101.15 7.03 o -3 5 1 2723.21 2873.20 38.42 o -2 5 1 978.45 1011.80 16.55 o -1 5 1 6456.81 6172.01 56.21 o 0 5 1 13175.45 13154.93 99.46 o 1 5 1 138.16 205.75 7.42 o 2 5 1 5630.26 6760.97 56.58 o 3 5 1 120.64 74.42 5.99 o 4 5 1 2746.22 2738.99 30.37 o 5 5 1 5237.97 5399.58 51.33 o 6 5 1 1204.39 1216.83 21.40 o 7 5 1 3660.88 3803.77 47.32 o 8 5 1 100.96 115.22 15.01 o 9 5 1 245.20 251.24 19.34 o 10 5 1 34.82 44.95 15.87 o 11 5 1 40.63 79.21 20.97 o 12 5 1 954.51 911.35 54.69 o -12 6 1 90.44 118.03 30.61 o -11 6 1 430.83 423.32 30.77 o -10 6 1 4878.24 4936.61 74.85 o -9 6 1 6748.42 6725.72 77.23 o -8 6 1 2599.29 2656.64 37.24 o -7 6 1 731.07 667.95 25.52 o -6 6 1 3814.39 3805.97 42.36 o -5 6 1 926.26 968.10 42.42 o -4 6 1 2250.31 2167.02 30.12 o -3 6 1 4666.66 4964.10 52.90 o -2 6 1 10412.47 10545.86 84.26 o -1 6 1 20603.40 20902.09 169.60 o 0 6 1 891.73 910.93 14.66 o 1 6 1 52.04 47.19 6.91 o 2 6 1 32005.03 32747.05 237.30 o 3 6 1 8540.22 8860.30 73.86 o 4 6 1 34.42 46.41 6.55 o 5 6 1 224.61 227.97 10.30 o 6 6 1 355.86 340.98 14.70 o 7 6 1 1340.36 1268.76 23.90 o 8 6 1 353.35 373.54 17.39 o 9 6 1 366.19 389.52 19.40 o 10 6 1 180.70 177.51 23.86 o 11 6 1 1639.73 1628.61 66.79 o -12 7 1 1462.03 1584.19 69.26 o -11 7 1 1376.07 1395.53 42.58 o -10 7 1 30.28 8.16 17.94 o -9 7 1 11.13 6.09 11.95 o -8 7 1 3181.19 3187.98 46.65 o -7 7 1 683.78 692.44 18.91 o -6 7 1 15216.65 15335.48 125.16 o -5 7 1 0.21 1.10 6.96 o -4 7 1 1053.62 964.56 18.62 o -3 7 1 4204.12 4175.07 42.32 o -2 7 1 13811.31 14343.60 112.09 o -1 7 1 251.11 224.07 10.00 o 0 7 1 5644.48 5720.40 51.24 o 1 7 1 12707.78 12940.98 101.93 o 2 7 1 5042.18 5341.00 49.41 o 3 7 1 236.94 240.87 9.65 o 4 7 1 115.76 135.13 8.83 o 5 7 1 3474.26 3610.33 45.66 o 6 7 1 1987.56 1873.45 37.27 o 7 7 1 46.75 40.57 12.14 o 8 7 1 12.07 16.12 12.78 o 9 7 1 9060.54 9249.64 116.94 o 10 7 1 23.94 43.92 24.70 o 11 7 1 30.10 26.85 37.55 o -11 8 1 37.61 29.46 28.51 o -10 8 1 184.52 178.74 23.53 o -9 8 1 162.79 180.21 21.34 o -8 8 1 47.16 39.59 13.49 o -7 8 1 361.89 328.98 18.13 o -6 8 1 3819.36 3733.52 55.06 o -5 8 1 766.18 734.90 18.55 o -4 8 1 9496.47 9509.65 82.71 o -3 8 1 60.77 72.15 8.11 o -2 8 1 458.60 394.40 20.49 o -1 8 1 2989.81 3003.26 33.52 o 0 8 1 1663.69 1720.35 23.71 o 1 8 1 6307.39 6458.62 72.81 o 2 8 1 1190.24 1226.26 23.44 o 3 8 1 574.39 595.47 17.91 o 4 8 1 3673.35 3512.75 55.63 o 5 8 1 7032.33 7027.30 74.82 o 6 8 1 13.10 15.56 10.00 o 7 8 1 3179.65 3084.66 53.03 o 8 8 1 1289.24 1263.80 40.53 o 9 8 1 216.34 219.11 24.35 o 10 8 1 1164.78 1134.14 55.31 o -11 9 1 971.16 1120.62 71.59 o -10 9 1 104.23 151.70 23.84 o -9 9 1 8.31 24.36 17.46 o -8 9 1 1.67 26.56 14.40 o -7 9 1 933.90 909.22 28.88 o -6 9 1 285.42 254.70 19.13 o -5 9 1 3859.24 3827.41 96.34 o -4 9 1 742.40 672.35 22.32 o -3 9 1 97.20 84.19 10.10 o -2 9 1 815.39 876.17 48.66 o -1 9 1 2723.96 2691.11 36.24 o 0 9 1 39.51 55.88 8.88 o 1 9 1 321.66 306.17 13.47 o 2 9 1 1536.72 1533.98 27.70 o 3 9 1 24270.88 24749.97 229.23 o 4 9 1 104.32 138.16 12.42 o 5 9 1 588.36 566.92 19.47 o 6 9 1 760.01 717.88 39.26 o 7 9 1 2702.56 2636.99 57.48 o 8 9 1 579.58 558.77 30.08 o 9 9 1 25.70 44.19 20.02 o 10 9 1 323.59 318.20 59.29 o -10 10 1 244.91 267.18 29.20 o -9 10 1 23.80 31.99 19.07 o -8 10 1 115.70 117.46 17.80 o -7 10 1 718.41 612.55 32.06 o -6 10 1 674.51 654.56 24.69 o -5 10 1 635.73 586.00 26.14 o -4 10 1 4278.23 4338.57 70.67 o -3 10 1 29.54 22.33 12.16 o -2 10 1 3.04 1.13 10.77 o -1 10 1 767.45 766.69 34.71 o 0 10 1 6217.90 6299.68 75.19 o 1 10 1 36.61 44.93 15.40 o 2 10 1 387.00 365.06 15.64 o 3 10 1 132.71 167.73 12.84 o 4 10 1 334.03 386.74 18.97 o 5 10 1 2044.76 2015.27 40.04 o 6 10 1 3971.89 3990.38 61.00 o 7 10 1 1008.22 1065.71 38.28 o 8 10 1 7314.44 7631.62 117.32 o 9 10 1 66.68 89.43 40.44 o -9 11 1 154.82 158.60 29.86 o -8 11 1 61.76 57.91 19.18 o -7 11 1 2271.02 2345.03 59.13 o -6 11 1 784.38 711.30 60.05 o -5 11 1 346.86 321.89 23.17 o -4 11 1 1255.45 1216.15 36.64 o -3 11 1 992.52 903.05 31.24 o -2 11 1 3193.76 3105.58 57.84 o -1 11 1 551.99 539.92 24.30 o 0 11 1 10.21 2.06 11.64 o 1 11 1 5906.82 6139.80 76.63 o 2 11 1 2639.35 2554.90 69.36 o 3 11 1 1589.53 1510.71 39.01 o 4 11 1 1355.35 1498.50 39.59 o 5 11 1 143.18 92.58 16.25 o 6 11 1 912.15 968.77 36.40 o 7 11 1 53.32 47.90 19.14 o 8 11 1 1435.72 1599.91 54.34 o -8 12 1 21.00 10.73 23.69 o -7 12 1 107.49 136.31 21.34 o -6 12 1 25.29 28.71 28.85 o -5 12 1 1514.92 1585.42 44.44 o -4 12 1 2178.25 2186.48 75.48 o -3 12 1 1379.04 1358.67 48.45 o -2 12 1 85.71 91.82 16.02 o -1 12 1 2354.34 2256.55 50.22 o 0 12 1 212.79 220.84 23.48 o 1 12 1 1505.83 1462.58 49.29 o 2 12 1 6453.32 6371.46 338.96 o 3 12 1 1991.03 1941.38 46.65 o 4 12 1 2998.67 2936.53 116.38 o 5 12 1 0.11 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