#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/81/2228106.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228106_Fobs loop_ _publ_author_name 'Harrison, William T. A.' 'Mayekar, A. N.' 'Yathirajan, H. S.' 'Narayana, B.' 'Sarojini, B. K.' _publ_section_title ; Ethyl 4-(2,4-dichlorophenyl)-6-(6-methoxy-2-naphthyl)-2-oxocyclohex-3-ene-1-carboxylate ; _journal_coeditor_code XU5016 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2478 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.840 _cell_angle_gamma 90.000 _cell_length_a 14.2156 _cell_length_b 5.8647 _cell_length_c 27.3752 _exptl_crystal_F_000 976.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file xu5016Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2010src0612' _shelx_refln_list_code 4 _shelx_f_calc_maximum 224.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 4548.17 4600.34 128.28 o 4 0 0 377.16 421.58 23.33 o 5 0 0 1298.51 1091.82 41.25 o 6 0 0 135.78 107.20 8.82 o 7 0 0 154.56 140.27 11.72 o 8 0 0 107.52 107.95 12.25 o 9 0 0 633.91 603.01 40.96 o 10 0 0 3431.04 3329.37 204.48 o 11 0 0 221.95 189.70 25.65 o 12 0 0 30.89 32.34 17.06 o 13 0 0 1039.65 1130.04 93.97 o 14 0 0 318.08 358.25 40.13 o 15 0 0 20.96 -14.74 24.90 o 16 0 0 643.59 641.02 81.55 o 17 0 0 85.52 89.26 31.36 o 18 0 0 101.86 115.64 56.55 o 1 1 0 3501.73 3232.22 77.63 o 2 1 0 104.51 155.20 7.92 o 3 1 0 96.51 139.84 5.67 o 4 1 0 126.97 149.89 6.08 o 5 1 0 178.75 217.14 8.25 o 6 1 0 8813.98 9131.30 199.39 o 7 1 0 6487.25 6399.06 151.40 o 8 1 0 468.34 429.41 25.16 o 9 1 0 358.78 337.71 16.59 o 10 1 0 2.67 -1.02 9.36 o 11 1 0 342.07 314.78 22.86 o 12 1 0 222.61 207.38 20.63 o 13 1 0 150.18 136.17 19.45 o 14 1 0 8.33 -0.05 14.22 o 15 1 0 37.62 16.94 16.64 o 16 1 0 23.55 8.33 24.49 o 17 1 0 2.69 -2.25 25.05 o 18 1 0 63.14 18.95 40.88 o 0 2 0 2120.57 2155.35 64.28 o 1 2 0 1420.44 1328.19 25.58 o 2 2 0 199.85 223.57 9.86 o 3 2 0 296.01 382.91 16.66 o 4 2 0 12.69 22.62 4.85 o 5 2 0 2084.83 2347.48 46.63 o 6 2 0 2012.05 2110.53 61.68 o 7 2 0 243.91 292.83 13.96 o 8 2 0 0.08 0.04 7.40 o 9 2 0 1102.02 1049.67 43.17 o 10 2 0 60.03 53.31 10.60 o 11 2 0 5.55 12.61 11.79 o 12 2 0 40.39 21.27 13.19 o 13 2 0 68.28 83.54 14.65 o 14 2 0 65.80 86.53 19.43 o 15 2 0 11.14 17.10 18.13 o 16 2 0 166.71 165.41 32.85 o 17 2 0 2.55 -20.38 27.34 o 1 3 0 839.62 764.24 23.02 o 2 3 0 1550.27 1593.06 40.87 o 3 3 0 23.17 20.24 6.63 o 4 3 0 852.18 854.47 32.63 o 5 3 0 1102.35 1256.30 52.10 o 6 3 0 30.28 38.68 7.62 o 7 3 0 96.35 84.58 8.19 o 8 3 0 297.13 308.75 16.66 o 9 3 0 159.50 129.16 11.73 o 10 3 0 54.71 71.51 14.18 o 11 3 0 8.55 2.20 12.77 o 12 3 0 646.14 731.56 45.07 o 13 3 0 187.89 139.88 36.27 o 14 3 0 133.43 74.75 26.06 o 15 3 0 178.42 182.37 30.57 o 16 3 0 15.00 -19.71 35.58 o 0 4 0 220.85 221.02 22.44 o 1 4 0 817.54 865.38 43.05 o 2 4 0 132.77 117.94 14.12 o 3 4 0 3680.61 3777.94 140.05 o 4 4 0 518.81 568.32 41.01 o 5 4 0 101.28 82.41 12.06 o 6 4 0 756.60 760.53 32.21 o 7 4 0 352.61 350.65 22.25 o 8 4 0 100.55 114.04 16.32 o 9 4 0 90.08 71.56 20.54 o 10 4 0 696.73 812.87 64.23 o 11 4 0 83.39 66.88 23.69 o 12 4 0 1.83 -12.49 20.05 o 13 4 0 212.19 256.15 34.61 o 14 4 0 53.22 15.34 36.53 o 15 4 0 81.74 81.88 45.52 o 1 5 0 7.54 10.18 13.87 o 2 5 0 2047.15 2277.75 107.35 o 3 5 0 955.46 1064.77 58.89 o 4 5 0 279.28 312.01 25.41 o 5 5 0 263.89 251.52 29.19 o 6 5 0 16.07 46.22 15.76 o 7 5 0 96.49 125.42 23.81 o 8 5 0 50.21 41.43 20.95 o 9 5 0 49.67 15.91 23.82 o 10 5 0 87.61 115.26 26.69 o 11 5 0 1.93 -34.12 22.85 o 12 5 0 65.61 113.57 44.61 o 13 5 0 100.35 70.27 41.43 o 0 6 0 140.28 121.19 29.62 o 1 6 0 22.89 27.58 17.02 o 2 6 0 1276.00 1512.30 95.19 o 3 6 0 2.66 31.22 31.58 o 4 6 0 549.26 633.14 64.45 o 5 6 0 25.44 -10.80 35.29 o 6 6 0 120.22 124.24 47.50 o 7 6 0 144.35 188.92 81.79 o 8 6 0 170.15 110.98 70.70 o 9 6 0 279.42 193.92 57.73 o 10 6 0 69.07 126.08 41.16 o 11 6 0 3.64 -19.53 42.49 o 1 7 0 151.49 170.83 59.80 o 2 7 0 115.06 79.46 51.28 o 3 7 0 189.33 226.05 48.35 o 4 7 0 0.41 17.38 30.06 o 5 7 0 9.49 -14.22 36.94 o 6 7 0 5.14 29.26 34.53 o 7 7 0 3.33 -8.60 49.38 o -18 1 1 83.44 65.25 26.40 o -17 1 1 13.09 -28.17 27.71 o -16 1 1 117.58 126.12 25.62 o -15 1 1 71.30 53.04 19.75 o -14 1 1 120.51 125.10 25.59 o -13 1 1 210.54 214.75 22.51 o -12 1 1 7.70 21.37 12.35 o -11 1 1 25.99 26.91 16.40 o -10 1 1 437.62 409.06 23.93 o -9 1 1 17.43 33.58 8.42 o -8 1 1 113.35 89.31 8.09 o -7 1 1 112.19 117.31 7.44 o -6 1 1 333.96 269.43 11.12 o -5 1 1 15.07 13.71 4.34 o -4 1 1 283.39 254.35 8.01 o -3 1 1 18379.06 17414.14 380.34 o -2 1 1 717.02 590.81 14.15 o -1 1 1 15640.73 14587.08 332.33 o 0 1 1 266.07 154.55 14.24 o 1 1 1 1.35 16.20 3.08 o 2 1 1 70.75 97.04 5.77 o 3 1 1 906.08 899.54 18.38 o 4 1 1 86.22 110.37 6.29 o 5 1 1 400.31 409.01 11.44 o 6 1 1 2815.99 3067.04 71.32 o 7 1 1 1542.68 1563.87 47.69 o 8 1 1 820.56 881.28 27.85 o 9 1 1 574.83 661.53 27.87 o 10 1 1 1809.44 1699.01 74.88 o 11 1 1 100.46 170.00 28.87 o 12 1 1 25.24 10.50 12.56 o 13 1 1 111.90 95.11 17.69 o 14 1 1 347.79 336.18 30.05 o 15 1 1 6.20 5.19 16.24 o 16 1 1 337.20 323.70 38.95 o 17 1 1 51.51 17.45 25.23 o 18 1 1 248.78 395.10 57.96 o -17 2 1 453.43 424.45 71.92 o -16 2 1 377.49 361.11 48.40 o -15 2 1 6.66 -0.17 25.45 o -14 2 1 60.39 90.27 24.34 o -13 2 1 761.43 750.26 43.97 o -12 2 1 1206.51 1252.51 59.42 o -11 2 1 244.35 236.71 20.55 o -10 2 1 518.40 518.77 29.35 o -9 2 1 524.53 535.75 25.41 o -8 2 1 178.71 185.92 12.21 o -7 2 1 1978.07 1769.06 55.15 o -6 2 1 3133.12 3225.39 83.38 o -5 2 1 501.61 375.58 12.58 o -4 2 1 89.85 70.84 5.68 o -3 2 1 8812.91 8683.59 151.08 o -2 2 1 2032.23 2093.53 36.86 o -1 2 1 44.40 53.09 5.11 o 0 2 1 790.57 762.04 16.83 o 1 2 1 43.10 62.25 5.16 o 2 2 1 7.32 10.50 3.79 o 3 2 1 2237.24 2460.55 48.28 o 4 2 1 7414.89 7031.11 125.45 o 5 2 1 2091.18 1890.23 39.17 o 6 2 1 141.32 135.85 9.69 o 7 2 1 1959.45 1944.01 59.94 o 8 2 1 18.13 30.30 7.29 o 9 2 1 998.05 946.61 56.28 o 10 2 1 741.09 824.94 36.68 o 11 2 1 14.42 20.22 12.57 o 12 2 1 0.17 -7.91 11.14 o 13 2 1 11.42 32.78 16.72 o 14 2 1 282.13 256.54 30.45 o 15 2 1 139.97 193.60 27.65 o 16 2 1 0.10 21.40 23.67 o 17 2 1 155.74 109.03 41.67 o -16 3 1 26.38 59.06 37.31 o -15 3 1 175.23 103.09 33.27 o -14 3 1 318.35 393.25 39.82 o -13 3 1 424.38 461.40 42.23 o -12 3 1 38.78 65.67 17.41 o -11 3 1 229.51 266.83 25.56 o -10 3 1 98.25 117.75 14.19 o -9 3 1 8.28 18.35 8.50 o -8 3 1 462.54 413.87 25.24 o -7 3 1 121.33 82.71 8.52 o -6 3 1 732.85 623.21 28.09 o -5 3 1 594.49 528.94 22.55 o -4 3 1 1776.80 1917.32 73.06 o -3 3 1 3424.88 3432.64 97.28 o -2 3 1 7.08 17.67 6.06 o -1 3 1 3269.79 3312.99 83.30 o 0 3 1 1860.73 1881.73 54.10 o 1 3 1 400.65 486.22 18.29 o 2 3 1 2170.32 2283.67 57.90 o 3 3 1 0.45 -2.07 5.57 o 4 3 1 4.41 0.91 6.40 o 5 3 1 2.99 0.68 8.57 o 6 3 1 139.13 135.48 9.87 o 7 3 1 72.55 70.49 8.27 o 8 3 1 83.34 74.30 9.36 o 9 3 1 89.18 112.21 16.44 o 10 3 1 408.39 423.26 23.34 o 11 3 1 332.36 360.00 24.07 o 12 3 1 63.57 51.63 20.80 o 13 3 1 724.85 832.90 54.86 o 14 3 1 74.03 49.63 19.80 o 15 3 1 5.72 4.65 34.06 o 16 3 1 22.60 -13.26 35.93 o -15 4 1 66.40 101.60 52.64 o -14 4 1 89.11 117.58 30.76 o -13 4 1 0.01 26.43 26.31 o -12 4 1 228.41 180.26 31.88 o -11 4 1 937.55 1080.55 78.15 o -10 4 1 14.44 81.66 28.42 o -9 4 1 125.57 128.91 20.93 o -8 4 1 58.68 64.67 15.16 o -7 4 1 512.67 509.67 34.77 o -6 4 1 88.39 74.25 11.85 o -5 4 1 1378.05 1397.38 63.11 o -4 4 1 1473.65 1465.74 56.40 o -3 4 1 287.36 300.01 16.50 o -2 4 1 1520.10 1486.88 53.52 o -1 4 1 246.06 235.08 20.76 o 0 4 1 422.90 417.02 22.36 o 1 4 1 562.47 579.56 27.88 o 2 4 1 269.08 330.40 23.01 o 3 4 1 762.32 749.19 36.26 o 4 4 1 784.17 808.34 34.65 o 5 4 1 267.83 208.62 22.15 o 6 4 1 72.40 47.15 13.18 o 7 4 1 782.31 754.08 31.59 o 8 4 1 255.95 227.18 17.70 o 9 4 1 15.20 30.80 18.92 o 10 4 1 91.72 135.37 28.79 o 11 4 1 596.14 629.78 50.78 o 12 4 1 179.10 234.22 33.88 o 13 4 1 2.44 -17.01 37.47 o 14 4 1 8.48 45.40 36.73 o 15 4 1 88.35 116.39 46.56 o -13 5 1 167.51 115.33 50.80 o -12 5 1 73.35 57.86 36.55 o -11 5 1 16.22 -15.86 29.38 o -10 5 1 1.43 13.14 28.19 o -9 5 1 426.44 422.91 45.58 o -8 5 1 70.43 77.73 19.96 o -7 5 1 37.32 13.38 20.16 o -6 5 1 447.17 479.67 33.49 o -5 5 1 686.05 768.11 45.59 o -4 5 1 1043.33 1077.83 68.21 o -3 5 1 184.43 170.22 19.24 o -2 5 1 37.64 60.79 15.66 o -1 5 1 1.76 28.24 11.86 o 0 5 1 36.43 54.56 14.18 o 1 5 1 14.94 35.13 13.17 o 2 5 1 1.80 19.55 13.54 o 3 5 1 406.36 415.18 31.82 o 4 5 1 1069.38 1040.50 63.56 o 5 5 1 74.32 93.72 19.32 o 6 5 1 176.15 236.21 41.22 o 7 5 1 435.34 505.24 57.27 o 8 5 1 20.08 64.91 29.77 o 9 5 1 2.94 56.58 26.03 o 10 5 1 0.66 23.53 28.06 o 11 5 1 126.55 160.38 33.80 o 12 5 1 0.15 10.09 42.48 o 13 5 1 55.83 47.69 43.33 o -11 6 1 34.65 59.15 50.76 o -10 6 1 4.87 9.25 34.35 o -9 6 1 127.91 64.19 49.48 o -8 6 1 21.97 19.37 40.61 o -7 6 1 15.68 41.51 38.98 o -6 6 1 0.85 1.61 30.25 o -5 6 1 66.74 101.04 37.50 o -4 6 1 40.25 47.91 33.15 o -3 6 1 136.53 138.42 25.92 o -2 6 1 1228.85 1469.52 86.89 o -1 6 1 60.92 99.98 21.84 o 0 6 1 138.06 107.01 19.50 o 1 6 1 1062.24 1259.03 72.01 o 2 6 1 42.15 20.09 18.17 o 3 6 1 19.48 69.97 31.01 o 4 6 1 106.05 104.76 33.77 o 5 6 1 95.85 77.45 34.17 o 6 6 1 41.31 43.30 36.21 o 7 6 1 19.77 36.10 32.67 o 8 6 1 15.00 -1.01 47.42 o 9 6 1 1.72 34.22 44.59 o 10 6 1 0.16 -15.85 32.73 o 11 6 1 26.19 -3.01 42.47 o -7 7 1 0.42 -42.76 50.68 o -6 7 1 19.51 34.56 34.41 o -5 7 1 0.45 31.89 67.42 o -4 7 1 16.88 -19.97 42.34 o -3 7 1 16.89 3.47 27.42 o -2 7 1 26.16 -57.55 67.40 o -1 7 1 7.63 31.02 63.33 o 0 7 1 59.43 -1.18 38.27 o 1 7 1 83.02 26.32 47.33 o 2 7 1 75.69 26.62 36.51 o 3 7 1 0.26 37.77 28.18 o 4 7 1 0.00 -6.45 33.55 o 5 7 1 6.84 46.18 35.50 o 6 7 1 3.89 -15.83 68.23 o 7 7 1 5.20 15.73 39.76 o -18 0 2 516.66 501.32 81.69 o -17 0 2 380.48 506.91 71.36 o -16 0 2 77.71 50.63 35.92 o -15 0 2 51.51 50.17 25.12 o -14 0 2 374.25 353.90 38.77 o -13 0 2 562.23 575.05 52.40 o -12 0 2 0.03 -13.95 14.99 o -11 0 2 503.41 359.10 36.64 o -10 0 2 651.13 733.08 57.10 o -9 0 2 55.19 49.22 11.73 o -8 0 2 6999.63 7017.85 252.22 o -7 0 2 3563.70 3553.07 138.15 o -6 0 2 1736.73 2039.75 65.63 o -5 0 2 16815.57 16774.10 472.37 o -4 0 2 11261.59 10873.57 309.78 o -3 0 2 123.50 145.73 8.25 o -2 0 2 943.09 913.84 40.58 o 2 0 2 32726.08 30393.61 1063.21 o 3 0 2 3584.99 3774.97 121.07 o 4 0 2 0.89 6.92 5.69 o 5 0 2 119.46 175.85 10.15 o 6 0 2 9.41 30.63 7.73 o 7 0 2 2890.95 2737.31 95.95 o 8 0 2 2266.87 2152.01 99.58 o 9 0 2 1322.98 1394.24 70.83 o 10 0 2 1339.07 1413.03 84.69 o 11 0 2 94.34 147.86 23.18 o 12 0 2 243.44 170.25 29.67 o 13 0 2 705.00 718.68 84.82 o 14 0 2 946.38 932.86 85.25 o 15 0 2 1510.22 1557.52 123.39 o 16 0 2 519.93 543.47 57.90 o 17 0 2 105.83 78.41 42.92 o 18 0 2 134.87 99.96 49.42 o -18 1 2 20.84 25.05 28.30 o -17 1 2 19.98 -25.40 33.01 o -16 1 2 39.92 126.51 21.32 o -15 1 2 29.51 -7.52 19.30 o -14 1 2 394.19 378.09 33.29 o -13 1 2 90.19 52.87 16.86 o -12 1 2 228.00 199.22 24.75 o -11 1 2 1596.95 1680.28 71.92 o -10 1 2 36.30 36.97 9.78 o -9 1 2 151.66 119.17 14.40 o -8 1 2 159.60 185.91 12.14 o -7 1 2 182.13 170.20 9.06 o -6 1 2 697.86 673.07 18.48 o -5 1 2 5.44 36.64 5.10 o -4 1 2 3941.73 4223.24 85.65 o -3 1 2 10012.09 9832.62 161.97 o -2 1 2 11453.23 10936.11 196.94 o -1 1 2 643.38 527.18 12.54 o 0 1 2 762.15 1050.58 26.98 o 1 1 2 2427.68 1907.12 41.64 o 2 1 2 30049.51 27820.52 444.48 o 3 1 2 3640.16 3840.08 67.47 o 4 1 2 104.16 178.74 6.83 o 5 1 2 1803.95 1709.34 37.92 o 6 1 2 728.23 706.98 19.02 o 7 1 2 2425.21 2465.94 68.39 o 8 1 2 370.05 405.22 25.26 o 9 1 2 1324.34 1377.94 51.58 o 10 1 2 106.15 139.56 13.18 o 11 1 2 117.01 88.96 14.15 o 12 1 2 433.83 462.15 25.98 o 13 1 2 19.38 18.97 17.20 o 14 1 2 10.01 14.17 15.56 o 15 1 2 579.97 598.31 42.23 o 16 1 2 324.69 325.52 36.75 o 17 1 2 54.27 39.58 25.11 o 18 1 2 97.94 36.81 28.36 o -17 2 2 1.43 37.77 47.19 o -16 2 2 1.04 33.09 28.76 o -15 2 2 32.14 16.54 19.48 o -14 2 2 150.11 156.86 27.97 o -13 2 2 174.49 136.32 20.85 o -12 2 2 340.52 341.69 22.66 o -11 2 2 452.06 485.59 44.65 o -10 2 2 724.54 678.08 35.30 o -9 2 2 215.31 220.05 19.72 o -8 2 2 500.90 498.20 24.94 o -7 2 2 189.35 201.88 18.14 o -6 2 2 5.86 8.10 5.55 o -5 2 2 346.60 428.34 12.48 o -4 2 2 473.28 411.19 12.33 o -3 2 2 278.41 304.09 10.24 o -2 2 2 493.49 489.36 13.76 o -1 2 2 28.04 35.28 4.69 o 0 2 2 13.43 18.53 4.16 o 1 2 2 380.93 359.13 12.65 o 2 2 2 95.11 95.23 6.18 o 3 2 2 90.70 83.75 5.38 o 4 2 2 1885.08 1798.74 37.49 o 5 2 2 2833.22 2944.36 58.25 o 6 2 2 0.09 10.92 4.58 o 7 2 2 0.02 9.90 5.34 o 8 2 2 780.93 749.45 26.96 o 9 2 2 875.42 869.97 38.51 o 10 2 2 369.99 335.31 19.07 o 11 2 2 241.13 226.40 19.38 o 12 2 2 88.28 112.87 15.83 o 13 2 2 182.12 182.71 22.20 o 14 2 2 764.38 831.62 57.93 o 15 2 2 273.74 284.03 31.76 o 16 2 2 12.56 -5.09 31.63 o 17 2 2 200.37 213.92 64.62 o -16 3 2 22.03 -13.07 29.52 o -15 3 2 2.55 14.68 28.85 o -14 3 2 16.36 41.34 23.77 o -13 3 2 117.30 97.96 21.79 o -12 3 2 76.03 73.11 27.75 o -11 3 2 491.75 462.78 40.24 o -10 3 2 8.19 1.66 19.92 o -9 3 2 13.22 28.58 8.32 o -8 3 2 400.63 414.11 19.12 o -7 3 2 12.92 28.73 7.51 o -6 3 2 139.49 109.08 8.85 o -5 3 2 1797.99 1773.33 67.36 o -4 3 2 1503.71 1637.00 46.03 o -3 3 2 1245.43 1406.00 43.74 o -2 3 2 1260.53 1199.53 32.64 o -1 3 2 638.35 606.97 19.46 o 0 3 2 109.50 113.68 8.76 o 1 3 2 125.99 85.06 7.58 o 2 3 2 973.10 956.18 27.81 o 3 3 2 69.88 73.65 6.29 o 4 3 2 39.07 67.68 12.45 o 5 3 2 277.55 237.27 13.06 o 6 3 2 29.81 21.37 7.82 o 7 3 2 2.72 -5.50 6.11 o 8 3 2 1384.80 1391.98 46.13 o 9 3 2 58.10 47.64 10.54 o 10 3 2 61.56 35.54 11.30 o 11 3 2 46.23 57.03 19.00 o 12 3 2 427.25 489.78 42.17 o 13 3 2 17.16 32.54 22.01 o 14 3 2 145.15 103.30 32.37 o 15 3 2 61.79 82.11 35.52 o 16 3 2 97.49 180.08 51.94 o -15 4 2 22.73 5.57 113.80 o -14 4 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49.28 o -6 5 2 492.53 541.92 46.47 o -5 5 2 151.40 145.64 18.61 o -4 5 2 8.96 -8.13 12.28 o -3 5 2 12.75 4.16 15.95 o -2 5 2 55.95 64.85 24.84 o -1 5 2 949.23 1090.69 60.01 o 0 5 2 393.80 404.91 27.54 o 1 5 2 212.91 209.71 19.75 o 2 5 2 535.11 542.42 35.68 o 3 5 2 0.18 -6.07 16.90 o 4 5 2 22.30 12.29 14.82 o 5 5 2 161.41 153.52 25.93 o 6 5 2 31.13 0.26 24.55 o 7 5 2 6.18 57.35 28.08 o 8 5 2 47.70 17.29 31.60 o 9 5 2 1.70 23.73 34.92 o 10 5 2 83.68 25.84 33.81 o 11 5 2 26.91 11.18 37.29 o 12 5 2 141.02 76.76 56.72 o 13 5 2 386.17 398.15 60.10 o -11 6 2 75.77 106.57 36.80 o -10 6 2 40.64 47.65 33.82 o -9 6 2 111.82 159.58 31.69 o -8 6 2 288.31 198.31 40.18 o -7 6 2 1.17 -19.35 34.94 o -6 6 2 302.42 450.48 62.65 o -5 6 2 8.65 55.72 32.31 o -4 6 2 1.90 4.09 26.36 o -3 6 2 539.65 569.70 47.07 o -2 6 2 148.82 183.73 27.16 o -1 6 2 114.14 140.99 20.88 o 0 6 2 2.61 3.87 16.31 o 1 6 2 47.74 53.16 19.23 o 2 6 2 13.25 25.46 30.44 o 3 6 2 5.09 20.38 36.18 o 4 6 2 840.92 865.99 79.94 o 5 6 2 164.91 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