#------------------------------------------------------------------------------ #$Date: 2010-12-22 21:36:50 +0200 (Wed, 22 Dec 2010) $ #$Revision: 5269 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2228129.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228129_Fobs loop_ _publ_author_name 'Zha, Mei-Qin' 'Li, Xing' 'Bing, Yue' 'Lu, Yue' _publ_section_title ; (\m-4,4'-Bipyridine-\k^2^N:N')bis[bis(N,N-dimethyldithiocarbamato-\k^2^S,S')zinc(II)] ; _journal_coeditor_code XU5042 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1465 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.070 _cell_angle_gamma 90.000 _cell_length_a 8.0490 _cell_length_b 13.8770 _cell_length_c 14.8134 _exptl_crystal_F_000 788.00 _reflns_d_resolution_high 0.7692 _[local]_cod_data_source_file xu5042Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sad in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 172.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 28788.97 28068.84 1007.28 o 2 0 0 1011.16 1087.22 48.65 o 3 0 0 20884.26 20031.90 681.38 o 4 0 0 24629.04 24274.78 718.17 o 5 0 0 84.37 73.48 9.77 o 6 0 0 793.41 729.94 39.59 o 7 0 0 57.99 96.64 19.00 o 8 0 0 2941.26 3191.36 136.67 o 9 0 0 132.76 151.75 27.08 o 10 0 0 219.99 214.94 31.71 o 1 1 0 9282.77 9084.39 224.43 o 2 1 0 5685.65 5686.69 148.18 o 3 1 0 7149.63 7214.25 153.13 o 4 1 0 171.18 189.72 9.12 o 5 1 0 873.94 937.19 26.11 o 6 1 0 305.60 336.53 17.59 o 7 1 0 1463.73 1518.66 47.18 o 8 1 0 372.81 412.07 21.37 o 9 1 0 14.76 8.90 11.07 o 10 1 0 4.73 -12.10 12.17 o 0 2 0 21209.95 22120.29 799.40 o 1 2 0 16889.33 16840.34 522.18 o 2 2 0 1866.11 2097.18 46.28 o 3 2 0 8124.52 7708.98 228.71 o 4 2 0 22206.11 22089.34 461.01 o 5 2 0 2738.97 2627.94 103.95 o 6 2 0 67.40 68.28 7.88 o 7 2 0 2118.71 2465.51 67.52 o 8 2 0 1236.65 1279.84 41.85 o 9 2 0 100.06 106.85 16.50 o 10 2 0 11.78 23.98 13.94 o 1 3 0 1160.13 1333.05 29.77 o 2 3 0 4161.50 4245.55 99.22 o 3 3 0 3624.48 3611.59 78.94 o 4 3 0 210.66 221.58 10.81 o 5 3 0 1317.02 1398.97 35.92 o 6 3 0 4931.89 5092.11 113.93 o 7 3 0 38.69 21.35 8.45 o 8 3 0 985.51 983.14 45.11 o 9 3 0 464.97 550.19 30.81 o 10 3 0 37.65 35.19 14.72 o 0 4 0 410.10 378.97 18.59 o 1 4 0 8.02 16.75 3.73 o 2 4 0 126.51 150.14 6.35 o 3 4 0 1152.61 1371.89 32.95 o 4 4 0 1511.29 1442.94 35.62 o 5 4 0 1187.88 1265.37 33.23 o 6 4 0 1198.02 1107.90 36.65 o 7 4 0 1352.65 1390.44 43.11 o 8 4 0 1064.31 1106.35 39.01 o 9 4 0 44.48 56.01 12.35 o 10 4 0 208.10 209.06 22.42 o 1 5 0 663.53 671.41 18.79 o 2 5 0 3594.52 3521.38 76.54 o 3 5 0 2242.24 2403.55 54.50 o 4 5 0 1792.43 1601.08 39.10 o 5 5 0 3124.65 3198.53 73.45 o 6 5 0 1561.30 1578.80 46.00 o 7 5 0 94.15 68.25 10.21 o 8 5 0 326.36 318.10 29.01 o 9 5 0 2164.76 2111.74 63.52 o 0 6 0 364.32 447.43 17.29 o 1 6 0 123.29 136.55 9.28 o 2 6 0 4148.90 4383.32 94.69 o 3 6 0 869.89 822.80 24.75 o 4 6 0 1146.21 1071.61 28.36 o 5 6 0 270.50 253.66 14.50 o 6 6 0 1427.48 1341.57 40.59 o 7 6 0 71.82 40.55 9.85 o 8 6 0 207.34 174.91 18.30 o 9 6 0 626.40 551.92 31.21 o 1 7 0 616.74 574.97 19.85 o 2 7 0 5421.64 5364.36 127.21 o 3 7 0 1500.28 1399.10 34.16 o 4 7 0 659.37 631.02 22.26 o 5 7 0 2327.97 2142.23 65.56 o 6 7 0 2543.34 2250.11 69.82 o 7 7 0 1.70 0.59 10.02 o 8 7 0 12.18 -7.39 10.42 o 9 7 0 1344.92 1350.33 54.00 o 0 8 0 1532.38 1519.48 64.36 o 1 8 0 27.58 40.06 8.80 o 2 8 0 41.54 44.33 5.99 o 3 8 0 10.94 17.68 5.59 o 4 8 0 280.35 294.76 14.39 o 5 8 0 208.47 162.86 14.09 o 6 8 0 565.01 548.18 26.67 o 7 8 0 72.56 63.78 13.12 o 8 8 0 0.54 8.85 10.99 o 9 8 0 7.04 14.47 13.23 o 1 9 0 129.62 141.97 12.59 o 2 9 0 528.91 504.97 23.02 o 3 9 0 1267.63 1132.87 33.25 o 4 9 0 233.27 190.76 13.47 o 5 9 0 346.48 338.39 19.82 o 6 9 0 1604.77 1496.99 51.63 o 7 9 0 1.38 2.96 9.79 o 8 9 0 176.54 249.49 31.82 o 0 10 0 57.48 56.81 15.70 o 1 10 0 252.91 266.15 16.54 o 2 10 0 375.18 326.14 20.92 o 3 10 0 545.88 585.33 21.29 o 4 10 0 376.54 338.95 18.76 o 5 10 0 82.45 49.57 10.80 o 6 10 0 419.92 373.76 22.72 o 7 10 0 64.31 44.08 12.81 o 8 10 0 169.36 197.03 20.44 o 1 11 0 1255.68 1168.54 39.30 o 2 11 0 33.60 17.78 7.33 o 3 11 0 745.46 588.08 25.13 o 4 11 0 33.32 12.61 11.72 o 5 11 0 266.95 235.20 17.88 o 6 11 0 940.17 906.24 37.74 o 7 11 0 103.31 79.48 14.99 o 8 11 0 44.73 28.38 13.54 o 0 12 0 4858.19 4924.81 192.44 o 1 12 0 438.04 510.71 23.44 o 2 12 0 5.45 -0.12 6.75 o 3 12 0 138.54 154.45 16.71 o 4 12 0 190.18 166.39 18.12 o 5 12 0 146.33 191.47 20.68 o 6 12 0 718.34 681.34 38.72 o 7 12 0 521.75 471.80 55.76 o 1 13 0 399.25 433.54 22.11 o 2 13 0 494.15 538.24 25.19 o 3 13 0 3.62 3.15 9.42 o 4 13 0 113.68 200.82 20.34 o 5 13 0 382.41 322.68 26.62 o 6 13 0 1387.33 1355.36 67.27 o 7 13 0 31.55 59.98 17.71 o 0 14 0 16.39 1.25 12.21 o 1 14 0 260.44 198.84 20.80 o 2 14 0 305.26 251.52 31.62 o 3 14 0 334.87 304.35 24.10 o 4 14 0 81.93 107.40 17.19 o 5 14 0 27.69 19.05 13.62 o 6 14 0 41.09 29.12 15.09 o 1 15 0 1484.16 1559.04 68.60 o 2 15 0 1760.02 1625.48 65.91 o 3 15 0 259.17 237.67 22.56 o 4 15 0 1.48 -2.30 11.81 o 5 15 0 205.84 180.20 23.59 o 0 16 0 1862.78 1785.63 89.44 o 1 16 0 882.57 825.49 39.46 o 2 16 0 2.97 -2.77 10.96 o 3 16 0 16.93 17.50 12.88 o 4 16 0 89.88 90.77 20.61 o 1 17 0 564.32 568.17 34.44 o 2 17 0 960.21 928.78 61.11 o 3 17 0 1066.14 1099.72 68.23 o 0 18 0 1239.71 1134.70 65.53 o -10 1 1 7.67 0.53 12.21 o -9 1 1 2.58 -10.15 10.15 o -8 1 1 72.68 65.57 15.52 o -7 1 1 1192.10 1067.29 35.10 o -6 1 1 1363.26 1342.89 35.63 o -5 1 1 249.34 291.23 18.12 o -4 1 1 3638.17 3665.82 81.23 o -3 1 1 681.00 763.91 19.88 o -2 1 1 16.66 15.71 3.67 o 0 1 1 129.83 143.72 5.57 o 1 1 1 152.16 131.40 7.80 o 2 1 1 3350.77 3552.89 76.89 o 3 1 1 737.00 844.55 31.37 o 4 1 1 49.54 39.16 5.28 o 5 1 1 283.19 337.21 15.34 o 6 1 1 3.64 13.16 5.94 o 7 1 1 817.25 900.90 28.14 o 8 1 1 171.87 170.83 15.21 o 9 1 1 184.25 189.53 19.71 o 10 1 1 92.63 94.14 17.66 o -10 2 1 75.50 108.18 18.78 o -9 2 1 0.54 0.52 11.16 o -8 2 1 282.75 330.29 19.37 o -7 2 1 27.37 12.08 7.89 o -6 2 1 29.77 33.19 6.45 o -5 2 1 3466.59 3256.38 74.24 o -4 2 1 175.37 176.42 8.55 o -3 2 1 492.73 496.14 14.36 o -2 2 1 4599.48 4996.54 106.13 o -1 2 1 2062.56 2061.28 44.24 o 0 2 1 5002.57 5203.45 157.87 o 1 2 1 1734.74 2081.80 49.27 o 2 2 1 7356.31 7317.28 174.57 o 3 2 1 3648.05 3314.19 72.83 o 4 2 1 7461.10 7425.18 159.41 o 5 2 1 680.42 622.21 19.73 o 6 2 1 9.13 17.22 6.06 o 7 2 1 1699.16 1686.29 44.79 o 8 2 1 3053.91 3178.79 85.46 o 9 2 1 55.00 27.37 18.84 o 10 2 1 9.93 4.95 12.68 o -10 3 1 21.98 14.78 13.21 o -9 3 1 13.12 13.92 11.65 o -8 3 1 3643.06 3720.79 97.70 o -7 3 1 56.98 28.70 8.71 o -6 3 1 1714.29 1646.25 47.00 o -5 3 1 459.90 565.77 19.27 o -4 3 1 4667.68 4902.69 117.05 o -3 3 1 180.12 239.88 9.17 o -2 3 1 13609.04 14414.30 300.81 o -1 3 1 1976.22 2146.79 46.36 o 0 3 1 39.81 39.63 2.59 o 1 3 1 2973.37 3122.01 73.03 o 2 3 1 6232.11 6175.17 148.96 o 3 3 1 920.08 1083.66 32.00 o 4 3 1 58.70 16.04 5.36 o 5 3 1 513.36 490.08 17.00 o 6 3 1 16.85 8.20 5.77 o 7 3 1 2269.99 2152.79 60.58 o 8 3 1 235.07 225.47 16.81 o 9 3 1 57.85 52.76 12.27 o 10 3 1 345.17 336.96 26.64 o -10 4 1 24.25 7.96 14.01 o -9 4 1 77.64 117.56 17.22 o -8 4 1 2066.45 2144.33 62.09 o -7 4 1 3951.45 3747.49 110.85 o -6 4 1 354.32 404.63 18.58 o -5 4 1 465.57 571.98 19.65 o -4 4 1 1731.84 1757.60 42.05 o -3 4 1 133.76 173.13 7.79 o -2 4 1 1618.06 1851.57 41.65 o -1 4 1 738.19 797.12 26.58 o 0 4 1 7032.66 7294.69 167.38 o 1 4 1 752.35 808.00 21.00 o 2 4 1 1214.55 1474.65 33.98 o 3 4 1 6861.43 6629.73 172.48 o 4 4 1 12213.71 10757.06 228.19 o 5 4 1 6.37 6.43 4.91 o 6 4 1 1926.71 1818.93 51.33 o 7 4 1 4552.02 4593.03 120.08 o 8 4 1 1196.85 1188.16 40.16 o 9 4 1 229.32 238.49 18.90 o -9 5 1 186.11 180.43 23.74 o -8 5 1 1020.21 980.58 35.31 o -7 5 1 15.07 12.23 10.65 o -6 5 1 1100.85 1087.55 34.79 o -5 5 1 340.57 324.04 13.35 o -4 5 1 487.81 479.06 17.59 o -3 5 1 657.41 672.22 19.02 o -2 5 1 77.91 78.67 4.95 o -1 5 1 454.73 518.13 13.68 o 0 5 1 2365.19 2290.09 49.89 o 1 5 1 35.76 33.76 4.09 o 2 5 1 364.59 317.34 10.41 o 3 5 1 1305.91 1152.46 31.24 o 4 5 1 8.66 6.32 4.26 o 5 5 1 1900.81 1842.60 45.61 o 6 5 1 1418.19 1368.07 37.14 o 7 5 1 104.12 73.42 11.50 o 8 5 1 120.02 109.57 13.52 o 9 5 1 15.12 2.06 11.56 o -9 6 1 270.36 272.34 22.95 o -8 6 1 1429.25 1364.94 50.48 o -7 6 1 1308.88 1260.98 40.45 o -6 6 1 24.17 12.55 7.74 o -5 6 1 2301.25 2370.23 62.46 o -4 6 1 5067.21 5092.61 111.60 o -3 6 1 2168.76 2186.06 54.76 o -2 6 1 63.98 77.42 6.03 o -1 6 1 3152.62 3303.51 79.08 o 0 6 1 6353.88 6233.20 131.88 o 1 6 1 2265.86 2266.04 55.76 o 2 6 1 9.59 10.42 3.20 o 3 6 1 3314.20 3161.62 70.66 o 4 6 1 3118.30 3004.82 68.68 o 5 6 1 39.03 17.89 5.77 o 6 6 1 452.65 468.55 20.74 o 7 6 1 1385.86 1478.42 45.61 o 8 6 1 656.09 722.90 42.19 o 9 6 1 6.23 16.03 12.52 o -9 7 1 14.06 26.63 15.62 o -8 7 1 160.27 132.82 17.39 o -7 7 1 259.06 245.72 19.35 o -6 7 1 367.31 399.02 24.03 o -5 7 1 3069.26 2794.37 72.26 o -4 7 1 617.37 597.78 18.59 o -3 7 1 2027.03 2299.61 52.74 o -2 7 1 12955.49 12787.04 268.95 o -1 7 1 10351.71 10467.11 242.35 o 0 7 1 61.05 86.55 5.45 o 1 7 1 5743.13 5578.65 145.97 o 2 7 1 4036.15 3883.11 84.77 o 3 7 1 441.04 406.77 13.56 o 4 7 1 259.10 213.85 10.59 o 5 7 1 50.01 45.23 10.57 o 6 7 1 380.44 400.48 31.06 o 7 7 1 592.03 529.68 27.49 o 8 7 1 96.89 80.94 14.44 o 9 7 1 362.77 410.64 31.46 o -9 8 1 595.66 494.83 42.86 o -8 8 1 531.74 495.49 44.43 o -7 8 1 117.12 104.45 14.36 o -6 8 1 678.42 731.76 31.24 o -5 8 1 1566.21 1536.25 50.39 o -4 8 1 3849.47 3818.71 106.95 o -3 8 1 8249.00 7958.85 187.07 o -2 8 1 3882.18 3655.60 89.05 o -1 8 1 5969.62 6094.89 143.96 o 0 8 1 7011.03 7051.56 165.13 o 1 8 1 7328.56 7233.59 169.63 o 2 8 1 188.57 194.91 10.25 o 3 8 1 477.86 591.06 20.41 o 4 8 1 113.13 173.90 11.87 o 5 8 1 966.27 965.50 41.50 o 6 8 1 477.23 366.56 21.79 o 7 8 1 65.01 39.49 12.07 o 8 8 1 6.82 11.68 11.09 o 9 8 1 34.04 41.53 13.96 o -9 9 1 402.96 349.16 52.70 o -8 9 1 323.89 282.02 23.23 o -7 9 1 88.62 106.19 14.90 o -6 9 1 4436.83 4276.45 122.76 o -5 9 1 1464.57 1647.35 64.52 o -4 9 1 165.06 154.49 13.09 o -3 9 1 2876.29 2816.55 71.38 o -2 9 1 19240.10 18697.62 430.64 o -1 9 1 3437.24 3548.73 98.10 o 0 9 1 67.42 92.32 8.89 o 1 9 1 2735.29 2920.84 72.39 o 2 9 1 15337.47 15411.35 356.86 o 3 9 1 735.05 757.37 25.00 o 4 9 1 438.36 419.49 29.20 o 5 9 1 359.05 458.46 23.32 o 6 9 1 3099.10 3350.58 99.57 o 7 9 1 36.91 4.57 14.82 o 8 9 1 68.55 56.38 14.54 o -8 10 1 208.53 272.75 31.90 o -7 10 1 935.50 1093.34 43.37 o -6 10 1 561.24 662.96 34.11 o -5 10 1 3178.57 3108.21 97.70 o -4 10 1 506.01 460.46 25.44 o -3 10 1 1904.69 1973.26 52.96 o -2 10 1 1081.35 1125.97 37.67 o -1 10 1 527.59 621.24 28.22 o 0 10 1 41.08 37.17 7.56 o 1 10 1 6811.72 6772.88 236.23 o 2 10 1 1884.40 1751.72 53.63 o 3 10 1 1569.10 1712.50 47.38 o 4 10 1 422.90 475.68 20.09 o 5 10 1 2465.30 2573.02 78.48 o 6 10 1 432.87 418.95 24.13 o 7 10 1 100.51 132.08 16.96 o 8 10 1 75.20 38.62 13.25 o -8 11 1 54.70 41.04 13.79 o -7 11 1 837.85 864.18 37.97 o -6 11 1 3213.11 3431.21 102.81 o -5 11 1 1755.69 1866.18 71.07 o -4 11 1 1932.04 1669.79 63.40 o -3 11 1 3593.57 3427.68 114.23 o -2 11 1 8347.60 8143.74 217.58 o -1 11 1 379.82 402.98 19.40 o 0 11 1 10.34 8.20 6.58 o 1 11 1 2341.62 2256.08 67.07 o 2 11 1 7106.46 7457.75 231.55 o 3 11 1 792.09 886.08 38.87 o 4 11 1 90.45 124.67 15.72 o 5 11 1 3796.09 3808.26 110.79 o 6 11 1 2692.48 2944.47 90.55 o 7 11 1 10.46 19.99 11.73 o 8 11 1 125.74 108.85 17.51 o -7 12 1 371.19 453.90 32.94 o -6 12 1 409.08 489.09 32.30 o -5 12 1 3.64 6.29 15.83 o -4 12 1 264.74 356.52 32.51 o -3 12 1 149.45 183.07 21.47 o -2 12 1 68.46 114.51 12.18 o -1 12 1 355.23 283.61 30.66 o 0 12 1 1186.37 1149.11 39.65 o 1 12 1 577.45 607.87 25.83 o 2 12 1 19.65 20.03 7.67 o 3 12 1 495.79 554.39 25.75 o 4 12 1 620.01 693.98 48.47 o 5 12 1 3.15 -2.82 11.00 o 6 12 1 87.45 64.87 16.45 o 7 12 1 218.99 191.34 23.85 o -7 13 1 3.62 14.41 14.96 o -6 13 1 231.46 306.70 27.69 o -5 13 1 562.51 706.47 48.29 o -4 13 1 1028.88 1020.87 46.03 o -3 13 1 739.48 682.08 34.79 o -2 13 1 438.54 447.68 22.48 o -1 13 1 387.98 410.70 24.86 o 0 13 1 2625.69 2386.36 72.49 o 1 13 1 5925.26 5965.84 163.85 o 2 13 1 1530.64 1538.11 59.24 o 3 13 1 20.06 28.06 11.36 o 4 13 1 1077.64 1089.29 48.39 o 5 13 1 1597.47 1622.48 66.61 o 6 13 1 1115.50 1138.94 100.34 o 7 13 1 441.54 348.05 36.11 o -6 14 1 260.89 281.07 27.46 o -5 14 1 602.53 603.64 36.81 o -4 14 1 123.13 196.74 21.71 o -3 14 1 486.76 579.90 33.08 o -2 14 1 148.41 168.12 18.20 o -1 14 1 91.15 123.96 16.52 o 0 14 1 1057.26 1160.90 41.80 o 1 14 1 40.86 30.43 9.98 o 2 14 1 686.80 778.86 37.54 o 3 14 1 283.38 266.16 22.59 o 4 14 1 686.67 667.68 37.18 o 5 14 1 12.62 7.65 12.69 o 6 14 1 35.90 63.50 17.35 o -5 15 1 29.86 16.96 14.96 o -4 15 1 163.43 151.76 20.68 o -3 15 1 153.33 182.00 20.82 o -2 15 1 20.51 32.77 14.84 o -1 15 1 361.20 370.56 26.17 o 0 15 1 159.61 185.28 16.90 o 1 15 1 513.04 577.18 41.62 o 2 15 1 6.65 14.83 11.34 o 3 15 1 260.08 232.39 22.66 o 4 15 1 231.46 209.58 34.04 o 5 15 1 911.04 908.41 47.43 o -4 16 1 358.11 371.89 29.36 o -3 16 1 45.04 40.95 23.84 o -2 16 1 12.64 15.46 12.22 o -1 16 1 427.16 394.30 27.44 o 0 16 1 227.71 247.49 19.89 o 1 16 1 5.54 15.96 10.14 o 2 16 1 62.68 71.90 15.42 o 3 16 1 309.91 325.26 27.08 o 4 16 1 1275.26 1179.62 57.16 o -3 17 1 0.56 -3.55 13.92 o -2 17 1 300.77 333.24 28.91 o -1 17 1 12.68 2.66 12.50 o 0 17 1 343.58 411.28 25.73 o 1 17 1 25.36 39.03 14.09 o 2 17 1 19.25 34.35 14.48 o 3 17 1 717.56 725.29 78.89 o 0 18 1 525.08 584.72 65.45 o -10 0 2 548.13 570.81 47.84 o -9 0 2 399.79 447.83 61.79 o -8 0 2 1630.24 1719.45 83.36 o -7 0 2 2659.51 2550.14 110.50 o -6 0 2 834.88 914.57 38.61 o -5 0 2 1293.49 1266.72 73.26 o -4 0 2 29748.00 29893.90 881.41 o -3 0 2 7465.65 7383.25 221.40 o -2 0 2 5953.61 6717.43 200.33 o -1 0 2 971.89 1121.66 34.64 o 0 0 2 20475.97 19203.08 2181.40 o 1 0 2 9440.79 9585.77 493.19 o 2 0 2 355.89 285.39 13.70 o 3 0 2 353.41 276.13 14.48 o 4 0 2 2523.38 2615.76 85.36 o 5 0 2 3.97 13.15 7.25 o 6 0 2 147.34 159.41 15.23 o 7 0 2 2745.38 2899.59 112.84 o 8 0 2 4317.07 4489.07 148.46 o 9 0 2 796.05 801.51 120.23 o 10 0 2 439.87 444.51 76.50 o -10 1 2 368.27 393.34 28.41 o -9 1 2 267.51 306.67 42.40 o -8 1 2 901.47 1061.51 41.94 o -7 1 2 535.51 500.62 21.83 o -6 1 2 1450.09 1417.81 37.28 o -5 1 2 11605.53 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