#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/79/2227998.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227998_Fobs loop_ _publ_author_name 'Fun, Hoong-Kun' 'Shahani, Tara' Nithinchandra 'Kalluraya, Balakrishna' _publ_section_title ; 4-[2,3-Dibromo-3-(4-bromophenyl)propanoyl]-2-phenyl-1,2,3-oxadiazol-2-ium-5-olate ; _journal_coeditor_code SJ5039 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2818 _journal_page_last o2819 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.973 _cell_angle_gamma 90.000 _cell_length_a 17.6996 _cell_length_b 5.8322 _cell_length_c 18.2445 _exptl_crystal_F_000 1024.00 _reflns_d_resolution_high 0.7105 _[local]_cod_data_source_file sj5039Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bk36m in P2(1)/n (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 321.34 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 304.37 309.10 8.01 o 4 0 0 7739.93 7647.22 150.42 o 6 0 0 772.61 740.37 21.76 o 8 0 0 17500.33 18763.60 317.14 o 10 0 0 16182.01 16085.58 269.46 o 12 0 0 6194.93 6042.98 120.88 o 14 0 0 11381.24 11278.86 313.58 o 16 0 0 2396.85 2309.37 66.91 o 18 0 0 3872.69 3822.74 101.66 o 20 0 0 2059.02 2036.88 67.30 o 22 0 0 130.80 198.71 81.25 o 1 1 0 840.93 849.50 10.97 o 2 1 0 15.25 33.72 5.87 o 3 1 0 3022.52 3140.20 40.12 o 4 1 0 2271.23 2282.64 30.25 o 5 1 0 103256.56 101829.64 1282.31 o 6 1 0 358.11 344.63 7.45 o 7 1 0 2521.49 2682.64 33.90 o 8 1 0 9246.68 9568.91 122.00 o 9 1 0 6256.23 6249.41 75.82 o 10 1 0 200.40 186.86 7.75 o 11 1 0 1401.64 1368.40 22.40 o 12 1 0 147.94 144.82 9.96 o 13 1 0 12713.73 12495.29 170.98 o 14 1 0 23.60 23.97 10.51 o 15 1 0 2611.36 2665.10 46.97 o 16 1 0 142.56 149.85 16.33 o 17 1 0 3698.89 3768.15 70.58 o 18 1 0 53.78 21.00 17.91 o 19 1 0 3225.73 3276.72 64.01 o 20 1 0 192.41 195.60 21.81 o 21 1 0 9.62 -3.61 30.20 o 22 1 0 216.65 222.58 35.36 o 23 1 0 75.01 79.94 29.56 o 0 2 0 85788.52 84069.20 1430.14 o 1 2 0 312.11 307.00 5.85 o 2 2 0 196.16 209.66 4.61 o 3 2 0 13348.16 13523.46 159.17 o 4 2 0 268.40 306.50 6.30 o 5 2 0 4255.04 4342.35 52.55 o 6 2 0 786.24 790.72 13.29 o 7 2 0 2423.36 2603.91 35.41 o 8 2 0 1049.13 1049.13 17.17 o 9 2 0 2463.08 2457.20 34.83 o 10 2 0 12564.94 12587.88 171.01 o 11 2 0 1243.68 1214.08 22.39 o 12 2 0 4101.70 4081.13 59.65 o 13 2 0 2049.05 2100.91 34.48 o 14 2 0 3834.15 4008.13 70.88 o 15 2 0 24.47 26.45 14.84 o 16 2 0 2200.16 2317.14 47.87 o 17 2 0 2822.98 2878.59 65.99 o 18 2 0 1799.95 1761.38 47.57 o 19 2 0 4.97 -9.92 20.97 o 20 2 0 1285.73 1263.69 93.25 o 21 2 0 34.65 -1.13 24.79 o 22 2 0 471.01 496.38 31.45 o 23 2 0 4.51 23.58 37.52 o 1 3 0 156.71 154.18 7.60 o 2 3 0 371.67 355.08 6.39 o 3 3 0 0.52 8.07 3.51 o 4 3 0 3640.36 3602.73 41.57 o 5 3 0 15993.25 16026.46 168.82 o 6 3 0 1358.70 1287.20 17.33 o 7 3 0 2749.58 2837.40 34.29 o 8 3 0 10762.06 10649.86 120.23 o 9 3 0 39.39 42.80 8.33 o 10 3 0 794.66 812.27 20.43 o 11 3 0 387.96 416.84 18.13 o 12 3 0 2537.55 2524.28 44.08 o 13 3 0 2080.68 2155.83 44.67 o 14 3 0 1068.53 1084.37 36.26 o 15 3 0 3695.43 3584.60 96.08 o 16 3 0 153.97 174.31 22.35 o 17 3 0 1366.97 1379.86 53.18 o 18 3 0 4.49 27.86 22.00 o 19 3 0 601.86 591.55 31.60 o 20 3 0 192.82 190.51 26.89 o 21 3 0 4.21 12.00 25.07 o 22 3 0 944.33 880.76 39.85 o 0 4 0 7005.05 6746.77 101.19 o 1 4 0 8.43 4.73 4.29 o 2 4 0 1017.36 1034.59 13.80 o 3 4 0 7624.44 7770.15 83.24 o 4 4 0 259.44 275.42 7.60 o 5 4 0 1277.32 1299.19 19.35 o 6 4 0 24.80 39.31 6.85 o 7 4 0 1353.25 1296.84 23.66 o 8 4 0 1176.18 1117.25 21.99 o 9 4 0 2545.69 2496.46 39.84 o 10 4 0 3410.03 3326.65 50.90 o 11 4 0 2636.73 2608.37 48.58 o 12 4 0 247.98 237.86 19.32 o 13 4 0 1993.38 2088.44 65.26 o 14 4 0 187.63 192.46 21.18 o 15 4 0 83.69 92.25 21.04 o 16 4 0 5.88 -3.27 21.09 o 17 4 0 2103.12 2146.52 74.88 o 18 4 0 192.78 186.42 25.24 o 19 4 0 64.49 61.11 25.52 o 20 4 0 313.90 353.65 29.19 o 1 5 0 121.08 130.95 6.59 o 2 5 0 1738.77 1803.06 29.09 o 3 5 0 645.11 658.18 17.22 o 4 5 0 955.45 966.16 21.30 o 5 5 0 1285.11 1208.32 25.32 o 6 5 0 1160.42 1172.84 24.94 o 7 5 0 495.87 520.04 17.13 o 8 5 0 6917.18 6797.37 105.62 o 9 5 0 41.17 59.51 13.39 o 10 5 0 218.52 226.40 20.02 o 11 5 0 160.12 164.32 19.79 o 12 5 0 203.08 219.93 21.69 o 13 5 0 370.90 353.73 24.53 o 14 5 0 164.78 152.56 23.13 o 15 5 0 991.28 1076.29 57.63 o 16 5 0 23.68 32.42 23.27 o 17 5 0 8.55 14.49 42.96 o 18 5 0 87.06 83.81 30.63 o 0 6 0 101.98 102.25 33.34 o 1 6 0 94.08 111.62 23.58 o 2 6 0 1054.92 1018.02 42.32 o 3 6 0 2293.14 2300.36 52.84 o 4 6 0 0.29 22.56 15.24 o 5 6 0 1355.46 1390.64 38.95 o 6 6 0 136.63 147.11 18.00 o 7 6 0 405.58 421.94 23.01 o 8 6 0 215.76 220.21 21.06 o 9 6 0 406.33 448.38 34.02 o 10 6 0 139.54 101.19 25.11 o 11 6 0 224.61 229.60 50.44 o 12 6 0 2.95 1.96 42.13 o 13 6 0 570.56 659.46 40.67 o 14 6 0 318.11 351.66 33.05 o 15 6 0 11.86 33.25 29.20 o 16 6 0 156.86 182.68 31.78 o 1 7 0 92.00 127.67 30.09 o 2 7 0 559.12 614.67 56.05 o 3 7 0 581.72 514.79 53.10 o 4 7 0 177.23 284.04 49.29 o 5 7 0 28.89 121.49 48.49 o 6 7 0 24.68 94.13 48.78 o 7 7 0 153.86 215.08 56.10 o 8 7 0 936.03 918.54 82.41 o 9 7 0 275.77 307.69 31.00 o 10 7 0 81.50 125.90 52.03 o 11 7 0 131.15 192.36 29.82 o 12 7 0 84.86 94.84 30.61 o -23 0 1 378.53 427.90 39.57 o -21 0 1 3214.83 3357.94 93.84 o -19 0 1 215.32 193.15 44.30 o -17 0 1 3451.56 3379.77 106.10 o -15 0 1 12732.53 12351.72 240.25 o -13 0 1 8090.92 7999.58 237.12 o -11 0 1 471.12 423.63 20.06 o -9 0 1 7518.66 7354.50 125.23 o -7 0 1 4526.56 4595.91 78.75 o -5 0 1 29749.59 29582.81 570.19 o -3 0 1 2227.84 2349.63 85.64 o 1 0 1 9354.16 8651.50 296.32 o 3 0 1 13733.12 13158.33 255.72 o 5 0 1 366.85 352.61 11.30 o 7 0 1 265.71 216.65 11.31 o 9 0 1 41378.50 40310.55 1020.80 o 11 0 1 4757.77 4747.40 130.14 o 13 0 1 3143.97 3139.79 95.88 o 15 0 1 7247.22 7152.37 199.45 o 17 0 1 1764.61 1819.65 59.35 o 19 0 1 786.23 764.76 42.14 o 21 0 1 1454.46 1441.28 57.88 o 23 0 1 4.50 10.81 38.98 o -24 1 1 482.50 517.42 34.32 o -23 1 1 260.92 286.45 38.20 o -22 1 1 2032.98 2071.27 56.46 o -21 1 1 3.91 -23.00 23.00 o -20 1 1 271.16 305.01 22.67 o -19 1 1 20.10 10.97 18.34 o -18 1 1 32.70 1.80 16.43 o -17 1 1 11.26 -0.41 15.73 o -16 1 1 344.86 371.24 19.09 o -15 1 1 0.44 7.76 11.46 o -14 1 1 504.54 482.90 18.71 o -13 1 1 2353.01 2307.02 37.00 o -12 1 1 189.51 215.82 12.95 o -11 1 1 380.51 360.39 10.86 o -10 1 1 27412.87 27194.43 319.12 o -9 1 1 2017.62 2090.97 27.67 o -8 1 1 20272.85 20553.76 241.15 o -7 1 1 4838.35 5210.61 62.74 o -6 1 1 51.62 76.58 6.38 o -5 1 1 11050.74 11167.80 140.45 o -4 1 1 12363.51 12949.26 175.21 o -3 1 1 373.90 350.87 9.45 o -2 1 1 2366.51 2457.55 32.19 o -1 1 1 2171.04 2119.39 26.11 o 0 1 1 5809.00 6064.31 73.25 o 1 1 1 1073.01 1072.75 14.70 o 2 1 1 1563.61 1526.31 24.69 o 3 1 1 131.91 128.79 3.92 o 4 1 1 34638.90 33888.74 464.26 o 5 1 1 96.40 113.18 4.35 o 6 1 1 8817.50 8817.11 105.04 o 7 1 1 277.79 249.52 7.38 o 8 1 1 18117.16 18429.76 232.55 o 9 1 1 6.62 6.42 5.69 o 10 1 1 613.55 636.52 13.58 o 11 1 1 0.23 2.04 7.61 o 12 1 1 16.08 15.80 9.30 o 13 1 1 8.87 15.09 9.65 o 14 1 1 3372.64 3328.78 51.26 o 15 1 1 167.42 149.94 13.94 o 16 1 1 33.46 19.44 15.52 o 17 1 1 856.08 915.27 30.47 o 18 1 1 11.69 15.93 17.85 o 19 1 1 376.82 382.27 22.83 o 20 1 1 2991.46 3067.70 62.50 o 21 1 1 18.26 13.40 20.24 o 22 1 1 833.19 753.25 46.04 o 23 1 1 40.11 37.32 26.10 o -23 2 1 93.89 36.20 25.92 o -22 2 1 73.11 32.81 25.06 o -21 2 1 940.99 977.51 39.67 o -20 2 1 1.34 -19.75 21.74 o -19 2 1 3.17 -20.78 20.78 o -18 2 1 3010.17 3044.81 69.52 o -17 2 1 1549.29 1549.49 51.02 o -16 2 1 814.59 824.49 60.22 o -15 2 1 2161.02 2338.31 61.92 o -14 2 1 145.13 142.28 12.50 o -13 2 1 1149.55 1170.67 27.78 o -12 2 1 31.20 29.19 8.43 o -11 2 1 238.04 242.56 9.85 o -10 2 1 793.24 794.70 16.58 o -9 2 1 5852.45 5754.54 74.45 o -8 2 1 2110.64 2015.06 26.50 o -7 2 1 2043.53 2107.33 29.05 o -6 2 1 442.65 520.97 9.85 o -5 2 1 22496.34 22478.86 263.38 o -4 2 1 792.20 761.20 11.34 o -3 2 1 4482.75 4713.36 53.49 o -2 2 1 7213.60 7295.43 77.95 o -1 2 1 10116.29 10079.69 108.36 o 0 2 1 14123.18 14537.27 163.59 o 1 2 1 2139.52 2174.09 23.22 o 2 2 1 2511.96 2697.18 29.72 o 3 2 1 6157.22 6325.21 76.11 o 4 2 1 1267.12 1256.64 15.97 o 5 2 1 839.42 835.48 13.38 o 6 2 1 701.64 661.29 11.97 o 7 2 1 1806.24 1879.54 26.62 o 8 2 1 576.39 565.49 11.33 o 9 2 1 12895.68 12621.66 149.87 o 10 2 1 3.93 2.68 6.68 o 11 2 1 1189.01 1200.84 22.76 o 12 2 1 6412.87 6397.20 90.09 o 13 2 1 1672.37 1690.61 44.34 o 14 2 1 644.95 663.64 18.95 o 15 2 1 1121.07 1208.22 47.57 o 16 2 1 4.02 -15.71 15.71 o 17 2 1 1042.43 1037.95 57.74 o 18 2 1 159.83 152.54 22.13 o 19 2 1 450.89 421.22 27.23 o 20 2 1 149.52 127.66 30.99 o 21 2 1 675.38 656.77 32.79 o 22 2 1 544.53 523.01 32.20 o -22 3 1 207.09 207.89 28.69 o -21 3 1 2.84 -17.74 25.29 o -20 3 1 97.35 111.20 24.53 o -19 3 1 598.24 602.42 32.30 o -18 3 1 21.94 26.05 22.64 o -17 3 1 0.91 4.58 21.11 o -16 3 1 616.43 623.38 29.62 o -15 3 1 457.19 501.55 32.66 o -14 3 1 317.08 333.03 25.70 o -13 3 1 3414.39 3675.04 71.69 o -12 3 1 57.79 65.01 10.14 o -11 3 1 438.17 425.65 14.14 o -10 3 1 4606.21 4620.13 72.89 o -9 3 1 2129.95 2107.68 33.03 o -8 3 1 1563.22 1563.87 21.91 o -7 3 1 3940.80 3911.75 46.10 o -6 3 1 274.72 283.34 7.27 o -5 3 1 5964.30 6026.89 72.82 o -4 3 1 830.43 829.02 12.24 o -3 3 1 2344.98 2323.59 26.58 o -2 3 1 655.59 642.38 9.66 o -1 3 1 3655.96 3707.51 36.85 o 0 3 1 8585.57 8878.79 90.19 o 1 3 1 3213.83 3065.44 32.34 o 2 3 1 521.29 562.67 8.07 o 3 3 1 8177.29 8431.39 94.11 o 4 3 1 11233.00 11512.05 129.03 o 5 3 1 4675.76 4685.54 54.04 o 6 3 1 164.91 179.18 6.54 o 7 3 1 2501.60 2470.21 35.65 o 8 3 1 4775.52 4721.80 55.27 o 9 3 1 269.35 314.86 15.82 o 10 3 1 9.80 18.49 8.01 o 11 3 1 776.55 760.39 18.08 o 12 3 1 18.88 26.84 10.86 o 13 3 1 1072.88 1103.84 30.03 o 14 3 1 1446.89 1500.20 42.24 o 15 3 1 2.53 4.90 19.14 o 16 3 1 120.91 145.67 24.97 o 17 3 1 2653.31 2769.61 56.42 o 18 3 1 2.52 -19.23 27.15 o 19 3 1 291.89 288.96 26.96 o 20 3 1 559.76 536.77 31.71 o 21 3 1 188.76 170.25 26.93 o 22 3 1 174.76 198.23 35.39 o -21 4 1 413.05 398.17 30.31 o -20 4 1 0.74 13.16 24.78 o -19 4 1 23.22 12.31 24.32 o -18 4 1 1731.86 1803.83 72.86 o -17 4 1 4.74 -8.54 21.48 o -16 4 1 405.38 407.19 26.33 o -15 4 1 364.83 375.65 24.12 o -14 4 1 1116.12 1161.32 37.03 o -13 4 1 115.37 133.25 18.64 o -12 4 1 26.28 39.63 16.28 o -11 4 1 16.32 25.01 12.29 o -10 4 1 4.83 24.09 8.90 o -9 4 1 240.86 251.79 11.20 o -8 4 1 5964.87 5842.24 83.70 o -7 4 1 718.45 698.68 15.44 o -6 4 1 376.66 384.85 10.97 o -5 4 1 3521.73 3433.69 46.39 o -4 4 1 1958.48 1910.43 24.56 o -3 4 1 70.40 63.50 4.53 o -2 4 1 9951.24 9959.20 104.62 o -1 4 1 193.48 174.75 5.32 o 0 4 1 11299.45 11817.58 118.90 o 1 4 1 155.25 182.34 5.51 o 2 4 1 1028.84 1084.61 14.61 o 3 4 1 110.79 120.22 6.20 o 4 4 1 483.84 488.55 10.80 o 5 4 1 1002.59 988.40 15.18 o 6 4 1 338.97 337.31 10.46 o 7 4 1 317.59 323.02 11.49 o 8 4 1 234.04 229.54 10.50 o 9 4 1 256.70 264.45 11.82 o 10 4 1 140.64 129.10 10.68 o 11 4 1 197.53 182.67 12.43 o 12 4 1 6989.67 7278.75 126.01 o 13 4 1 1471.65 1429.64 41.34 o 14 4 1 775.54 794.07 33.80 o 15 4 1 416.60 414.03 28.60 o 16 4 1 78.14 70.25 22.72 o 17 4 1 50.32 44.97 23.80 o 18 4 1 97.88 86.75 24.95 o 19 4 1 397.01 384.76 29.01 o 20 4 1 1.09 -12.94 30.36 o -19 5 1 551.78 560.27 38.10 o -18 5 1 19.63 24.14 23.67 o -17 5 1 39.95 38.30 23.82 o -16 5 1 165.70 169.40 27.85 o -15 5 1 5.03 36.69 30.65 o -14 5 1 9.11 25.67 20.82 o -13 5 1 4923.76 4970.59 103.33 o -12 5 1 15.25 15.56 19.14 o -11 5 1 39.78 20.94 20.32 o -10 5 1 85.24 69.30 17.47 o -9 5 1 238.41 232.55 15.00 o -8 5 1 19.33 7.45 10.02 o -7 5 1 1541.08 1525.52 30.23 o -6 5 1 731.93 736.65 21.69 o -5 5 1 3780.23 3866.58 61.17 o -4 5 1 16.71 46.30 9.51 o -3 5 1 849.10 883.88 20.07 o -2 5 1 524.40 495.80 15.59 o -1 5 1 1030.86 1041.34 19.67 o 0 5 1 314.43 308.73 8.84 o 1 5 1 2371.59 2394.84 27.89 o 2 5 1 34.52 37.69 8.89 o 3 5 1 1271.06 1306.97 29.13 o 4 5 1 0.75 10.74 10.94 o 5 5 1 4590.51 4642.06 67.84 o 6 5 1 439.11 462.51 16.82 o 7 5 1 2498.04 2577.56 50.07 o 8 5 1 121.72 129.51 13.43 o 9 5 1 1539.15 1510.89 41.37 o 10 5 1 443.98 428.73 23.00 o 11 5 1 218.37 219.64 21.19 o 12 5 1 9.29 33.08 19.85 o 13 5 1 365.13 376.49 25.17 o 14 5 1 119.94 153.80 44.38 o 15 5 1 6.10 19.80 47.67 o 16 5 1 132.78 115.53 28.17 o 17 5 1 1425.45 1504.00 60.51 o 18 5 1 153.78 217.11 33.05 o -16 6 1 303.76 318.06 33.42 o -15 6 1 6.38 22.30 27.90 o -14 6 1 258.69 235.38 47.92 o -13 6 1 8.35 13.72 25.94 o -12 6 1 118.46 118.96 36.72 o -11 6 1 431.55 488.50 34.85 o -10 6 1 341.21 381.55 24.34 o -9 6 1 9.86 27.81 25.87 o -8 6 1 1129.97 1150.58 37.09 o -7 6 1 541.18 521.91 24.61 o -6 6 1 33.87 41.97 17.14 o -5 6 1 321.66 345.15 20.31 o -4 6 1 550.96 551.30 21.66 o -3 6 1 6.46 -5.22 12.34 o -2 6 1 1537.43 1654.63 54.67 o -1 6 1 159.51 149.65 24.61 o 0 6 1 2241.71 2303.10 66.81 o 1 6 1 364.26 368.74 27.99 o 2 6 1 1017.14 1082.43 70.96 o 3 6 1 213.93 229.85 26.51 o 4 6 1 271.60 282.91 19.70 o 5 6 1 71.91 98.67 17.53 o 6 6 1 64.03 69.56 17.85 o 7 6 1 178.38 202.98 23.62 o 8 6 1 471.94 575.15 36.62 o 9 6 1 529.75 564.45 36.47 o 10 6 1 32.85 44.04 24.95 o 11 6 1 65.10 113.14 27.11 o 12 6 1 1925.10 2017.47 66.52 o 13 6 1 33.70 37.80 27.96 o 14 6 1 356.25 385.56 56.33 o 15 6 1 2.85 24.97 29.53 o 16 6 1 3.74 13.60 29.92 o -12 7 1 117.16 109.06 28.97 o -11 7 1 0.87 10.56 26.72 o -10 7 1 155.37 196.88 28.75 o -9 7 1 4.46 45.88 35.71 o -8 7 1 510.26 515.74 34.02 o -7 7 1 456.48 536.25 65.48 o -6 7 1 208.92 308.75 55.56 o -5 7 1 137.53 197.37 49.48 o -4 7 1 112.98 143.30 30.02 o -3 7 1 209.48 296.49 31.94 o -2 7 1 69.31 106.14 28.84 o -1 7 1 145.53 189.80 41.40 o 0 7 1 0.74 10.67 37.73 o 1 7 1 55.32 123.80 40.87 o 2 7 1 20.80 93.19 40.55 o 3 7 1 629.23 675.08 57.00 o 4 7 1 385.43 403.69 52.62 o 5 7 1 405.88 440.91 56.41 o 6 7 1 207.63 247.15 53.25 o 7 7 1 1084.42 1119.60 83.14 o 8 7 1 199.41 312.25 59.51 o 9 7 1 35.27 67.72 48.78 o 10 7 1 35.45 22.07 28.51 o 11 7 1 68.01 130.61 29.92 o 12 7 1 2.83 47.52 30.88 o -24 0 2 12.62 -26.47 83.53 o -22 0 2 2.35 8.70 73.72 o -20 0 2 2222.11 2240.01 88.82 o -18 0 2 7169.66 7047.34 171.60 o -16 0 2 102.84 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