#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/82/2228254.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228254_Fobs loop_ _publ_author_name 'Li, Lu' 'Wang, Guo-Xi' _publ_section_title ; (R)-2-Methylpiperazine-1,4-diium tetrachloridoantimonate(III) chloride ; _journal_coeditor_code BX2322 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1629 _journal_volume 66 _journal_year 2010 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.7453 _cell_length_b 10.7729 _cell_length_c 16.3181 _exptl_crystal_F_000 776.00 _reflns_d_resolution_high 0.7695 _[local]_cod_data_source_file bx2322Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' shelxl in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 213.61 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 14906.23 14446.83 277.73 o 4 0 0 25726.97 25234.28 692.68 o 6 0 0 9338.91 9878.42 228.85 o 8 0 0 3317.48 3282.12 407.21 o 10 0 0 496.14 538.54 168.68 o 1 1 0 15245.53 15403.40 122.11 o 2 1 0 9022.14 9374.55 66.95 o 3 1 0 0.00 -0.30 10.18 o 4 1 0 3769.00 3791.73 37.80 o 5 1 0 17442.49 17750.33 177.52 o 6 1 0 5.49 10.60 4.63 o 7 1 0 2465.92 2509.46 64.60 o 8 1 0 1577.33 1608.16 44.18 o 9 1 0 37.39 35.94 14.32 o 1 2 0 11408.82 10886.78 56.11 o 2 2 0 3548.39 3504.41 49.75 o 3 2 0 30071.79 29580.91 163.19 o 4 2 0 669.30 639.01 13.53 o 5 2 0 259.73 246.02 15.04 o 6 2 0 3127.83 3145.86 47.92 o 7 2 0 1314.46 1309.44 29.74 o 8 2 0 619.37 628.95 38.58 o 9 2 0 337.66 315.71 27.50 o 2 3 0 41850.96 39422.27 211.48 o 3 3 0 86.22 106.97 10.26 o 4 3 0 141.81 163.60 10.47 o 5 3 0 530.27 522.37 14.43 o 6 3 0 23.57 58.15 14.16 o 7 3 0 385.92 334.33 20.58 o 8 3 0 775.69 844.19 44.48 o 9 3 0 73.58 76.84 13.40 o 0 4 0 7.73 40.87 15.19 o 1 4 0 86.75 79.19 8.17 o 2 4 0 19.53 42.29 8.30 o 3 4 0 9807.50 10004.41 68.36 o 4 4 0 16.88 31.47 5.32 o 5 4 0 1002.75 972.93 27.69 o 6 4 0 154.34 152.44 11.78 o 7 4 0 860.24 792.44 27.48 o 8 4 0 2.12 5.33 5.59 o 9 4 0 229.16 208.13 22.40 o 1 5 0 5858.22 6042.60 54.76 o 2 5 0 4640.70 4630.21 37.79 o 3 5 0 832.57 816.57 17.54 o 4 5 0 666.83 665.33 18.46 o 5 5 0 1957.50 2029.48 34.37 o 6 5 0 0.37 17.91 6.85 o 7 5 0 11.19 12.74 6.61 o 8 5 0 746.03 758.09 35.46 o 9 5 0 149.94 127.16 18.93 o 0 6 0 14833.71 14340.88 251.22 o 1 6 0 1122.78 1046.56 27.59 o 2 6 0 139.67 153.99 12.44 o 3 6 0 1669.87 1598.46 26.15 o 4 6 0 1333.31 1327.79 28.67 o 5 6 0 15.37 20.08 6.25 o 6 6 0 38.21 56.93 6.58 o 7 6 0 6.47 14.37 5.90 o 8 6 0 441.40 391.68 36.16 o 9 6 0 64.09 55.21 13.14 o 1 7 0 5294.58 5371.90 72.00 o 2 7 0 0.06 6.01 6.59 o 3 7 0 106.55 122.52 12.27 o 4 7 0 1.52 12.35 5.05 o 5 7 0 6785.98 6982.75 105.91 o 6 7 0 35.48 19.33 7.31 o 7 7 0 766.14 700.41 32.60 o 8 7 0 0.14 -1.74 12.78 o 0 8 0 14339.95 14937.90 336.22 o 1 8 0 2210.68 2157.19 58.07 o 2 8 0 946.66 928.59 34.23 o 3 8 0 4258.70 4347.40 58.00 o 4 8 0 1476.70 1500.78 39.26 o 5 8 0 14.50 25.28 6.93 o 6 8 0 1639.03 1723.64 42.24 o 7 8 0 84.22 85.47 16.99 o 8 8 0 394.45 261.66 58.58 o 1 9 0 3517.69 3404.75 78.06 o 2 9 0 8472.71 8742.67 124.21 o 3 9 0 351.89 335.08 32.68 o 4 9 0 744.73 832.23 36.61 o 5 9 0 1735.56 1732.42 44.47 o 6 9 0 4.44 9.60 6.80 o 7 9 0 278.94 275.15 25.11 o 0 10 0 26.44 26.87 18.21 o 1 10 0 1366.52 1338.45 46.36 o 2 10 0 66.76 92.62 16.92 o 3 10 0 10668.90 11583.72 214.74 o 4 10 0 49.90 55.75 13.74 o 5 10 0 1324.03 1281.25 41.56 o 6 10 0 37.76 32.35 12.46 o 7 10 0 1140.66 1134.47 125.05 o 1 11 0 1258.89 1259.01 45.65 o 2 11 0 6530.87 7017.90 145.58 o 3 11 0 164.10 144.96 17.44 o 4 11 0 1522.25 1608.08 46.77 o 5 11 0 448.52 430.21 32.46 o 6 11 0 2.95 18.84 13.08 o 0 12 0 3464.04 3742.74 100.98 o 1 12 0 502.98 499.91 36.85 o 2 12 0 94.81 111.39 15.63 o 3 12 0 1365.04 1392.01 44.35 o 4 12 0 340.02 278.93 52.72 o 5 12 0 164.62 147.45 20.45 o 1 13 0 1076.08 1036.66 42.86 o 2 13 0 7.45 10.54 9.99 o 3 13 0 35.67 32.99 13.24 o 0 14 0 2781.49 2741.54 124.12 o 1 0 1 1921.43 1929.49 35.12 o 2 0 1 11459.18 11120.48 75.83 o 3 0 1 910.56 850.87 13.13 o 4 0 1 45627.74 45111.68 396.34 o 5 0 1 263.39 236.33 13.42 o 6 0 1 148.59 130.76 13.45 o 7 0 1 515.20 498.65 29.95 o 8 0 1 6849.22 7250.80 113.62 o 9 0 1 740.35 786.67 44.80 o 10 0 1 898.34 892.52 53.23 o -10 1 1 58.73 28.37 18.87 o -9 1 1 3952.94 4281.37 116.80 o -8 1 1 326.90 336.32 25.40 o -7 1 1 873.61 850.38 31.95 o -6 1 1 685.86 665.30 20.54 o -5 1 1 6379.15 6310.30 127.37 o -4 1 1 6007.81 6090.41 61.54 o -3 1 1 18197.49 18110.54 164.12 o -2 1 1 1112.66 1088.74 19.79 o -1 1 1 10685.85 10301.85 71.90 o 1 1 1 10324.29 10094.88 50.75 o 2 1 1 1013.77 1001.49 13.87 o 3 1 1 18303.89 18237.29 146.18 o 4 1 1 5874.87 5988.69 45.77 o 5 1 1 6541.16 6688.98 79.95 o 6 1 1 648.77 622.31 18.10 o 7 1 1 902.97 876.20 28.04 o 8 1 1 336.36 308.67 29.57 o 9 1 1 3908.07 4321.81 111.42 o 10 1 1 56.12 73.47 25.99 o -9 2 1 167.34 153.53 17.46 o -8 2 1 1019.20 1020.52 37.71 o -7 2 1 5094.57 5187.71 82.85 o -6 2 1 4334.66 4332.98 85.63 o -5 2 1 3501.24 3606.47 42.10 o -4 2 1 7380.90 7644.93 57.58 o -3 2 1 1094.97 1093.50 14.96 o -2 2 1 17913.52 17651.36 108.01 o -1 2 1 10284.42 9611.63 125.98 o 0 2 1 6869.19 6702.02 87.39 o 1 2 1 10088.92 9626.89 65.05 o 2 2 1 18282.42 18290.17 203.94 o 3 2 1 1063.45 1041.42 14.27 o 4 2 1 7171.18 7300.34 65.51 o 5 2 1 3678.37 3813.38 47.14 o 6 2 1 4290.02 4248.23 58.37 o 7 2 1 5090.65 5323.31 87.17 o 8 2 1 1042.82 1043.17 37.97 o 9 2 1 182.06 173.38 20.40 o -9 3 1 383.62 359.44 36.75 o -8 3 1 306.45 288.64 22.12 o -7 3 1 1366.33 1356.98 35.38 o -6 3 1 11504.52 12466.25 126.21 o -5 3 1 1541.76 1499.02 28.55 o -4 3 1 483.50 451.44 22.67 o -3 3 1 2729.96 2697.22 29.16 o -2 3 1 18330.89 18159.67 112.88 o -1 3 1 4842.29 4565.89 41.45 o 0 3 1 159.94 118.47 13.59 o 1 3 1 4895.58 4705.33 36.02 o 2 3 1 17926.62 17444.54 91.32 o 3 3 1 2780.14 2765.70 26.45 o 4 3 1 594.06 565.31 12.81 o 5 3 1 1660.79 1637.34 25.31 o 6 3 1 11369.80 12034.08 130.29 o 7 3 1 1374.30 1358.13 32.80 o 8 3 1 249.06 228.57 18.92 o 9 3 1 378.71 356.19 31.99 o -9 4 1 173.29 158.32 20.38 o -8 4 1 5.00 10.86 8.29 o -7 4 1 3215.49 3341.73 56.29 o -6 4 1 572.18 535.86 18.69 o -5 4 1 2250.80 2292.98 41.88 o -4 4 1 45.68 63.41 8.50 o -3 4 1 1485.55 1430.20 22.39 o -2 4 1 348.34 326.87 8.14 o -1 4 1 8058.67 7836.73 54.49 o 1 4 1 7828.41 7523.30 74.10 o 2 4 1 326.54 305.73 8.94 o 3 4 1 1464.77 1417.10 17.91 o 4 4 1 27.34 35.44 4.25 o 5 4 1 2437.93 2506.08 38.85 o 6 4 1 585.78 572.93 16.96 o 7 4 1 3205.78 3305.26 50.22 o 8 4 1 3.94 12.83 9.11 o 9 4 1 173.53 163.92 25.02 o -9 5 1 1012.68 956.25 65.02 o -8 5 1 193.82 202.75 22.45 o -7 5 1 774.63 753.77 28.12 o -6 5 1 2288.21 2276.48 43.97 o -5 5 1 2070.75 2102.20 37.29 o -4 5 1 2206.80 2171.44 30.63 o -3 5 1 1161.66 1192.18 20.29 o -2 5 1 2736.85 2762.65 24.47 o -1 5 1 1443.75 1528.81 26.03 o 0 5 1 7990.61 7961.30 100.43 o 1 5 1 1328.01 1433.39 17.36 o 2 5 1 2906.69 2905.57 34.47 o 3 5 1 1141.66 1154.05 24.14 o 4 5 1 2273.46 2256.44 31.70 o 5 5 1 1981.86 1950.95 32.88 o 6 5 1 2298.88 2269.40 43.32 o 7 5 1 752.05 709.14 32.69 o 8 5 1 183.65 188.58 20.20 o 9 5 1 1015.30 968.90 62.37 o -9 6 1 396.67 293.03 68.30 o -8 6 1 1627.67 1672.74 57.44 o -7 6 1 512.56 461.88 22.66 o -6 6 1 661.48 610.11 21.21 o -5 6 1 874.84 880.04 22.57 o -4 6 1 8986.57 9178.71 123.73 o -3 6 1 309.91 309.60 16.73 o -2 6 1 681.68 674.83 12.16 o -1 6 1 99.56 154.12 26.14 o 0 6 1 762.40 755.47 23.70 o 1 6 1 62.10 75.48 6.46 o 2 6 1 495.84 502.22 17.16 o 3 6 1 375.73 373.58 17.91 o 4 6 1 9055.09 9284.19 120.86 o 5 6 1 936.83 959.42 22.51 o 6 6 1 663.40 628.22 21.36 o 7 6 1 547.53 520.07 34.58 o 8 6 1 1607.39 1648.52 40.67 o 9 6 1 391.78 329.64 68.71 o -8 7 1 277.87 257.93 36.30 o -7 7 1 210.25 176.64 15.22 o -6 7 1 131.66 121.53 11.86 o -5 7 1 829.68 814.64 27.03 o -4 7 1 1552.89 1546.03 32.90 o -3 7 1 4772.98 4868.03 79.37 o -2 7 1 219.13 226.52 17.50 o -1 7 1 6327.49 6431.18 92.13 o 0 7 1 11.99 41.59 14.84 o 1 7 1 6157.41 6253.59 65.31 o 2 7 1 192.01 196.27 10.97 o 3 7 1 4849.95 4989.64 80.30 o 4 7 1 1538.44 1505.94 33.94 o 5 7 1 920.46 915.88 31.12 o 6 7 1 135.46 113.62 12.18 o 7 7 1 214.70 204.82 17.70 o 8 7 1 255.58 187.48 39.63 o -8 8 1 1011.55 1049.73 41.91 o -7 8 1 1655.94 1652.99 41.30 o -6 8 1 25.58 23.89 6.48 o -5 8 1 1333.94 1332.20 34.40 o -4 8 1 3884.92 3884.69 74.00 o -3 8 1 2056.32 2090.86 45.25 o -2 8 1 1851.99 1939.33 49.37 o -1 8 1 1939.77 1876.67 49.61 o 0 8 1 458.28 468.60 30.21 o 1 8 1 2018.90 1986.54 46.48 o 2 8 1 1860.04 1871.11 33.15 o 3 8 1 2002.37 2034.14 36.98 o 4 8 1 3952.32 3983.61 80.21 o 5 8 1 1280.24 1277.10 33.65 o 6 8 1 21.05 22.58 6.10 o 7 8 1 1645.66 1612.82 46.42 o 8 8 1 963.11 918.53 60.18 o -7 9 1 594.26 611.66 56.18 o -6 9 1 3394.03 3493.06 67.56 o -5 9 1 644.44 617.22 28.20 o -4 9 1 1426.76 1443.88 43.77 o -3 9 1 1741.22 1788.33 52.39 o -2 9 1 3702.43 3822.97 119.90 o -1 9 1 594.19 604.39 34.24 o 0 9 1 2258.29 2393.80 54.71 o 1 9 1 605.48 594.37 35.24 o 2 9 1 3722.19 3889.49 80.55 o 3 9 1 1760.06 1754.48 33.83 o 4 9 1 1355.32 1319.38 34.30 o 5 9 1 675.36 668.65 36.49 o 6 9 1 3411.68 3558.83 71.58 o 7 9 1 604.07 598.22 50.52 o -7 10 1 1775.98 1812.32 104.94 o -6 10 1 560.92 527.85 34.35 o -5 10 1 1427.96 1415.26 45.56 o -4 10 1 162.58 174.78 21.20 o -3 10 1 240.34 273.41 28.61 o -2 10 1 396.02 431.25 43.29 o -1 10 1 5577.04 5941.41 128.72 o 0 10 1 96.51 100.05 15.25 o 1 10 1 5519.14 5803.80 127.50 o 2 10 1 412.38 447.62 29.74 o 3 10 1 257.58 268.60 33.06 o 4 10 1 141.89 128.75 15.36 o 5 10 1 1463.15 1388.31 41.91 o 6 10 1 550.85 519.86 30.30 o 7 10 1 1761.50 1655.68 119.30 o -6 11 1 2585.58 2637.93 77.95 o -5 11 1 408.62 398.28 33.79 o -4 11 1 504.43 505.37 36.30 o -3 11 1 103.64 114.98 18.07 o -2 11 1 1992.03 2030.92 67.06 o -1 11 1 512.43 470.13 44.27 o 0 11 1 2565.67 2601.66 74.02 o 1 11 1 479.57 412.80 37.84 o 2 11 1 2043.72 2116.87 56.32 o 3 11 1 94.73 112.06 16.79 o 4 11 1 530.25 495.02 39.46 o 5 11 1 375.90 384.38 29.92 o 6 11 1 2568.82 2594.91 66.02 o -5 12 1 825.71 836.01 38.41 o -4 12 1 1089.81 1121.96 45.29 o -3 12 1 110.71 102.91 17.41 o -2 12 1 404.76 413.30 27.42 o -1 12 1 1123.06 1124.28 49.92 o 0 12 1 25.38 35.22 10.74 o 1 12 1 1103.32 1120.44 46.22 o 2 12 1 428.34 406.05 32.19 o 3 12 1 114.55 121.87 16.92 o 4 12 1 1082.96 1029.64 48.52 o 5 12 1 832.12 794.82 51.67 o -3 13 1 1104.04 1108.66 47.79 o -2 13 1 154.89 151.64 21.36 o -1 13 1 833.86 821.12 58.79 o 0 13 1 710.34 729.67 48.73 o 1 13 1 861.25 873.02 72.12 o 2 13 1 158.11 142.72 18.11 o 3 13 1 1080.29 1055.61 43.31 o 1 0 2 28051.23 25535.85 326.77 o 2 0 2 642.59 674.34 11.25 o 3 0 2 121.39 126.08 10.01 o 4 0 2 4076.36 4148.83 41.61 o 5 0 2 6347.66 6671.19 68.99 o 6 0 2 508.65 534.32 14.85 o 7 0 2 2.43 6.60 5.21 o 8 0 2 641.71 653.86 36.28 o 9 0 2 9.65 9.29 11.09 o 10 0 2 87.40 49.73 24.47 o -9 1 2 58.34 65.19 13.72 o -8 1 2 510.79 515.05 25.34 o -7 1 2 2410.94 2453.34 73.90 o -6 1 2 186.18 173.40 19.15 o -5 1 2 6002.08 6079.91 71.56 o -4 1 2 1947.82 1821.07 25.59 o -3 1 2 2834.89 2874.15 28.99 o -2 1 2 3766.12 3921.55 41.48 o 0 1 2 5952.47 6237.71 35.61 o 2 1 2 3816.84 3992.97 29.73 o 3 1 2 2991.69 3109.85 29.78 o 4 1 2 2003.71 1959.76 25.50 o 5 1 2 5842.95 5877.46 70.38 o 6 1 2 119.16 110.44 11.65 o 7 1 2 2388.74 2372.15 54.74 o 8 1 2 485.26 453.31 26.46 o 9 1 2 74.12 60.39 14.72 o -9 2 2 319.45 305.15 24.83 o -8 2 2 820.70 810.20 45.92 o -7 2 2 405.16 380.16 27.74 o -6 2 2 5926.88 5857.61 86.38 o -5 2 2 703.18 655.23 18.48 o -4 2 2 3340.26 3429.68 43.16 o -3 2 2 5812.00 5988.05 52.30 o -2 2 2 33028.16 31746.14 556.04 o -1 2 2 3933.01 3832.46 32.62 o 0 2 2 15836.02 15616.40 166.08 o 1 2 2 4002.79 3949.69 27.01 o 2 2 2 32728.73 31608.16 334.78 o 3 2 2 5855.50 5946.30 38.17 o 4 2 2 3200.95 3247.25 43.27 o 5 2 2 743.13 734.22 15.71 o 6 2 2 5970.16 6178.84 115.96 o 7 2 2 505.97 494.60 33.32 o 8 2 2 833.08 803.11 28.80 o 9 2 2 322.30 274.31 22.82 o -9 3 2 235.99 223.17 26.21 o -8 3 2 619.22 611.97 31.46 o -7 3 2 1166.00 1106.21 44.67 o -6 3 2 70.45 82.01 13.90 o -5 3 2 1203.20 1179.09 26.15 o -4 3 2 1295.66 1326.63 24.23 o -3 3 2 14012.28 14124.25 99.02 o -2 3 2 25071.24 24109.11 163.44 o -1 3 2 10308.34 10377.76 74.18 o 0 3 2 865.84 846.08 16.09 o 1 3 2 10570.25 10644.06 62.48 o 2 3 2 25362.39 24839.84 263.05 o 3 3 2 13954.83 13974.02 80.59 o 4 3 2 1205.27 1201.92 20.14 o 5 3 2 1114.12 1036.41 19.71 o 6 3 2 73.43 71.42 6.85 o 7 3 2 1161.14 1099.31 26.46 o 8 3 2 608.33 620.22 27.38 o 9 3 2 249.45 225.97 43.17 o -9 4 2 1031.10 1043.81 44.25 o -8 4 2 296.98 281.79 27.60 o -7 4 2 1779.17 1707.71 57.20 o -6 4 2 375.36 347.95 30.23 o -5 4 2 3429.63 3520.19 59.08 o -4 4 2 461.34 466.50 14.29 o -3 4 2 14126.50 13962.77 102.00 o -2 4 2 13042.76 12849.58 87.12 o -1 4 2 5531.09 5552.98 44.91 o 0 4 2 4.92 30.73 6.80 o 1 4 2 5837.59 5855.34 40.38 o 2 4 2 13013.77 12915.39 81.91 o 3 4 2 14145.04 13966.52 84.14 o 4 4 2 403.31 417.41 11.40 o 5 4 2 3326.47 3383.31 46.81 o 6 4 2 345.20 335.15 16.49 o 7 4 2 1783.42 1778.97 34.06 o 8 4 2 312.28 337.17 22.46 o 9 4 2 1055.43 1079.79 49.73 o -9 5 2 166.18 159.88 20.23 o -8 5 2 1515.76 1557.76 44.15 o -7 5 2 557.87 503.47 28.23 o -6 5 2 515.63 517.14 24.40 o -5 5 2 1886.78 1833.76 52.57 o -4 5 2 5578.05 5670.11 69.76 o -3 5 2 5603.51 5596.26 54.85 o -2 5 2 5914.19 5901.69 51.34 o -1 5 2 4995.42 5137.65 95.51 o 0 5 2 16504.64 15819.26 208.29 o 1 5 2 5031.49 5022.63 38.70 o 2 5 2 5740.21 5680.23 50.85 o 3 5 2 5774.70 5827.39 66.68 o 4 5 2 5485.32 5559.24 58.95 o 5 5 2 1962.80 1916.69 30.35 o 6 5 2 523.30 510.06 18.62 o 7 5 2 647.94 593.32 35.96 o 8 5 2 1563.17 1632.28 46.52 o 9 5 2 162.62 173.03 30.05 o -9 6 2 74.82 51.52 12.76 o -8 6 2 823.22 811.31 32.51 o -7 6 2 74.17 67.37 10.12 o -6 6 2 2129.74 2165.53 40.06 o -5 6 2 2710.86 2705.09 38.89 o -4 6 2 3947.99 4018.25 54.44 o -3 6 2 279.14 280.11 10.32 o -2 6 2 3467.53 3379.37 41.30 o 0 6 2 24699.47 24335.94 211.09 o 2 6 2 3598.84 3583.44 43.65 o 3 6 2 313.76 323.59 18.19 o 4 6 2 3912.79 4011.73 64.80 o 5 6 2 2579.81 2541.41 37.77 o 6 6 2 2043.68 2040.15 37.05 o 7 6 2 91.15 95.23 13.13 o 8 6 2 811.19 768.99 39.38 o 9 6 2 93.20 84.00 39.87 o -8 7 2 562.80 520.34 42.31 o -7 7 2 1021.37 1006.15 29.98 o -6 7 2 961.80 917.19 28.73 o -5 7 2 3556.72 3601.74 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