#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:53:51 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181201 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/80/2228099.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228099_Fobs loop_ _publ_author_name 'Tan, Kong Wai' 'Maah, M. Jamil' 'Ng, Seik Weng' _publ_section_title ; 5-Ethyl-5-methyl-4-phenyl-5H-1,2,4-triazol-3(4H)-thione ; _journal_coeditor_code XU5008 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2224 _journal_volume 66 _journal_year 2010 _space_group_IT_number 114 _symmetry_space_group_name_Hall 'P -4 2n' _symmetry_space_group_name_H-M 'P -4 21 c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 17.9621 _cell_length_b 17.9621 _cell_length_c 6.9992 _exptl_crystal_F_000 928.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file xu5008Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P-421c 837 Friedel pairs merged' _shelx_refln_list_code 4 _shelx_f_calc_maximum 209.63 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'y, -x, -z' '-y, x, -z' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-y+1/2, -x+1/2, z+1/2' 'y+1/2, x+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 537.11 236.82 10.56 o 1 2 0 1302.11 1470.30 36.60 o 2 2 0 31387.66 30439.41 1015.40 o 1 3 0 2649.61 2563.65 62.89 o 2 3 0 5573.76 6156.17 162.61 o 3 3 0 12527.95 16003.26 536.56 o 0 4 0 994.82 1051.16 51.14 o 1 4 0 14607.88 13253.24 314.45 o 2 4 0 2218.49 1490.11 39.38 o 3 4 0 136.32 155.99 11.45 o 4 4 0 19706.69 19365.55 649.55 o 1 5 0 2272.63 2155.39 51.11 o 2 5 0 1807.67 1240.83 34.21 o 3 5 0 25.00 133.62 9.49 o 4 5 0 66.02 62.46 9.84 o 5 5 0 667.22 531.84 27.38 o 0 6 0 6885.66 6192.96 212.16 o 1 6 0 4879.19 4488.55 110.23 o 2 6 0 4126.91 4758.97 101.74 o 3 6 0 711.10 1016.44 30.22 o 4 6 0 942.03 1406.96 39.62 o 5 6 0 1330.65 1519.51 39.39 o 6 6 0 4670.45 3972.75 141.97 o 1 7 0 1082.90 1146.99 33.26 o 2 7 0 65.10 111.71 8.25 o 3 7 0 1490.39 974.31 27.88 o 4 7 0 1840.43 1793.13 49.39 o 5 7 0 15.66 10.84 8.01 o 6 7 0 277.16 399.32 18.89 o 7 7 0 3263.24 3698.39 116.53 o 0 8 0 26.08 25.67 11.23 o 1 8 0 1870.26 1846.25 50.33 o 2 8 0 4779.99 4769.28 103.43 o 3 8 0 1688.76 1372.19 37.34 o 4 8 0 461.99 539.21 21.48 o 5 8 0 2499.64 2282.35 62.10 o 6 8 0 37.24 46.78 10.02 o 7 8 0 121.18 77.92 12.72 o 8 8 0 80.88 73.10 19.61 o 1 9 0 1.41 13.45 7.39 o 2 9 0 1387.46 1470.34 37.07 o 3 9 0 1295.37 1035.11 30.77 o 4 9 0 10.10 22.24 8.49 o 5 9 0 3881.55 4167.97 106.99 o 6 9 0 177.37 153.87 13.58 o 7 9 0 301.19 388.01 23.24 o 8 9 0 229.01 268.93 16.78 o 9 9 0 52.99 50.68 18.24 o 0 10 0 394.41 594.65 32.97 o 1 10 0 1022.18 1074.40 31.79 o 2 10 0 253.20 315.87 16.63 o 3 10 0 1392.07 1386.32 39.29 o 4 10 0 16.70 12.84 8.57 o 5 10 0 367.19 338.52 17.67 o 6 10 0 450.31 338.03 18.25 o 7 10 0 218.07 179.97 16.33 o 8 10 0 52.19 131.91 14.31 o 9 10 0 438.51 487.34 23.28 o 10 10 0 352.38 376.36 34.04 o 1 11 0 612.53 626.70 23.46 o 2 11 0 134.35 133.95 14.10 o 3 11 0 142.68 191.28 21.44 o 4 11 0 583.45 652.32 25.01 o 5 11 0 82.83 46.49 15.89 o 6 11 0 1240.94 1125.77 36.01 o 7 11 0 1626.01 1696.63 48.78 o 8 11 0 610.54 558.20 26.88 o 9 11 0 17.96 7.97 12.20 o 10 11 0 671.92 666.42 31.78 o 11 11 0 179.18 221.80 30.07 o 0 12 0 240.72 237.68 21.03 o 1 12 0 333.75 311.69 17.53 o 2 12 0 105.13 73.38 11.62 o 3 12 0 86.84 85.22 14.17 o 4 12 0 579.19 700.04 27.25 o 5 12 0 80.45 107.95 13.89 o 6 12 0 1118.07 1157.71 37.48 o 7 12 0 2368.96 2658.01 75.52 o 8 12 0 20.95 39.33 13.08 o 9 12 0 206.93 139.74 15.63 o 10 12 0 144.80 233.32 24.07 o 11 12 0 589.43 611.56 31.95 o 12 12 0 414.67 463.30 52.32 o 1 13 0 732.36 624.54 23.80 o 2 13 0 136.25 117.58 20.24 o 3 13 0 907.69 952.43 36.34 o 4 13 0 586.86 786.18 30.06 o 5 13 0 160.49 170.05 16.30 o 6 13 0 775.27 858.24 32.54 o 7 13 0 353.43 352.04 21.74 o 8 13 0 999.76 978.55 36.01 o 9 13 0 50.60 24.58 13.25 o 10 13 0 1084.84 937.84 37.00 o 11 13 0 1.53 31.44 15.39 o 12 13 0 131.27 111.95 18.82 o 13 13 0 294.01 319.69 33.87 o 0 14 0 105.20 135.88 20.07 o 1 14 0 473.75 550.88 23.20 o 2 14 0 14.92 26.74 12.28 o 3 14 0 24.20 4.36 13.08 o 4 14 0 1.92 14.74 13.78 o 5 14 0 482.66 514.92 25.47 o 6 14 0 70.48 131.23 16.85 o 7 14 0 49.20 48.28 14.61 o 8 14 0 532.38 671.52 30.34 o 9 14 0 1043.82 1134.07 41.70 o 10 14 0 70.55 111.56 18.71 o 11 14 0 182.18 172.76 20.65 o 12 14 0 10.04 5.70 16.05 o 13 14 0 109.78 133.62 20.85 o 14 14 0 262.59 236.24 70.60 o 1 15 0 827.42 941.18 54.01 o 2 15 0 54.29 44.06 14.22 o 3 15 0 1278.64 1265.51 46.24 o 4 15 0 338.70 311.14 23.57 o 5 15 0 552.75 640.37 31.58 o 6 15 0 680.66 798.13 34.26 o 7 15 0 358.96 406.43 27.17 o 8 15 0 967.43 884.97 53.55 o 9 15 0 165.21 156.07 21.51 o 10 15 0 354.05 333.61 27.54 o 11 15 0 254.73 215.45 24.57 o 12 15 0 83.90 124.39 22.54 o 13 15 0 0.01 -0.78 19.24 o 14 15 0 37.81 -1.81 20.28 o 15 15 0 106.04 41.77 32.60 o 0 16 0 3107.82 3045.89 125.67 o 1 16 0 41.85 60.19 16.45 o 2 16 0 162.73 156.60 23.09 o 3 16 0 144.66 168.38 20.95 o 4 16 0 48.46 77.74 15.95 o 5 16 0 0.13 0.21 15.09 o 6 16 0 160.44 137.15 23.07 o 7 16 0 367.61 359.34 30.49 o 8 16 0 8.10 14.00 18.95 o 9 16 0 0.05 -22.12 16.87 o 10 16 0 20.54 63.95 19.73 o 11 16 0 214.03 234.72 25.97 o 12 16 0 0.16 -16.10 19.06 o 13 16 0 111.78 67.59 22.47 o 14 16 0 39.93 19.46 25.95 o 1 17 0 512.51 488.91 39.07 o 2 17 0 1.99 -20.39 15.72 o 3 17 0 243.83 194.53 23.13 o 4 17 0 397.28 330.20 27.04 o 5 17 0 10.31 10.92 18.74 o 6 17 0 0.88 20.89 21.56 o 7 17 0 186.42 167.60 25.13 o 8 17 0 399.17 581.86 39.08 o 9 17 0 190.89 157.26 23.66 o 10 17 0 1.40 21.54 19.57 o 11 17 0 6.14 -11.65 19.61 o 12 17 0 46.17 51.95 21.73 o 0 18 0 515.95 404.91 42.07 o 1 18 0 12.25 27.94 20.60 o 2 18 0 605.99 611.13 35.14 o 3 18 0 0.71 25.58 17.54 o 4 18 0 52.32 69.90 23.87 o 5 18 0 260.87 222.28 27.84 o 6 18 0 14.68 33.47 25.95 o 7 18 0 0.48 12.68 20.33 o 8 18 0 169.01 192.61 33.42 o 9 18 0 89.43 71.39 24.98 o 10 18 0 4.34 -3.36 20.39 o 11 18 0 64.74 62.52 22.94 o 1 19 0 242.71 184.85 24.87 o 2 19 0 45.65 56.54 20.83 o 3 19 0 5.94 2.90 19.83 o 4 19 0 18.43 30.78 22.46 o 5 19 0 190.91 258.18 30.69 o 6 19 0 0.22 5.82 21.45 o 7 19 0 81.62 75.72 24.62 o 8 19 0 218.84 192.08 27.09 o 9 19 0 139.22 83.75 25.28 o 0 20 0 97.91 -3.43 27.54 o 1 20 0 4.30 9.60 19.26 o 2 20 0 2.75 -18.23 20.35 o 3 20 0 179.25 101.04 25.04 o 4 20 0 98.77 104.22 26.42 o 5 20 0 87.48 52.62 24.87 o 6 20 0 0.06 1.08 22.92 o 7 20 0 21.11 49.23 25.16 o 1 21 0 53.18 112.93 27.65 o 2 21 0 41.99 64.91 26.05 o 3 21 0 183.05 244.17 50.21 o 0 1 1 5454.61 5229.56 102.42 o -1 2 1 2925.52 2924.76 66.91 o 0 2 1 3580.55 3570.80 75.93 o 1 2 1 2917.03 2962.38 66.65 o -2 3 1 5155.36 4702.06 114.62 o -1 3 1 5071.96 5364.73 130.40 o 0 3 1 6964.14 7430.25 196.18 o 1 3 1 5021.85 5381.11 119.90 o 2 3 1 5196.16 4721.72 99.17 o -3 4 1 5784.48 6170.22 148.96 o -2 4 1 8122.61 8490.79 187.01 o -1 4 1 5464.93 5596.54 125.39 o 0 4 1 3744.82 3330.75 82.95 o 1 4 1 5483.99 5619.28 149.71 o 2 4 1 8081.02 8380.43 176.49 o 3 4 1 5758.57 6136.95 129.95 o -4 5 1 3830.59 2578.86 61.58 o -3 5 1 750.52 834.65 25.43 o -2 5 1 970.90 979.51 34.32 o -1 5 1 2956.32 2571.44 56.91 o 0 5 1 1673.05 1113.58 33.94 o 1 5 1 2998.17 2674.43 82.48 o 2 5 1 970.60 917.92 50.72 o 3 5 1 734.97 816.03 25.35 o 4 5 1 3896.88 2621.35 58.58 o -5 6 1 75.02 131.04 14.91 o -4 6 1 1248.83 1249.85 33.60 o -3 6 1 5417.65 4287.46 97.76 o -2 6 1 589.77 691.15 19.09 o -1 6 1 1245.29 891.91 26.19 o 0 6 1 3943.46 3787.34 94.03 o 1 6 1 1206.32 843.64 26.97 o 2 6 1 586.94 671.83 22.58 o 3 6 1 5310.87 4224.10 107.23 o 4 6 1 1185.51 1246.89 33.83 o 5 6 1 76.40 105.10 9.02 o -6 7 1 852.59 909.19 34.88 o -5 7 1 522.58 509.34 20.06 o -4 7 1 425.82 466.23 17.04 o -3 7 1 660.67 607.82 21.98 o -2 7 1 739.87 527.63 32.17 o -1 7 1 966.55 981.71 32.42 o 0 7 1 1197.47 1055.61 30.65 o 1 7 1 971.55 977.77 27.05 o 2 7 1 733.12 574.54 21.88 o 3 7 1 678.80 587.53 21.87 o 4 7 1 428.56 466.20 19.27 o 5 7 1 501.71 513.70 19.30 o 6 7 1 857.58 878.51 25.88 o -7 8 1 95.52 90.65 15.31 o -6 8 1 486.96 482.86 19.14 o -5 8 1 5768.44 5851.16 125.52 o -4 8 1 77.33 105.63 10.22 o -3 8 1 385.59 421.13 21.55 o -2 8 1 878.90 937.19 27.45 o -1 8 1 760.92 855.74 29.84 o 0 8 1 211.00 280.81 13.08 o 1 8 1 761.59 878.28 25.59 o 2 8 1 892.23 974.16 31.08 o 3 8 1 387.92 429.15 22.15 o 4 8 1 73.47 115.65 11.46 o 5 8 1 5693.73 5806.97 146.93 o 6 8 1 469.12 460.50 27.94 o 7 8 1 94.84 83.87 10.22 o -8 9 1 1005.06 1036.43 37.47 o -7 9 1 27.33 48.24 10.09 o -6 9 1 151.72 176.11 15.34 o -5 9 1 293.58 292.12 17.17 o -4 9 1 790.15 655.70 22.33 o -3 9 1 749.79 751.25 24.01 o -2 9 1 612.85 726.98 23.91 o -1 9 1 545.60 456.23 19.08 o 0 9 1 1851.12 1417.92 38.44 o 1 9 1 522.23 465.33 24.01 o 2 9 1 613.49 760.55 27.51 o 3 9 1 734.26 688.45 24.25 o 4 9 1 764.81 595.35 22.60 o 5 9 1 306.03 279.96 15.67 o 6 9 1 152.99 193.06 15.60 o 7 9 1 30.40 65.62 12.25 o 8 9 1 1004.28 1027.81 31.13 o -9 10 1 99.87 59.66 15.83 o -8 10 1 371.98 373.75 26.43 o -7 10 1 1078.78 1058.34 33.91 o -6 10 1 284.95 350.95 26.64 o -5 10 1 677.76 631.64 25.01 o -4 10 1 599.17 673.99 23.70 o -3 10 1 1112.05 1054.67 31.57 o -2 10 1 442.44 515.52 18.79 o -1 10 1 78.85 83.41 13.02 o 0 10 1 2107.44 1926.54 50.36 o 1 10 1 82.12 83.33 10.15 o 2 10 1 429.65 483.98 31.88 o 3 10 1 1133.14 1086.51 40.95 o 4 10 1 592.06 652.75 35.49 o 5 10 1 672.33 653.48 27.85 o 6 10 1 285.49 361.28 18.95 o 7 10 1 1058.85 1056.94 34.55 o 8 10 1 372.04 412.51 20.97 o 9 10 1 103.13 60.48 12.91 o -10 11 1 1123.18 1088.09 43.14 o -9 11 1 26.68 28.27 13.89 o -8 11 1 464.40 489.07 26.92 o -7 11 1 89.97 119.37 12.53 o -6 11 1 298.28 245.39 15.34 o -5 11 1 83.88 102.59 11.58 o -4 11 1 165.64 180.86 14.55 o -3 11 1 480.44 385.47 17.20 o -2 11 1 161.69 131.82 12.09 o -1 11 1 320.89 346.71 26.05 o 0 11 1 7.25 -3.75 8.19 o 1 11 1 330.87 315.30 16.33 o 2 11 1 156.30 131.01 14.20 o 3 11 1 482.40 401.89 34.92 o 4 11 1 164.23 171.21 14.34 o 5 11 1 89.02 74.22 12.33 o 6 11 1 294.88 271.91 17.65 o 7 11 1 92.01 108.24 13.77 o 8 11 1 471.72 584.90 25.45 o 9 11 1 26.70 33.06 12.59 o 10 11 1 1117.87 1149.83 36.83 o -11 12 1 17.64 12.47 15.29 o -10 12 1 314.31 256.92 23.45 o -9 12 1 577.38 587.30 27.11 o -8 12 1 58.83 66.02 13.66 o -7 12 1 604.96 726.23 32.18 o -6 12 1 514.05 527.67 21.91 o -5 12 1 595.89 581.24 22.55 o -4 12 1 655.41 737.32 25.67 o -3 12 1 86.74 100.77 11.66 o -2 12 1 108.83 112.18 13.09 o -1 12 1 609.35 527.29 39.72 o 0 12 1 0.52 23.27 12.63 o 1 12 1 588.74 507.36 21.26 o 2 12 1 108.58 109.20 14.81 o 3 12 1 88.39 66.48 13.75 o 4 12 1 645.11 684.37 30.29 o 5 12 1 600.90 574.43 25.01 o 6 12 1 511.35 507.90 26.06 o 7 12 1 609.44 667.64 28.31 o 8 12 1 56.46 66.78 13.91 o 9 12 1 569.49 529.49 24.85 o 10 12 1 313.22 338.58 20.59 o 11 12 1 17.82 18.64 13.27 o -12 13 1 93.51 79.82 18.90 o -11 13 1 107.09 141.37 20.16 o -10 13 1 124.18 124.71 21.08 o -9 13 1 135.00 167.42 17.71 o -8 13 1 53.80 42.77 13.87 o -7 13 1 162.39 186.27 22.11 o -6 13 1 228.25 183.34 17.18 o -5 13 1 94.49 96.92 12.36 o -4 13 1 50.16 69.05 14.80 o -3 13 1 386.90 373.17 24.32 o -2 13 1 91.08 75.45 12.48 o -1 13 1 107.20 145.23 14.78 o 0 13 1 3.13 18.73 10.65 o 1 13 1 104.43 122.04 15.91 o 2 13 1 90.17 87.16 15.00 o 3 13 1 400.28 400.27 23.73 o 4 13 1 48.41 53.59 14.49 o 5 13 1 96.40 103.74 15.47 o 6 13 1 231.80 193.67 19.79 o 7 13 1 164.31 147.53 21.27 o 8 13 1 53.43 48.37 16.52 o 9 13 1 137.88 210.54 24.13 o 10 13 1 124.33 136.69 17.69 o 11 13 1 112.15 134.52 18.11 o 12 13 1 95.34 44.27 18.95 o -13 14 1 41.81 93.65 21.09 o -12 14 1 57.76 79.17 20.05 o -11 14 1 328.67 334.99 31.01 o -10 14 1 171.57 86.99 23.94 o -9 14 1 172.25 165.30 18.54 o -8 14 1 28.58 46.87 14.44 o -7 14 1 379.87 375.80 22.06 o -6 14 1 139.11 193.95 17.10 o -5 14 1 186.02 226.28 16.41 o -4 14 1 99.71 143.24 15.20 o -3 14 1 504.62 510.98 27.70 o -2 14 1 284.72 263.58 18.09 o -1 14 1 245.46 247.52 20.42 o 0 14 1 124.88 100.36 16.81 o 1 14 1 254.55 255.99 20.97 o 2 14 1 284.70 276.20 21.67 o 3 14 1 491.74 511.07 27.84 o 4 14 1 96.50 135.87 18.47 o 5 14 1 184.19 244.99 29.15 o 6 14 1 133.49 159.95 27.20 o 7 14 1 390.76 402.94 26.39 o 8 14 1 26.88 43.02 16.44 o 9 14 1 179.36 244.78 22.77 o 10 14 1 171.36 131.09 21.69 o 11 14 1 339.59 337.36 35.15 o 12 14 1 58.12 47.79 19.05 o 13 14 1 40.09 34.00 19.58 o -14 15 1 48.86 56.99 21.84 o -13 15 1 115.79 84.24 22.28 o -12 15 1 1.79 23.32 18.58 o -11 15 1 68.77 76.63 20.42 o -10 15 1 26.30 13.72 16.23 o -9 15 1 21.97 15.62 14.59 o -8 15 1 50.65 35.28 14.02 o -7 15 1 134.49 94.53 15.71 o -6 15 1 60.50 27.02 13.23 o -5 15 1 155.24 175.72 17.30 o -4 15 1 17.25 17.62 15.71 o -3 15 1 340.54 332.82 33.05 o -2 15 1 148.05 113.82 16.60 o -1 15 1 61.19 20.23 14.91 o 0 15 1 48.35 51.68 16.04 o 1 15 1 66.88 29.59 15.35 o 2 15 1 149.68 135.80 18.81 o 3 15 1 346.19 373.65 24.90 o 4 15 1 17.75 9.86 14.18 o 5 15 1 160.57 158.76 20.42 o 6 15 1 61.11 28.01 16.17 o 7 15 1 135.18 109.14 19.98 o 8 15 1 51.05 24.66 16.80 o 9 15 1 23.40 33.69 16.69 o 10 15 1 25.02 4.99 17.22 o 11 15 1 69.80 76.52 20.49 o 12 15 1 1.80 17.36 19.69 o 13 15 1 118.35 71.17 25.16 o 14 15 1 48.92 44.63 21.52 o -13 16 1 127.17 118.78 24.45 o -12 16 1 6.24 41.74 19.75 o -11 16 1 48.83 52.56 22.49 o -10 16 1 231.95 215.58 24.02 o -9 16 1 239.34 220.83 23.98 o -8 16 1 7.01 20.72 14.71 o -7 16 1 202.09 257.72 30.22 o -6 16 1 280.93 299.18 24.03 o -5 16 1 308.42 269.97 30.25 o -4 16 1 257.96 289.19 48.30 o -3 16 1 252.01 280.93 26.80 o -2 16 1 139.60 90.60 16.47 o -1 16 1 174.99 133.88 19.20 o 0 16 1 455.27 425.17 26.99 o 1 16 1 171.22 153.38 19.89 o 2 16 1 132.49 152.89 26.07 o 3 16 1 252.35 240.64 22.71 o 4 16 1 258.58 206.53 22.65 o 5 16 1 317.18 260.24 24.19 o 6 16 1 275.30 302.73 39.82 o 7 16 1 202.36 233.00 23.84 o 8 16 1 7.25 33.24 18.25 o 9 16 1 244.71 293.83 33.60 o 10 16 1 233.32 206.50 25.46 o 11 16 1 47.24 51.96 20.24 o 12 16 1 5.94 -12.24 21.64 o 13 16 1 127.80 144.00 27.49 o -12 17 1 15.19 19.44 20.82 o -11 17 1 138.29 110.10 26.93 o -10 17 1 52.33 73.14 24.20 o -9 17 1 12.82 -8.80 20.48 o -8 17 1 7.56 27.72 17.63 o -7 17 1 69.15 82.06 18.82 o -6 17 1 62.77 39.12 18.54 o -5 17 1 307.14 294.26 47.93 o -4 17 1 14.06 -3.85 18.26 o -3 17 1 73.32 90.78 22.25 o -2 17 1 146.14 166.08 24.45 o -1 17 1 350.05 344.39 27.71 o 0 17 1 3.80 -2.26 18.03 o 1 17 1 351.96 359.26 27.08 o 2 17 1 147.02 137.31 21.06 o 3 17 1 77.87 82.09 19.49 o 4 17 1 14.11 10.83 17.27 o 5 17 1 310.76 323.59 31.16 o 6 17 1 63.92 42.34 18.36 o 7 17 1 69.04 79.04 20.68 o 8 17 1 7.44 28.81 20.90 o 9 17 1 13.05 1.08 20.23 o 10 17 1 50.07 131.88 26.22 o 11 17 1 141.62 150.58 26.69 o 12 17 1 15.19 29.95 23.70 o -11 18 1 47.61 62.07 26.08 o -10 18 1 0.10 -2.86 23.52 o -9 18 1 350.64 352.08 37.42 o -8 18 1 125.48 102.02 21.79 o -7 18 1 312.86 327.51 29.82 o -6 18 1 15.54 15.03 19.05 o -5 18 1 134.59 117.36 21.62 o -4 18 1 159.41 139.73 30.60 o -3 18 1 95.48 82.04 23.51 o -2 18 1 469.89 486.45 35.55 o -1 18 1 2.23 14.05 22.59 o 0 18 1 21.40 27.36 18.24 o 1 18 1 2.24 -1.32 19.01 o 2 18 1 471.19 441.94 34.45 o 3 18 1 96.57 115.02 27.76 o 4 18 1 155.24 153.14 25.81 o 5 18 1 134.14 81.26 21.57 o 6 18 1 16.33 8.64 19.23 o 7 18 1 317.29 321.53 31.55 o 8 18 1 126.09 126.24 28.11 o 9 18 1 345.07 328.75 33.28 o 10 18 1 0.11 45.60 24.60 o 11 18 1 50.13 30.96 24.58 o -9 19 1 45.24 29.77 24.92 o -8 19 1 15.26 21.94 22.78 o -7 19 1 58.12 23.42 20.55 o -6 19 1 12.80 20.11 21.69 o -5 19 1 79.29 92.84 22.05 o -4 19 1 12.28 17.86 19.33 o -3 19 1 188.81 109.95 25.40 o -2 19 1 74.20 63.57 23.42 o -1 19 1 211.16 165.90 26.56 o 0 19 1 278.75 231.20 29.51 o 1 19 1 211.91 183.41 24.57 o 2 19 1 74.09 93.31 21.81 o 3 19 1 193.73 190.05 28.00 o 4 19 1 12.13 -7.97 22.10 o 5 19 1 79.58 112.54 26.02 o 6 19 1 12.13 37.88 26.32 o 7 19 1 60.74 45.68 27.46 o 8 19 1 14.35 19.39 26.07 o 9 19 1 45.21 24.03 25.61 o -7 20 1 56.50 62.40 22.74 o -6 20 1 45.45 30.40 21.85 o -5 20 1 86.61 57.65 22.50 o -4 20 1 12.34 2.24 20.29 o -3 20 1 92.74 135.30 27.18 o -2 20 1 139.95 136.05 26.07 o -1 20 1 31.86 45.80 23.42 o 0 20 1 1.06 16.56 22.30 o 1 20 1 31.58 26.08 24.74 o 2 20 1 141.05 148.09 25.71 o 3 20 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24.19 o 3 19 2 121.25 137.49 27.30 o 4 19 2 16.44 20.63 20.69 o 5 19 2 232.35 175.74 26.67 o 6 19 2 6.20 26.36 21.16 o 7 19 2 7.73 42.01 21.68 o 8 19 2 80.25 158.34 28.48 o -5 20 2 12.62 42.06 22.01 o -4 20 2 173.15 169.75 26.59 o -3 20 2 58.07 77.40 23.27 o -2 20 2 4.09 4.27 23.60 o -1 20 2 10.82 -30.97 21.69 o 0 20 2 273.77 343.42 47.86 o 1 20 2 11.16 32.50 27.32 o 2 20 2 3.85 22.04 26.55 o 3 20 2 60.18 96.30 34.75 o 4 20 2 171.70 120.44 32.40 o 5 20 2 14.13 25.40 27.01 o 0 1 3 108.95 116.48 7.73 o -1 2 3 367.54 401.40 16.21 o 0 2 3 988.13 920.76 24.04 o 1 2 3 356.66 347.88 17.18 o -2 3 3 491.18 591.29 20.90 o -1 3 3 1666.11 1905.78 48.43 o 0 3 3 42.85 19.54 6.67 o 1 3 3 1651.57 1838.95 47.71 o 2 3 3 503.75 602.48 22.61 o -3 4 3 1159.15 1310.40 39.44 o -2 4 3 1275.28 1316.07 37.11 o -1 4 3 1060.15 1291.43 45.15 o 0 4 3 129.15 141.40 17.05 o 1 4 3 1091.79 1304.83 35.69 o 2 4 3 1258.47 1376.49 36.92 o 3 4 3 1160.64 1311.29 36.19 o -4 5 3 2814.86 2695.80 71.86 o -3 5 3 988.14 1096.94 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