#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/80/2228015.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228015_Fobs loop_ _publ_author_name 'Kargar, Hadi' 'Kia, Reza' 'Tahir, Muhammad Nawaz' 'Sahraei, Atefeh' _publ_section_title ; {6,6'-Dimethoxy-2,2'-[4,5-dimethyl-o-phenylenebis(nitrilomethylidyne)]diphenolato}nickel(II) ; _journal_coeditor_code SU2210 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1246 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.730 _cell_angle_gamma 90.000 _cell_length_a 12.8057 _cell_length_b 12.6514 _cell_length_c 13.0263 _exptl_crystal_F_000 960.00 _reflns_d_resolution_high 0.7483 _[local]_cod_data_source_file su2210Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AS6N_0m in P2(1)/n DARK RED PLATE' _shelx_refln_list_code 4 _shelx_f_calc_maximum 301.27 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13019.14 12893.47 151.33 o 4 0 0 16037.33 16078.87 171.53 o 6 0 0 30.98 29.36 9.23 o 8 0 0 670.63 604.66 30.28 o 10 0 0 15.36 108.01 22.31 o 12 0 0 91.85 96.02 82.94 o 14 0 0 2.15 -35.42 35.42 o 16 0 0 9.88 65.52 54.12 o 2 1 0 474.02 410.96 6.34 o 3 1 0 781.50 770.15 11.31 o 4 1 0 3035.41 3107.16 30.53 o 5 1 0 453.88 479.11 12.15 o 6 1 0 1029.76 954.39 27.58 o 7 1 0 102.77 106.58 10.78 o 8 1 0 941.91 977.46 25.96 o 9 1 0 2.45 -2.14 10.29 o 10 1 0 255.55 288.57 26.54 o 11 1 0 6.21 -2.29 16.29 o 12 1 0 170.00 112.32 26.23 o 13 1 0 29.51 19.19 27.36 o 14 1 0 122.09 160.10 36.27 o 15 1 0 18.87 9.38 30.32 o 16 1 0 92.20 124.83 41.07 o 0 2 0 6917.33 7110.24 91.57 o 1 2 0 55.18 51.85 2.87 o 2 2 0 71577.82 71249.20 490.55 o 3 2 0 90762.20 90508.50 609.48 o 4 2 0 25795.68 25756.66 191.33 o 5 2 0 2271.23 2362.88 27.37 o 6 2 0 2234.59 2171.15 31.25 o 7 2 0 952.42 1034.98 27.23 o 8 2 0 77.01 41.01 9.81 o 9 2 0 183.15 194.29 15.71 o 10 2 0 54.47 71.48 14.65 o 11 2 0 111.60 98.88 21.26 o 12 2 0 1.38 -4.32 17.91 o 13 2 0 40.42 64.65 30.49 o 14 2 0 17.35 6.10 28.04 o 15 2 0 0.90 4.02 32.52 o 16 2 0 23.12 53.16 43.88 o 1 3 0 107.22 94.49 4.45 o 2 3 0 11830.86 11858.94 94.72 o 3 3 0 950.44 896.71 12.72 o 4 3 0 3.21 -4.46 4.46 o 5 3 0 3527.41 3660.57 38.55 o 6 3 0 2916.31 2807.80 37.67 o 7 3 0 402.92 475.20 18.47 o 8 3 0 171.44 190.48 15.59 o 9 3 0 139.94 140.68 15.79 o 10 3 0 724.01 783.94 29.15 o 11 3 0 90.38 65.52 23.77 o 12 3 0 198.92 280.61 28.23 o 13 3 0 91.51 115.13 29.40 o 14 3 0 133.98 129.73 40.16 o 15 3 0 26.62 38.70 38.84 o 16 3 0 74.84 59.20 41.81 o 0 4 0 59.26 55.67 7.47 o 1 4 0 52.69 71.18 7.16 o 2 4 0 1653.96 1553.78 18.94 o 3 4 0 896.94 966.24 14.46 o 4 4 0 5853.65 5752.21 51.05 o 5 4 0 12984.25 13350.31 116.65 o 6 4 0 9959.21 9498.52 98.20 o 7 4 0 5560.92 5506.24 74.11 o 8 4 0 1006.69 1036.30 30.26 o 9 4 0 1257.39 1327.72 35.35 o 10 4 0 20.97 13.02 15.27 o 11 4 0 187.57 201.99 23.24 o 12 4 0 0.18 8.86 19.60 o 13 4 0 218.67 226.33 33.72 o 14 4 0 2.35 4.55 33.65 o 15 4 0 104.86 81.68 43.41 o 16 4 0 22.55 27.36 43.81 o 1 5 0 6553.84 6255.58 65.98 o 2 5 0 1424.94 1468.77 20.22 o 3 5 0 3253.63 2826.03 32.95 o 4 5 0 417.02 379.23 14.61 o 5 5 0 477.53 517.38 13.43 o 6 5 0 666.03 721.66 17.63 o 7 5 0 3393.50 3422.00 55.04 o 8 5 0 67.21 61.26 13.02 o 9 5 0 11.88 20.56 13.82 o 10 5 0 1181.10 1231.37 44.19 o 11 5 0 103.05 93.20 22.66 o 12 5 0 181.38 249.57 33.85 o 13 5 0 28.84 -11.00 28.96 o 14 5 0 69.81 69.96 38.95 o 15 5 0 11.21 19.06 38.41 o 0 6 0 9.58 12.52 6.35 o 1 6 0 111.35 131.33 7.63 o 2 6 0 782.74 779.09 18.46 o 3 6 0 95.58 93.96 9.22 o 4 6 0 0.99 1.25 6.24 o 5 6 0 741.13 884.23 19.78 o 6 6 0 54.60 30.75 10.64 o 7 6 0 3268.40 3208.79 53.91 o 8 6 0 858.88 872.10 44.16 o 9 6 0 2500.52 2452.32 49.05 o 10 6 0 369.58 394.07 26.73 o 11 6 0 1064.02 1117.38 58.14 o 12 6 0 1.32 28.54 22.50 o 13 6 0 208.87 320.82 36.64 o 14 6 0 3.42 -22.81 28.48 o 15 6 0 94.11 111.36 44.56 o 1 7 0 2696.38 2453.25 33.13 o 2 7 0 839.93 865.09 19.82 o 3 7 0 5057.19 5015.19 52.01 o 4 7 0 155.25 171.43 10.26 o 5 7 0 869.77 815.31 21.24 o 6 7 0 416.27 452.85 21.40 o 7 7 0 435.92 448.37 22.05 o 8 7 0 772.75 679.75 30.38 o 9 7 0 273.58 317.58 26.64 o 10 7 0 51.56 53.65 19.63 o 11 7 0 200.83 185.15 26.08 o 12 7 0 92.19 79.40 27.60 o 13 7 0 23.35 -13.91 24.79 o 14 7 0 45.32 10.91 32.79 o 15 7 0 3.35 -6.54 37.75 o 0 8 0 796.14 868.10 24.87 o 1 8 0 163.98 176.89 11.32 o 2 8 0 862.74 873.74 20.76 o 3 8 0 326.03 338.86 14.76 o 4 8 0 152.15 128.35 10.25 o 5 8 0 997.62 1259.44 25.08 o 6 8 0 114.67 132.80 15.62 o 7 8 0 353.27 375.42 28.38 o 8 8 0 76.07 94.01 17.64 o 9 8 0 1076.76 982.15 46.09 o 10 8 0 17.20 -18.06 18.06 o 11 8 0 372.37 443.47 43.76 o 12 8 0 23.70 -0.97 24.36 o 13 8 0 559.50 701.82 51.00 o 14 8 0 17.12 64.94 35.13 o 1 9 0 1897.32 1831.74 27.06 o 2 9 0 1.41 4.41 6.73 o 3 9 0 1795.69 1763.05 30.52 o 4 9 0 105.47 97.18 12.06 o 5 9 0 2070.69 1892.15 32.39 o 6 9 0 287.21 282.64 15.26 o 7 9 0 412.37 418.16 21.70 o 8 9 0 1.86 -13.26 15.17 o 9 9 0 4.22 7.33 17.37 o 10 9 0 40.29 0.69 18.50 o 11 9 0 0.47 23.14 22.37 o 12 9 0 21.71 15.73 27.33 o 13 9 0 65.43 19.87 30.32 o 14 9 0 19.25 -13.95 34.12 o 0 10 0 1740.17 1781.53 52.83 o 1 10 0 69.79 47.52 9.35 o 2 10 0 387.02 347.12 14.02 o 3 10 0 1052.12 1013.29 24.75 o 4 10 0 214.13 233.79 19.56 o 5 10 0 142.05 195.59 14.43 o 6 10 0 458.26 421.24 22.65 o 7 10 0 247.19 248.67 19.05 o 8 10 0 41.74 29.79 17.38 o 9 10 0 146.79 132.64 23.00 o 10 10 0 97.47 96.62 25.42 o 11 10 0 192.69 196.51 43.23 o 12 10 0 16.53 18.47 31.05 o 13 10 0 146.74 184.36 49.23 o 1 11 0 1221.07 1234.25 35.82 o 2 11 0 21.76 6.35 8.94 o 3 11 0 384.01 378.41 20.96 o 4 11 0 218.71 220.68 18.33 o 5 11 0 233.69 270.65 20.36 o 6 11 0 83.13 61.62 15.60 o 7 11 0 169.92 166.20 21.42 o 8 11 0 169.50 154.46 23.14 o 9 11 0 119.87 99.72 22.98 o 10 11 0 40.38 51.87 22.48 o 11 11 0 6.66 -20.38 22.87 o 12 11 0 4.06 54.96 30.40 o 0 12 0 1577.16 1576.57 50.88 o 1 12 0 10.60 18.43 11.97 o 2 12 0 490.29 491.85 21.34 o 3 12 0 3.34 18.16 12.92 o 4 12 0 674.79 679.37 36.41 o 5 12 0 100.22 97.23 17.19 o 6 12 0 77.72 66.35 19.24 o 7 12 0 121.06 140.34 19.68 o 8 12 0 130.97 83.26 21.57 o 9 12 0 23.71 7.21 21.66 o 10 12 0 80.84 97.25 31.47 o 11 12 0 48.55 40.48 26.98 o 1 13 0 73.02 49.23 14.20 o 2 13 0 232.99 248.85 19.44 o 3 13 0 130.27 116.05 17.96 o 4 13 0 22.60 6.78 15.12 o 5 13 0 14.79 -2.10 15.52 o 6 13 0 100.94 113.15 19.05 o 7 13 0 86.00 97.93 20.65 o 8 13 0 38.62 59.27 21.78 o 9 13 0 0.76 17.22 22.55 o 10 13 0 147.59 157.00 37.37 o 0 14 0 458.06 455.07 36.18 o 1 14 0 1.88 -13.41 13.41 o 2 14 0 509.06 500.61 27.36 o 3 14 0 4.18 -15.09 15.09 o 4 14 0 380.01 380.74 35.88 o 5 14 0 0.05 -8.07 16.83 o 6 14 0 226.12 252.52 25.66 o 7 14 0 11.93 25.46 22.85 o 8 14 0 44.57 56.60 26.03 o 9 14 0 11.69 -26.41 26.41 o 1 15 0 6.11 17.67 15.40 o 2 15 0 0.16 -12.27 21.79 o 3 15 0 0.14 -16.50 18.34 o 4 15 0 32.24 34.18 20.11 o 5 15 0 24.91 19.23 19.62 o 6 15 0 109.85 118.12 25.11 o 7 15 0 22.51 -7.91 23.74 o 0 16 0 277.93 249.78 38.80 o 1 16 0 0.02 3.31 23.19 o 2 16 0 136.02 153.75 26.03 o 3 16 0 0.22 -3.95 21.56 o 4 16 0 196.44 211.46 33.80 o 5 16 0 15.91 20.29 22.78 o -15 0 1 223.75 279.64 62.80 o -13 0 1 29.08 22.37 39.27 o -11 0 1 6.87 1.24 25.85 o -9 0 1 1069.49 1049.37 35.52 o -7 0 1 1237.79 1206.46 27.60 o -5 0 1 1746.07 1824.31 34.55 o -3 0 1 13850.99 13512.65 172.97 o -1 0 1 28591.14 27497.60 446.96 o 1 0 1 17550.51 17007.36 196.77 o 3 0 1 10027.17 9407.70 108.57 o 5 0 1 16.48 219.41 25.21 o 7 0 1 125.11 131.98 18.40 o 9 0 1 252.85 247.38 26.04 o 11 0 1 561.74 603.57 52.80 o 13 0 1 381.04 367.18 61.27 o 15 0 1 102.70 72.38 51.65 o -16 1 1 12.22 76.42 38.27 o -15 1 1 1.17 26.54 32.60 o -14 1 1 57.91 67.33 31.76 o -13 1 1 71.06 80.88 29.67 o -12 1 1 2.16 -17.60 21.74 o -11 1 1 332.06 370.14 23.79 o -10 1 1 876.46 880.62 40.76 o -9 1 1 243.41 301.37 15.37 o -8 1 1 175.51 160.39 12.00 o -7 1 1 1746.30 1803.43 31.80 o -6 1 1 8.90 1.88 6.25 o -5 1 1 536.41 508.46 16.31 o -4 1 1 3933.66 4146.32 41.23 o -3 1 1 20.10 18.41 5.25 o -2 1 1 16571.95 16253.75 134.33 o -1 1 1 10516.58 10302.46 87.74 o 0 1 1 1128.12 1060.61 11.06 o 1 1 1 6175.44 6079.42 53.37 o 2 1 1 11323.66 11288.58 94.92 o 3 1 1 7513.80 7018.27 60.52 o 4 1 1 1090.42 1086.38 17.32 o 5 1 1 1533.03 1408.38 21.35 o 6 1 1 7.17 9.20 6.62 o 7 1 1 4019.30 3809.27 49.93 o 8 1 1 20.96 21.64 10.56 o 9 1 1 1837.39 1808.37 41.42 o 10 1 1 35.77 36.89 16.54 o 11 1 1 436.55 555.48 41.05 o 12 1 1 12.89 53.46 24.70 o 13 1 1 290.79 290.72 66.72 o 14 1 1 3.63 -17.47 28.65 o 15 1 1 19.56 -28.22 28.22 o 16 1 1 17.95 35.21 50.57 o -16 2 1 11.80 3.93 39.53 o -15 2 1 41.51 63.13 34.35 o -14 2 1 21.00 10.31 28.76 o -13 2 1 247.27 265.30 39.41 o -12 2 1 16.99 42.32 24.24 o -11 2 1 688.23 626.24 44.62 o -10 2 1 51.19 47.80 15.24 o -9 2 1 90.84 61.78 10.16 o -8 2 1 1075.70 1216.50 30.58 o -7 2 1 293.31 221.78 12.42 o -6 2 1 10.59 9.55 7.20 o -5 2 1 6186.46 6453.68 59.21 o -4 2 1 1820.62 1772.11 20.14 o -3 2 1 16.62 7.21 4.92 o -2 2 1 593.00 593.12 9.68 o -1 2 1 9962.90 9996.51 79.87 o 0 2 1 5.15 -0.61 2.88 o 1 2 1 4170.86 4235.35 44.46 o 2 2 1 21746.53 21274.09 160.68 o 3 2 1 23889.52 24173.99 174.22 o 4 2 1 4829.03 4832.38 42.73 o 5 2 1 230.74 385.54 12.28 o 6 2 1 1288.98 1221.68 22.42 o 7 2 1 109.02 117.73 10.33 o 8 2 1 594.79 583.95 22.73 o 9 2 1 695.49 713.75 25.10 o 10 2 1 106.67 189.00 17.91 o 11 2 1 239.66 246.01 26.96 o 12 2 1 59.32 4.72 23.85 o 13 2 1 270.60 213.62 47.00 o 14 2 1 2.38 -26.76 26.76 o 15 2 1 149.11 199.56 54.44 o 16 2 1 4.37 6.84 43.35 o -16 3 1 35.86 15.87 39.21 o -15 3 1 51.35 22.35 37.01 o -14 3 1 386.98 471.31 49.35 o -13 3 1 28.44 20.96 23.98 o -12 3 1 349.87 368.00 31.03 o -11 3 1 42.22 44.92 18.32 o -10 3 1 521.46 591.38 26.39 o -9 3 1 100.60 110.55 15.67 o -8 3 1 3.30 -9.80 9.80 o -7 3 1 176.09 219.78 14.29 o -6 3 1 10.47 -4.25 7.05 o -5 3 1 7348.48 7943.00 73.40 o -4 3 1 9168.72 8905.02 77.23 o -3 3 1 4169.97 4181.40 38.94 o -2 3 1 1829.12 1804.56 22.42 o -1 3 1 2293.95 2109.16 19.66 o 0 3 1 1038.29 1103.57 12.79 o 1 3 1 69.91 75.40 5.56 o 2 3 1 930.85 995.62 14.66 o 3 3 1 6171.30 5971.82 52.93 o 4 3 1 438.49 503.71 13.30 o 5 3 1 11667.87 11460.70 104.84 o 6 3 1 271.65 282.26 13.01 o 7 3 1 1265.63 1261.91 26.41 o 8 3 1 1.98 -2.33 10.44 o 9 3 1 935.44 886.54 29.84 o 10 3 1 4.10 4.31 13.56 o 11 3 1 475.05 500.31 39.29 o 12 3 1 147.73 162.10 29.21 o 13 3 1 73.56 70.09 27.00 o 14 3 1 25.07 15.01 33.86 o 15 3 1 37.07 40.29 43.10 o 16 3 1 10.47 -14.10 40.61 o -16 4 1 56.08 72.61 42.57 o -15 4 1 12.94 24.10 38.92 o -14 4 1 7.82 37.56 35.67 o -13 4 1 167.39 158.20 41.64 o -12 4 1 1.48 6.34 20.11 o -11 4 1 566.10 613.86 31.84 o -10 4 1 94.67 82.49 16.70 o -9 4 1 570.17 551.26 22.98 o -8 4 1 52.95 55.67 11.89 o -7 4 1 1957.08 1913.71 29.52 o -6 4 1 7.50 27.82 7.36 o -5 4 1 6471.83 7593.01 70.83 o -4 4 1 153.27 175.52 7.91 o -3 4 1 6359.28 6010.64 53.48 o -2 4 1 38.49 18.47 4.47 o -1 4 1 885.00 863.14 11.19 o 0 4 1 8.42 4.83 4.06 o 1 4 1 2246.56 2245.15 25.75 o 2 4 1 3659.63 3634.57 39.47 o 3 4 1 0.53 -0.29 4.98 o 4 4 1 2983.72 2845.91 31.92 o 5 4 1 4461.12 4559.24 49.33 o 6 4 1 14366.82 14355.65 147.46 o 7 4 1 1208.27 1282.84 29.74 o 8 4 1 1466.51 1412.02 37.30 o 9 4 1 138.79 143.82 16.08 o 10 4 1 858.58 882.13 52.03 o 11 4 1 31.87 14.94 17.62 o 12 4 1 41.34 27.87 20.97 o 13 4 1 65.45 37.90 29.16 o 14 4 1 18.89 14.99 34.57 o 15 4 1 82.24 97.12 43.80 o 16 4 1 8.30 -4.00 42.31 o -16 5 1 81.20 76.50 45.40 o -15 5 1 3.95 27.12 38.72 o -14 5 1 249.93 137.10 42.48 o -13 5 1 100.61 56.25 26.51 o -12 5 1 451.68 517.06 36.23 o -11 5 1 388.77 411.12 27.99 o -10 5 1 239.71 337.18 24.43 o -9 5 1 0.05 7.63 12.51 o -8 5 1 3575.75 3564.53 51.95 o -7 5 1 609.36 609.11 18.23 o -6 5 1 2289.70 2238.58 32.30 o -5 5 1 326.43 344.32 11.83 o -4 5 1 55.02 24.13 6.10 o -3 5 1 794.83 763.36 17.77 o -2 5 1 821.87 821.24 13.65 o -1 5 1 72.97 79.17 5.33 o 0 5 1 1274.31 1324.23 18.56 o 1 5 1 2382.35 2234.51 35.68 o 2 5 1 577.05 680.16 20.20 o 3 5 1 624.77 674.90 16.18 o 4 5 1 75.97 87.74 7.95 o 5 5 1 1804.65 1831.57 28.79 o 6 5 1 17.90 16.22 6.87 o 7 5 1 1825.50 1812.58 36.97 o 8 5 1 776.09 783.91 25.55 o 9 5 1 853.98 891.71 32.31 o 10 5 1 283.87 328.90 32.97 o 11 5 1 50.16 57.04 19.45 o 12 5 1 76.64 3.37 21.80 o 13 5 1 35.46 5.99 27.02 o 14 5 1 106.70 119.61 41.78 o 15 5 1 1.64 -16.18 37.81 o -15 6 1 0.44 2.67 35.41 o -14 6 1 63.54 41.41 32.54 o -13 6 1 9.13 26.37 24.91 o -12 6 1 65.98 82.51 25.89 o -11 6 1 196.08 188.27 24.86 o -10 6 1 48.62 76.04 17.99 o -9 6 1 10.54 -12.43 12.43 o -8 6 1 2923.57 2888.02 42.88 o -7 6 1 195.57 212.39 13.69 o -6 6 1 270.91 302.75 15.30 o -5 6 1 1151.23 1176.22 22.71 o -4 6 1 1478.53 1403.58 24.33 o -3 6 1 1446.86 1801.33 23.37 o -2 6 1 1035.60 1231.73 18.93 o -1 6 1 154.16 204.69 7.87 o 0 6 1 2549.59 2576.56 36.33 o 1 6 1 116.21 126.29 9.04 o 2 6 1 593.85 521.35 16.38 o 3 6 1 67.82 87.19 7.91 o 4 6 1 2662.49 2605.79 38.11 o 5 6 1 30.59 50.03 9.30 o 6 6 1 2122.56 2102.58 35.35 o 7 6 1 38.71 51.18 9.65 o 8 6 1 3325.82 3157.86 51.78 o 9 6 1 1464.98 1435.88 38.81 o 10 6 1 1866.47 1853.45 51.75 o 11 6 1 9.85 -19.05 19.05 o 12 6 1 233.52 153.44 42.74 o 13 6 1 9.47 -22.39 22.39 o 14 6 1 67.72 59.10 33.80 o 15 6 1 28.84 50.76 42.82 o -15 7 1 27.73 38.60 41.17 o -14 7 1 33.27 5.55 35.91 o -13 7 1 11.69 10.08 24.96 o -12 7 1 431.21 468.93 40.67 o -11 7 1 6.33 16.05 19.74 o -10 7 1 1860.70 1787.95 52.10 o -9 7 1 131.73 114.99 16.91 o -8 7 1 2042.53 2046.49 40.32 o -7 7 1 12.52 3.39 10.15 o -6 7 1 1366.85 1410.81 29.64 o -5 7 1 151.18 181.51 12.04 o -4 7 1 2176.12 2161.27 29.73 o -3 7 1 25.26 33.86 6.50 o -2 7 1 466.69 418.12 12.43 o -1 7 1 1508.78 1535.60 21.59 o 0 7 1 1014.73 1038.45 18.65 o 1 7 1 126.85 124.80 10.75 o 2 7 1 1132.33 1213.69 24.16 o 3 7 1 349.19 389.17 17.23 o 4 7 1 33.19 10.28 7.58 o 5 7 1 42.11 31.51 8.98 o 6 7 1 3.14 -9.57 9.57 o 7 7 1 162.60 174.29 14.48 o 8 7 1 624.46 626.41 29.40 o 9 7 1 75.91 37.92 18.32 o 10 7 1 276.81 331.35 27.98 o 11 7 1 56.97 27.49 25.77 o 12 7 1 504.08 473.86 39.83 o 13 7 1 20.81 5.95 27.25 o 14 7 1 102.29 158.56 39.29 o 15 7 1 0.03 0.00 71.76 o -14 8 1 74.90 47.26 30.22 o -13 8 1 22.33 42.79 30.31 o -12 8 1 33.96 -19.57 23.33 o -11 8 1 357.82 344.40 31.73 o -10 8 1 6.46 17.50 18.14 o -9 8 1 12.19 5.97 16.09 o -8 8 1 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