#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/82/2228218.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228218_Fobs loop_ _publ_author_name 'Shakuntala, K.' 'Foro, Sabine' 'Gowda, B. Thimme' 'Nirmala, P. G.' 'Fuess, Hartmut' _publ_section_title ; N-(2,3-Dichlorophenyl)-4-methylbenzenesulfonamide ; _journal_coeditor_code BQ2248 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3062 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.300 _cell_angle_gamma 90.000 _cell_length_a 14.0350 _cell_length_b 12.3860 _cell_length_c 15.9930 _exptl_crystal_F_000 1296.00 _reflns_d_resolution_high 0.8375 _[local]_cod_data_source_file bq2248Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' S33 P 21/N' _shelx_refln_list_code 4 _shelx_f_calc_maximum 530.26 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4412.35 2006.59 24.10 o 4 0 0 11467.33 7211.02 576.40 o 6 0 0 8217.29 6373.00 591.55 o 8 0 0 1706.91 1827.98 203.47 o 10 0 0 65.40 83.41 11.04 o 12 0 0 703.91 827.14 40.75 o 14 0 0 64.30 57.41 7.19 o 16 0 0 3.80 -5.73 9.87 o 1 1 0 364.91 340.02 80.38 o 2 1 0 86.61 60.43 11.90 o 3 1 0 9643.16 5956.59 1015.52 o 4 1 0 5110.42 2889.63 184.74 o 5 1 0 11565.46 7294.41 89.33 o 6 1 0 0.06 5.44 1.24 o 7 1 0 3166.74 2509.37 16.62 o 8 1 0 1165.10 1128.97 42.31 o 9 1 0 4947.06 4942.37 360.70 o 10 1 0 1444.12 1510.40 104.04 o 11 1 0 2406.65 2654.70 207.68 o 12 1 0 20.07 19.38 3.66 o 13 1 0 1289.44 1537.62 132.78 o 14 1 0 884.01 998.32 76.14 o 15 1 0 2.78 2.27 8.53 o 16 1 0 37.56 52.03 3.13 o 0 2 0 10418.70 13213.00 106.14 o 1 2 0 801.57 910.74 235.31 o 2 2 0 11339.06 8832.15 4175.18 o 3 2 0 424.21 343.05 83.63 o 4 2 0 5404.54 3759.55 657.61 o 5 2 0 658.91 462.97 35.73 o 6 2 0 1459.79 1144.60 10.20 o 7 2 0 184.04 128.55 17.84 o 8 2 0 4072.79 3413.45 307.69 o 9 2 0 528.69 506.13 28.46 o 10 2 0 632.28 632.04 11.17 o 11 2 0 766.56 764.82 13.31 o 12 2 0 175.55 209.85 28.63 o 13 2 0 360.02 405.22 11.15 o 14 2 0 0.64 6.79 3.60 o 15 2 0 435.56 544.79 10.54 o 16 2 0 39.56 47.80 3.09 o 1 3 0 683.31 701.69 127.05 o 2 3 0 146.87 143.20 46.35 o 3 3 0 6540.26 6328.33 2169.33 o 4 3 0 187.35 158.96 51.29 o 5 3 0 365.77 343.73 47.60 o 6 3 0 1099.06 848.01 16.40 o 7 3 0 2087.08 1597.40 92.48 o 8 3 0 15.38 13.72 3.51 o 9 3 0 46.27 37.53 5.52 o 10 3 0 287.27 264.32 18.60 o 11 3 0 103.92 107.12 4.14 o 12 3 0 130.36 119.41 7.62 o 13 3 0 47.11 52.68 6.52 o 14 3 0 6.95 2.61 6.52 o 15 3 0 59.65 71.22 3.48 o 16 3 0 63.73 79.75 3.35 o 0 4 0 772.84 871.43 9.98 o 1 4 0 122.82 138.78 15.50 o 2 4 0 6988.97 7968.97 2035.03 o 3 4 0 24.00 72.82 30.19 o 4 4 0 11.05 12.35 4.18 o 5 4 0 2.50 5.88 4.10 o 6 4 0 384.84 328.22 33.56 o 7 4 0 4147.30 3393.36 120.33 o 8 4 0 901.12 793.45 85.98 o 9 4 0 4.83 45.33 22.91 o 10 4 0 476.22 419.38 113.77 o 11 4 0 35.99 40.38 8.28 o 12 4 0 1348.38 1406.93 116.46 o 13 4 0 19.79 11.59 5.44 o 14 4 0 68.72 84.00 3.96 o 15 4 0 3.53 0.87 4.43 o 1 5 0 621.72 774.28 107.62 o 2 5 0 1282.71 1359.93 301.12 o 3 5 0 453.30 412.79 109.30 o 4 5 0 215.88 245.39 46.25 o 5 5 0 2557.67 2532.15 571.65 o 6 5 0 2275.26 2049.00 225.76 o 7 5 0 4212.02 3929.60 124.33 o 8 5 0 83.02 92.88 6.36 o 9 5 0 174.21 164.85 29.30 o 10 5 0 146.50 142.11 31.89 o 11 5 0 4049.93 3863.91 835.57 o 12 5 0 394.17 396.59 73.53 o 13 5 0 14.11 19.98 6.19 o 14 5 0 0.58 0.43 6.02 o 15 5 0 1.16 2.86 4.68 o 0 6 0 150.63 190.76 5.53 o 1 6 0 2071.05 2194.90 218.32 o 2 6 0 8276.78 9721.39 1670.95 o 3 6 0 3398.39 3466.12 836.48 o 4 6 0 1053.06 1271.64 353.85 o 5 6 0 355.26 419.25 82.61 o 6 6 0 0.96 5.00 2.14 o 7 6 0 772.40 707.92 11.06 o 8 6 0 2136.02 1964.57 113.28 o 9 6 0 560.39 518.62 64.97 o 10 6 0 14.10 12.45 3.13 o 11 6 0 1.79 1.59 5.08 o 12 6 0 635.78 600.68 135.30 o 13 6 0 53.02 69.12 20.74 o 14 6 0 550.72 570.28 50.22 o 15 6 0 23.92 28.83 2.54 o 1 7 0 439.00 466.52 21.82 o 2 7 0 2852.92 3001.60 494.12 o 3 7 0 1990.64 2208.22 475.00 o 4 7 0 751.48 750.37 163.45 o 5 7 0 277.44 223.94 46.34 o 6 7 0 217.83 190.98 22.53 o 7 7 0 1.93 -4.19 4.19 o 8 7 0 1690.45 1558.02 126.84 o 9 7 0 457.30 416.57 67.86 o 10 7 0 1113.51 923.73 220.50 o 11 7 0 947.37 828.75 206.46 o 12 7 0 180.03 184.46 50.40 o 13 7 0 196.30 172.12 34.08 o 14 7 0 121.30 152.82 26.70 o 0 8 0 1721.49 1533.36 21.02 o 1 8 0 1035.33 940.82 62.81 o 2 8 0 582.30 581.93 56.19 o 3 8 0 64.46 86.43 16.65 o 4 8 0 1233.72 1130.44 217.48 o 5 8 0 1766.11 1700.00 224.88 o 6 8 0 55.15 41.20 9.20 o 7 8 0 1622.48 1432.09 17.40 o 8 8 0 421.99 399.79 51.49 o 9 8 0 444.23 401.94 65.92 o 10 8 0 495.01 445.70 96.40 o 11 8 0 0.62 -0.95 5.27 o 12 8 0 454.01 370.48 126.10 o 13 8 0 179.78 188.36 60.12 o 1 9 0 2343.12 2308.81 132.53 o 2 9 0 970.24 817.15 89.26 o 3 9 0 2.35 3.27 3.45 o 4 9 0 215.11 211.65 47.40 o 5 9 0 8.27 23.09 2.84 o 6 9 0 1649.70 1545.04 43.05 o 7 9 0 108.06 109.48 4.02 o 8 9 0 468.28 457.21 76.67 o 9 9 0 704.58 636.42 114.02 o 10 9 0 307.85 316.83 89.58 o 11 9 0 0.95 0.69 4.22 o 12 9 0 83.29 82.66 28.20 o 13 9 0 0.83 4.00 2.59 o 0 10 0 1550.99 1542.05 25.53 o 1 10 0 158.32 133.93 4.14 o 2 10 0 1044.40 1050.76 61.24 o 3 10 0 3497.86 3381.35 207.87 o 4 10 0 84.82 76.24 6.19 o 5 10 0 12.94 13.14 2.88 o 6 10 0 383.67 379.19 21.46 o 7 10 0 111.53 104.28 14.81 o 8 10 0 609.60 644.66 74.23 o 9 10 0 313.00 266.03 58.66 o 10 10 0 155.32 165.02 52.49 o 11 10 0 111.69 99.04 33.14 o 12 10 0 69.95 69.02 29.37 o 1 11 0 9.10 16.39 8.03 o 2 11 0 645.41 612.14 12.11 o 3 11 0 105.66 98.03 4.02 o 4 11 0 4.76 7.66 3.33 o 5 11 0 601.92 597.74 18.72 o 6 11 0 12.70 5.52 3.39 o 7 11 0 10.43 4.27 3.49 o 8 11 0 1.54 3.37 7.36 o 9 11 0 111.37 105.98 22.01 o 10 11 0 25.29 26.37 10.45 o 11 11 0 53.81 35.90 13.47 o 0 12 0 167.86 147.67 6.19 o 1 12 0 8.80 9.95 2.96 o 2 12 0 419.44 390.93 8.66 o 3 12 0 36.28 23.38 3.18 o 4 12 0 42.99 39.34 3.19 o 5 12 0 107.88 128.77 30.71 o 6 12 0 159.68 158.61 29.13 o 7 12 0 128.61 131.07 31.55 o 8 12 0 1.61 3.13 4.43 o 9 12 0 26.43 23.04 10.54 o 1 13 0 65.37 77.14 3.55 o 2 13 0 919.95 1005.02 92.09 o 3 13 0 9.63 13.28 2.83 o 4 13 0 175.05 175.73 27.29 o 5 13 0 177.91 169.79 32.57 o 6 13 0 579.59 558.43 147.18 o 7 13 0 19.39 19.40 2.45 o 0 14 0 10.13 2.34 6.36 o 1 14 0 1434.92 1496.94 82.89 o 2 14 0 77.77 81.02 6.36 o 3 14 0 66.60 73.98 16.06 o 4 14 0 2.24 2.49 3.45 o 5 14 0 33.04 43.89 8.95 o -15 0 1 225.87 275.59 28.39 o -13 0 1 33.82 46.76 8.11 o -11 0 1 4.29 7.58 3.17 o -9 0 1 9.07 26.84 6.19 o -7 0 1 255.32 253.05 41.58 o -5 0 1 7.27 4.45 1.24 o -3 0 1 2531.06 1845.04 35.19 o -1 0 1 34.46 52.27 1.07 o 1 0 1 5.10 13.56 0.71 o 3 0 1 28.24 27.27 2.59 o 5 0 1 293.65 207.33 4.45 o 7 0 1 4037.08 3091.19 84.94 o 9 0 1 1735.62 1661.46 50.09 o 11 0 1 1254.48 1513.24 19.99 o 13 0 1 2.56 -4.36 5.90 o 15 0 1 139.82 128.22 11.05 o -16 1 1 345.06 408.99 47.21 o -15 1 1 6.77 7.92 5.69 o -14 1 1 164.21 174.46 9.04 o -13 1 1 279.65 289.22 31.83 o -12 1 1 850.62 957.31 92.35 o -11 1 1 1257.21 1379.68 141.48 o -10 1 1 90.46 95.45 8.28 o -9 1 1 154.70 179.22 18.50 o -8 1 1 31.07 59.32 20.41 o -7 1 1 940.49 823.00 102.68 o -6 1 1 1076.44 782.22 92.55 o -5 1 1 4736.23 3202.54 230.07 o -4 1 1 3570.42 2189.22 39.31 o -3 1 1 63539.27 48078.59 5632.77 o -2 1 1 908.38 711.01 174.51 o -1 1 1 27202.17 34109.84 2076.98 o 0 1 1 5.65 14.16 6.02 o 1 1 1 174.19 148.95 59.56 o 2 1 1 92.35 67.71 25.14 o 3 1 1 264.86 130.20 40.67 o 4 1 1 392.38 248.79 24.47 o 5 1 1 8.82 26.59 8.36 o 6 1 1 29.77 24.16 1.76 o 7 1 1 75.76 63.30 8.28 o 8 1 1 2570.70 2165.14 133.52 o 9 1 1 4.68 14.93 2.30 o 10 1 1 510.99 509.62 15.95 o 11 1 1 8.15 12.54 4.26 o 12 1 1 1157.91 1394.26 28.15 o 13 1 1 118.08 158.25 13.31 o 14 1 1 489.77 516.71 14.94 o 15 1 1 220.73 293.94 6.22 o 16 1 1 0.47 8.29 2.57 o -16 2 1 141.10 176.33 20.93 o -15 2 1 6.37 0.59 5.32 o -14 2 1 34.51 38.16 8.70 o -13 2 1 331.47 350.77 18.60 o -12 2 1 514.10 572.65 36.33 o -11 2 1 858.41 942.46 79.08 o -10 2 1 2395.40 2373.18 171.29 o -9 2 1 108.12 97.67 3.00 o -8 2 1 8431.30 7484.13 326.44 o -7 2 1 2829.67 2077.05 15.23 o -6 2 1 3084.58 1820.60 190.18 o -5 2 1 4784.31 3121.44 164.26 o -4 2 1 8057.27 6162.82 286.56 o -3 2 1 5519.89 4573.44 17.60 o -2 2 1 399.39 482.36 75.96 o -1 2 1 3583.77 3694.61 182.43 o 0 2 1 36428.10 41749.29 17135.50 o 1 2 1 179.72 181.84 97.74 o 2 2 1 17243.54 10515.56 8332.67 o 3 2 1 2245.96 1718.07 592.69 o 4 2 1 3.74 12.16 6.94 o 5 2 1 15.47 12.56 1.18 o 6 2 1 1026.70 712.51 8.12 o 7 2 1 1892.52 1453.89 155.98 o 8 2 1 7986.55 6803.03 978.66 o 9 2 1 918.02 778.95 89.93 o 10 2 1 701.73 663.28 68.33 o 11 2 1 724.93 790.52 28.57 o 12 2 1 1378.24 1615.35 19.39 o 13 2 1 55.18 46.15 7.70 o 14 2 1 469.91 535.38 11.16 o 15 2 1 24.03 28.51 3.12 o 16 2 1 59.64 72.15 3.12 o -16 3 1 2.47 9.63 3.76 o -15 3 1 110.05 145.30 6.61 o -14 3 1 2.69 -2.39 5.26 o -13 3 1 0.19 -3.04 5.69 o -12 3 1 521.63 560.47 11.30 o -11 3 1 941.33 977.51 17.34 o -10 3 1 355.50 344.21 6.93 o -9 3 1 11.88 8.83 2.17 o -8 3 1 183.08 176.76 12.39 o -7 3 1 578.23 459.70 7.61 o -6 3 1 292.06 214.75 5.95 o -5 3 1 2923.97 1935.58 149.70 o -4 3 1 1349.05 1232.53 190.27 o -3 3 1 35.23 82.80 6.86 o -2 3 1 92.23 75.33 10.72 o -1 3 1 295.35 235.08 4.03 o 0 3 1 1834.39 1865.79 426.38 o 1 3 1 35027.29 40839.52 15868.28 o 2 3 1 673.51 594.86 254.00 o 3 3 1 19128.68 12765.01 7342.71 o 4 3 1 1855.08 1379.57 314.99 o 5 3 1 148.27 185.37 25.46 o 6 3 1 116.50 75.15 4.19 o 7 3 1 104.92 107.14 19.83 o 8 3 1 1808.05 1467.98 189.09 o 9 3 1 26.74 64.10 29.10 o 10 3 1 48.86 70.37 13.05 o 11 3 1 44.26 52.29 5.94 o 12 3 1 47.81 72.41 10.20 o 13 3 1 164.73 196.01 10.13 o 14 3 1 115.55 108.34 4.19 o 15 3 1 103.09 84.61 3.72 o 16 3 1 48.36 53.08 2.83 o -16 4 1 23.15 25.30 2.60 o -15 4 1 47.49 46.45 4.94 o -14 4 1 805.19 929.13 29.18 o -13 4 1 12.21 22.40 3.43 o -12 4 1 14.38 7.44 5.56 o -11 4 1 170.39 181.76 24.53 o -10 4 1 4477.38 3931.12 478.21 o -9 4 1 1113.97 901.60 125.96 o -8 4 1 607.02 459.96 29.83 o -7 4 1 1190.77 889.23 19.51 o -6 4 1 1745.16 1486.83 137.28 o -5 4 1 312.34 238.02 51.92 o -4 4 1 7126.37 7392.56 1851.27 o -3 4 1 631.55 687.35 150.98 o -2 4 1 126.10 150.75 10.80 o -1 4 1 351.88 392.94 11.26 o 0 4 1 87.57 78.21 15.49 o 1 4 1 821.83 885.51 256.62 o 2 4 1 18278.06 14384.94 7357.40 o 3 4 1 1333.84 1305.11 475.68 o 4 4 1 10327.45 9679.31 3039.24 o 5 4 1 744.81 657.68 102.67 o 6 4 1 926.63 796.08 45.27 o 7 4 1 1097.60 897.61 77.46 o 8 4 1 485.48 456.67 62.28 o 9 4 1 143.41 148.20 30.13 o 10 4 1 2957.26 2762.81 546.84 o 11 4 1 1066.95 982.21 187.67 o 12 4 1 93.30 103.11 8.20 o 13 4 1 14.57 26.21 3.48 o 14 4 1 10.74 18.98 3.13 o 15 4 1 6.98 -2.00 6.44 o -15 5 1 91.04 94.56 3.48 o -14 5 1 175.18 218.35 10.13 o -13 5 1 122.73 126.58 9.04 o -12 5 1 7.67 4.01 3.90 o -11 5 1 27.32 28.13 5.77 o -10 5 1 3163.81 2586.91 547.17 o -9 5 1 410.09 294.25 33.71 o -8 5 1 904.66 729.48 65.16 o -7 5 1 42.16 49.41 14.14 o -6 5 1 825.86 686.59 95.07 o -5 5 1 274.22 290.56 56.58 o -4 5 1 4.86 5.02 1.28 o -3 5 1 1891.04 2554.20 500.22 o -2 5 1 1155.62 1350.98 109.32 o -1 5 1 33.48 66.54 3.76 o 0 5 1 7.09 57.57 28.51 o 1 5 1 72.72 65.73 11.97 o 2 5 1 276.27 268.69 56.61 o 3 5 1 992.56 1060.29 287.28 o 4 5 1 2883.31 2797.16 734.67 o 5 5 1 1090.45 834.61 151.39 o 6 5 1 425.59 398.17 39.52 o 7 5 1 300.02 249.15 5.27 o 8 5 1 417.91 352.41 42.19 o 9 5 1 192.30 168.64 22.27 o 10 5 1 21.22 20.52 3.09 o 11 5 1 706.69 654.35 163.84 o 12 5 1 0.04 14.88 8.11 o 13 5 1 231.09 230.27 32.75 o 14 5 1 151.57 183.19 14.31 o 15 5 1 8.01 15.52 2.71 o -15 6 1 7.17 5.41 2.42 o -14 6 1 191.44 199.96 22.19 o -13 6 1 76.90 124.97 17.90 o -12 6 1 729.42 636.25 116.73 o -11 6 1 22.51 22.28 6.19 o -10 6 1 291.09 268.45 37.03 o -9 6 1 1.86 1.03 3.39 o -8 6 1 1.71 12.51 6.27 o -7 6 1 32.97 37.13 2.84 o -6 6 1 2090.52 1973.17 313.25 o -5 6 1 2896.94 2884.92 589.18 o -4 6 1 3985.08 4344.27 954.63 o -3 6 1 887.71 988.92 170.04 o -2 6 1 129.12 132.72 6.45 o -1 6 1 499.69 562.94 7.43 o 0 6 1 8275.82 9315.13 1166.53 o 1 6 1 5283.52 5759.71 1126.48 o 2 6 1 5770.03 6358.79 1738.66 o 3 6 1 631.84 590.36 173.75 o 4 6 1 7026.38 7139.49 1807.96 o 5 6 1 550.28 591.83 84.92 o 6 6 1 386.51 335.19 32.46 o 7 6 1 915.23 896.07 22.65 o 8 6 1 6.38 -4.07 4.07 o 9 6 1 23.08 19.33 2.78 o 10 6 1 215.68 198.65 54.43 o 11 6 1 10.97 11.36 14.05 o 12 6 1 33.40 37.22 11.79 o 13 6 1 4.33 2.07 3.89 o 14 6 1 143.58 157.01 24.86 o 15 6 1 29.60 36.63 3.51 o -14 7 1 313.89 320.64 55.33 o -13 7 1 168.57 163.03 31.90 o -12 7 1 138.78 110.04 23.77 o -11 7 1 345.11 282.76 80.46 o -10 7 1 199.07 156.91 33.74 o -9 7 1 1081.89 1030.65 151.05 o -8 7 1 456.86 407.44 22.65 o -7 7 1 386.08 482.23 105.73 o -6 7 1 1035.39 939.19 133.56 o -5 7 1 0.26 10.10 3.68 o -4 7 1 2831.22 2775.59 531.51 o -3 7 1 193.03 271.34 44.30 o -2 7 1 2306.84 2904.79 203.78 o -1 7 1 1908.24 2211.86 26.01 o 0 7 1 2488.72 2611.09 300.28 o 1 7 1 702.87 554.23 91.87 o 2 7 1 0.57 4.12 2.76 o 3 7 1 292.66 225.79 48.78 o 4 7 1 1649.34 1569.95 313.13 o 5 7 1 1411.23 1379.94 204.30 o 6 7 1 21.30 17.96 6.27 o 7 7 1 126.69 155.29 3.73 o 8 7 1 649.89 615.40 63.33 o 9 7 1 1984.19 1913.16 323.80 o 10 7 1 1634.72 1533.72 368.92 o 11 7 1 269.87 242.18 70.62 o 12 7 1 5.06 5.09 2.88 o 13 7 1 85.87 87.94 18.49 o 14 7 1 0.23 -1.97 2.83 o -14 8 1 20.55 19.11 2.19 o -13 8 1 14.30 8.95 4.26 o -12 8 1 75.75 74.40 27.19 o -11 8 1 392.76 317.23 100.70 o -10 8 1 50.07 48.35 8.62 o -9 8 1 211.35 223.42 38.43 o -8 8 1 888.24 732.84 30.37 o -7 8 1 57.99 65.70 4.18 o -6 8 1 64.53 63.09 6.27 o -5 8 1 203.36 184.32 22.61 o -4 8 1 366.71 334.80 59.78 o -3 8 1 336.27 374.69 49.63 o -2 8 1 3.41 19.63 9.78 o -1 8 1 4.76 11.18 3.43 o 0 8 1 85.34 74.29 5.94 o 1 8 1 357.10 294.16 49.22 o 2 8 1 414.99 334.83 60.73 o 3 8 1 794.99 722.94 147.30 o 4 8 1 2.11 27.94 2.24 o 5 8 1 368.18 359.74 23.39 o 6 8 1 652.54 660.95 13.52 o 7 8 1 251.62 228.93 18.76 o 8 8 1 856.19 804.79 87.81 o 9 8 1 3.00 2.12 5.08 o 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o -7 10 1 1397.35 1338.19 99.37 o -6 10 1 797.11 832.24 64.65 o -5 10 1 7.63 5.27 2.72 o -4 10 1 587.01 549.44 12.93 o -3 10 1 16.37 11.31 3.07 o -2 10 1 635.36 621.54 14.87 o -1 10 1 4360.25 4188.48 145.54 o 0 10 1 1258.86 1233.57 100.89 o 1 10 1 447.40 416.72 32.21 o 2 10 1 1088.44 1023.90 58.47 o 3 10 1 809.86 752.92 22.12 o 4 10 1 9.14 14.90 3.68 o 5 10 1 229.12 240.83 19.26 o 6 10 1 296.40 294.06 15.92 o 7 10 1 1144.23 1215.07 157.26 o 8 10 1 276.90 252.46 57.64 o 9 10 1 563.86 533.25 148.43 o 10 10 1 29.08 25.07 4.01 o 11 10 1 4.49 4.28 3.18 o 12 10 1 19.60 22.83 8.11 o -11 11 1 69.52 66.50 27.02 o -10 11 1 2.95 10.72 5.60 o -9 11 1 99.55 126.54 33.81 o -8 11 1 3.43 10.40 3.68 o -7 11 1 44.22 51.00 10.29 o -6 11 1 677.39 693.82 91.91 o -5 11 1 30.36 35.18 3.42 o -4 11 1 961.96 882.56 16.24 o -3 11 1 241.44 224.72 5.53 o -2 11 1 376.65 295.67 6.28 o -1 11 1 625.61 607.60 12.23 o 0 11 1 1509.14 1504.44 45.20 o 1 11 1 116.51 152.65 11.38 o 2 11 1 2523.64 2671.21 53.17 o 3 11 1 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