#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:53:51 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181201 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/80/2228018.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228018_Fobs loop_ _publ_author_name 'Arman, Hadi D.' 'Kaulgud, Trupta' 'Tiekink, Edward R. T.' _publ_section_title ; 2,2'-(Disulfanediyl)dibenzoic acid--2,9-dimethylphenanthroline--tetrahydrofuran (1/2/1) ; _journal_coeditor_code SU2213 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2602 _journal_volume 66 _journal_year 2010 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.637 _cell_angle_gamma 90.000 _cell_length_a 14.0110 _cell_length_b 8.5160 _cell_length_c 17.4030 _exptl_crystal_F_000 836.00 _reflns_d_resolution_high 0.7697 _cod_data_source_file su2213Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' cd0358d in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 183.31 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 -10 0 3.85 2.53 2.86 o 7 -10 0 255.88 280.43 42.54 o 2 -9 0 40.63 26.06 7.83 o 3 -9 0 173.56 135.90 24.18 o 4 -9 0 426.52 433.11 38.33 o 5 -9 0 222.35 202.52 39.91 o 6 -9 0 42.80 28.13 11.51 o 7 -9 0 34.56 47.77 14.24 o 8 -9 0 10.79 17.83 6.18 o 9 -9 0 31.49 46.42 14.15 o 1 -8 0 270.47 191.04 22.86 o 2 -8 0 153.03 110.08 21.78 o 3 -8 0 13.93 17.67 5.43 o 4 -8 0 37.72 31.02 7.93 o 5 -8 0 60.00 48.53 10.92 o 6 -8 0 3.25 7.93 4.54 o 7 -8 0 410.72 452.29 41.65 o 8 -8 0 17.71 22.60 7.01 o 9 -8 0 131.95 132.35 27.60 o 10 -8 0 5.49 5.76 3.22 o 11 -8 0 59.98 84.84 20.07 o 1 -7 0 363.04 376.95 16.55 o 2 -7 0 136.69 119.22 23.56 o 3 -7 0 697.31 707.68 42.14 o 4 -7 0 135.89 123.76 20.50 o 5 -7 0 451.32 522.23 45.50 o 6 -7 0 165.08 170.31 29.51 o 7 -7 0 177.64 200.52 33.19 o 8 -7 0 3.49 6.65 4.70 o 9 -7 0 704.74 983.56 325.23 o 10 -7 0 242.59 249.67 35.50 o 11 -7 0 502.48 614.87 43.33 o 12 -7 0 21.77 38.95 10.07 o 13 -7 0 16.08 18.32 11.12 o 0 -6 0 669.78 639.58 89.12 o 1 -6 0 55.75 32.11 6.51 o 2 -6 0 370.89 333.69 24.71 o 3 -6 0 330.16 470.64 31.88 o 4 -6 0 30.21 29.87 6.74 o 5 -6 0 101.73 163.74 34.21 o 6 -6 0 591.82 766.47 41.65 o 7 -6 0 79.18 124.59 23.69 o 8 -6 0 23.47 23.69 9.64 o 9 -6 0 11.93 13.65 7.50 o 10 -6 0 44.33 56.55 13.36 o 11 -6 0 18.21 7.60 4.67 o 12 -6 0 112.31 165.97 13.95 o 13 -6 0 23.07 6.51 4.05 o 14 -6 0 28.77 28.59 13.19 o 2 -5 0 520.47 612.53 32.57 o 3 -5 0 2136.28 2484.02 60.57 o 4 -5 0 357.43 416.43 25.89 o 5 -5 0 947.86 1080.42 33.19 o 6 -5 0 289.00 290.01 20.00 o 7 -5 0 34.31 32.57 9.51 o 8 -5 0 465.72 517.82 41.85 o 9 -5 0 1277.09 1431.31 61.75 o 10 -5 0 240.49 297.83 43.29 o 11 -5 0 632.28 704.49 50.40 o 12 -5 0 135.18 148.01 20.30 o 13 -5 0 29.15 37.96 14.01 o 14 -5 0 22.58 17.86 9.24 o 15 -5 0 188.44 227.85 45.99 o 0 -4 0 453.23 638.56 18.59 o 1 -4 0 1811.44 1847.05 32.80 o 2 -4 0 1777.43 1681.83 31.65 o 3 -4 0 725.47 684.19 24.25 o 4 -4 0 353.95 297.06 24.43 o 5 -4 0 574.85 597.09 14.96 o 6 -4 0 134.34 148.90 21.52 o 7 -4 0 1487.47 1447.43 32.17 o 8 -4 0 79.64 60.57 13.42 o 9 -4 0 14.68 18.03 7.01 o 10 -4 0 366.14 400.27 43.66 o 11 -4 0 5.73 13.29 8.49 o 12 -4 0 232.83 236.41 48.26 o 13 -4 0 37.93 18.65 10.30 o 14 -4 0 6.47 23.39 10.66 o 15 -4 0 74.81 70.86 15.92 o 1 -3 0 194.13 156.55 7.94 o 2 -3 0 621.23 588.09 20.89 o 3 -3 0 1922.08 1735.16 35.33 o 4 -3 0 2078.33 1973.39 69.97 o 5 -3 0 674.81 677.60 29.61 o 6 -3 0 392.94 471.80 29.61 o 7 -3 0 257.54 252.36 32.21 o 8 -3 0 66.59 86.06 12.57 o 9 -3 0 647.47 740.48 44.18 o 10 -3 0 10.16 9.84 4.87 o 11 -3 0 186.94 179.69 28.39 o 12 -3 0 21.24 23.16 7.73 o 13 -3 0 32.55 45.76 13.78 o 14 -3 0 58.95 76.92 19.71 o 15 -3 0 221.21 260.26 34.94 o 16 -3 0 63.95 115.67 26.91 o 0 -2 0 634.39 1015.01 27.12 o 1 -2 0 713.55 1035.96 14.80 o 2 -2 0 4237.80 4199.75 54.76 o 3 -2 0 2576.80 2560.15 81.54 o 4 -2 0 2752.75 2631.37 115.97 o 5 -2 0 519.55 444.79 29.31 o 6 -2 0 752.82 778.61 27.50 o 7 -2 0 331.01 340.96 19.61 o 8 -2 0 792.27 754.10 24.21 o 9 -2 0 279.72 275.03 37.34 o 10 -2 0 44.51 42.57 10.23 o 11 -2 0 0.62 5.56 4.44 o 12 -2 0 45.80 58.36 13.32 o 13 -2 0 129.47 200.48 43.00 o 14 -2 0 278.54 369.65 33.66 o 15 -2 0 164.10 155.58 26.42 o 16 -2 0 21.13 -0.03 9.05 o 1 -1 0 1213.09 1039.03 18.54 o 2 -1 0 11292.85 10662.50 532.92 o 3 -1 0 462.13 437.05 68.31 o 4 -1 0 203.02 216.34 15.17 o 5 -1 0 17.20 23.56 4.90 o 6 -1 0 858.54 885.76 30.10 o 7 -1 0 601.64 677.84 24.90 o 8 -1 0 64.75 63.95 9.28 o 9 -1 0 64.67 83.17 10.66 o 10 -1 0 1510.47 1504.21 36.06 o 11 -1 0 406.17 429.92 53.49 o 12 -1 0 363.56 372.41 54.02 o 13 -1 0 66.73 75.86 15.96 o 14 -1 0 3.43 11.28 5.49 o 15 -1 0 16.56 20.13 9.80 o 16 -1 0 18.34 7.76 6.18 o 17 -1 0 46.74 57.18 14.84 o 2 0 0 6856.34 6760.75 71.42 o 3 0 0 1921.83 1916.25 48.31 o 4 0 0 4787.28 4761.84 56.39 o 5 0 0 3186.62 3441.37 43.36 o 6 0 0 1819.30 2027.99 35.50 o 7 0 0 20.67 52.47 7.99 o 8 0 0 236.58 277.83 35.30 o 9 0 0 539.25 481.11 44.25 o 10 0 0 285.29 289.60 36.78 o 11 0 0 391.38 445.61 95.11 o 12 0 0 1597.89 1506.48 84.61 o 13 0 0 3.88 2.96 5.56 o 14 0 0 27.22 24.58 12.60 o 15 0 0 24.92 21.58 7.40 o 16 0 0 212.60 247.20 37.90 o 17 0 0 14.59 33.49 12.14 o 1 1 0 1211.06 1045.59 14.02 o 3 1 0 455.54 459.20 28.49 o 4 1 0 201.72 204.63 19.21 o 5 1 0 15.95 27.90 4.31 o 6 1 0 863.26 946.98 32.64 o 7 1 0 605.03 639.97 33.79 o 8 1 0 63.42 44.58 7.70 o 9 1 0 65.64 81.59 12.47 o 10 1 0 1504.66 1529.05 39.54 o 11 1 0 412.51 463.64 55.83 o 12 1 0 358.74 354.41 20.82 o 13 1 0 66.71 59.05 13.65 o 14 1 0 3.41 17.50 7.83 o 15 1 0 15.67 18.75 8.45 o 16 1 0 18.89 16.55 6.38 o 17 1 0 46.36 56.03 13.19 o 0 2 0 645.95 1080.84 40.60 o 1 2 0 715.42 1051.22 39.74 o 2 2 0 4221.94 4164.47 33.87 o 3 2 0 2565.86 2562.49 17.85 o 5 2 0 520.31 432.94 26.71 o 6 2 0 754.28 757.19 30.27 o 7 2 0 329.81 358.23 27.21 o 8 2 0 789.71 753.14 26.45 o 9 2 0 276.03 247.99 30.69 o 10 2 0 43.77 69.94 14.80 o 11 2 0 0.51 14.18 7.04 o 12 2 0 51.42 57.34 11.55 o 13 2 0 131.49 181.96 36.94 o 14 2 0 275.56 279.37 43.69 o 15 2 0 158.06 142.22 29.08 o 16 2 0 20.46 30.95 8.83 o 1 3 0 195.55 182.82 10.06 o 2 3 0 623.14 509.47 11.63 o 3 3 0 1904.11 1704.05 28.32 o 4 3 0 2067.65 1947.92 19.07 o 5 3 0 653.65 695.23 16.96 o 6 3 0 394.34 413.89 21.25 o 7 3 0 255.01 236.01 18.69 o 8 3 0 70.42 84.68 11.88 o 9 3 0 654.98 756.43 48.23 o 10 3 0 12.31 12.83 6.65 o 11 3 0 197.11 171.89 26.15 o 12 3 0 18.97 19.37 7.88 o 13 3 0 31.60 48.37 13.23 o 14 3 0 58.99 83.35 14.10 o 15 3 0 220.88 233.68 25.57 o 16 3 0 66.06 90.84 15.00 o 0 4 0 437.20 632.34 10.49 o 1 4 0 1818.90 1988.25 33.34 o 2 4 0 1789.16 1825.53 55.15 o 3 4 0 729.12 677.03 18.75 o 4 4 0 355.16 331.70 20.73 o 5 4 0 588.18 617.29 17.72 o 6 4 0 125.38 127.51 9.10 o 7 4 0 1496.29 1553.84 34.31 o 8 4 0 77.28 71.00 10.58 o 9 4 0 15.55 8.13 3.06 o 10 4 0 367.25 374.51 24.58 o 11 4 0 6.43 14.52 4.22 o 12 4 0 228.19 219.73 45.48 o 13 4 0 38.99 26.04 7.16 o 14 4 0 5.41 6.26 4.77 o 15 4 0 75.74 85.06 26.45 o 1 5 0 449.95 450.31 20.98 o 2 5 0 505.39 545.12 42.02 o 3 5 0 2171.37 2603.65 137.84 o 4 5 0 368.32 416.35 20.67 o 6 5 0 289.68 293.88 40.74 o 7 5 0 33.80 25.90 5.95 o 8 5 0 469.83 473.85 60.42 o 9 5 0 1294.30 1352.45 62.56 o 10 5 0 223.86 214.79 22.75 o 11 5 0 631.15 659.04 37.90 o 12 5 0 134.63 122.37 20.35 o 13 5 0 30.54 33.20 7.25 o 14 5 0 23.35 15.49 3.82 o 15 5 0 190.23 171.77 23.57 o 0 6 0 675.26 692.50 21.61 o 1 6 0 55.31 46.54 6.44 o 2 6 0 370.92 328.36 15.67 o 3 6 0 329.90 457.13 25.40 o 4 6 0 30.54 27.96 9.67 o 5 6 0 100.10 162.95 20.71 o 6 6 0 594.35 671.05 65.40 o 7 6 0 78.32 40.00 8.42 o 8 6 0 24.01 17.46 8.57 o 9 6 0 12.18 3.81 4.39 o 10 6 0 43.60 33.53 5.23 o 11 6 0 18.25 13.31 9.80 o 12 6 0 114.07 118.43 24.97 o 13 6 0 22.55 14.64 7.17 o 14 6 0 28.31 13.72 6.02 o 1 7 0 362.68 404.49 32.14 o 2 7 0 142.95 150.78 18.54 o 3 7 0 686.94 726.50 29.65 o 4 7 0 136.18 137.85 12.84 o 5 7 0 468.18 540.13 28.15 o 6 7 0 168.91 135.01 16.05 o 7 7 0 179.50 205.06 26.19 o 8 7 0 2.50 -0.99 7.86 o 9 7 0 703.77 795.12 57.24 o 10 7 0 256.94 247.07 35.37 o 11 7 0 500.53 566.35 69.09 o 12 7 0 19.59 6.74 4.80 o 13 7 0 15.41 26.32 13.82 o 0 8 0 127.84 200.02 35.56 o 1 8 0 265.08 259.25 23.58 o 2 8 0 150.50 150.51 15.17 o 3 8 0 14.17 13.57 4.88 o 4 8 0 37.22 50.33 7.04 o 5 8 0 61.67 54.46 7.14 o 6 8 0 3.86 11.56 3.32 o 7 8 0 413.62 520.06 35.79 o 8 8 0 17.19 34.87 10.43 o 9 8 0 129.62 134.62 25.04 o 10 8 0 5.84 5.10 8.72 o 11 8 0 60.97 74.91 19.74 o 1 9 0 252.71 299.98 29.48 o 2 9 0 42.65 38.56 13.97 o 3 9 0 175.07 174.92 18.97 o 4 9 0 422.60 517.35 53.14 o 5 9 0 223.45 256.43 17.10 o 6 9 0 43.34 49.71 8.60 o 7 9 0 34.46 32.64 7.72 o 8 9 0 10.87 14.27 3.51 o 9 9 0 33.44 27.87 11.91 o 0 10 0 313.24 371.65 52.47 o 1 10 0 16.53 26.18 8.08 o 2 10 0 28.61 31.01 6.98 o 3 10 0 55.20 55.46 10.85 o 4 10 0 44.71 45.11 6.80 o 5 10 0 205.01 192.36 22.22 o 6 10 0 4.00 9.51 4.56 o 7 10 0 253.44 262.17 41.27 o 1 11 0 8.54 10.88 4.56 o -7 -10 1 7.57 11.71 5.30 o -6 -10 1 14.72 10.72 4.28 o 5 -10 1 23.88 24.77 8.55 o 6 -10 1 226.51 177.55 38.69 o 7 -10 1 97.56 82.94 20.53 o -10 -9 1 48.34 35.63 11.61 o -9 -9 1 54.99 58.53 13.46 o -8 -9 1 8.23 5.00 4.51 o -7 -9 1 82.46 67.74 16.12 o -6 -9 1 83.19 52.54 16.05 o -5 -9 1 165.35 126.82 27.34 o -4 -9 1 30.53 34.28 7.90 o -3 -9 1 58.15 39.87 11.68 o -2 -9 1 5.20 5.23 2.14 o 2 -9 1 31.44 22.90 6.68 o 3 -9 1 9.29 13.42 5.07 o 4 -9 1 55.94 45.56 11.19 o 5 -9 1 59.26 59.48 13.85 o 6 -9 1 52.10 60.11 15.66 o 7 -9 1 117.15 103.00 20.33 o 8 -9 1 24.49 14.15 8.82 o 9 -9 1 49.59 47.83 14.48 o -12 -8 1 200.56 195.94 35.33 o -11 -8 1 7.57 -1.15 5.82 o -10 -8 1 277.22 299.64 44.15 o -9 -8 1 90.03 99.12 20.89 o -8 -8 1 62.33 45.37 12.14 o -7 -8 1 44.41 55.76 14.31 o -6 -8 1 108.17 144.85 31.71 o -5 -8 1 214.06 223.02 45.17 o -4 -8 1 213.72 205.42 26.98 o -3 -8 1 305.41 357.97 28.00 o -2 -8 1 417.10 447.94 26.75 o -1 -8 1 67.01 49.12 10.26 o 1 -8 1 345.15 334.81 22.44 o 2 -8 1 85.34 73.10 14.61 o 3 -8 1 296.20 257.82 24.44 o 4 -8 1 220.73 248.28 39.87 o 5 -8 1 121.19 100.87 21.58 o 6 -8 1 26.72 29.74 9.74 o 7 -8 1 64.81 53.07 15.36 o 8 -8 1 523.38 637.77 47.01 o 9 -8 1 31.01 35.10 11.42 o 10 -8 1 177.42 166.70 30.56 o 11 -8 1 16.91 17.73 9.80 o -13 -7 1 42.05 76.32 16.09 o -12 -7 1 24.96 18.26 8.39 o -11 -7 1 160.99 202.56 31.45 o -10 -7 1 391.08 490.94 35.69 o -9 -7 1 127.94 157.12 30.30 o -8 -7 1 58.98 66.45 15.63 o -7 -7 1 162.96 191.67 26.88 o -6 -7 1 27.31 56.12 11.25 o -5 -7 1 33.70 60.70 18.19 o -4 -7 1 326.59 376.46 25.63 o -3 -7 1 67.86 60.34 12.34 o -2 -7 1 152.07 156.46 26.68 o -1 -7 1 170.11 147.62 24.41 o 0 -7 1 107.62 93.55 9.75 o 1 -7 1 73.69 80.63 15.76 o 2 -7 1 13.48 8.69 4.11 o 3 -7 1 96.01 80.54 14.54 o 4 -7 1 87.24 66.75 11.91 o 5 -7 1 219.99 239.50 23.79 o 6 -7 1 33.92 41.16 11.94 o 7 -7 1 160.72 188.47 36.78 o 8 -7 1 513.76 624.44 46.78 o 9 -7 1 68.95 66.03 18.62 o 10 -7 1 84.26 88.92 21.02 o 11 -7 1 54.70 39.15 11.48 o 12 -7 1 66.85 66.75 15.13 o -14 -6 1 2.00 10.72 7.99 o -13 -6 1 81.99 95.70 18.78 o -12 -6 1 77.92 101.29 22.44 o -11 -6 1 3.88 -2.86 6.28 o -10 -6 1 658.76 815.62 60.04 o -9 -6 1 376.05 456.86 60.04 o -8 -6 1 307.64 314.31 36.65 o -7 -6 1 204.41 182.19 28.92 o -6 -6 1 466.43 441.17 28.92 o -5 -6 1 873.45 802.39 27.80 o -4 -6 1 3243.67 3304.18 56.03 o -3 -6 1 203.34 155.51 14.31 o -2 -6 1 1167.15 1118.48 28.16 o -1 -6 1 1050.53 1104.30 24.90 o 0 -6 1 68.32 57.88 8.29 o 1 -6 1 615.42 713.14 18.78 o 2 -6 1 318.89 377.61 21.32 o 3 -6 1 795.93 961.39 43.46 o 4 -6 1 113.21 143.24 21.05 o 5 -6 1 535.35 591.02 40.70 o 6 -6 1 7.07 6.42 5.95 o 7 -6 1 153.43 134.03 46.39 o 8 -6 1 10.00 7.24 7.57 o 9 -6 1 130.45 163.60 34.81 o 10 -6 1 175.18 193.38 39.25 o 11 -6 1 254.90 311.91 37.96 o 12 -6 1 110.46 129.49 34.35 o 13 -6 1 8.58 -1.28 6.42 o 14 -6 1 74.62 94.85 20.43 o -15 -5 1 2.28 11.71 5.59 o -14 -5 1 9.44 8.39 7.70 o -13 -5 1 18.05 37.01 11.19 o -12 -5 1 0.82 8.26 7.17 o -11 -5 1 80.71 95.83 18.78 o -10 -5 1 65.62 55.30 13.06 o -9 -5 1 94.64 110.64 19.44 o -8 -5 1 594.59 631.02 40.73 o -7 -5 1 599.48 590.84 63.95 o -6 -5 1 599.32 544.95 48.62 o -5 -5 1 393.74 387.97 30.10 o -4 -5 1 367.20 331.58 27.17 o -3 -5 1 162.92 181.90 25.99 o -2 -5 1 428.60 439.88 23.85 o -1 -5 1 125.21 115.68 12.47 o 0 -5 1 134.14 112.73 6.77 o 1 -5 1 61.67 45.00 7.47 o 2 -5 1 298.11 300.40 49.54 o 3 -5 1 457.02 536.74 33.00 o 4 -5 1 374.31 499.33 43.85 o 5 -5 1 598.35 558.19 36.78 o 6 -5 1 41.46 42.10 14.38 o 7 -5 1 132.96 142.98 24.08 o 8 -5 1 224.26 243.48 29.87 o 9 -5 1 788.41 910.82 63.33 o 10 -5 1 309.24 381.16 46.72 o 11 -5 1 79.50 113.47 21.75 o 12 -5 1 51.22 44.97 12.21 o 13 -5 1 46.61 35.27 12.07 o 14 -5 1 1.56 20.36 6.55 o 15 -5 1 23.12 15.00 10.07 o -16 -4 1 55.32 61.55 14.74 o -15 -4 1 31.46 30.10 11.71 o -14 -4 1 22.00 28.13 9.64 o -13 -4 1 175.55 197.49 33.72 o -12 -4 1 197.27 187.82 36.45 o -11 -4 1 345.00 387.05 50.43 o -10 -4 1 271.57 275.59 35.20 o -9 -4 1 169.21 221.90 35.66 o -8 -4 1 327.99 382.08 27.54 o -7 -4 1 282.06 321.71 41.45 o -6 -4 1 453.97 441.89 53.13 o -5 -4 1 181.91 185.05 11.71 o -4 -4 1 3235.42 3564.01 56.65 o -3 -4 1 1008.35 1186.38 36.39 o -2 -4 1 394.51 496.96 17.17 o -1 -4 1 187.19 319.84 7.67 o 0 -4 1 1141.10 849.40 23.03 o 1 -4 1 278.53 193.24 8.66 o 2 -4 1 866.57 793.94 34.84 o 3 -4 1 2133.49 2066.71 85.82 o 4 -4 1 1653.75 1559.36 58.77 o 5 -4 1 259.76 229.74 51.34 o 6 -4 1 188.32 248.78 33.42 o 7 -4 1 8.23 9.15 4.41 o 8 -4 1 253.90 332.93 34.08 o 9 -4 1 756.06 826.31 44.05 o 10 -4 1 117.09 112.74 17.17 o 11 -4 1 294.27 409.16 64.84 o 12 -4 1 217.98 255.95 30.79 o 13 -4 1 70.61 70.83 19.84 o 14 -4 1 138.08 148.67 29.67 o 15 -4 1 22.16 31.06 16.22 o -16 -3 1 32.48 25.50 10.10 o -15 -3 1 24.90 15.36 8.06 o -14 -3 1 168.58 198.44 31.68 o -13 -3 1 447.27 544.86 71.75 o -12 -3 1 42.34 36.48 10.63 o -11 -3 1 4.89 9.18 5.26 o -10 -3 1 57.14 60.01 12.40 o -9 -3 1 251.78 288.95 28.49 o -8 -3 1 1033.92 1188.59 34.31 o -7 -3 1 446.24 486.07 39.71 o -6 -3 1 972.21 972.87 33.46 o -5 -3 1 3352.89 3592.70 38.37 o -4 -3 1 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