#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/80/2228075.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228075_Fobs loop_ _publ_author_name 'Assani, Abderrazzak' 'Saadi, Mohamed' 'El Ammari, Lahcen' _publ_section_title ; The \g-polymorph of AgZnPO~4~ with an ABW zeolite-type framework topology ; _journal_coeditor_code WM2407 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i74 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.304 _cell_angle_gamma 90.000 _cell_length_a 5.1664 _cell_length_b 10.4183 _cell_length_c 7.3263 _exptl_crystal_F_000 496.00 _reflns_d_resolution_high 0.6196 _[local]_cod_data_source_file wm2407Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' EL_ASSA508v in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 265.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 70534.23 76234.72 2009.31 o 4 0 0 1746.75 1793.07 41.01 o 6 0 0 1590.86 1608.15 49.09 o 8 0 0 2495.54 2585.04 91.18 o 1 1 0 1542.62 1582.33 21.96 o 2 1 0 7432.35 7186.63 90.73 o 3 1 0 8172.08 8440.32 222.32 o 4 1 0 12111.83 12290.51 175.25 o 5 1 0 4811.17 4798.43 81.76 o 6 1 0 3810.83 3839.86 76.06 o 7 1 0 746.39 737.53 19.64 o 8 1 0 149.79 141.22 8.72 o 0 2 0 2.28 -2.12 2.12 o 1 2 0 32658.55 36867.22 536.51 o 2 2 0 14.42 21.14 1.85 o 3 2 0 3795.94 3687.16 53.52 o 4 2 0 97.67 98.03 2.65 o 5 2 0 1.00 0.47 1.29 o 6 2 0 86.02 77.01 3.47 o 7 2 0 375.95 379.16 12.61 o 8 2 0 23.85 28.99 5.32 o 1 3 0 2598.42 2616.84 34.44 o 2 3 0 6714.45 6803.18 92.40 o 3 3 0 11056.00 11558.40 147.18 o 4 3 0 10464.56 10695.26 142.86 o 5 3 0 5719.32 5692.57 88.64 o 6 3 0 3602.96 3582.32 57.29 o 7 3 0 592.18 593.95 16.98 o 8 3 0 225.31 218.32 10.53 o 0 4 0 67503.77 64511.78 2780.43 o 1 4 0 349.47 461.12 6.12 o 2 4 0 22076.91 23079.02 265.80 o 3 4 0 208.52 208.90 3.63 o 4 4 0 363.78 370.43 6.70 o 5 4 0 402.97 408.47 11.79 o 6 4 0 1002.65 1011.55 18.58 o 7 4 0 353.21 344.73 18.87 o 8 4 0 1466.80 1490.75 35.35 o 1 5 0 15.12 26.45 1.30 o 2 5 0 2161.05 2140.35 25.79 o 3 5 0 123.57 126.03 2.75 o 4 5 0 4017.27 4010.92 52.10 o 5 5 0 411.46 415.44 9.16 o 6 5 0 1210.41 1189.26 21.54 o 7 5 0 173.72 166.15 8.42 o 0 6 0 448.09 490.42 11.69 o 1 6 0 5461.61 5384.06 63.90 o 2 6 0 82.34 93.36 1.98 o 3 6 0 424.56 424.75 8.44 o 4 6 0 57.10 53.11 2.51 o 5 6 0 5.48 8.76 2.75 o 6 6 0 107.50 107.06 4.85 o 7 6 0 78.68 84.12 7.65 o 1 7 0 491.89 492.44 7.56 o 2 7 0 1435.89 1440.85 16.66 o 3 7 0 2530.12 2530.36 29.60 o 4 7 0 2951.29 2914.17 42.20 o 5 7 0 1516.25 1562.34 27.30 o 6 7 0 1265.59 1253.49 25.11 o 7 7 0 102.63 108.92 8.41 o 0 8 0 3291.11 3427.21 69.01 o 1 8 0 259.06 253.86 5.05 o 2 8 0 1056.53 1104.08 14.58 o 3 8 0 1.79 1.97 1.14 o 4 8 0 13.45 18.59 2.22 o 5 8 0 227.63 230.81 7.63 o 6 8 0 38.33 40.10 4.23 o 7 8 0 315.28 304.68 13.44 o 1 9 0 271.89 282.57 6.57 o 2 9 0 7.04 12.23 2.67 o 3 9 0 546.25 555.08 10.16 o 4 9 0 49.70 55.54 5.41 o 5 9 0 64.41 71.80 9.44 o 6 9 0 9.31 10.15 4.90 o 7 9 0 5.51 11.01 5.26 o 0 10 0 436.27 451.62 21.99 o 1 10 0 348.52 342.05 8.23 o 2 10 0 276.86 269.97 6.63 o 3 10 0 40.54 38.58 3.24 o 4 10 0 62.99 70.55 11.86 o 5 10 0 42.56 46.58 7.70 o 6 10 0 2.25 0.70 9.60 o 1 11 0 10.25 9.30 2.41 o 2 11 0 134.91 144.37 5.12 o 3 11 0 13.11 16.43 3.09 o 4 11 0 459.37 458.83 13.92 o 5 11 0 6.51 34.69 16.35 o 6 11 0 274.08 285.18 31.12 o 0 12 0 350.11 345.85 14.21 o 1 12 0 35.26 39.42 3.69 o 2 12 0 215.53 200.79 8.77 o 3 12 0 70.07 73.98 5.09 o 4 12 0 0.13 5.60 3.57 o 5 12 0 117.67 109.88 11.08 o 1 13 0 72.51 75.09 5.31 o 2 13 0 676.81 685.50 19.24 o 3 13 0 175.73 177.34 8.96 o 4 13 0 903.90 899.39 27.02 o 5 13 0 31.81 32.77 10.68 o 0 14 0 3007.22 2999.72 90.78 o 1 14 0 150.53 142.25 6.51 o 2 14 0 1669.37 1681.85 39.31 o 3 14 0 54.16 51.69 6.14 o 4 14 0 187.54 192.28 11.55 o 1 15 0 131.91 132.76 9.50 o 2 15 0 3.67 9.92 4.44 o 3 15 0 573.04 552.19 17.71 o 0 16 0 1313.35 1214.72 79.89 o 1 16 0 322.53 340.84 15.35 o 2 16 0 773.94 734.67 25.16 o -7 0 1 1413.92 1391.85 45.23 o -5 0 1 396.96 355.16 10.94 o -3 0 1 892.36 1009.76 42.34 o -1 0 1 4000.31 4189.67 111.91 o 1 0 1 7641.73 8318.37 238.39 o 3 0 1 3511.75 3444.85 77.88 o 5 0 1 242.50 249.40 9.80 o 7 0 1 23.20 14.98 10.57 o -8 1 1 3.16 -3.54 3.54 o -7 1 1 24.40 22.43 4.18 o -6 1 1 18.80 27.15 1.86 o -5 1 1 122.48 117.85 5.49 o -4 1 1 27.08 21.07 1.73 o -3 1 1 843.55 803.05 13.74 o -2 1 1 1782.00 1934.40 28.89 o -1 1 1 1480.40 1507.70 29.06 o 0 1 1 2069.13 2153.54 42.57 o 1 1 1 13.09 15.64 1.39 o 2 1 1 2231.97 2183.81 30.67 o 3 1 1 18.99 16.86 0.93 o 4 1 1 2393.60 2313.60 38.28 o 5 1 1 0.50 1.03 1.74 o 6 1 1 512.19 491.13 14.79 o 7 1 1 5.94 6.51 3.44 o 8 1 1 0.94 2.53 3.98 o -8 2 1 6.62 0.24 3.62 o -7 2 1 105.40 97.51 7.35 o -6 2 1 37.06 39.32 2.75 o -5 2 1 880.35 878.24 15.90 o -4 2 1 135.65 157.36 4.31 o -3 2 1 1865.27 1840.36 28.76 o -2 2 1 3276.80 3471.20 49.52 o -1 2 1 388.66 377.88 6.37 o 0 2 1 7549.12 8293.63 220.29 o 1 2 1 1498.99 1526.63 25.04 o 2 2 1 7.98 4.44 0.84 o 3 2 1 3071.19 3104.44 43.83 o 4 2 1 334.20 311.89 5.78 o 5 2 1 1216.38 1218.45 22.21 o 6 2 1 304.74 299.46 9.18 o 7 2 1 129.40 120.70 7.31 o 8 2 1 377.30 381.21 18.48 o -8 3 1 295.71 281.34 11.76 o -7 3 1 128.39 146.88 7.87 o -6 3 1 377.03 354.15 9.19 o -5 3 1 178.87 176.19 4.99 o -4 3 1 225.82 220.94 4.92 o -3 3 1 6217.21 6326.26 84.93 o -2 3 1 4.20 7.67 1.15 o -1 3 1 18400.28 18982.93 234.21 o 0 3 1 1819.69 1935.31 34.49 o 1 3 1 8095.54 8175.24 110.59 o 2 3 1 578.53 611.51 9.74 o 3 3 1 1198.36 1209.52 16.92 o 4 3 1 548.10 529.81 8.60 o 5 3 1 16.61 21.74 2.11 o 6 3 1 800.31 762.03 17.37 o 7 3 1 383.54 377.25 12.84 o 8 3 1 225.22 242.04 13.65 o -8 4 1 10.05 16.22 4.61 o -7 4 1 1250.54 1201.41 28.57 o -6 4 1 652.18 631.06 12.98 o -5 4 1 1130.03 1103.13 18.03 o -4 4 1 2978.02 3020.10 41.99 o -3 4 1 231.12 223.27 4.47 o -2 4 1 3233.53 3162.34 39.14 o -1 4 1 79.30 92.99 3.16 o 0 4 1 32.83 15.84 1.02 o 1 4 1 845.07 821.57 10.39 o 2 4 1 2915.80 2990.85 39.49 o 3 4 1 1931.92 1867.66 25.43 o 4 4 1 4533.18 4496.55 62.63 o 5 4 1 284.19 293.96 6.51 o 6 4 1 2244.50 2174.66 37.05 o 7 4 1 18.06 21.17 4.18 o 8 4 1 471.62 474.61 15.91 o -7 5 1 130.46 126.40 7.46 o -6 5 1 1473.06 1501.55 26.50 o -5 5 1 20.49 23.82 1.97 o -4 5 1 271.32 297.17 7.14 o -3 5 1 71.82 81.41 2.36 o -2 5 1 4322.20 4387.65 51.85 o -1 5 1 1025.24 1010.48 13.62 o 0 5 1 16589.19 16008.12 281.73 o 1 5 1 2422.29 2522.45 31.94 o 2 5 1 13648.87 14206.75 182.63 o 3 5 1 404.05 397.28 7.05 o 4 5 1 4172.86 4126.46 57.92 o 5 5 1 29.39 31.89 2.43 o 6 5 1 78.17 78.26 3.42 o 7 5 1 92.97 96.74 6.87 o -7 6 1 843.20 837.82 25.24 o -6 6 1 401.90 396.70 10.60 o -5 6 1 5289.85 5347.22 73.20 o -4 6 1 1183.49 1213.77 17.31 o -3 6 1 10373.92 10557.92 117.43 o -2 6 1 3748.05 3756.18 42.71 o -1 6 1 4224.01 4263.03 51.15 o 0 6 1 3359.46 3464.36 43.56 o 1 6 1 1316.27 1305.58 17.56 o 2 6 1 7.34 9.07 1.35 o 3 6 1 7870.23 7960.74 103.44 o 4 6 1 687.77 682.99 11.64 o 5 6 1 4067.96 4135.84 66.56 o 6 6 1 448.81 440.09 10.01 o 7 6 1 454.23 438.58 16.41 o -7 7 1 586.74 648.31 21.23 o -6 7 1 297.23 298.93 9.33 o -5 7 1 42.82 39.42 3.03 o -4 7 1 91.47 92.47 3.34 o -3 7 1 7005.27 7182.32 84.43 o -2 7 1 207.02 210.97 3.68 o -1 7 1 21930.15 21740.91 302.45 o 0 7 1 2519.10 2549.15 32.65 o 1 7 1 15441.03 15537.16 202.94 o 2 7 1 1883.19 1915.84 24.97 o 3 7 1 3159.52 3200.95 40.70 o 4 7 1 42.54 43.19 2.52 o 5 7 1 7.58 13.82 2.28 o 6 7 1 105.21 115.23 5.30 o 7 7 1 782.46 771.51 23.85 o -7 8 1 491.43 480.37 17.93 o -6 8 1 1172.59 1155.38 27.66 o -5 8 1 1381.15 1404.77 27.47 o -4 8 1 5454.56 5423.34 74.83 o -3 8 1 1862.32 1867.47 26.34 o -2 8 1 8142.67 8049.83 96.99 o -1 8 1 1077.91 1050.04 13.87 o 0 8 1 2125.10 2128.00 27.73 o 1 8 1 277.10 303.71 5.76 o 2 8 1 758.28 794.75 12.20 o 3 8 1 2282.79 2337.99 30.50 o 4 8 1 3857.36 3938.65 56.31 o 5 8 1 877.21 908.91 15.68 o 6 8 1 2632.31 2747.48 55.91 o 7 8 1 70.04 76.30 7.56 o -7 9 1 67.99 64.19 7.43 o -6 9 1 2020.34 2033.83 53.10 o -5 9 1 2.27 2.97 3.58 o -4 9 1 328.17 327.31 8.21 o -3 9 1 199.53 197.04 5.11 o -2 9 1 3410.23 3410.51 46.20 o -1 9 1 916.79 912.48 14.92 o 0 9 1 13467.28 13393.63 198.01 o 1 9 1 1250.28 1219.10 20.77 o 2 9 1 10868.46 10960.47 166.27 o 3 9 1 200.75 189.09 5.20 o 4 9 1 2412.43 2401.42 41.99 o 5 9 1 10.83 10.82 2.84 o 6 9 1 22.23 32.74 6.18 o 7 9 1 25.76 20.61 10.54 o -6 10 1 398.53 404.47 38.45 o -5 10 1 3923.61 3883.89 91.14 o -4 10 1 911.89 907.11 22.56 o -3 10 1 5399.90 5395.01 88.04 o -2 10 1 1032.24 1071.29 18.52 o -1 10 1 1347.42 1307.22 20.75 o 0 10 1 62.64 70.68 5.78 o 1 10 1 968.12 960.55 18.98 o 2 10 1 1094.09 1084.63 20.95 o 3 10 1 4381.65 4281.25 72.60 o 4 10 1 1793.90 1854.17 42.64 o 5 10 1 2452.34 2464.30 55.18 o 6 10 1 690.20 707.56 28.82 o -6 11 1 2.41 4.53 6.30 o -5 11 1 2.43 3.09 4.16 o -4 11 1 2.20 1.15 3.13 o -3 11 1 2836.52 2873.65 54.24 o -2 11 1 6.39 11.54 2.35 o -1 11 1 9137.98 8900.30 143.72 o 0 11 1 279.68 277.03 7.78 o 1 11 1 7025.70 6980.90 116.92 o 2 11 1 585.90 557.79 14.37 o 3 11 1 1444.75 1423.29 27.03 o 4 11 1 302.45 285.82 18.76 o 5 11 1 33.43 36.67 7.73 o 6 11 1 76.85 63.74 9.63 o -5 12 1 606.64 579.65 20.03 o -4 12 1 1535.89 1451.01 34.15 o -3 12 1 1292.48 1337.49 35.34 o -2 12 1 2493.17 2452.60 42.63 o -1 12 1 671.16 658.22 15.52 o 0 12 1 809.44 799.34 17.84 o 1 12 1 184.55 191.56 6.64 o 2 12 1 148.91 144.51 6.90 o 3 12 1 1731.16 1744.02 39.88 o 4 12 1 1289.47 1279.79 34.95 o 5 12 1 1022.59 1077.23 39.20 o -5 13 1 77.47 94.43 8.37 o -4 13 1 57.78 60.46 11.13 o -3 13 1 148.64 152.47 7.29 o -2 13 1 1194.11 1229.01 26.13 o -1 13 1 119.68 112.58 5.68 o 0 13 1 3827.18 3923.34 68.13 o 1 13 1 31.03 29.72 4.70 o 2 13 1 2872.51 2907.82 62.78 o 3 13 1 12.18 25.77 4.81 o 4 13 1 511.85 536.77 23.71 o 5 13 1 34.16 36.05 13.92 o -4 14 1 498.89 502.71 19.19 o -3 14 1 362.74 381.89 13.95 o -2 14 1 368.45 396.06 13.62 o -1 14 1 7.52 12.42 3.67 o 0 14 1 0.97 3.63 3.40 o 1 14 1 758.02 759.18 17.94 o 2 14 1 669.37 705.43 20.10 o 3 14 1 1286.82 1277.69 31.86 o 4 14 1 870.29 867.84 33.72 o -3 15 1 313.14 297.87 13.77 o -2 15 1 55.30 57.58 5.96 o -1 15 1 1352.21 1364.83 32.81 o 0 15 1 30.92 36.63 4.98 o 1 15 1 1168.52 1191.21 35.52 o 2 15 1 27.30 20.41 4.94 o 3 15 1 282.51 287.39 12.22 o -2 16 1 244.80 230.31 12.78 o -1 16 1 491.37 510.01 16.23 o 0 16 1 171.41 154.41 8.51 o 1 16 1 12.96 20.49 5.84 o 2 16 1 1.72 3.32 4.39 o -8 0 2 1330.83 1389.04 47.18 o -6 0 2 1563.59 1629.77 39.81 o -4 0 2 48.81 33.21 2.58 o -2 0 2 9599.33 9741.20 185.54 o 0 0 2 38999.53 37242.67 1679.65 o 2 0 2 33165.69 34393.06 968.70 o 4 0 2 2568.60 2439.80 66.39 o 6 0 2 505.44 513.02 17.02 o 8 0 2 806.97 779.08 31.12 o -8 1 2 110.30 87.34 7.17 o -7 1 2 299.11 262.69 12.00 o -6 1 2 1412.05 1361.99 24.07 o -5 1 2 5465.47 5426.39 84.93 o -4 1 2 7580.99 7735.67 104.45 o -3 1 2 22036.33 22730.48 324.83 o -2 1 2 13485.25 14069.33 188.64 o -1 1 2 17106.12 17523.79 266.82 o 0 1 2 1572.18 1548.77 27.67 o 1 1 2 385.13 443.31 5.96 o 2 1 2 1210.57 1111.03 15.58 o 3 1 2 8075.15 8060.79 128.24 o 4 1 2 2493.13 2455.18 40.78 o 5 1 2 7152.07 7031.67 112.37 o 6 1 2 1576.38 1537.46 28.24 o 7 1 2 2402.44 2411.82 51.37 o 8 1 2 351.25 323.76 12.97 o -8 2 2 20.76 19.44 4.73 o -7 2 2 4509.21 4626.21 81.78 o -6 2 2 92.56 89.71 4.03 o -5 2 2 2154.88 2171.10 35.84 o -4 2 2 16.80 16.10 1.46 o -3 2 2 1840.36 1889.28 26.62 o -2 2 2 560.52 575.78 9.52 o -1 2 2 26561.70 25536.85 408.44 o 0 2 2 2796.22 2891.92 43.20 o 1 2 2 57482.67 54937.15 694.26 o 2 2 2 1317.07 1359.88 19.77 o 3 2 2 22671.10 22951.45 295.01 o 4 2 2 47.27 50.38 3.25 o 5 2 2 525.67 534.56 11.63 o 6 2 2 68.89 67.57 4.41 o 7 2 2 867.19 857.34 20.25 o 8 2 2 99.83 115.73 13.47 o -8 3 2 195.81 169.66 9.39 o -7 3 2 116.68 113.83 5.78 o -6 3 2 724.97 693.68 13.89 o -5 3 2 3882.32 3893.65 57.69 o -4 3 2 2936.12 2976.40 39.21 o -3 3 2 16219.55 16484.67 207.89 o -2 3 2 4960.28 5143.74 63.52 o -1 3 2 9711.23 9676.49 139.22 o 0 3 2 151.13 139.76 3.87 o 1 3 2 1883.34 2033.93 27.47 o 2 3 2 952.54 902.25 13.53 o 3 3 2 10903.22 11061.13 142.58 o 4 3 2 907.99 866.11 13.47 o 5 3 2 7669.01 7595.26 121.29 o 6 3 2 645.07 608.09 14.92 o 7 3 2 2093.82 2083.63 41.26 o 8 3 2 223.02 231.45 11.21 o -7 4 2 13.15 16.19 3.69 o -6 4 2 494.41 528.80 12.60 o -5 4 2 13.08 14.37 2.11 o -4 4 2 359.71 344.38 6.21 o -3 4 2 0.09 6.24 2.99 o -2 4 2 7242.76 7402.28 86.94 o -1 4 2 7.98 9.18 0.96 o 0 4 2 22401.21 22343.06 355.64 o 1 4 2 12.97 19.11 1.12 o 2 4 2 18992.06 19416.60 236.54 o 3 4 2 14.44 20.33 1.86 o 4 4 2 1983.06 1951.32 27.04 o 5 4 2 8.57 14.38 1.50 o 6 4 2 125.31 132.92 6.36 o 7 4 2 3.92 2.13 3.19 o -7 5 2 355.84 333.51 17.44 o -6 5 2 629.18 656.18 14.32 o -5 5 2 2719.13 2733.57 41.57 o -4 5 2 4026.01 4044.46 52.87 o -3 5 2 8176.37 8271.75 105.24 o -2 5 2 6434.11 6475.30 84.46 o -1 5 2 5159.92 5154.94 66.47 o 0 5 2 558.56 531.37 8.25 o 1 5 2 4.73 9.67 0.97 o 2 5 2 1097.72 1075.17 13.75 o 3 5 2 1515.09 1516.70 21.27 o 4 5 2 1994.50 1956.12 28.89 o 5 5 2 2171.91 2119.22 31.50 o 6 5 2 1143.05 1108.60 23.74 o 7 5 2 1225.33 1225.37 29.99 o -7 6 2 1067.11 1112.51 27.18 o -6 6 2 694.15 694.76 14.42 o -5 6 2 221.64 244.02 6.81 o -4 6 2 586.30 583.09 14.96 o -3 6 2 1366.26 1380.70 19.36 o -2 6 2 83.72 79.57 3.32 o -1 6 2 9641.93 9460.48 123.77 o 0 6 2 1982.19 1998.88 27.39 o 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