#------------------------------------------------------------------------------
#$Date: 2016-04-03 04:53:51 +0300 (Sun, 03 Apr 2016) $
#$Revision: 181201 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/80/2228073.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2228073_Fobs
loop_
_publ_author_name
'Gougeon, Patrick'
'Gall, Philippe'
'Salloum, Diala'
'Potel, Michel'
_publ_section_title
;
 V~1.42~In~1.83~Mo~15~Se~19~
;
_journal_coeditor_code           WM2403
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              i73
_journal_volume                  66
_journal_year                    2010
_space_group_IT_number           176
_symmetry_space_group_name_Hall  '-P 6c'
_symmetry_space_group_name_H-M   'P 63/m'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                120.000
_cell_length_a                   9.7361
_cell_length_b                   9.7361
_cell_length_c                   19.3090
_exptl_crystal_F_000             2796.66
_reflns_d_resolution_high        0.6201
_cod_data_source_file            wm2403Isup2.hkl
_cod_data_source_block           I
#BEGIN Tags that were not found in dictionaries:
_shelx_title
'                                   import in P 63/m'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            1425.63
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'-y, x-y, z'
'-x+y, -x, z'
'x-y, x, z+1/2'
'y, -x+y, z+1/2'
'-x, -y, -z'
'x, y, -z-1/2'
'y, -x+y, -z'
'x-y, x, -z'
'-x+y, -x, -z-1/2'
'-y, x-y, -z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
-1 2 0 45231.71 45264.40 930.09 o
0 2 0 271.89 388.35 40.03 o
-2 3 0 820.69 1197.44 54.46 o
-1 3 0 7249.60 6974.57 142.23 o
0 3 0 462374.28 456513.53 9590.64 o
-3 4 0 71998.86 74028.16 1206.06 o
-2 4 0 156081.56 150038.13 2708.36 o
-1 4 0 1906.49 1725.33 70.45 o
0 4 0 939.85 866.76 94.61 o
-4 5 0 1007.17 707.85 88.45 o
-3 5 0 13176.59 12119.41 302.40 o
-2 5 0 9995.14 9573.39 210.46 o
-1 5 0 49784.58 52943.52 826.25 o
0 5 0 10502.85 10604.55 254.80 o
-5 6 0 213.52 310.31 115.00 o
-4 6 0 27.97 240.95 104.38 o
-3 6 0 130862.84 139949.61 2395.15 o
-2 6 0 6982.89 8327.04 332.12 o
-1 6 0 5014.87 4962.59 243.08 o
0 6 0 1073742.75 1135022.50 19193.97 o
-6 7 0 4338.61 4677.02 200.10 o
-5 7 0 22793.90 24508.45 540.32 o
-4 7 0 748.52 845.82 131.07 o
-3 7 0 4497.53 5036.47 175.74 o
-2 7 0 261754.92 281495.16 4520.15 o
-1 7 0 12207.46 12629.51 352.17 o
0 7 0 1854.84 1708.88 166.65 o
-7 8 0 11592.44 12004.71 483.16 o
-6 8 0 7224.64 7310.09 391.62 o
-5 8 0 10168.13 10488.84 309.94 o
-4 8 0 44240.60 47734.83 1038.80 o
-3 8 0 82.55 313.00 145.98 o
-2 8 0 2010.32 2233.57 148.89 o
-1 8 0 211470.36 231057.75 5433.87 o
0 8 0 233.73 240.48 205.44 o
-8 9 0 74.36 58.63 225.99 o
-7 9 0 393.88 389.78 198.15 o
-6 9 0 1647.14 1487.02 259.58 o
-5 9 0 29053.82 31858.03 533.18 o
-4 9 0 16.42 66.33 167.97 o
-3 9 0 12022.10 12047.99 334.09 o
-2 9 0 7577.71 8954.89 368.76 o
-1 9 0 2789.78 2666.53 290.27 o
0 9 0 4200.57 4427.88 355.15 o
-9 10 0 22711.28 22574.38 690.09 o
-8 10 0 17389.20 18732.84 656.87 o
-7 10 0 119.02 363.24 258.35 o
-6 10 0 52.27 334.29 224.98 o
-5 10 0 47808.76 52004.22 1262.05 o
-4 10 0 4644.64 4244.61 253.48 o
-3 10 0 5853.03 5779.98 304.35 o
-2 10 0 640.36 417.18 286.63 o
-1 10 0 24.52 114.17 245.78 o
0 10 0 5304.23 4906.18 418.61 o
-10 11 0 12504.27 13789.65 499.16 o
-9 11 0 46.43 198.74 307.86 o
-8 11 0 1347.98 851.94 303.97 o
-7 11 0 27071.52 27994.55 612.67 o
-6 11 0 652.87 645.21 286.08 o
-5 11 0 2134.03 2382.08 222.25 o
-4 11 0 6408.58 5987.97 447.93 o
-3 11 0 5098.06 4549.16 424.32 o
-2 11 0 87.88 346.78 302.59 o
-1 11 0 40181.38 41527.32 961.06 o
0 11 0 10.93 68.75 380.10 o
-11 12 0 1633.91 1643.93 415.00 o
-10 12 0 108.53 564.16 385.10 o
-9 12 0 31.10 -80.21 336.94 o
-8 12 0 502.71 277.58 307.28 o
-7 12 0 940.60 698.55 331.31 o
-6 12 0 71487.41 74721.82 2902.03 o
-5 12 0 15.49 203.05 261.06 o
-4 12 0 13952.67 12622.59 711.86 o
-3 12 0 7457.63 7359.79 581.61 o
-2 12 0 68.36 646.63 366.04 o
-1 12 0 513.02 838.41 456.49 o
0 12 0 26800.89 26910.52 820.21 o
-12 13 0 1.84 -627.19 627.19 o
-11 13 0 20103.37 19541.72 772.80 o
-10 13 0 21.30 -349.13 372.09 o
-9 13 0 461.23 269.02 402.22 o
-8 13 0 349453.25 364730.22 9007.97 o
-7 13 0 1392.76 1107.49 345.85 o
-6 13 0 43.41 542.48 352.47 o
-5 13 0 21641.42 20700.60 959.02 o
-4 13 0 184.39 160.18 444.58 o
-3 13 0 75.56 -239.12 464.87 o
-2 13 0 110008.16 113354.77 1876.29 o
-1 13 0 1936.47 1550.12 639.92 o
0 13 0 351.62 497.09 638.86 o
-13 14 0 1113.29 821.83 645.11 o
-12 14 0 10489.92 10245.58 678.28 o
-11 14 0 152.12 -497.53 497.53 o
-10 14 0 10012.29 9337.38 903.41 o
-9 14 0 139.63 568.39 508.81 o
-8 14 0 969.42 -126.85 453.06 o
-7 14 0 7152.48 6604.46 815.45 o
-6 14 0 1229.27 1362.36 571.84 o
-5 14 0 1548.67 1079.61 677.89 o
-4 14 0 41.52 727.21 576.39 o
-3 14 0 478.12 -920.64 920.64 o
-2 14 0 4353.09 3091.81 794.69 o
-1 14 0 98877.82 97556.26 2753.08 o
-11 15 0 327.30 -777.69 777.69 o
-10 15 0 376.57 974.13 855.06 o
-9 15 0 3079.03 3532.04 840.60 o
-8 15 0 43.00 -270.90 719.01 o
-7 15 0 42.64 -755.56 755.56 o
-6 15 0 23119.98 23003.88 940.82 o
-5 15 0 2686.40 2874.92 882.49 o
-4 15 0 1776.67 63.98 991.99 o
0 1 1 78397.90 42446.98 6057.95 o
-1 2 1 491.16 489.21 19.59 o
0 2 1 6959.07 7112.62 125.60 o
-2 3 1 37202.93 38194.89 648.37 o
-1 3 1 39998.81 39154.43 511.71 o
0 3 1 368.15 392.32 39.68 o
-3 4 1 239969.64 240654.03 3246.91 o
-2 4 1 8179.99 8325.98 150.94 o
-1 4 1 7442.84 7258.65 154.83 o
0 4 1 163.04 250.68 44.23 o
-4 5 1 239.34 341.92 65.22 o
-3 5 1 5396.62 5462.10 121.62 o
-2 5 1 98337.83 100355.47 1197.67 o
-1 5 1 79.02 210.42 44.66 o
0 5 1 2902.15 2968.56 97.09 o
-5 6 1 4060.06 4270.80 131.96 o
-4 6 1 705.68 754.67 62.14 o
-3 6 1 312.09 332.00 63.03 o
-2 6 1 28954.69 30469.66 537.01 o
-1 6 1 60414.04 63146.26 752.09 o
0 6 1 52.96 454.51 96.24 o
-6 7 1 3740.09 3800.17 126.08 o
-5 7 1 19.08 146.31 97.29 o
-4 7 1 1158.34 964.17 89.74 o
-3 7 1 3740.91 3763.50 113.98 o
-2 7 1 248.70 313.77 81.01 o
-1 7 1 185642.73 200203.23 2675.34 o
0 7 1 48445.06 50590.61 926.55 o
-7 8 1 2.74 21.16 116.09 o
-6 8 1 18788.99 18854.42 567.50 o
-5 8 1 5169.66 4817.91 171.41 o
-4 8 1 4366.45 4666.79 175.31 o
-3 8 1 8707.99 8540.92 207.09 o
-2 8 1 3325.84 3272.20 112.69 o
-1 8 1 8.32 68.32 128.82 o
0 8 1 110.14 133.75 129.31 o
-8 9 1 4205.63 4353.75 203.65 o
-7 9 1 1868.30 1879.42 164.99 o
-6 9 1 1240.63 1108.90 166.01 o
-5 9 1 106630.09 116161.20 1425.46 o
-4 9 1 218.06 399.86 113.60 o
-3 9 1 681.12 672.03 119.43 o
-2 9 1 20048.97 21011.97 416.60 o
-1 9 1 6599.01 6901.01 236.74 o
0 9 1 178.80 42.88 162.95 o
-9 10 1 86898.32 92157.16 1570.04 o
-8 10 1 2631.63 2317.20 192.40 o
-7 10 1 3512.23 3697.31 201.29 o
-6 10 1 7656.94 7673.99 229.04 o
-5 10 1 15.38 -89.27 144.40 o
-4 10 1 11098.05 11726.82 236.39 o
-3 10 1 30520.64 32354.23 652.43 o
-2 10 1 1475.77 1406.17 189.20 o
-1 10 1 3784.32 3608.22 203.56 o
0 10 1 1049.53 862.28 218.15 o
-10 11 1 29.29 88.86 247.23 o
-9 11 1 7931.76 8055.59 290.97 o
-8 11 1 1505.58 1174.91 203.04 o
-7 11 1 114.50 87.94 189.70 o
-6 11 1 281.06 198.27 193.66 o
-5 11 1 36.80 -102.09 157.72 o
-4 11 1 378.96 700.01 159.12 o
-3 11 1 3106.78 2433.69 273.56 o
-2 11 1 2591.23 2502.38 234.91 o
-1 11 1 168.13 150.83 221.15 o
0 11 1 1691.93 1488.22 257.08 o
-11 12 1 264.08 425.93 277.51 o
-10 12 1 165.69 -94.23 259.18 o
-9 12 1 32.92 -234.71 234.71 o
-8 12 1 2052.82 1560.08 220.02 o
-7 12 1 35436.57 36589.95 814.50 o
-6 12 1 55.09 -11.69 219.77 o
-5 12 1 3685.78 3675.17 209.24 o
-4 12 1 23924.99 24751.64 561.34 o
-3 12 1 146.32 93.39 278.77 o
-2 12 1 2919.30 2463.92 287.28 o
-1 12 1 521.85 244.03 311.97 o
0 12 1 397.94 273.98 355.04 o
-12 13 1 52.33 -354.92 374.69 o
-11 13 1 100.88 -162.52 325.03 o
-10 13 1 337.31 160.98 284.00 o
-9 13 1 32.88 86.27 257.92 o
-8 13 1 80.81 277.56 297.43 o
-7 13 1 37002.04 36135.03 787.53 o
-6 13 1 1127.06 1311.08 255.00 o
-5 13 1 319.37 60.32 345.84 o
-4 13 1 1544.19 2134.75 352.94 o
-3 13 1 371.77 607.35 336.50 o
-2 13 1 192.39 47.70 356.56 o
-1 13 1 35659.69 35241.99 943.53 o
0 13 1 5479.20 4460.93 456.96 o
-13 14 1 315.17 -203.14 449.01 o
-12 14 1 21362.62 19272.27 649.11 o
-11 14 1 1670.53 764.55 371.08 o
-10 14 1 459.37 454.82 337.54 o
-9 14 1 31.67 -241.01 325.39 o
-8 14 1 6903.72 6961.72 507.63 o
-7 14 1 21.78 -411.22 411.22 o
-6 14 1 3377.84 3057.17 471.15 o
-5 14 1 374.83 412.63 428.30 o
-4 14 1 1243.37 1043.50 476.26 o
-3 14 1 427.25 141.77 483.91 o
-2 14 1 21838.62 20303.41 665.75 o
-1 14 1 2.44 -472.27 472.27 o
-11 15 1 2635.41 1034.37 537.56 o
-10 15 1 610.22 978.05 494.05 o
-9 15 1 462.68 57.53 559.06 o
-8 15 1 334.87 622.62 553.98 o
-7 15 1 1493.97 2030.33 536.59 o
-6 15 1 370.54 112.31 507.28 o
-5 15 1 16981.39 15699.04 703.07 o
-4 15 1 5407.65 5184.61 634.24 o
0 1 2 49097.23 45290.61 760.91 o
-1 2 2 2086.35 1653.65 26.65 o
0 2 2 22289.44 21730.44 280.32 o
-2 3 2 60661.59 59571.04 777.61 o
-1 3 2 25113.13 24029.99 326.55 o
0 3 2 3112.81 2646.98 70.17 o
-3 4 2 163771.09 160418.91 2445.48 o
-2 4 2 1156.19 981.99 38.82 o
-1 4 2 5949.34 6384.30 109.46 o
0 4 2 529.98 454.96 49.96 o
-4 5 2 99.77 251.23 53.59 o
-3 5 2 35681.89 35758.79 460.07 o
-2 5 2 109522.63 112678.28 1550.06 o
-1 5 2 2556.42 2182.56 72.57 o
0 5 2 2775.20 2733.73 77.15 o
-5 6 2 15404.91 15613.33 273.63 o
-4 6 2 189.79 212.46 63.89 o
-3 6 2 666.29 646.88 61.93 o
-2 6 2 17498.13 17511.46 341.03 o
-1 6 2 43766.35 45750.93 871.93 o
0 6 2 858.45 811.16 75.73 o
-6 7 2 5307.79 5155.38 150.83 o
-5 7 2 1101.02 825.74 136.08 o
-4 7 2 372.48 414.68 89.21 o
-3 7 2 4410.14 4061.31 126.07 o
-2 7 2 8042.45 8174.68 187.99 o
-1 7 2 176127.05 189159.98 2600.45 o
0 7 2 40275.43 43206.46 761.28 o
-7 8 2 741.61 327.94 133.56 o
-6 8 2 21733.37 21714.12 408.73 o
-5 8 2 25511.90 26776.83 537.75 o
-4 8 2 526.30 474.84 89.77 o
-3 8 2 23416.20 24513.46 392.26 o
-2 8 2 85.65 136.98 84.60 o
-1 8 2 4793.42 4661.20 165.99 o
0 8 2 8461.72 8075.41 264.33 o
-8 9 2 10276.77 10257.38 461.34 o
-7 9 2 887.58 747.52 158.85 o
-6 9 2 0.59 46.18 134.47 o
-5 9 2 98506.20 104354.26 1778.14 o
-4 9 2 514.87 561.70 111.39 o
-3 9 2 44.95 -60.73 107.64 o
-2 9 2 24289.34 24084.47 301.40 o
-1 9 2 6343.44 5991.61 200.80 o
0 9 2 58.57 340.56 180.67 o
-9 10 2 75676.84 78418.31 1531.98 o
-8 10 2 2291.31 2154.44 194.48 o
-7 10 2 2821.68 2673.22 184.04 o
-6 10 2 8605.86 8583.81 241.48 o
-5 10 2 2094.38 2188.26 172.85 o
-4 10 2 3709.39 3797.68 203.26 o
-3 10 2 42824.19 45414.73 577.46 o
-2 10 2 973.14 967.39 190.67 o
-1 10 2 6177.89 6586.56 287.74 o
0 10 2 2267.02 1770.25 220.19 o
-10 11 2 154.63 208.00 236.61 o
-9 11 2 10460.14 10169.08 292.68 o
-8 11 2 7237.85 6903.19 253.96 o
-7 11 2 977.91 737.03 197.32 o
-6 11 2 152.57 364.32 188.99 o
-5 11 2 657.38 501.07 179.75 o
-4 11 2 162.32 51.71 147.84 o
-3 11 2 13757.53 13362.41 305.22 o
-2 11 2 5146.10 5404.55 385.71 o
-1 11 2 1639.54 1870.16 253.89 o
0 11 2 2570.13 2011.72 275.64 o
-11 12 2 282.31 -298.31 298.31 o
-10 12 2 515.50 478.57 259.86 o
-9 12 2 2.25 225.58 225.76 o
-8 12 2 744.62 382.76 222.92 o
-7 12 2 29462.60 29728.11 702.00 o
-6 12 2 20.48 -32.68 204.27 o
-5 12 2 12036.15 11636.96 311.02 o
-4 12 2 14029.46 14266.78 355.18 o
-3 12 2 73.68 146.78 285.60 o
-2 12 2 1566.79 1502.47 269.14 o
-1 12 2 1883.31 1779.48 317.76 o
0 12 2 32.60 34.84 341.43 o
-12 13 2 775.26 366.55 364.66 o
-11 13 2 730.97 668.80 321.28 o
-10 13 2 3623.87 3336.98 319.05 o
-9 13 2 64.80 -257.21 257.21 o
-8 13 2 6810.77 6431.39 331.40 o
-7 13 2 33992.63 31992.66 767.27 o
-6 13 2 58.67 -266.48 293.35 o
-5 13 2 1184.18 747.17 319.67 o
-4 13 2 307.91 -380.91 380.91 o
-3 13 2 306.94 103.42 335.39 o
-2 13 2 2068.67 2759.19 377.76 o
-1 13 2 27222.30 25814.34 602.62 o
0 13 2 1618.30 1577.71 427.39 o
-13 14 2 3.80 535.24 471.36 o
-12 14 2 9566.92 9098.79 481.73 o
-11 14 2 2594.41 2368.51 428.51 o
-10 14 2 70.66 6.22 371.91 o
-9 14 2 22.26 164.64 351.80 o
-8 14 2 3480.66 2909.42 351.01 o
-7 14 2 3.98 -301.64 388.08 o
-6 14 2 3729.01 3948.58 464.55 o
-5 14 2 273.10 370.94 450.78 o
-4 14 2 202.47 -253.44 463.62 o
-3 14 2 24.17 111.71 490.70 o
-2 14 2 16142.05 15281.78 789.72 o
-1 14 2 730.90 1431.34 513.43 o
-11 15 2 8031.25 7631.78 764.05 o
-10 15 2 1516.57 672.41 490.34 o
-9 15 2 15.41 324.05 567.81 o
-8 15 2 4003.42 3837.46 622.24 o
-7 15 2 5253.07 4183.20 592.63 o
-6 15 2 4.58 858.00 519.73 o
-5 15 2 24323.82 21773.24 1328.04 o
-4 15 2 4744.50 5452.96 653.40 o
0 1 3 1736.15 1840.28 68.93 o
-1 2 3 48.76 197.54 22.54 o
0 2 3 742.83 1057.34 50.38 o
-2 3 3 28686.73 27555.48 370.66 o
-1 3 3 14886.30 13355.08 186.89 o
0 3 3 44.45 114.22 25.47 o
-3 4 3 343394.78 336399.81 4377.32 o
-2 4 3 17019.44 16422.70 206.24 o
-1 4 3 21289.74 21601.39 328.30 o
0 4 3 44.57 121.08 42.79 o
-4 5 3 10.04 72.56 58.90 o
-3 5 3 230776.50 232834.97 2686.15 o
-2 5 3 50075.14 49152.87 579.92 o
-1 5 3 252.55 219.05 48.91 o
0 5 3 20726.51 21534.05 275.07 o
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-2 6 3 23456.77 24144.07 435.02 o
-1 6 3 6063.91 6179.86 131.47 o
0 6 3 4.70 114.59 70.78 o
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-4 7 3 37024.89 39129.30 555.20 o
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-2 7 3 3.93 67.20 76.78 o
-1 7 3 922.11 1176.38 105.26 o
0 7 3 56.83 76.84 104.46 o
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-7 10 3 41.20 277.85 166.75 o
-6 10 3 534.54 397.11 181.39 o
-5 10 3 43.58 62.57 143.95 o
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-2 10 3 1672.28 1532.14 235.18 o
-1 10 3 11.77 -116.75 192.28 o
0 10 3 21602.34 21741.52 376.54 o
-10 11 3 195.54 353.04 236.20 o
-9 11 3 33106.18 34217.76 582.00 o
-8 11 3 500.13 717.20 204.36 o
-7 11 3 382.67 305.27 194.67 o
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-4 11 3 12.35 226.14 160.10 o
-3 11 3 120334.69 130244.87 1541.44 o
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-1 11 3 145.04 -260.53 260.53 o
0 11 3 509.43 298.80 268.13 o
-11 12 3 113.28 39.83 294.71 o
-10 12 3 603.82 929.48 266.54 o
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-8 12 3 472.27 170.53 235.66 o
-7 12 3 691.93 585.03 223.40 o
-6 12 3 15.88 -174.71 202.53 o
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