#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/81/2228122.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228122_Fobs loop_ _publ_author_name 'Keng, Thy Chun' 'Lo, Kong Mun' 'Ng, Seik Weng' _publ_section_title ; Tribenzylbis(triphenylarsine oxide-\kO)tin(IV) tetraphenylborate ; _journal_coeditor_code XU5034 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1372 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 69.220 _cell_angle_beta 73.972 _cell_angle_gamma 62.683 _cell_length_a 14.3288 _cell_length_b 14.9477 _cell_length_c 19.0994 _exptl_crystal_F_000 1388.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file xu5034Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 269.21 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4861.96 4604.65 38.76 o 3 0 0 11.24 18.19 13.45 o 4 0 0 1428.25 1464.51 36.74 o 5 0 0 440.50 434.02 27.97 o 6 0 0 133.79 124.11 23.30 o 7 0 0 1307.80 1390.09 50.91 o 8 0 0 2348.45 2342.63 66.37 o 9 0 0 525.29 429.28 43.50 o 10 0 0 487.61 453.94 67.95 o 10 0 0 1160.37 838.64 201.05 o 11 0 0 6585.53 7241.44 227.87 o 11 0 0 6179.87 6468.74 229.52 o 12 0 0 429.66 342.06 101.89 o 13 0 0 1182.92 1299.41 157.19 o 14 0 0 588.54 527.57 151.51 o 15 0 0 219.55 14.24 170.70 o 16 0 0 53.35 -292.41 194.94 o -15 1 0 4.65 -19.41 146.04 o -15 1 0 86.55 -54.36 250.02 o -14 1 0 898.15 519.88 172.57 o -13 1 0 17.17 -5.32 144.03 o -12 1 0 3667.24 3636.58 190.98 o -11 1 0 1849.99 1879.91 114.55 o -10 1 0 4800.19 4895.72 143.81 o -9 1 0 1591.58 1714.02 131.88 o -9 1 0 1192.16 1303.37 83.12 o -8 1 0 589.59 630.54 156.83 o -8 1 0 37.61 11.94 32.43 o -7 1 0 728.98 772.49 47.46 o -6 1 0 1807.88 1986.05 55.94 o -5 1 0 120.39 185.37 24.30 o -4 1 0 1011.73 952.54 37.32 o -3 1 0 13.31 79.02 15.89 o -2 1 0 4301.08 4834.96 49.54 o -1 1 0 60999.47 67667.41 516.43 o -1 1 0 36384.92 42856.87 225.35 o 2 1 0 29847.11 10963.44 60.83 o 3 1 0 19901.18 22851.46 204.07 o 3 1 0 13769.66 18389.33 204.07 o 4 1 0 2971.25 2432.80 48.90 o 4 1 0 2766.00 2555.97 96.50 o 5 1 0 210.58 156.76 31.57 o 5 1 0 4051.83 4385.05 118.57 o 6 1 0 1802.89 2086.57 106.28 o 6 1 0 1289.59 1503.48 50.48 o 7 1 0 544.98 532.54 35.09 o 8 1 0 2918.52 3149.41 69.03 o 9 1 0 1380.80 1134.61 55.37 o 10 1 0 12365.85 12753.90 186.24 o 11 1 0 259.00 215.29 52.06 o 12 1 0 81.68 154.89 51.20 o 13 1 0 233.21 236.00 87.15 o 13 1 0 804.73 683.75 157.55 o 14 1 0 475.26 386.78 159.56 o 15 1 0 66.28 -218.81 162.08 o 16 1 0 656.43 513.34 191.92 o -15 2 0 466.14 365.07 120.59 o -14 2 0 38.53 -75.29 138.35 o -14 2 0 41.53 83.91 231.90 o -13 2 0 2731.53 2683.97 203.78 o -12 2 0 1583.19 1405.33 164.09 o -11 2 0 2525.32 2552.88 125.76 o -10 2 0 3146.16 3473.49 128.93 o -9 2 0 493.81 390.88 79.02 o -8 2 0 3082.94 2880.27 89.95 o -7 2 0 1644.57 1830.87 69.61 o -7 2 0 2781.87 2859.56 194.00 o -6 2 0 475.24 600.99 45.95 o -6 2 0 3512.47 3774.64 200.33 o -5 2 0 122.32 118.00 24.88 o -4 2 0 3626.62 3601.34 62.92 o -3 2 0 4485.00 4528.43 62.56 o -2 2 0 16945.50 18473.10 119.51 o -1 2 0 1911.70 2086.79 35.59 o 0 2 0 10131.18 8490.45 59.97 o 1 2 0 15618.65 14710.18 148.70 o 1 2 0 8005.50 6766.07 48.68 o 2 2 0 2451.32 1861.94 46.74 o 2 2 0 6155.52 3439.05 48.90 o 3 2 0 64908.52 66599.89 191.13 o 4 2 0 9103.46 6658.07 62.77 o 5 2 0 7154.20 7735.37 95.06 o 6 2 0 424.48 367.87 39.55 o 6 2 0 50.33 47.39 40.99 o 7 2 0 6517.99 6773.19 111.17 o 7 2 0 6484.49 7040.11 143.88 o 8 2 0 2124.53 2208.45 68.74 o 8 2 0 2310.69 2479.82 126.84 o 9 2 0 13002.62 13095.24 132.16 o 10 2 0 11.94 11.86 28.40 o 11 2 0 4675.15 4948.93 129.29 o 12 2 0 887.83 866.25 78.09 o 13 2 0 36.76 36.38 50.48 o 14 2 0 109.19 125.98 84.27 o 15 2 0 729.88 665.92 179.84 o 16 2 0 725.75 435.10 193.50 o 17 2 0 230.95 -3.09 203.06 o -14 3 0 1893.62 1825.84 169.77 o -13 3 0 783.42 882.86 130.29 o -12 3 0 2851.20 2507.72 242.47 o -12 3 0 2893.49 3118.13 272.52 o -11 3 0 2799.54 2588.47 181.99 o -10 3 0 95.73 67.23 83.48 o -9 3 0 657.23 644.85 87.44 o -8 3 0 23.31 5.54 60.54 o -7 3 0 7771.52 7535.47 120.23 o -6 3 0 6085.81 6373.68 123.75 o -6 3 0 44.54 149.85 56.37 o -5 3 0 8.69 -7.05 25.10 o -5 3 0 135.78 294.46 118.50 o -4 3 0 18301.73 18637.98 326.17 o -4 3 0 2329.02 2444.23 65.51 o -3 3 0 6564.19 6208.80 88.16 o -2 3 0 4903.55 4782.26 65.22 o -1 3 0 9612.47 8921.67 78.02 o 0 3 0 3262.74 2714.81 46.74 o 1 3 0 1326.63 1159.13 26.75 o 2 3 0 130.61 31.78 10.28 o 2 3 0 364.01 155.96 42.35 o 3 3 0 11648.20 11193.62 100.02 o 3 3 0 11816.36 11541.86 170.42 o 4 3 0 1627.65 1587.76 39.76 o 5 3 0 111.74 161.86 31.28 o 6 3 0 163.18 114.91 26.03 o 7 3 0 1911.81 2269.36 72.41 o 8 3 0 11481.30 11908.15 124.40 o 9 3 0 1238.98 1250.73 86.65 o 9 3 0 2070.36 1978.21 89.52 o 10 3 0 4825.84 4836.76 106.35 o 10 3 0 5050.00 5188.09 201.27 o 11 3 0 3918.32 3926.72 199.32 o 11 3 0 2567.80 2366.36 127.56 o 12 3 0 12.18 12.44 43.36 o 13 3 0 19.11 24.81 47.46 o 14 3 0 917.65 921.69 90.03 o 15 3 0 7.24 35.52 87.08 o 16 3 0 167.08 133.03 100.17 o 17 3 0 132.95 758.25 218.16 o -14 4 0 65.18 -5.68 105.49 o -13 4 0 1122.32 1023.51 143.38 o -12 4 0 3337.76 3364.27 188.25 o -11 4 0 335.23 265.19 204.50 o -11 4 0 330.34 202.70 137.41 o -10 4 0 2376.70 2536.34 157.04 o -10 4 0 414.91 320.13 130.37 o -9 4 0 996.42 1035.59 103.54 o -8 4 0 2406.00 2381.82 94.70 o -7 4 0 4780.42 5005.96 109.58 o -6 4 0 80.92 96.86 54.29 o -5 4 0 11921.18 9169.25 51.48 o -4 4 0 11192.19 11465.13 170.49 o -4 4 0 16536.49 16036.34 209.32 o -3 4 0 6671.57 7059.02 127.06 o -3 4 0 6934.12 6981.79 143.02 o -2 4 0 6096.60 6136.97 90.03 o -2 4 0 16348.76 17415.93 299.63 o -1 4 0 18243.43 18413.56 123.32 o 0 4 0 2881.21 2804.34 55.51 o 1 4 0 1395.92 1593.80 35.67 o 2 4 0 1755.02 2125.54 36.53 o 3 4 0 3413.36 3731.85 53.64 o 4 4 0 10.35 35.09 19.34 o 5 4 0 84.38 165.53 40.56 o 5 4 0 30.07 90.67 34.08 o 6 4 0 483.95 561.51 47.31 o 7 4 0 5838.51 5444.65 94.48 o 8 4 0 1310.34 991.44 43.79 o 9 4 0 3896.59 3671.02 102.03 o 10 4 0 7493.62 8221.95 123.32 o 11 4 0 2638.91 2735.38 92.97 o 12 4 0 379.67 504.92 85.35 o 12 4 0 1330.17 1529.15 165.67 o 13 4 0 464.75 548.50 70.83 o 14 4 0 133.17 170.20 60.90 o 15 4 0 21.26 -11.72 81.54 o 16 4 0 265.88 225.21 103.47 o 17 4 0 570.31 482.99 126.34 o -13 5 0 1339.53 1204.64 154.60 o -12 5 0 158.22 241.82 104.77 o -11 5 0 771.95 894.22 125.55 o -10 5 0 3.95 -12.01 73.42 o -9 5 0 1974.45 1645.28 207.38 o -9 5 0 431.15 505.07 94.48 o -8 5 0 498.06 429.49 127.42 o -8 5 0 2574.34 2395.91 149.21 o -7 5 0 13.20 -53.50 66.23 o -7 5 0 9.71 -2.23 70.47 o -6 5 0 4076.38 4215.78 102.61 o -5 5 0 11966.20 12168.45 145.75 o -4 5 0 1417.13 1602.64 67.59 o -3 5 0 9816.04 10064.12 140.36 o -3 5 0 8671.75 9748.45 226.72 o -2 5 0 12255.98 11826.75 180.84 o -2 5 0 12182.43 12726.15 165.82 o -1 5 0 548.35 623.71 46.88 o -1 5 0 614.21 646.08 77.08 o 0 5 0 3152.09 3095.34 64.21 o 1 5 0 1908.44 2070.53 44.73 o 2 5 0 2517.52 2503.77 45.30 o 3 5 0 8.47 9.56 12.44 o 4 5 0 7221.49 7816.55 86.07 o 5 5 0 1785.46 2046.59 54.29 o 6 5 0 9682.86 10683.30 104.55 o 7 5 0 3497.05 3785.28 113.32 o 7 5 0 1545.34 1754.87 101.46 o 8 5 0 2871.74 2494.13 81.97 o 9 5 0 6827.85 7143.94 110.09 o 10 5 0 1698.92 1246.13 50.69 o 11 5 0 1323.85 1246.56 71.91 o 12 5 0 6431.71 6834.38 162.94 o 13 5 0 244.52 351.05 99.52 o 14 5 0 255.53 252.32 86.07 o 14 5 0 2082.22 2382.39 212.99 o 15 5 0 67.44 16.61 59.25 o 16 5 0 7.34 -42.14 87.15 o 17 5 0 1124.52 908.32 143.16 o -13 6 0 6.74 -117.93 99.45 o -12 6 0 576.38 465.02 121.38 o -11 6 0 28.51 76.72 94.92 o -10 6 0 23.35 -22.15 80.25 o -9 6 0 40.75 -6.62 52.56 o -8 6 0 13.87 -34.16 33.72 o -8 6 0 1107.83 780.90 193.64 o -7 6 0 3659.42 3653.04 233.84 o -7 6 0 692.48 683.40 72.27 o -6 6 0 3104.59 2915.79 144.75 o -6 6 0 1289.29 1137.34 101.10 o -5 6 0 1071.86 1137.34 78.45 o -4 6 0 3622.97 3358.44 91.75 o -3 6 0 11138.99 10595.43 132.24 o -2 6 0 898.38 1124.39 59.75 o -1 6 0 2797.50 2881.71 134.82 o -1 6 0 3707.43 3645.42 88.08 o 0 6 0 909.24 945.85 78.45 o 0 6 0 385.01 390.95 42.71 o 1 6 0 757.35 671.82 88.52 o 1 6 0 515.72 540.52 38.47 o 2 6 0 56.36 28.04 16.47 o 3 6 0 93.57 131.30 21.07 o 4 6 0 2625.07 2667.93 50.98 o 5 6 0 4861.03 5194.92 72.84 o 6 6 0 1513.78 1781.98 58.89 o 7 6 0 5028.04 4571.86 78.38 o 8 6 0 8958.08 9394.24 135.40 o 9 6 0 1223.50 1322.93 68.60 o 10 6 0 1442.01 1542.53 74.57 o 11 6 0 3815.15 3636.86 120.44 o 12 6 0 997.49 870.06 64.28 o 13 6 0 1175.96 1081.54 94.41 o 14 6 0 3601.62 3917.87 156.90 o 15 6 0 334.16 227.22 120.30 o 16 6 0 1829.30 1829.36 161.72 o 17 6 0 240.75 231.39 108.58 o -12 7 0 196.86 153.38 186.24 o -12 7 0 239.01 282.73 260.95 o -11 7 0 38.77 -165.82 143.52 o -11 7 0 1189.78 1174.59 274.18 o -10 7 0 173.91 115.27 116.85 o -9 7 0 19.27 -89.24 73.27 o -8 7 0 390.87 398.58 71.40 o -7 7 0 572.57 676.06 64.43 o -6 7 0 476.31 495.07 180.05 o -6 7 0 473.67 464.59 65.15 o -5 7 0 2843.00 3089.52 209.68 o -5 7 0 2520.92 2434.74 100.17 o -4 7 0 8365.60 7659.94 184.37 o -4 7 0 9343.57 9457.88 200.04 o -3 7 0 955.34 949.95 70.83 o -2 7 0 4643.91 4951.81 98.94 o -1 7 0 354.86 392.39 48.61 o 0 7 0 1087.07 1218.88 55.30 o 1 7 0 880.00 470.77 70.97 o 1 7 0 2490.06 2672.17 74.57 o 2 7 0 164.57 182.21 34.73 o 2 7 0 585.59 657.08 66.37 o 3 7 0 2287.20 2466.95 53.86 o 4 7 0 3034.08 3040.33 63.71 o 5 7 0 68.92 68.31 12.08 o 6 7 0 7021.19 7129.56 92.61 o 7 7 0 5373.99 5297.75 97.86 o 8 7 0 109.07 100.52 31.93 o 9 7 0 2698.01 3285.03 80.46 o 10 7 0 6452.95 6538.92 241.89 o 10 7 0 106.67 164.38 41.63 o 11 7 0 2118.28 2192.85 104.34 o 12 7 0 358.77 346.44 86.00 o 13 7 0 2179.41 2215.71 119.72 o 14 7 0 73.21 47.89 86.07 o 15 7 0 2044.70 1561.01 105.34 o 16 7 0 97.17 133.10 165.46 o 17 7 0 1867.72 1773.49 220.54 o -11 8 0 320.02 -58.89 180.05 o -10 8 0 374.44 374.85 235.78 o -10 8 0 15.15 -217.59 149.49 o -9 8 0 21.41 45.09 89.74 o -8 8 0 14.10 -30.27 59.25 o -7 8 0 54.26 -24.23 55.08 o -6 8 0 1919.29 1905.37 87.80 o -5 8 0 6979.53 6645.99 131.08 o -4 8 0 16.68 -17.90 36.17 o -3 8 0 4627.47 4892.70 157.69 o -3 8 0 4548.67 4259.86 148.63 o -2 8 0 437.41 415.76 76.80 o -2 8 0 400.43 429.42 98.30 o -1 8 0 419.55 458.62 59.54 o 0 8 0 651.78 784.14 54.29 o 1 8 0 1109.54 941.68 41.56 o 2 8 0 650.29 697.49 48.18 o 3 8 0 4964.56 5084.62 91.10 o 3 8 0 2017.58 2017.54 129.29 o 4 8 0 1491.16 1436.75 86.93 o 4 8 0 1002.16 1011.65 54.86 o 5 8 0 5472.06 5520.30 89.09 o 5 8 0 9324.95 9506.63 264.83 o 6 8 0 5542.69 5714.30 96.71 o 7 8 0 458.58 582.01 41.06 o 8 8 0 2545.56 2907.16 84.20 o 9 8 0 0.94 -0.72 27.11 o 10 8 0 769.27 727.11 75.29 o 11 8 0 452.45 379.09 155.53 o 11 8 0 16.11 19.41 40.48 o 12 8 0 605.59 595.74 77.87 o 12 8 0 1472.29 1483.49 185.95 o 13 8 0 429.66 388.94 114.62 o 14 8 0 320.39 246.42 116.92 o 15 8 0 24.96 64.36 121.23 o 16 8 0 918.12 819.66 150.36 o 17 8 0 1020.40 920.76 259.80 o -10 9 0 361.81 385.92 189.11 o -9 9 0 236.54 39.26 172.36 o -8 9 0 113.76 -99.95 161.64 o -7 9 0 1090.45 1190.76 128.86 o -7 9 0 1183.60 1297.69 224.42 o -6 9 0 4086.98 4405.11 122.46 o -5 9 0 14.75 20.13 43.58 o -4 9 0 3540.22 3769.32 106.21 o -3 9 0 2516.13 2698.56 92.26 o -2 9 0 1691.79 1701.30 75.36 o -1 9 0 47.89 -21.36 82.48 o -1 9 0 8.97 6.83 51.92 o 0 9 0 346.68 341.41 91.97 o 0 9 0 1318.42 1273.74 81.83 o 1 9 0 351.50 305.96 36.67 o 2 9 0 2046.40 2020.42 68.74 o 3 9 0 1434.19 1365.78 58.03 o 4 9 0 6323.28 6193.48 94.20 o 5 9 0 11135.39 11599.17 124.47 o 6 9 0 303.04 361.33 78.09 o 6 9 0 151.45 202.78 38.18 o 7 9 0 2807.75 2829.50 80.61 o 7 9 0 8755.93 8125.17 267.78 o 8 9 0 17.58 29.34 27.11 o 9 9 0 159.72 196.66 28.40 o 10 9 0 9.85 13.37 32.50 o 11 9 0 10.82 56.30 35.16 o 12 9 0 144.63 205.65 45.30 o 13 9 0 779.27 756.88 91.61 o 13 9 0 1087.67 1139.42 194.72 o 14 9 0 139.55 139.64 92.54 o 14 9 0 527.66 406.99 203.06 o 15 9 0 971.08 1098.94 151.36 o 16 9 0 1297.42 1429.85 167.97 o -9 10 0 226.46 117.64 178.47 o -8 10 0 745.22 806.07 180.92 o -7 10 0 3167.47 3405.18 211.04 o -6 10 0 879.58 742.21 162.29 o -6 10 0 98.18 126.12 71.55 o -5 10 0 2033.26 2080.17 96.93 o -4 10 0 2149.09 2078.88 93.41 o -3 10 0 344.59 366.36 54.50 o -2 10 0 3.98 -7.05 36.67 o -1 10 0 895.80 906.74 62.63 o 0 10 0 109.50 155.10 38.90 o 1 10 0 2.52 24.30 46.16 o 1 10 0 1796.38 1012.72 80.53 o 2 10 0 240.92 213.42 62.20 o 2 10 0 3.00 -29.19 71.62 o 3 10 0 4153.90 3910.25 89.24 o 4 10 0 10392.46 10324.70 125.12 o 5 10 0 359.08 336.16 50.12 o 6 10 0 5836.40 5827.55 100.38 o 7 10 0 2320.21 1580.21 55.37 o 8 10 0 680.99 710.43 73.92 o 9 10 0 43.38 55.66 36.53 o 9 10 0 1850.18 1734.01 192.49 o 10 10 0 529.85 520.96 47.82 o 11 10 0 3.07 -14.74 42.42 o 12 10 0 7.20 17.11 37.39 o 13 10 0 6.90 -7.62 48.25 o 14 10 0 1127.32 1287.91 123.82 o 15 10 0 1912.32 2179.54 149.49 o 16 10 0 8.97 -51.99 91.82 o -8 11 0 938.93 941.68 193.64 o -7 11 0 770.05 780.83 180.77 o -6 11 0 2048.38 2226.79 151.22 o -5 11 0 2126.74 2140.64 145.39 o -5 11 0 1368.86 1335.01 174.23 o -4 11 0 34.45 61.84 135.76 o -4 11 0 30.34 11.72 65.87 o -3 11 0 365.06 398.36 59.54 o -2 11 0 153.67 153.52 48.39 o -1 11 0 540.15 613.93 59.47 o 0 11 0 78.45 130.08 41.56 o 1 11 0 205.05 124.76 37.03 o 2 11 0 290.67 291.15 42.28 o 3 11 0 14219.51 14506.61 245.77 o 3 11 0 5427.35 5663.18 138.99 o 4 11 0 614.21 575.61 79.67 o 5 11 0 6452.97 6630.82 144.89 o 6 11 0 4499.53 4252.24 122.82 o 7 11 0 1950.79 1987.05 99.88 o 8 11 0 994.47 859.57 101.82 o 9 11 0 184.63 224.49 99.01 o 10 11 0 231.42 115.27 111.81 o 11 11 0 40.46 19.63 62.49 o 12 11 0 81.17 9.71 48.75 o 13 11 0 1010.93 1140.50 91.46 o 14 11 0 3807.65 4014.08 142.09 o 15 11 0 40.47 19.99 70.90 o 16 11 0 1802.50 2088.37 157.19 o 17 11 0 69.26 -17.69 80.61 o -7 12 0 1989.08 1616.95 355.93 o -6 12 0 705.55 496.30 297.19 o -5 12 0 44.33 26.10 128.21 o -4 12 0 820.44 816.42 131.66 o -3 12 0 194.50 199.54 108.94 o -3 12 0 190.27 298.63 120.51 o -2 12 0 309.91 358.67 84.35 o -2 12 0 1607.53 1712.37 150.79 o -1 12 0 519.44 448.91 58.75 o 0 12 0 54.52 57.24 49.47 o 1 12 0 6.96 27.76 45.88 o 2 12 0 617.69 615.73 68.31 o 3 12 0 56.35 13.81 42.42 o 4 12 0 6479.53 6717.10 147.84 o 5 12 0 5160.79 5400.86 168.98 o 5 12 0 3082.62 2954.76 207.66 o 6 12 0 941.77 909.40 91.39 o 7 12 0 1166.20 1095.63 94.70 o 8 12 0 1334.58 1153.09 89.81 o 9 12 0 168.26 80.89 101.10 o 10 12 0 62.48 -54.94 106.85 o 11 12 0 70.71 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